JP2019123811A - はんだ付け用樹脂組成物、やに入りはんだ、フラックスコートはんだ及び液状フラックス - Google Patents
はんだ付け用樹脂組成物、やに入りはんだ、フラックスコートはんだ及び液状フラックス Download PDFInfo
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- JP2019123811A JP2019123811A JP2018005918A JP2018005918A JP2019123811A JP 2019123811 A JP2019123811 A JP 2019123811A JP 2018005918 A JP2018005918 A JP 2018005918A JP 2018005918 A JP2018005918 A JP 2018005918A JP 2019123811 A JP2019123811 A JP 2019123811A
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- Japan
- Prior art keywords
- acid
- reaction product
- resin composition
- linoleic
- trimer
- Prior art date
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- Granted
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- 239000011342 resin composition Substances 0.000 title claims abstract description 100
- 230000004907 flux Effects 0.000 title claims abstract description 54
- 239000007788 liquid Substances 0.000 title claims abstract description 35
- 239000011347 resin Substances 0.000 title claims abstract description 31
- 229920005989 resin Polymers 0.000 title claims abstract description 31
- 238000005476 soldering Methods 0.000 title description 47
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 claims abstract description 183
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 claims abstract description 183
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 claims abstract description 183
- 239000005642 Oleic acid Substances 0.000 claims abstract description 183
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 claims abstract description 183
- 239000002253 acid Substances 0.000 claims abstract description 183
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 claims abstract description 183
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims abstract description 183
- 239000000539 dimer Substances 0.000 claims abstract description 149
- 239000007795 chemical reaction product Substances 0.000 claims abstract description 146
- CFQZKFWQLAHGSL-FNTYJUCDSA-N (3e,5e,7e,9e,11e,13e,15e,17e)-18-[(3e,5e,7e,9e,11e,13e,15e,17e)-18-[(3e,5e,7e,9e,11e,13e,15e)-octadeca-3,5,7,9,11,13,15,17-octaenoyl]oxyoctadeca-3,5,7,9,11,13,15,17-octaenoyl]oxyoctadeca-3,5,7,9,11,13,15,17-octaenoic acid Chemical compound OC(=O)C\C=C\C=C\C=C\C=C\C=C\C=C\C=C\C=C\OC(=O)C\C=C\C=C\C=C\C=C\C=C\C=C\C=C\C=C\OC(=O)C\C=C\C=C\C=C\C=C\C=C\C=C\C=C\C=C CFQZKFWQLAHGSL-FNTYJUCDSA-N 0.000 claims abstract description 123
- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 claims abstract description 101
- OYHQOLUKZRVURQ-HZJYTTRNSA-N Linoleic acid Chemical compound CCCCC\C=C/C\C=C/CCCCCCCC(O)=O OYHQOLUKZRVURQ-HZJYTTRNSA-N 0.000 claims abstract description 85
- 235000020778 linoleic acid Nutrition 0.000 claims abstract description 85
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 claims abstract description 85
- 229910052739 hydrogen Inorganic materials 0.000 claims abstract description 76
- 239000001257 hydrogen Substances 0.000 claims abstract description 76
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims abstract description 75
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims abstract description 60
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims abstract description 60
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims abstract description 60
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- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 15
- 150000002896 organic halogen compounds Chemical class 0.000 claims description 6
- 150000002903 organophosphorus compounds Chemical class 0.000 claims description 5
- 230000000694 effects Effects 0.000 description 91
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- 239000007864 aqueous solution Substances 0.000 description 42
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 24
- -1 phenol modified rosin Chemical class 0.000 description 23
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 20
- 229910019142 PO4 Inorganic materials 0.000 description 18
- 239000010452 phosphate Substances 0.000 description 18
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 18
- 238000011156 evaluation Methods 0.000 description 17
- 238000009736 wetting Methods 0.000 description 15
- 230000000052 comparative effect Effects 0.000 description 13
- 239000007787 solid Substances 0.000 description 12
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 11
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 11
- 229960004488 linolenic acid Drugs 0.000 description 11
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 11
- 229910052751 metal Inorganic materials 0.000 description 11
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 10
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 10
- 239000001361 adipic acid Substances 0.000 description 10
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- 239000002184 metal Substances 0.000 description 10
- 150000003505 terpenes Chemical class 0.000 description 10
- 235000007586 terpenes Nutrition 0.000 description 10
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 9
- 238000000034 method Methods 0.000 description 8
- TYFQFVWCELRYAO-UHFFFAOYSA-N suberic acid Chemical compound OC(=O)CCCCCCC(O)=O TYFQFVWCELRYAO-UHFFFAOYSA-N 0.000 description 8
- 229910044991 metal oxide Inorganic materials 0.000 description 7
- 150000004706 metal oxides Chemical class 0.000 description 7
- 239000000203 mixture Substances 0.000 description 7
- 239000000047 product Substances 0.000 description 7
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- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 6
- 239000012190 activator Substances 0.000 description 6
- 238000012795 verification Methods 0.000 description 6
- 239000000654 additive Substances 0.000 description 5
- 230000000996 additive effect Effects 0.000 description 5
- 125000000217 alkyl group Chemical group 0.000 description 5
- 235000005985 organic acids Nutrition 0.000 description 5
- 150000003839 salts Chemical class 0.000 description 5
- 239000013638 trimer Substances 0.000 description 5
- RTBFRGCFXZNCOE-UHFFFAOYSA-N 1-methylsulfonylpiperidin-4-one Chemical compound CS(=O)(=O)N1CCC(=O)CC1 RTBFRGCFXZNCOE-UHFFFAOYSA-N 0.000 description 4
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 description 4
- CPELXLSAUQHCOX-UHFFFAOYSA-N Hydrogen bromide Chemical compound Br CPELXLSAUQHCOX-UHFFFAOYSA-N 0.000 description 4
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 4
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Natural products OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 4
- 239000004698 Polyethylene Substances 0.000 description 4
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 4
- 150000007513 acids Chemical class 0.000 description 4
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- JFCQEDHGNNZCLN-UHFFFAOYSA-N anhydrous glutaric acid Natural products OC(=O)CCCC(O)=O JFCQEDHGNNZCLN-UHFFFAOYSA-N 0.000 description 4
- 238000006243 chemical reaction Methods 0.000 description 4
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- 229930195729 fatty acid Natural products 0.000 description 4
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- 235000021355 Stearic acid Nutrition 0.000 description 3
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
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- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 3
- 150000004678 hydrides Chemical class 0.000 description 3
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 3
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- QMMJWQMCMRUYTG-UHFFFAOYSA-N 1,2,4,5-tetrachloro-3-(trifluoromethyl)benzene Chemical compound FC(F)(F)C1=C(Cl)C(Cl)=CC(Cl)=C1Cl QMMJWQMCMRUYTG-UHFFFAOYSA-N 0.000 description 2
- KOMNUTZXSVSERR-UHFFFAOYSA-N 1,3,5-tris(prop-2-enyl)-1,3,5-triazinane-2,4,6-trione Chemical compound C=CCN1C(=O)N(CC=C)C(=O)N(CC=C)C1=O KOMNUTZXSVSERR-UHFFFAOYSA-N 0.000 description 2
- ULQISTXYYBZJSJ-UHFFFAOYSA-N 12-hydroxyoctadecanoic acid Chemical compound CCCCCCC(O)CCCCCCCCCCC(O)=O ULQISTXYYBZJSJ-UHFFFAOYSA-N 0.000 description 2
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- SEGLCEQVOFDUPX-UHFFFAOYSA-N di-(2-ethylhexyl)phosphoric acid Chemical compound CCCCC(CC)COP(O)(=O)OCC(CC)CCCC SEGLCEQVOFDUPX-UHFFFAOYSA-N 0.000 description 1
- WBJBEMDHFMUSAY-UHFFFAOYSA-N dibutyl phosphono phosphate Chemical compound CCCCOP(=O)(OP(O)(O)=O)OCCCC WBJBEMDHFMUSAY-UHFFFAOYSA-N 0.000 description 1
- 150000001991 dicarboxylic acids Chemical class 0.000 description 1
- 230000000447 dimerizing effect Effects 0.000 description 1
- 125000003438 dodecyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 description 1
- MCPKSFINULVDNX-UHFFFAOYSA-N drometrizole Chemical compound CC1=CC=C(O)C(N2N=C3C=CC=CC3=N2)=C1 MCPKSFINULVDNX-UHFFFAOYSA-N 0.000 description 1
- QYDYPVFESGNLHU-UHFFFAOYSA-N elaidic acid methyl ester Natural products CCCCCCCCC=CCCCCCCCC(=O)OC QYDYPVFESGNLHU-UHFFFAOYSA-N 0.000 description 1
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- 150000002148 esters Chemical class 0.000 description 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 description 1
- 125000001153 fluoro group Chemical group F* 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
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- 229910000040 hydrogen fluoride Inorganic materials 0.000 description 1
- XMBWDFGMSWQBCA-UHFFFAOYSA-N hydrogen iodide Chemical compound I XMBWDFGMSWQBCA-UHFFFAOYSA-N 0.000 description 1
- 229910000043 hydrogen iodide Inorganic materials 0.000 description 1
- 125000004029 hydroxymethyl group Chemical group [H]OC([H])([H])* 0.000 description 1
- RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Substances C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 description 1
- 229910000765 intermetallic Inorganic materials 0.000 description 1
- 229910052740 iodine Inorganic materials 0.000 description 1
- 239000011630 iodine Substances 0.000 description 1
- QPPQHRDVPBTVEV-UHFFFAOYSA-N isopropyl dihydrogen phosphate Chemical compound CC(C)OP(O)(O)=O QPPQHRDVPBTVEV-UHFFFAOYSA-N 0.000 description 1
- XUGNVMKQXJXZCD-UHFFFAOYSA-N isopropyl palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC(C)C XUGNVMKQXJXZCD-UHFFFAOYSA-N 0.000 description 1
- 125000002463 lignoceryl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 1
- 239000011976 maleic acid Substances 0.000 description 1
- 239000001630 malic acid Substances 0.000 description 1
- 235000011090 malic acid Nutrition 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- QYDYPVFESGNLHU-KHPPLWFESA-N methyl oleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC QYDYPVFESGNLHU-KHPPLWFESA-N 0.000 description 1
- 229940073769 methyl oleate Drugs 0.000 description 1
- XLSZMDLNRCVEIJ-UHFFFAOYSA-N methylimidazole Natural products CC1=CNC=N1 XLSZMDLNRCVEIJ-UHFFFAOYSA-N 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- REOJLIXKJWXUGB-UHFFFAOYSA-N mofebutazone Chemical group O=C1C(CCCC)C(=O)NN1C1=CC=CC=C1 REOJLIXKJWXUGB-UHFFFAOYSA-N 0.000 description 1
- 150000002762 monocarboxylic acid derivatives Chemical class 0.000 description 1
- 150000002763 monocarboxylic acids Chemical class 0.000 description 1
- OKQVTLCUHATGDD-UHFFFAOYSA-N n-(benzotriazol-1-ylmethyl)-2-ethyl-n-(2-ethylhexyl)hexan-1-amine Chemical compound C1=CC=C2N(CN(CC(CC)CCCC)CC(CC)CCCC)N=NC2=C1 OKQVTLCUHATGDD-UHFFFAOYSA-N 0.000 description 1
- QGLKNQRTHJUNFJ-UHFFFAOYSA-N n-(benzotriazol-1-ylmethyl)-2-ethylhexan-1-amine Chemical compound C1=CC=C2N(CNCC(CC)CCCC)N=NC2=C1 QGLKNQRTHJUNFJ-UHFFFAOYSA-N 0.000 description 1
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- UHGIMQLJWRAPLT-UHFFFAOYSA-N octadecyl dihydrogen phosphate Chemical compound CCCCCCCCCCCCCCCCCCOP(O)(O)=O UHGIMQLJWRAPLT-UHFFFAOYSA-N 0.000 description 1
- 229940073665 octyldodecyl myristate Drugs 0.000 description 1
- 235000021313 oleic acid Nutrition 0.000 description 1
- 125000001117 oleyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])/C([H])=C([H])\C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 1
- 125000005010 perfluoroalkyl group Chemical group 0.000 description 1
- 229960005323 phenoxyethanol Drugs 0.000 description 1
- 229940081066 picolinic acid Drugs 0.000 description 1
- 229920002587 poly(1,3-butadiene) polymer Polymers 0.000 description 1
- 229920003216 poly(methylphenylsiloxane) Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920005862 polyol Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920005606 polypropylene copolymer Polymers 0.000 description 1
- 229920001343 polytetrafluoroethylene Polymers 0.000 description 1
- 239000004810 polytetrafluoroethylene Substances 0.000 description 1
- 229920002451 polyvinyl alcohol Polymers 0.000 description 1
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 description 1
- LOAUVZALPPNFOQ-UHFFFAOYSA-N quinaldic acid Chemical compound C1=CC=CC2=NC(C(=O)O)=CC=C21 LOAUVZALPPNFOQ-UHFFFAOYSA-N 0.000 description 1
- 229920003987 resole Polymers 0.000 description 1
- 229960004889 salicylic acid Drugs 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 229920005792 styrene-acrylic resin Polymers 0.000 description 1
- 150000003440 styrenes Chemical class 0.000 description 1
- 239000003784 tall oil Substances 0.000 description 1
- 239000003760 tallow Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- WJCNZQLZVWNLKY-UHFFFAOYSA-N thiabendazole Chemical compound S1C=NC(C=2NC3=CC=CC=C3N=2)=C1 WJCNZQLZVWNLKY-UHFFFAOYSA-N 0.000 description 1
- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
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- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
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- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
- B23K35/36—Selection of non-metallic compositions, e.g. coatings, fluxes; Selection of soldering or welding materials, conjoint with selection of non-metallic compositions, both selections being of interest
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- B—PERFORMING OPERATIONS; TRANSPORTING
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- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
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- B23K35/24—Selection of soldering or welding materials proper
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- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
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- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
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- B23K35/3616—Halogen compounds
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- B23K35/00—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting
- B23K35/22—Rods, electrodes, materials, or media, for use in soldering, welding, or cutting characterised by the composition or nature of the material
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Abstract
Description
本実施の形態の樹脂組成物は、オレイン酸とリノール酸の反応物であるダイマー酸、オレイン酸とリノール酸の反応物であるトリマー酸、オレイン酸とリノール酸の反応物であるダイマー酸に水素を添加した水添ダイマー酸またはオレイン酸とリノール酸の反応物であるトリマー酸に水素を添加した水添トリマー酸のいずれか、あるいは、オレイン酸とリノール酸の反応物であるダイマー酸、オレイン酸とリノール酸の反応物であるトリマー酸、オレイン酸とリノール酸の反応物であるダイマー酸に水素を添加した水添ダイマー酸及びオレイン酸とリノール酸の反応物であるトリマー酸に水素を添加した水添トリマー酸の2種以上とロジンとを含む。
本実施の形態のやに入りはんだは、上述した樹脂組成物が充填された線状のはんだである。やに入りはんだに使用される樹脂組成物は、はんだを線状に加工する工程で流れ出さないように常温で固形であること、あるいは流れ出さないような所定の高粘度であることが求められる。なお、やに入りはんだで使用される場合に樹脂組成物に求められる粘度は、例えば3500Pa・s以上である。
本実施の形態のフラックスコートはんだは、上述した樹脂組成物で被覆されたはんだである。はんだは、ボールと称す球状、カラム、ペレット等と称す円柱等の柱状の形状である。はんだを被覆した状態の樹脂組成物は、常温でははんだの表面に付着した固形である。
本実施の形態の液状フラックスは、上述した樹脂組成物を溶剤で希釈したものであり、液体の様態で使用する用途に適用される。液状フラックスは、フラックスの全量を100とした場合、樹脂組成物を1wt%以上25wt%以下、溶剤を75wt%以上99wt%含む。液状フラックスで使用される溶剤は、イソプロピルアルコールであることが好ましい。
オレイン酸とリノール酸の反応物であるダイマー酸、オレイン酸とリノール酸の反応物であるトリマー酸、オレイン酸とリノール酸の反応物であるダイマー酸に水素を添加した水添ダイマー酸またはオレイン酸とリノール酸の反応物であるトリマー酸に水素を添加した水添トリマー酸のいずれか、あるいは、オレイン酸とリノール酸の反応物であるダイマー酸、オレイン酸とリノール酸の反応物であるトリマー酸、オレイン酸とリノール酸の反応物であるダイマー酸に水素を添加した水添ダイマー酸及びオレイン酸とリノール酸の反応物であるトリマー酸に水素を添加した水添トリマー酸の2種以上の合計を1wt%以上40wt%以下、ロジンを30wt%以上99wt%以下含む樹脂組成物は、常温で固形または所定の粘性を持つ様態となる。また、はんだの融点を超える温度までの加熱でロジンの粘性が低下して流れ、かつ、オレイン酸とリノール酸の反応物であるダイマー酸、オレイン酸とリノール酸の反応物であるトリマー酸、オレイン酸とリノール酸の反応物であるダイマー酸に水素を添加した水添ダイマー酸またはオレイン酸とリノール酸の反応物であるトリマー酸に水素を添加した水添トリマー酸の揮発が抑制されて金属酸化物に対する活性を持つ。
(1)検証方法
はんだの濡れ広がり性の評価は、実施例、比較例の樹脂組成物を使用したやに入りはんだを試料として用意した。はんだは、Sn−3Ag−0.5Cuと表記される組成であり、Agを3.0wt%、Cuを0.5wt%含み、残部がSnである。やに入りはんだの直径はφ0.8mm、やに入りはんだの全量を100とした場合、はんだが97wt%、樹脂組成物が3wt%である。このやに入りハンダを使用し、JIS 3197 8.3.1.1に準拠して濡れ広がり率を算出した。
〇:濡れ広がり率が70%以上であった
×:濡れ広がり率が70%未満であった
(1)検証方法
水溶液比抵抗の評価は、実施例、比較例の樹脂組成物をイソプロピルアルコールで希釈して液状の試料とした。試料の全量を100とした場合、樹脂組成物が25wt%、イソプロピルアルコールが75wt%である。各試料を用いて、JIS 3197 8.1.1に準拠して水溶液比抵抗を測定した。
〇:水溶液比抵抗が500Ωm以上であった
×:水溶液比抵抗が500Ωm未満であった
(1)検証方法
実施例、比較例の樹脂組成物を試料とし、25℃における状態を観察して、固形及び液体のいずれであるかを判定した。
〇:25℃における状態が固形あった
×:25℃における状態が液体であった
〇:濡れ広がり評価、水溶液比抵抗評価及び加工性評価の何れも〇であった
×:濡れ広がり評価、水溶液比抵抗評価及び加工性評価の何れか、または全てが×であった
本実施の形態のはんだ付け用樹脂組成物は、オレイン酸とリノール酸の反応物であるダイマー酸、オレイン酸とリノール酸の反応物であるトリマー酸、オレイン酸とリノール酸の反応物であるダイマー酸に水素を添加した水添ダイマー酸またはオレイン酸とリノール酸の反応物であるトリマー酸に水素を添加した水添トリマー酸のいずれか、あるいは、オレイン酸とリノール酸の反応物であるダイマー酸、オレイン酸とリノール酸の反応物であるトリマー酸、オレイン酸とリノール酸の反応物であるダイマー酸に水素を添加した水添ダイマー酸及びオレイン酸とリノール酸の反応物であるトリマー酸に水素を添加した水添トリマー酸の2種以上とロジンとを含む。
本実施の形態のやに入りはんだは、上述したはんだ付け用樹脂組成物が充填された線状のはんだである。やに入りはんだに使用されるはんだ付け用樹脂組成物は、はんだを線状に加工する工程で流れ出さないように常温で固形であること、あるいは流れ出さないような所定の高粘度であることが求められる。なお、やに入りはんだで使用される場合にはんだ付け用樹脂組成物に求められる粘度は、例えば3500Pa・s以上である。
本実施の形態のフラックスコートはんだは、上述したはんだ付け用樹脂組成物で被覆されたはんだである。はんだは、ボールと称す球状、カラム、ペレット等と称す円柱等の柱状の形状である。はんだを被覆した状態のはんだ付け用樹脂組成物は、常温でははんだの表面に付着した固形である。
本実施の形態の液状フラックスは、上述したはんだ付け用樹脂組成物を溶剤で希釈したものであり、液体の様態で使用する用途に適用される。液状フラックスは、フラックスの全量を100とした場合、はんだ付け用樹脂組成物を1wt%以上25wt%以下、溶剤を75wt%以上99wt%含む。液状フラックスで使用される溶剤は、イソプロピルアルコールであることが好ましい。
オレイン酸とリノール酸の反応物であるダイマー酸、オレイン酸とリノール酸の反応物であるトリマー酸、オレイン酸とリノール酸の反応物であるダイマー酸に水素を添加した水添ダイマー酸またはオレイン酸とリノール酸の反応物であるトリマー酸に水素を添加した水添トリマー酸のいずれか、あるいは、オレイン酸とリノール酸の反応物であるダイマー酸、オレイン酸とリノール酸の反応物であるトリマー酸、オレイン酸とリノール酸の反応物であるダイマー酸に水素を添加した水添ダイマー酸及びオレイン酸とリノール酸の反応物であるトリマー酸に水素を添加した水添トリマー酸の2種以上の合計を1wt%以上40wt%以下、ロジンを30wt%以上99wt%以下含むはんだ付け用樹脂組成物は、常温で固形または所定の粘性を持つ様態となる。また、はんだの融点を超える温度までの加熱でロジンの粘性が低下して流れ、かつ、オレイン酸とリノール酸の反応物であるダイマー酸、オレイン酸とリノール酸の反応物であるトリマー酸、オレイン酸とリノール酸の反応物であるダイマー酸に水素を添加した水添ダイマー酸またはオレイン酸とリノール酸の反応物であるトリマー酸に水素を添加した水添トリマー酸の揮発が抑制されて金属酸化物に対する活性を持つ。
(1)検証方法
はんだの濡れ広がり性の評価は、実施例、比較例のはんだ付け用樹脂組成物を使用したやに入りはんだを試料として用意した。はんだは、Sn−3Ag−0.5Cuと表記される組成であり、Agを3.0wt%、Cuを0.5wt%含み、残部がSnである。やに入りはんだの直径はφ0.8mm、やに入りはんだの全量を100とした場合、はんだが97wt%、はんだ付け用樹脂組成物が3wt%である。このやに入りハンダを使用し、JIS 3197 8.3.1.1に準拠して濡れ広がり率を算出した。
(1)検証方法
水溶液比抵抗の評価は、実施例、比較例のはんだ付け用樹脂組成物をイソプロピルアルコールで希釈して液状の試料とした。試料の全量を100とした場合、はんだ付け用樹脂組成物が25wt%、イソプロピルアルコールが75wt%である。各試料を用いて、JIS 3197 8.1.1に準拠して水溶液比抵抗を測定した。
(1)検証方法
実施例、比較例のはんだ付け用樹脂組成物を試料とし、25℃における状態を観察して、固形及び液体のいずれであるかを判定した。
Claims (13)
- オレイン酸とリノール酸の反応物であるダイマー酸、オレイン酸とリノール酸の反応物であるトリマー酸、オレイン酸とリノール酸の反応物であるダイマー酸に水素を添加した水添ダイマー酸またはオレイン酸とリノール酸の反応物であるトリマー酸に水素を添加した水添トリマー酸のいずれか、あるいは、オレイン酸とリノール酸の反応物であるダイマー酸、オレイン酸とリノール酸の反応物であるトリマー酸、オレイン酸とリノール酸の反応物であるダイマー酸に水素を添加した水添ダイマー酸及びオレイン酸とリノール酸の反応物であるトリマー酸に水素を添加した水添トリマー酸の2種以上の合計を1wt%以上40wt%以下、
ロジンを30wt%以上99wt%以下含む
ことを特徴とする樹脂組成物。 - さらに有機酸を0wt%以上4wt%以下含む
ことを特徴とする請求項1に記載の樹脂組成物。 - さらにアミンを0wt%以上2wt%以下含む
ことを特徴とする請求項1または請求項2に記載の樹脂組成物。 - さらに有機ハロゲン化合物を0wt%以上5wt%以下含む
ことを特徴とする請求項1〜請求項3の何れか1項に記載の樹脂組成物。 - さらにアミンハロゲン化水素酸塩を0wt%以上1wt%以下含む
ことを特徴とする請求項1〜請求項4の何れか1項に記載の樹脂組成物。 - さらに溶剤を0wt%以上13wt%以下含む
ことを特徴とする請求項1〜請求項5の何れか1項に記載の樹脂組成物。 - さらに消泡剤を0wt%以上3wt%以下含む
ことを特徴とする請求項1〜請求項6の何れか1項に記載の樹脂組成物。 - さらにシリコーンオイルを0wt%以上5wt%以下含む
ことを特徴とする請求項1〜請求項7の何れか1項に記載の樹脂組成物。 - さらに有機リン化合物を0wt%以上10wt%以下含む
ことを特徴とする請求項1〜請求項8の何れか1項に記載の樹脂組成物。 - さらに他の樹脂を0wt%以上40wt%以下含む
ことを特徴とする請求項1〜請求項9の何れか1項に記載の樹脂組成物。 - 請求項1〜請求項10の何れか1項に記載の樹脂組成物が線状のはんだに充填された
ことを特徴とするやに入りはんだ。 - 請求項1〜請求項10の何れか1項に記載の樹脂組成物ではんだを被覆した
ことを特徴とするフラックスコートはんだ。 - 請求項1〜請求項10の何れか1項に記載の樹脂組成物と溶剤からなる
ことを特徴とする液状フラックス。
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JP2018005918A JP6501003B1 (ja) | 2018-01-17 | 2018-01-17 | はんだ付け用樹脂組成物、やに入りはんだ、フラックスコートはんだ及び液状フラックス |
MYPI2020003695A MY182969A (en) | 2018-01-17 | 2019-01-15 | Resin composition for soldering, resin flux cored solder, flux coated solder, and liquid flux |
PCT/JP2019/000970 WO2019142795A1 (ja) | 2018-01-17 | 2019-01-15 | はんだ付け用樹脂組成物、やに入りはんだ、フラックスコートはんだ及び液状フラックス |
US16/960,002 US11292089B2 (en) | 2018-01-17 | 2019-01-15 | Resin composition for soldering, resin flux cored solder, flux coated solder, and liquid flux |
DE112019000443.3T DE112019000443T5 (de) | 2018-01-17 | 2019-01-15 | Harzzusammensetzung zum löten, röhrenlot mit harzflussmittelseele, flussmittelbeschichtetes lot und flüssiges flussmittel |
SG11202006009XA SG11202006009XA (en) | 2018-01-17 | 2019-01-15 | Resin composition for soldering, resin flux cored solder, flux coated solder, and liquid flux |
CN201980009043.7A CN111587162B (zh) | 2018-01-17 | 2019-01-15 | 焊接用树脂组合物、树脂芯焊料、焊剂皮焊料及液态焊剂 |
TW108101784A TWI714949B (zh) | 2018-01-17 | 2019-01-17 | 焊接用樹脂組合物、包芯焊料、塗覆助焊劑焊料及液狀助焊劑 |
PH12020551092A PH12020551092A1 (en) | 2018-01-17 | 2020-07-17 | Resin composition for soldering, resin flux cored solder, flux coated solder, and liquid flux |
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CN113020841A (zh) * | 2019-12-25 | 2021-06-25 | 千住金属工业株式会社 | 助焊剂、包芯软钎料和软钎焊方法 |
KR20230096100A (ko) * | 2020-12-11 | 2023-06-29 | 센주긴조쿠고교 가부시키가이샤 | 송진 함유 땜납용 플럭스, 송진 함유 땜납 및 납땜 방법 |
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JP7407781B2 (ja) | 2020-12-11 | 2024-01-04 | 千住金属工業株式会社 | やに入りはんだ用フラックス、やに入りはんだ及びはんだ付け方法 |
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JP6338007B1 (ja) * | 2017-11-02 | 2018-06-06 | 千住金属工業株式会社 | フラックス及びソルダペースト |
JP6399242B1 (ja) * | 2018-01-17 | 2018-10-03 | 千住金属工業株式会社 | フラックス及びソルダペースト |
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JP2021030276A (ja) * | 2019-08-27 | 2021-03-01 | 株式会社タムラ製作所 | フラックス及び成形はんだ |
JP2021053653A (ja) * | 2019-09-27 | 2021-04-08 | 株式会社タムラ製作所 | はんだ付け用フラックス組成物 |
CN113020841A (zh) * | 2019-12-25 | 2021-06-25 | 千住金属工业株式会社 | 助焊剂、包芯软钎料和软钎焊方法 |
CN113020841B (zh) * | 2019-12-25 | 2022-09-27 | 千住金属工业株式会社 | 助焊剂、包芯软钎料和软钎焊方法 |
KR20230096100A (ko) * | 2020-12-11 | 2023-06-29 | 센주긴조쿠고교 가부시키가이샤 | 송진 함유 땜납용 플럭스, 송진 함유 땜납 및 납땜 방법 |
KR102661293B1 (ko) | 2020-12-11 | 2024-04-30 | 센주긴조쿠고교 가부시키가이샤 | 송진 함유 땜납용 플럭스, 송진 함유 땜납 및 납땜 방법 |
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TW201940598A (zh) | 2019-10-16 |
CN111587162B (zh) | 2022-03-04 |
MY182969A (en) | 2021-02-05 |
JP6501003B1 (ja) | 2019-04-17 |
SG11202006009XA (en) | 2020-08-28 |
US11292089B2 (en) | 2022-04-05 |
WO2019142795A1 (ja) | 2019-07-25 |
US20200391329A1 (en) | 2020-12-17 |
PH12020551092A1 (en) | 2021-09-06 |
DE112019000443T5 (de) | 2020-10-01 |
TWI714949B (zh) | 2021-01-01 |
CN111587162A (zh) | 2020-08-25 |
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