JPS59121158A - 多結晶透明スピネル焼結体の製造法 - Google Patents
多結晶透明スピネル焼結体の製造法Info
- Publication number
 - JPS59121158A JPS59121158A JP57232545A JP23254582A JPS59121158A JP S59121158 A JPS59121158 A JP S59121158A JP 57232545 A JP57232545 A JP 57232545A JP 23254582 A JP23254582 A JP 23254582A JP S59121158 A JPS59121158 A JP S59121158A
 - Authority
 - JP
 - Japan
 - Prior art keywords
 - sintered body
 - spinel
 - spinel sintered
 - polycrystalline transparent
 - transparent spinel
 - Prior art date
 - Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
 - Granted
 
Links
- 229910052596 spinel Inorganic materials 0.000 title claims description 67
 - 239000011029 spinel Substances 0.000 title claims description 67
 - 238000004519 manufacturing process Methods 0.000 title claims description 11
 - KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 28
 - 239000000843 powder Substances 0.000 claims description 24
 - 239000000203 mixture Substances 0.000 claims description 15
 - 230000005540 biological transmission Effects 0.000 claims description 14
 - SMZOGRDCAXLAAR-UHFFFAOYSA-N aluminium isopropoxide Chemical compound [Al+3].CC(C)[O-].CC(C)[O-].CC(C)[O-] SMZOGRDCAXLAAR-UHFFFAOYSA-N 0.000 claims description 12
 - ORPJQHHQRCLVIC-UHFFFAOYSA-N magnesium;propan-2-olate Chemical compound CC(C)O[Mg]OC(C)C ORPJQHHQRCLVIC-UHFFFAOYSA-N 0.000 claims description 11
 - 238000010304 firing Methods 0.000 claims description 8
 - 230000007062 hydrolysis Effects 0.000 claims description 8
 - 238000006460 hydrolysis reaction Methods 0.000 claims description 8
 - 239000002244 precipitate Substances 0.000 claims description 8
 - 229910052739 hydrogen Inorganic materials 0.000 claims description 6
 - 239000001257 hydrogen Substances 0.000 claims description 6
 - UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 5
 - 238000009835 boiling Methods 0.000 claims description 3
 - 238000000465 moulding Methods 0.000 claims description 2
 - XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
 - 238000010438 heat treatment Methods 0.000 description 8
 - 238000005245 sintering Methods 0.000 description 8
 - 239000000243 solution Substances 0.000 description 8
 - 239000000047 product Substances 0.000 description 7
 - XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 5
 - 239000000463 material Substances 0.000 description 5
 - 238000000280 densification Methods 0.000 description 4
 - 238000001704 evaporation Methods 0.000 description 4
 - 230000008020 evaporation Effects 0.000 description 4
 - 238000000034 method Methods 0.000 description 4
 - 239000011148 porous material Substances 0.000 description 4
 - 239000002994 raw material Substances 0.000 description 4
 - 238000010992 reflux Methods 0.000 description 4
 - 238000002834 transmittance Methods 0.000 description 4
 - OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
 - FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 3
 - XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 3
 - 229910052799 carbon Inorganic materials 0.000 description 3
 - 238000001035 drying Methods 0.000 description 3
 - 239000012535 impurity Substances 0.000 description 3
 - 229910052749 magnesium Inorganic materials 0.000 description 3
 - 239000011777 magnesium Substances 0.000 description 3
 - 239000006104 solid solution Substances 0.000 description 3
 - 229910052782 aluminium Inorganic materials 0.000 description 2
 - PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 2
 - 239000007864 aqueous solution Substances 0.000 description 2
 - 238000000149 argon plasma sintering Methods 0.000 description 2
 - 229910052593 corundum Inorganic materials 0.000 description 2
 - 239000010431 corundum Substances 0.000 description 2
 - 230000000694 effects Effects 0.000 description 2
 - 238000001914 filtration Methods 0.000 description 2
 - 230000003301 hydrolyzing effect Effects 0.000 description 2
 - 230000003287 optical effect Effects 0.000 description 2
 - 230000001590 oxidative effect Effects 0.000 description 2
 - 239000002245 particle Substances 0.000 description 2
 - 230000035699 permeability Effects 0.000 description 2
 - 241001070941 Castanea Species 0.000 description 1
 - 235000014036 Castanea Nutrition 0.000 description 1
 - ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
 - 238000002441 X-ray diffraction Methods 0.000 description 1
 - 230000015572 biosynthetic process Effects 0.000 description 1
 - 230000000052 comparative effect Effects 0.000 description 1
 - 239000013078 crystal Substances 0.000 description 1
 - 230000007423 decrease Effects 0.000 description 1
 - 230000018044 dehydration Effects 0.000 description 1
 - 238000006297 dehydration reaction Methods 0.000 description 1
 - 238000010586 diagram Methods 0.000 description 1
 - 238000004090 dissolution Methods 0.000 description 1
 - 238000011049 filling Methods 0.000 description 1
 - 239000007789 gas Substances 0.000 description 1
 - 150000002431 hydrogen Chemical class 0.000 description 1
 - 230000002706 hydrostatic effect Effects 0.000 description 1
 - 150000004679 hydroxides Chemical class 0.000 description 1
 - -1 isopropanol Magnesium isopropoxide Chemical compound 0.000 description 1
 - 238000005259 measurement Methods 0.000 description 1
 - 229910052751 metal Inorganic materials 0.000 description 1
 - 239000002184 metal Substances 0.000 description 1
 - 238000002156 mixing Methods 0.000 description 1
 - 229910052750 molybdenum Inorganic materials 0.000 description 1
 - 239000011733 molybdenum Substances 0.000 description 1
 - 238000000926 separation method Methods 0.000 description 1
 - 230000002195 synergetic effect Effects 0.000 description 1
 - 238000003786 synthesis reaction Methods 0.000 description 1
 - WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
 - 229910052721 tungsten Inorganic materials 0.000 description 1
 - 239000010937 tungsten Substances 0.000 description 1
 
Classifications
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- C—CHEMISTRY; METALLURGY
 - C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
 - C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
 - C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
 - C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
 - C04B35/44—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminates
 - C04B35/443—Magnesium aluminate spinel
 
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- C—CHEMISTRY; METALLURGY
 - C01—INORGANIC CHEMISTRY
 - C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
 - C01F7/00—Compounds of aluminium
 - C01F7/02—Aluminium oxide; Aluminium hydroxide; Aluminates
 - C01F7/34—Preparation of aluminium hydroxide by precipitation from solutions containing aluminium salts
 - C01F7/36—Preparation of aluminium hydroxide by precipitation from solutions containing aluminium salts from organic aluminium salts
 
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 - C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
 - C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
 - C04B35/626—Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
 - C04B35/62605—Treating the starting powders individually or as mixtures
 - C04B35/6261—Milling
 - C04B35/6262—Milling of calcined, sintered clinker or ceramics
 
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 - C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
 - C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
 - C04B2235/30—Constituents and secondary phases not being of a fibrous nature
 - C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
 - C04B2235/3201—Alkali metal oxides or oxide-forming salts thereof
 - C04B2235/3203—Lithium oxide or oxide-forming salts thereof
 
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 - C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
 - C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
 - C04B2235/30—Constituents and secondary phases not being of a fibrous nature
 - C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
 - C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
 - C04B2235/3208—Calcium oxide or oxide-forming salts thereof, e.g. lime
 
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 - C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
 - C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
 - C04B2235/30—Constituents and secondary phases not being of a fibrous nature
 - C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
 - C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
 
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 - C04B2235/30—Constituents and secondary phases not being of a fibrous nature
 - C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
 - C04B2235/3217—Aluminum oxide or oxide forming salts thereof, e.g. bauxite, alpha-alumina
 - C04B2235/3222—Aluminates other than alumino-silicates, e.g. spinel (MgAl2O4)
 
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 - C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
 - C04B2235/441—Alkoxides, e.g. methoxide, tert-butoxide
 
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 - C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
 - C04B2235/444—Halide containing anions, e.g. bromide, iodate, chlorite
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 - C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
 - C04B2235/54—Particle size related information
 - C04B2235/5409—Particle size related information expressed by specific surface values
 
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 - C04B2235/74—Physical characteristics
 - C04B2235/79—Non-stoichiometric products, e.g. perovskites (ABO3) with an A/B-ratio other than 1
 
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 - C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
 - C04B2235/9646—Optical properties
 - C04B2235/9653—Translucent or transparent ceramics other than alumina
 
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
 - Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
 - Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
 - Y10S264/00—Plastic and nonmetallic article shaping or treating: processes
 - Y10S264/91—Sintering to produce translucent inorganic article
 
 
Landscapes
- Chemical & Material Sciences (AREA)
 - Engineering & Computer Science (AREA)
 - Ceramic Engineering (AREA)
 - Organic Chemistry (AREA)
 - Manufacturing & Machinery (AREA)
 - Materials Engineering (AREA)
 - Structural Engineering (AREA)
 - Inorganic Chemistry (AREA)
 - Life Sciences & Earth Sciences (AREA)
 - Geology (AREA)
 - Compositions Of Oxide Ceramics (AREA)
 
Priority Applications (4)
| Application Number | Priority Date | Filing Date | Title | 
|---|---|---|---|
| JP57232545A JPS59121158A (ja) | 1982-12-27 | 1982-12-27 | 多結晶透明スピネル焼結体の製造法 | 
| US06/498,576 US4543346A (en) | 1982-12-27 | 1983-05-26 | Polycrystalline transparent spinel sintered body and method of producing the same | 
| DE19833319346 DE3319346A1 (de) | 1982-12-27 | 1983-05-27 | Polykristalliner durchsichtiger spinnel-sinterkoerper und verfahren zu dessen herstellung | 
| US06/754,995 US4584151A (en) | 1982-12-27 | 1985-07-15 | Method of producing a polycrystalline transparent spinel sintered body | 
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title | 
|---|---|---|---|
| JP57232545A JPS59121158A (ja) | 1982-12-27 | 1982-12-27 | 多結晶透明スピネル焼結体の製造法 | 
Publications (2)
| Publication Number | Publication Date | 
|---|---|
| JPS59121158A true JPS59121158A (ja) | 1984-07-13 | 
| JPS6359985B2 JPS6359985B2 (en, 2012) | 1988-11-22 | 
Family
ID=16940996
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date | 
|---|---|---|---|
| JP57232545A Granted JPS59121158A (ja) | 1982-12-27 | 1982-12-27 | 多結晶透明スピネル焼結体の製造法 | 
Country Status (3)
| Country | Link | 
|---|---|
| US (2) | US4543346A (en, 2012) | 
| JP (1) | JPS59121158A (en, 2012) | 
| DE (1) | DE3319346A1 (en, 2012) | 
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title | 
|---|---|---|---|---|
| JPS6272556A (ja) * | 1985-09-25 | 1987-04-03 | 三菱マテリアル株式会社 | 緻密な多結晶MgAl↓2O↓4スピネルの製造方法 | 
| JPH01116601A (ja) * | 1987-10-30 | 1989-05-09 | Sumitomo Electric Ind Ltd | スピネル系透光性複合材 | 
| JPH01230465A (ja) * | 1988-03-09 | 1989-09-13 | Sumitomo Electric Ind Ltd | 透光性スピネル焼結体の製造方法 | 
| JPH01230464A (ja) * | 1988-03-09 | 1989-09-13 | Sumitomo Electric Ind Ltd | 透光性スピネル焼結体の製造方法 | 
| WO2006106670A1 (ja) * | 2005-03-30 | 2006-10-12 | Sumitomo Electric Industries, Ltd. | スピネル焼結体、光透過窓および光透過レンズ | 
| JP2008523426A (ja) * | 2004-12-09 | 2008-07-03 | カール・ツアイス・エスエムテイ・アーゲー | マイクロリソグラフィ投影露光装置用の透過光学素子および対物レンズ | 
| WO2008108276A1 (ja) | 2007-03-02 | 2008-09-12 | Sumitomo Electric Industries, Ltd. | スピネル焼結体、その製造方法、透明基板と液晶プロジェクター | 
| WO2009069553A1 (ja) * | 2007-11-26 | 2009-06-04 | Sumitomo Electric Industries, Ltd. | 多結晶透明セラミックス基板の製造方法およびスピネル基板の製造方法 | 
| WO2009128269A1 (ja) * | 2008-04-18 | 2009-10-22 | 三井金属鉱業株式会社 | スピネル焼結体 | 
| JP2009280455A (ja) * | 2008-05-23 | 2009-12-03 | Sumitomo Electric Ind Ltd | 透明多結晶スピネル基板とその製造方法、および電気光学装置 | 
| US9624136B2 (en) | 2014-07-01 | 2017-04-18 | Corning Incorporated | Transparent spinel article and tape cast methods for making | 
| CN108484156A (zh) * | 2018-04-12 | 2018-09-04 | 武汉理工大学 | 一种基于粉体抗水解处理及凝胶注模成型的尖晶石固溶体透明陶瓷制备方法 | 
Families Citing this family (29)
| Publication number | Priority date | Publication date | Assignee | Title | 
|---|---|---|---|---|
| JPS61286263A (ja) * | 1985-06-14 | 1986-12-16 | 日本特殊陶業株式会社 | 低温焼結磁器組成物 | 
| US4748139A (en) * | 1986-06-02 | 1988-05-31 | The Dow Chemical Company | Preparation of precursor materials convertible into bi- and poly-metal spinels | 
| US4837069A (en) * | 1987-01-07 | 1989-06-06 | Minnesota Mining And Manufacturing Company | Transparent alumina microspheres | 
| US4930731A (en) * | 1987-05-06 | 1990-06-05 | Coors Porcelain Company | Dome and window for missiles and launch tubes with high ultraviolet transmittance | 
| US5244849A (en) * | 1987-05-06 | 1993-09-14 | Coors Porcelain Company | Method for producing transparent polycrystalline body with high ultraviolet transmittance | 
| US5001093A (en) * | 1987-05-06 | 1991-03-19 | Coors Porcelain Company | Transparent polycrystalline body with high ultraviolet transmittance | 
| US4983555A (en) * | 1987-05-06 | 1991-01-08 | Coors Porcelain Company | Application of transparent polycrystalline body with high ultraviolet transmittance | 
| DE3887697T2 (de) * | 1987-05-06 | 1994-05-11 | Coors Porcelain Co | Transparenter polykristalliner gegenstand mit erhöhter ultraviolettdurchlässigkeit, verfahren zur herstellung und anwendung. | 
| DE68916282T2 (de) * | 1988-03-09 | 1995-01-26 | Sumitomo Electric Industries | Verfahren zur Herstellung eines lichtdurchlässigen Körpers aus gesintertem Spinell. | 
| US5082739A (en) * | 1988-04-22 | 1992-01-21 | Coors Porcelain Company | Metallized spinel with high transmittance and process for producing | 
| FR2639936B1 (fr) * | 1988-12-06 | 1991-01-25 | Thomson Csf | Piece en ceramique a plusieurs proprietes ameliorees et procede de fabrication d'une telle piece | 
| US5413973A (en) * | 1989-06-08 | 1995-05-09 | The United States Of America As Represented By The United States Department Of Energy | Method for thermal processing alumina-enriched spinel single crystals | 
| US5013696A (en) * | 1989-09-25 | 1991-05-07 | General Electric Company | Preparation of high uniformity polycrystalline ceramics by presintering, hot isostatic pressing and sintering and the resulting ceramic | 
| DE4227720C2 (de) * | 1991-09-18 | 1998-05-20 | Fraunhofer Ges Forschung | Verfahren zur Herstellung von Beschichtungen aus Spinell sowie Verwendung der danach hergestellten Träger | 
| KR100186949B1 (ko) * | 1996-02-12 | 1999-05-15 | 재단법인 한국화학연구소 | 알킬알루미늄알킬산마그네슘과 그 제조 방법 및이를이용한알루민산마그네슘의합성 | 
| JP3511083B2 (ja) * | 1999-08-06 | 2004-03-29 | 独立行政法人産業技術総合研究所 | 高輝度応力発光材料、その製造方法及びそれを用いた発光方法 | 
| JP4172459B2 (ja) * | 2004-04-22 | 2008-10-29 | セイコーエプソン株式会社 | 電気光学装置及び電子機器 | 
| US7211325B2 (en) | 2005-03-24 | 2007-05-01 | The United States Of America As Represented By The Secretary Of The Navy | Fluoride salt coated magnesium aluminate | 
| US7528086B2 (en) * | 2005-03-24 | 2009-05-05 | The United States Of America As Represented By The Secretary Of The Navy | Magnesium aluminate transparent ceramic having low scattering and absorption loss | 
| US7247591B2 (en) * | 2005-05-26 | 2007-07-24 | Osram Sylvania Inc. | Translucent PCA ceramic, ceramic discharge vessel, and method of making | 
| WO2008074503A1 (en) * | 2006-12-21 | 2008-06-26 | Carl Zeiss Smt Ag | Transmitting optical element | 
| IL191836A (en) * | 2008-05-29 | 2011-06-30 | Univ Ben Gurion | A single-stage thermal process for the production of a transparent sonicated spinel | 
| US8313725B2 (en) * | 2008-07-16 | 2012-11-20 | Materials And Electrochemical Research (Mer) Corporation | Ready-to-sinter spinel nanomixture and method for preparing same | 
| US8871139B2 (en) * | 2009-06-24 | 2014-10-28 | Ben-Gurion University Of The Negev Research And Development Authority | Manufacturing transparent yttrium aluminum garnet by spark plasma sintering | 
| DE102009055987B4 (de) | 2009-11-20 | 2018-10-18 | Schott Ag | Spinell-Optokeramiken | 
| DE102009055984A1 (de) | 2009-11-20 | 2011-06-09 | Schott Ag | Gefärbte Spinell-Optokeramiken | 
| US9309156B2 (en) * | 2014-05-27 | 2016-04-12 | Fraunhofer-Gesellschaft Zur Foerderung Der Angewandten Forschung E.V. | Transparent spinel ceramics and method for the production thereof | 
| CN109790075B (zh) * | 2016-10-05 | 2022-10-25 | 信越化学工业株式会社 | 透明尖晶石烧结体、光学构件以及透明尖晶石烧结体的制造方法 | 
| US20230127014A1 (en) * | 2021-10-19 | 2023-04-27 | Georgia Tech Research Corporation | Method for Manufacturing Transparent Ceramic Materials | 
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title | 
|---|---|---|---|---|
| JPS53106713A (en) * | 1977-03-01 | 1978-09-18 | Nippon Telegraph & Telephone | Process for making light permeable mgal204 ceramics | 
| JPS5727055A (en) * | 1980-07-25 | 1982-02-13 | Nec Corp | Semiconductor device | 
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title | 
|---|---|---|---|---|
| US3212401A (en) * | 1960-06-01 | 1965-10-19 | Gen Electric | Inhomogeneous magnesia-alumina optical lens | 
| JPS5527837A (en) * | 1978-08-14 | 1980-02-28 | Ngk Insulators Ltd | Polycrystal transparent spinel sintered article and its manufacture | 
| JPS6048466B2 (ja) * | 1980-05-15 | 1985-10-28 | 日本碍子株式会社 | 多結晶透明アルミナ焼結体の製造法 | 
- 
        1982
        
- 1982-12-27 JP JP57232545A patent/JPS59121158A/ja active Granted
 
 - 
        1983
        
- 1983-05-26 US US06/498,576 patent/US4543346A/en not_active Expired - Fee Related
 - 1983-05-27 DE DE19833319346 patent/DE3319346A1/de active Granted
 
 - 
        1985
        
- 1985-07-15 US US06/754,995 patent/US4584151A/en not_active Expired - Fee Related
 
 
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title | 
|---|---|---|---|---|
| JPS53106713A (en) * | 1977-03-01 | 1978-09-18 | Nippon Telegraph & Telephone | Process for making light permeable mgal204 ceramics | 
| JPS5727055A (en) * | 1980-07-25 | 1982-02-13 | Nec Corp | Semiconductor device | 
Cited By (19)
| Publication number | Priority date | Publication date | Assignee | Title | 
|---|---|---|---|---|
| JPS6272556A (ja) * | 1985-09-25 | 1987-04-03 | 三菱マテリアル株式会社 | 緻密な多結晶MgAl↓2O↓4スピネルの製造方法 | 
| JPH01116601A (ja) * | 1987-10-30 | 1989-05-09 | Sumitomo Electric Ind Ltd | スピネル系透光性複合材 | 
| JPH01230465A (ja) * | 1988-03-09 | 1989-09-13 | Sumitomo Electric Ind Ltd | 透光性スピネル焼結体の製造方法 | 
| JPH01230464A (ja) * | 1988-03-09 | 1989-09-13 | Sumitomo Electric Ind Ltd | 透光性スピネル焼結体の製造方法 | 
| JP2008523426A (ja) * | 2004-12-09 | 2008-07-03 | カール・ツアイス・エスエムテイ・アーゲー | マイクロリソグラフィ投影露光装置用の透過光学素子および対物レンズ | 
| US8570488B2 (en) | 2004-12-09 | 2013-10-29 | Carl Zeiss Smt Gmbh | Transmitting optical element and objective for a microlithographic projection exposure apparatus | 
| US7741238B2 (en) | 2005-03-30 | 2010-06-22 | Sumitomo Electric Industries, Ltd. | Spinel sintered body, light transmitting window and light transmitting lens | 
| WO2006106670A1 (ja) * | 2005-03-30 | 2006-10-12 | Sumitomo Electric Industries, Ltd. | スピネル焼結体、光透過窓および光透過レンズ | 
| JP2006273679A (ja) * | 2005-03-30 | 2006-10-12 | Sumitomo Electric Ind Ltd | スピネル焼結体、光透過窓および光透過レンズ | 
| US8097550B2 (en) | 2005-03-30 | 2012-01-17 | Sumitomo Electric Industries, Ltd. | Spinel sintered body, light transmitting window and light transmitting lens | 
| WO2008108276A1 (ja) | 2007-03-02 | 2008-09-12 | Sumitomo Electric Industries, Ltd. | スピネル焼結体、その製造方法、透明基板と液晶プロジェクター | 
| WO2009069553A1 (ja) * | 2007-11-26 | 2009-06-04 | Sumitomo Electric Industries, Ltd. | 多結晶透明セラミックス基板の製造方法およびスピネル基板の製造方法 | 
| JP2009126750A (ja) * | 2007-11-26 | 2009-06-11 | Sumitomo Electric Ind Ltd | 多結晶透明セラミックス基板の製造方法およびスピネル基板の製造方法 | 
| JP2009256150A (ja) * | 2008-04-18 | 2009-11-05 | Mitsui Mining & Smelting Co Ltd | スピネル焼結体 | 
| WO2009128269A1 (ja) * | 2008-04-18 | 2009-10-22 | 三井金属鉱業株式会社 | スピネル焼結体 | 
| JP2009280455A (ja) * | 2008-05-23 | 2009-12-03 | Sumitomo Electric Ind Ltd | 透明多結晶スピネル基板とその製造方法、および電気光学装置 | 
| US9624136B2 (en) | 2014-07-01 | 2017-04-18 | Corning Incorporated | Transparent spinel article and tape cast methods for making | 
| CN108484156A (zh) * | 2018-04-12 | 2018-09-04 | 武汉理工大学 | 一种基于粉体抗水解处理及凝胶注模成型的尖晶石固溶体透明陶瓷制备方法 | 
| CN108484156B (zh) * | 2018-04-12 | 2021-03-23 | 武汉理工大学 | 一种基于粉体抗水解处理及凝胶注模成型的尖晶石固溶体透明陶瓷制备方法 | 
Also Published As
| Publication number | Publication date | 
|---|---|
| US4543346A (en) | 1985-09-24 | 
| DE3319346C2 (en, 2012) | 1989-03-30 | 
| JPS6359985B2 (en, 2012) | 1988-11-22 | 
| US4584151A (en) | 1986-04-22 | 
| DE3319346A1 (de) | 1984-06-28 | 
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