JP2021001357A - 樹脂組成物、その成形品、および樹脂組成物の製造方法 - Google Patents
樹脂組成物、その成形品、および樹脂組成物の製造方法 Download PDFInfo
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- FMZUHGYZWYNSOA-VVBFYGJXSA-N (1r)-1-[(4r,4ar,8as)-2,6-diphenyl-4,4a,8,8a-tetrahydro-[1,3]dioxino[5,4-d][1,3]dioxin-4-yl]ethane-1,2-diol Chemical compound C([C@@H]1OC(O[C@@H]([C@@H]1O1)[C@H](O)CO)C=2C=CC=CC=2)OC1C1=CC=CC=C1 FMZUHGYZWYNSOA-VVBFYGJXSA-N 0.000 claims abstract description 5
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- 229910052782 aluminium Inorganic materials 0.000 description 3
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- 125000003277 amino group Chemical group 0.000 description 3
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- 125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- 125000001624 naphthyl group Chemical group 0.000 description 1
- 125000005186 naphthyloxy group Chemical group C1(=CC=CC2=CC=CC=C12)O* 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 239000001005 nitro dye Substances 0.000 description 1
- 125000001400 nonyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 229920003986 novolac Polymers 0.000 description 1
- 229940078552 o-xylene Drugs 0.000 description 1
- NOPZJEGEHWRZSE-UHFFFAOYSA-N octadecyl formate Chemical group CCCCCCCCCCCCCCCCCCOC=O NOPZJEGEHWRZSE-UHFFFAOYSA-N 0.000 description 1
- 125000002801 octanoyl group Chemical group C(CCCCCCC)(=O)* 0.000 description 1
- AXRSHKZFNKUGQB-UHFFFAOYSA-N octyl diphenyl phosphite Chemical compound C=1C=CC=CC=1OP(OCCCCCCCC)OC1=CC=CC=C1 AXRSHKZFNKUGQB-UHFFFAOYSA-N 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- ACMVLJBSYFHILY-UHFFFAOYSA-N oxo-di(tridecoxy)phosphanium Chemical compound CCCCCCCCCCCCCO[P+](=O)OCCCCCCCCCCCCC ACMVLJBSYFHILY-UHFFFAOYSA-N 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 125000004817 pentamethylene group Chemical group [H]C([H])([*:2])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[*:1] 0.000 description 1
- UZRCGISJYYLJMA-UHFFFAOYSA-N phenol;styrene Chemical compound OC1=CC=CC=C1.C=CC1=CC=CC=C1 UZRCGISJYYLJMA-UHFFFAOYSA-N 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 125000000951 phenoxy group Chemical group [H]C1=C([H])C([H])=C(O*)C([H])=C1[H] 0.000 description 1
- 229960000969 phenyl salicylate Drugs 0.000 description 1
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N phenylbenzene Natural products C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000010452 phosphate Substances 0.000 description 1
- UEZVMMHDMIWARA-UHFFFAOYSA-M phosphonate Chemical compound [O-]P(=O)=O UEZVMMHDMIWARA-UHFFFAOYSA-M 0.000 description 1
- 150000003008 phosphonic acid esters Chemical class 0.000 description 1
- XZTOTRSSGPPNTB-UHFFFAOYSA-N phosphono dihydrogen phosphate;1,3,5-triazine-2,4,6-triamine Chemical compound NC1=NC(N)=NC(N)=N1.OP(O)(=O)OP(O)(O)=O XZTOTRSSGPPNTB-UHFFFAOYSA-N 0.000 description 1
- MWFNQNPDUTULBC-UHFFFAOYSA-N phosphono dihydrogen phosphate;piperazine Chemical compound C1CNCCN1.OP(O)(=O)OP(O)(O)=O MWFNQNPDUTULBC-UHFFFAOYSA-N 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- XFZRQAZGUOTJCS-UHFFFAOYSA-N phosphoric acid;1,3,5-triazine-2,4,6-triamine Chemical compound OP(O)(O)=O.NC1=NC(N)=NC(N)=N1 XFZRQAZGUOTJCS-UHFFFAOYSA-N 0.000 description 1
- NQQWFVUVBGSGQN-UHFFFAOYSA-N phosphoric acid;piperazine Chemical compound OP(O)(O)=O.C1CNCCN1 NQQWFVUVBGSGQN-UHFFFAOYSA-N 0.000 description 1
- 239000001007 phthalocyanine dye Substances 0.000 description 1
- 125000000612 phthaloyl group Chemical group C(C=1C(C(=O)*)=CC=CC1)(=O)* 0.000 description 1
- 229960005141 piperazine Drugs 0.000 description 1
- 229960001954 piperazine phosphate Drugs 0.000 description 1
- 125000005936 piperidyl group Chemical group 0.000 description 1
- 229920013639 polyalphaolefin Polymers 0.000 description 1
- 229920006122 polyamide resin Polymers 0.000 description 1
- 229920001083 polybutene Polymers 0.000 description 1
- 229920000728 polyester Polymers 0.000 description 1
- 229920006146 polyetheresteramide block copolymer Polymers 0.000 description 1
- 239000002685 polymerization catalyst Substances 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920001955 polyphenylene ether Polymers 0.000 description 1
- 229920001451 polypropylene glycol Polymers 0.000 description 1
- 229920005630 polypropylene random copolymer Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- 150000005599 propionic acid derivatives Chemical class 0.000 description 1
- 125000001501 propionyl group Chemical group O=C([*])C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000002572 propoxy group Chemical group [*]OC([H])([H])C(C([H])([H])[H])([H])[H] 0.000 description 1
- 125000001436 propyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 1
- 125000004309 pyranyl group Chemical group O1C(C=CC=C1)* 0.000 description 1
- 125000003226 pyrazolyl group Chemical group 0.000 description 1
- 125000004076 pyridyl group Chemical group 0.000 description 1
- 125000000714 pyrimidinyl group Chemical group 0.000 description 1
- 125000000168 pyrrolyl group Chemical group 0.000 description 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 description 1
- 125000005493 quinolyl group Chemical group 0.000 description 1
- GDESWOTWNNGOMW-UHFFFAOYSA-N resorcinol monobenzoate Chemical compound OC1=CC=CC(OC(=O)C=2C=CC=CC=2)=C1 GDESWOTWNNGOMW-UHFFFAOYSA-N 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 150000004671 saturated fatty acids Chemical class 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000001587 sorbitan monostearate Substances 0.000 description 1
- 235000011076 sorbitan monostearate Nutrition 0.000 description 1
- 229940035048 sorbitan monostearate Drugs 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 125000003696 stearoyl group Chemical group O=C([*])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 150000003440 styrenes Chemical class 0.000 description 1
- 125000005504 styryl group Chemical group 0.000 description 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-L succinate(2-) Chemical compound [O-]C(=O)CCC([O-])=O KDYFGRWQOYBRFD-UHFFFAOYSA-L 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 125000000472 sulfonyl group Chemical group *S(*)(=O)=O 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical class CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- LVEOKSIILWWVEO-UHFFFAOYSA-N tetradecyl 3-(3-oxo-3-tetradecoxypropyl)sulfanylpropanoate Chemical compound CCCCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCCCC LVEOKSIILWWVEO-UHFFFAOYSA-N 0.000 description 1
- NZNAAUDJKMURFU-UHFFFAOYSA-N tetrakis(2,2,6,6-tetramethylpiperidin-4-yl) butane-1,2,3,4-tetracarboxylate Chemical compound C1C(C)(C)NC(C)(C)CC1OC(=O)CC(C(=O)OC1CC(C)(C)NC(C)(C)C1)C(C(=O)OC1CC(C)(C)NC(C)(C)C1)CC(=O)OC1CC(C)(C)NC(C)(C)C1 NZNAAUDJKMURFU-UHFFFAOYSA-N 0.000 description 1
- 125000003698 tetramethyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 125000000383 tetramethylene group Chemical group [H]C([H])([*:1])C([H])([H])C([H])([H])C([H])([H])[*:2] 0.000 description 1
- 125000001113 thiadiazolyl group Chemical group 0.000 description 1
- 239000001017 thiazole dye Substances 0.000 description 1
- 125000000335 thiazolyl group Chemical group 0.000 description 1
- 239000001003 triarylmethane dye Substances 0.000 description 1
- 125000001425 triazolyl group Chemical group 0.000 description 1
- MZHULIWXRDLGRR-UHFFFAOYSA-N tridecyl 3-(3-oxo-3-tridecoxypropyl)sulfanylpropanoate Chemical compound CCCCCCCCCCCCCOC(=O)CCSCCC(=O)OCCCCCCCCCCCCC MZHULIWXRDLGRR-UHFFFAOYSA-N 0.000 description 1
- IVIIAEVMQHEPAY-UHFFFAOYSA-N tridodecyl phosphite Chemical compound CCCCCCCCCCCCOP(OCCCCCCCCCCCC)OCCCCCCCCCCCC IVIIAEVMQHEPAY-UHFFFAOYSA-N 0.000 description 1
- XZZNDPSIHUTMOC-UHFFFAOYSA-N triphenyl phosphate Chemical compound C=1C=CC=CC=1OP(OC=1C=CC=CC=1)(=O)OC1=CC=CC=C1 XZZNDPSIHUTMOC-UHFFFAOYSA-N 0.000 description 1
- LENZDBCJOHFCAS-UHFFFAOYSA-N tris Chemical compound OCC(N)(CO)CO LENZDBCJOHFCAS-UHFFFAOYSA-N 0.000 description 1
- KOWVWXQNQNCRRS-UHFFFAOYSA-N tris(2,4-dimethylphenyl) phosphate Chemical compound CC1=CC(C)=CC=C1OP(=O)(OC=1C(=CC(C)=CC=1)C)OC1=CC=C(C)C=C1C KOWVWXQNQNCRRS-UHFFFAOYSA-N 0.000 description 1
- DECPGQLXYYCNEZ-UHFFFAOYSA-N tris(6-methylheptyl) phosphite Chemical compound CC(C)CCCCCOP(OCCCCCC(C)C)OCCCCCC(C)C DECPGQLXYYCNEZ-UHFFFAOYSA-N 0.000 description 1
- JZNDMMGBXUYFNQ-UHFFFAOYSA-N tris(dodecylsulfanyl)phosphane Chemical compound CCCCCCCCCCCCSP(SCCCCCCCCCCCC)SCCCCCCCCCCCC JZNDMMGBXUYFNQ-UHFFFAOYSA-N 0.000 description 1
- PEXOFOFLXOCMDX-UHFFFAOYSA-N tritridecyl phosphite Chemical compound CCCCCCCCCCCCCOP(OCCCCCCCCCCCCC)OCCCCCCCCCCCCC PEXOFOFLXOCMDX-UHFFFAOYSA-N 0.000 description 1
- 125000002221 trityl group Chemical group [H]C1=C([H])C([H])=C([H])C([H])=C1C([*])(C1=C(C(=C(C(=C1[H])[H])[H])[H])[H])C1=C([H])C([H])=C([H])C([H])=C1[H] 0.000 description 1
- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 239000001993 wax Substances 0.000 description 1
- 239000001018 xanthene dye Substances 0.000 description 1
- 239000010457 zeolite Substances 0.000 description 1
- 239000011667 zinc carbonate Substances 0.000 description 1
- 229910000010 zinc carbonate Inorganic materials 0.000 description 1
- 235000004416 zinc carbonate Nutrition 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
Images
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-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/34—Heterocyclic compounds having nitrogen in the ring
- C08K5/3467—Heterocyclic compounds having nitrogen in the ring having more than two nitrogen atoms in the ring
- C08K5/3477—Six-membered rings
- C08K5/3492—Triazines
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/15—Heterocyclic compounds having oxygen in the ring
- C08K5/156—Heterocyclic compounds having oxygen in the ring having two oxygen atoms in the ring
- C08K5/1575—Six-membered rings
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/16—Nitrogen-containing compounds
- C08K5/34—Heterocyclic compounds having nitrogen in the ring
- C08K5/3467—Heterocyclic compounds having nitrogen in the ring having more than two nitrogen atoms in the ring
- C08K5/3477—Six-membered rings
- C08K5/3492—Triazines
- C08K5/34924—Triazines containing cyanurate groups; Tautomers thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/0008—Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
- C08K5/0083—Nucleating agents promoting the crystallisation of the polymer matrix
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
Description
前記核剤が、下記一般式(2)で表されるアセタール化合物(ただし、ジベンジリデンソルビトールおよびビス(4−メチルベンジリデン)ソルビトールを除く)を含み、
前記ポリオレフィン系樹脂100質量部に対する前記核剤の含有量が、0.005質量部以上0.08質量部以下であることを特徴とするものである。
前記核剤が、下記一般式(2)で表されるアセタール化合物(ただし、ジベンジリデンソルビトールおよびビス(4−メチルベンジリデン)ソルビトールを除く)を含み、
前記樹脂組成物中における前記核剤の含有量が、前記ポリオレフィン系樹脂100質量部に対して0.005質量部以上0.08質量部以下となるように、前記核剤を配合することを特徴とするものである。
<樹脂組成物>
本発明の樹脂組成物は、ポリオレフィン系樹脂と核剤とを含む。本発明の組成物においては、核剤が、ポリオレフィン系樹脂の融点よりも150℃高い温度において融解するもの、または、ポリオレフィン系樹脂の融点よりも150℃高い温度においてポリオレフィン系樹脂に溶解するものであり、かつ、核剤が、ポリオレフィン系樹脂100質量部に対して0.2質量部添加した場合、ポリオレフィン系樹脂の結晶化温度を7℃以上向上させるものである。また、本発明の樹脂組成物においては、ポリオレフィン系樹脂100質量部に対する核剤の含有量が、0.005質量部以上0.1質量部未満である。かかる構成とすることで、本発明の樹脂組成物は、樹脂成分の結晶性が抑制されたものになる。その理由は以下のとおりであると考えられる。
本発明の樹脂組成物に係るポリオレフィン系樹脂は、分子量、重合度、密度、軟化点、溶媒への不溶分の割合、立体規則性の程度、触媒残渣の有無、原料となるモノマーの種類や配合比率、重合触媒の種類(例えば、チーグラー触媒、メタロセン触媒等)等に関わらず、使用することができる。なお、本発明の樹脂組成物においては、ポリオレフィン系樹脂とは、ポリオレフィンの割合が樹脂成分中70質量%以上のものをいい、好ましくは80質量%以上、より好ましくは90質量%以上、特に好ましくは100質量%である。
本発明の樹脂組成物に係る核剤は、ポリオレフィン系樹脂の融点よりも150℃高い温度において融解する核剤、またはポリオレフィン系樹脂の融点よりも150℃高い温度においてポリオレフィン系樹脂に溶解する核剤である。核剤がポリオレフィン系樹脂の融点よりも150℃高い温度において融解するものである場合、樹脂組成物の成形加工時に、核剤は融解して液体状態となり、可塑化したポリオレフィン系樹脂の溶融液中に拡散される。核剤がポリオレフィン系樹脂の融点よりも150℃高い温度においてポリオレフィン系樹脂に溶解するものである場合、樹脂組成物の成形加工時に、核剤は可塑化したポリオレフィン系樹脂の溶融液中に溶解し、溶融液中に拡散される。
0≦y2/y1<10,2≦y1+y2≦20
で表される条件を満たす数を表し、pは0または正の数を表す。
次に、本発明の成形品について説明する。
本発明の成形品は、本発明の樹脂組成物を成形して得られる成形品である。
<核剤をポリオレフィン系樹脂100質量部に対して0.2質量部添加した場合の結晶化温度の確認>
下記の核剤1〜6をポリオレフィン系樹脂100質量部に対して0.2質量部添加した場合における、ポリオレフィン系樹脂の結晶化温度を確認した。下記のポリオレフィン系樹脂、核剤、酸化防止剤および脂肪酸金属塩を表1に示す割合で配合し、ヘンシェルミキサーを用いて混合した後、二軸押出機(日本製鋼所製 TEX−28V)を用いて230℃の押出温度で溶融混練し、造粒することにより、実験例1〜6および参照例1の樹脂組成物ペレットを得た。表1において各成分の配合量の単位は質量部である。得られた樹脂組成物ペレットにつき、下記の手順で、結晶化温度を測定した。
核剤1:化合物No.59のトリアジン化合物、融点202.7℃
核剤2:化合物No.58のトリアジン化合物、融点189.3℃
核剤3:化合物No.50のトリアジン化合物、融点217.7℃
核剤4:化合物No.60のアセタール化合物、融点274.8℃
核剤5:化合物No.61のアセタール化合物、融点244.7℃
核剤6:リチウム 2、2’−メチレンビス(4,6−ジ第三ブチルフェニル)ホスフェート、融点400℃以上(吸熱ピーク観測されず)
酸化防止剤1:テトラキス[メチレン−3−(3’,5’−ジ第三ブチル−4’−ヒドロキシフェニル)プロピオネート]メタン
酸化防止剤2:トリス(2,4−ジ−tert−ブチルフェニル)ホスファイト
脂肪酸金属塩:ステアリン酸カルシウム
なお、核剤の「融点」は、示差走査熱量測定装置(パーキンエルマー社製ダイアモンド)にて窒素雰囲気下、核剤を50℃から400℃まで、10℃/分で昇温した際に観測される吸熱ピークの温度(℃)である。
得られた樹脂組成物ペレットを細かく破断して、その5mgをアルミパンに充填し、示差走査熱量測定装置(パーキンエルマー社製ダイアモンド)により結晶化温度を測定した。結晶化温度は、50℃から10℃/minの速度で230℃まで昇温し、5分間保持後、10℃/minで50℃まで冷却した際、冷却過程において観測された発熱ピークの温度(℃)として求めた。結果を表1に示す。
<樹脂組成物の調製および特性評価>
ポリオレフィン系樹脂、核剤、酸化防止剤および脂肪酸金属塩を表2〜4に示す割合で配合し、ヘンシェルミキサーを用いて混合した後、二軸押出機(日本製鋼所製 TEX−28V)を用いて230℃の押出温度で溶融混練し、造粒することにより、実施例1〜4、参考例1〜6、比較例1〜7の樹脂組成物ペレットを得た。表2〜4において各成分の配合量の単位は質量部である。また、得られた樹脂組成物ペレットについて、実験例1と同様の手順で結晶化温度を測定した。結果を表2〜4に示す。
ポリオレフィン系樹脂、核剤、酸化防止剤および脂肪酸金属塩を表5に示す割合で配合し、ヘンシェルミキサーを用いて混合した後、二軸押出機(東洋精機製作所製 ラボプラストミルマイクロ)を用いて230℃の押出温度で溶融混練し、造粒することにより、実施例5〜6、比較例8の樹脂組成物ペレットを得た。表5において各成分の配合量の単位は質量部である。得られた樹脂組成物ペレットを50tプレス機を用いて230℃、10MPa、5minの条件で溶融圧縮し、一辺の長さ10cm、厚み1.0mmの正方形シートを得た。得られたシートから直径25mmの円盤状の試験片を切り出し、この試片について、流動場結晶化温度を以下の手順で測定した。
Claims (5)
- ポリオレフィン系樹脂と、核剤と、を含む樹脂組成物であって、
前記核剤が、下記一般式(2)で表されるアセタール化合物(ただし、ジベンジリデンソルビトールおよびビス(4−メチルベンジリデン)ソルビトールを除く)を含み、
前記ポリオレフィン系樹脂100質量部に対する前記核剤の含有量が、0.005質量部以上0.08質量部以下であることを特徴とする樹脂組成物。
(一般式(2)中、R1は水素原子または炭素原子数1〜4のアルキル基を表し、R2、R3、R4およびR5はそれぞれ独立に水素原子、ハロゲン原子、シアノ基、炭素原子数1〜4のアルキル基または炭素原子数1〜4のアルコキシ基を表し、あるいはR2およびR3またはR4およびR5が互いに連結して炭素原子数3〜6のアルキレン基または炭素原子数1〜4のアルキレンジオキシ基を表し、Xは単結合、−CH(OH)−基または−CH(OH)CH(OH)−基を表す。) - 前記核剤の融点が、150〜300℃である請求項1または2記載の樹脂組成物。
- 請求項1〜3のうちいずれか一項記載の樹脂組成物を成形して得られることを特徴とする成形品。
- ポリオレフィン系樹脂に核剤を配合する工程を含む樹脂組成物の製造方法であって、
前記核剤が、下記一般式(2)で表されるアセタール化合物(ただし、ジベンジリデンソルビトールおよびビス(4−メチルベンジリデン)ソルビトールを除く)を含み、
前記樹脂組成物中における前記核剤の含有量が、前記ポリオレフィン系樹脂100質量部に対して0.005質量部以上0.08質量部以下となるように、前記核剤を配合することを特徴とする樹脂組成物の製造方法。
(一般式(2)中、R1は水素原子または炭素原子数1〜4のアルキル基を表し、R2、R3、R4およびR5はそれぞれ独立に水素原子、ハロゲン原子、シアノ基、炭素原子数1〜4のアルキル基または炭素原子数1〜4のアルコキシ基を表し、あるいはR2およびR3またはR4およびR5が互いに連結して炭素原子数3〜6のアルキレン基または炭素原子数1〜4のアルキレンジオキシ基を表し、Xは単結合、−CH(OH)−基または−CH(OH)CH(OH)−基を表す。)
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