JP2016041073A5 - - Google Patents
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- JP2016041073A5 JP2016041073A5 JP2015207779A JP2015207779A JP2016041073A5 JP 2016041073 A5 JP2016041073 A5 JP 2016041073A5 JP 2015207779 A JP2015207779 A JP 2015207779A JP 2015207779 A JP2015207779 A JP 2015207779A JP 2016041073 A5 JP2016041073 A5 JP 2016041073A5
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- Prior art keywords
- extract
- effluent
- aqueous solution
- lacanca
- activated carbon
- Prior art date
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- OKTJSMMVPCPJKN-UHFFFAOYSA-N carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 18
- 239000007864 aqueous solution Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 235000013399 edible fruits Nutrition 0.000 claims description 3
- 239000007787 solid Substances 0.000 claims description 2
- 239000012528 membrane Substances 0.000 claims 4
- 239000011347 resin Substances 0.000 claims 4
- 229920005989 resin Polymers 0.000 claims 4
- 239000003456 ion exchange resin Substances 0.000 claims 3
- 229920003303 ion-exchange polymer Polymers 0.000 claims 3
- 229920000642 polymer Polymers 0.000 claims 3
- RPYRMTHVSUWHSV-CUZJHZIBSA-N Rebaudioside D Chemical compound O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O RPYRMTHVSUWHSV-CUZJHZIBSA-N 0.000 claims 2
- 239000007921 spray Substances 0.000 claims 2
- GHBNZZJYBXQAHG-KUVSNLSMSA-N (2R,3R,4S,5S,6R)-2-[[(2R,3S,4S,5R,6R)-6-[[(3S,8S,9R,10R,11R,13R,14S,17R)-17-[(2R,5R)-5-[(2S,3R,4S,5S,6R)-4,5-dihydroxy-3-[(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy-6-[[(2R,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy Chemical compound C([C@H]1O[C@H]([C@@H]([C@@H](O)[C@@H]1O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@H](CC[C@@H](C)[C@@H]1[C@]2(C[C@@H](O)[C@@]3(C)[C@H]4C(C([C@@H](O[C@H]5[C@@H]([C@@H](O)[C@H](O)[C@@H](CO[C@H]6[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O6)O)O5)O)CC4)(C)C)=CC[C@H]3[C@]2(C)CC1)C)C(C)(C)O)O[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O GHBNZZJYBXQAHG-KUVSNLSMSA-N 0.000 claims 1
- 239000001512 FEMA 4601 Substances 0.000 claims 1
- HELXLJCILKEWJH-SEAGSNCFSA-N Rebaudioside A Natural products O=C(O[C@H]1[C@@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1)[C@@]1(C)[C@@H]2[C@](C)([C@H]3[C@@]4(CC(=C)[C@@](O[C@H]5[C@H](O[C@H]6[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O6)[C@@H](O[C@H]6[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O6)[C@H](O)[C@@H](CO)O5)(C4)CC3)CC2)CCC1 HELXLJCILKEWJH-SEAGSNCFSA-N 0.000 claims 1
- DRSKVOAJKLUMCL-UHFFFAOYSA-N Rebaudioside B Chemical compound C1CC2C3(C)CCCC(C)(C(O)=O)C3CCC2(C2)CC(=C)C21OC(C1OC2C(C(O)C(O)C(CO)O2)O)OC(CO)C(O)C1OC1OC(CO)C(O)C(O)C1O DRSKVOAJKLUMCL-UHFFFAOYSA-N 0.000 claims 1
- 240000001132 Stevia rebaudiana Species 0.000 claims 1
- 239000004383 Steviol glycoside Substances 0.000 claims 1
- HELXLJCILKEWJH-NCGAPWICSA-N Stevioside A3 Chemical group O([C@H]1[C@H](O)[C@@H](CO)O[C@H]([C@@H]1O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@]12C(=C)C[C@@]3(C1)CC[C@@H]1[C@@](C)(CCC[C@]1([C@@H]3CC2)C)C(=O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O HELXLJCILKEWJH-NCGAPWICSA-N 0.000 claims 1
- 125000000129 anionic group Chemical group 0.000 claims 1
- 238000001704 evaporation Methods 0.000 claims 1
- 238000001728 nano-filtration Methods 0.000 claims 1
- 235000019203 rebaudioside A Nutrition 0.000 claims 1
- 238000001223 reverse osmosis Methods 0.000 claims 1
- 235000019411 steviol glycoside Nutrition 0.000 claims 1
- 150000008144 steviol glycosides Chemical class 0.000 claims 1
- 235000019202 steviosides Nutrition 0.000 claims 1
- 239000000126 substance Substances 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 2
- 235000019749 Dry matter Nutrition 0.000 description 1
- 239000008367 deionised water Substances 0.000 description 1
- 238000010828 elution Methods 0.000 description 1
- 230000002708 enhancing Effects 0.000 description 1
- 239000012527 feed solution Substances 0.000 description 1
- 239000010419 fine particle Substances 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
Description
典型的な工程では、カラムには必要量の活性炭（典型的には顆粒状）が充填され、脱イオン水をカラムの頂部から底部、又は底部から頂部へ（下降又は上昇方向へ）、１時間当たり1〜10ベッド体積(bed volume）の範囲で流した。通す水量は2〜5ベッド体積であってもよい。水を活性炭と接触させる際、水温を上昇させてもよい（例えば135°Ｆ〜185°F）。これにより、ラカンカ果実抽出物水溶液が実質的にカラムを通過する際、炭素から重金属などの望ましくない物質の溶出を減らす助けとなる。一度、残留する気泡及び炭素由来の微細粒子を水で置換え、ラカンカ果実抽出物の水溶液を、１時間当たり1〜10 のベッド体積の流速でカラムへ供給する。該カラムはジャケットでカバーされ、ジャケット温度を送液(feed solution)と同温度に維持する。その温度範囲は典型的には室温〜71℃である。初めにカラム中の移動相を水で置換する。流出液中に物質の存在が示された時点ですぐ、風味向上物質の流出液として集める。ＲＩ（refractive index）測定により流出液中の固体物質の存在を確認することができる。ＲＩと乾燥物質との相関関係は、典型的にはこの目的のために構築される。
Claims (14)
- ラカンカ抽出物を精製する方法であって、ラカンカ抽出物を活性炭と接触させることを含み、ここでモグロサイドＶが乾燥固体基準でラカンカ抽出物の少なくとも４０％を占め、活性炭との接触時にラカンカ抽出物が水溶液の形態であり、前記水溶液を、１３５〜１８５°Ｆの表面積１００ｍ２／ｇ以上の粒状活性炭に一時間当たり流速１〜１０床体積で通過させる、方法。
- 前記ラカンカ抽出物は予めマクロ多孔性高分子吸着樹脂と接触させたものである、請求項１に記載の方法。
- 前記ラカンカ抽出物は予めマクロ多孔性高分子吸着樹脂及びイオン交換樹脂の双方と接触させたものである、請求項１に記載の方法。
- 前記ラカンカ抽出物は予め、最初にマクロ多孔性高分子吸着樹脂と、次にイオン交換樹脂と接触させたものである、請求項１に記載の方法。
- 前記ラカンカ抽出物は予めアニオン性樹脂であるイオン交換樹脂と接触させたものである、請求項１に記載の方法。
- 活性炭と接触させる前記ラカンカ抽出物は水溶液の形態である、請求項１に記載の方法。
- 活性炭と接触させる前記ラカンカ抽出物の水溶液は予め、ラカンカ果物の粉末化乾燥抽出物を水に溶解させることにより、水溶液として調製されたものである、請求項１に記載の方法。
- 前記水溶液を精密濾過する、請求項７に記載の方法。
- 前記水溶液を前記の粒状活性炭のカラムに通過させて流出液を取得し、続いて前記流出液を濃縮する、請求項１に記載の方法。
- 前記流出液をエバポレーション又は膜濃縮により濃縮する、請求項９に記載の方法。
- ナノ濾過膜又は逆浸透膜を用いて前記流出液を膜濃縮する、請求項９に記載の方法。
- 濃縮に続いて前記流出液を乾燥させる、請求項９に記載の方法。
- 噴霧乾燥器又は噴霧凝集器を用いて前記流出液を乾燥させる、請求項１２に記載の方法。
- 濃縮に続いて前記流出液を、レバウディオサイドＡ、レバウディオサイドＢ、レバウディオサイドＤ、ステビオール配糖体、及び精製ステビア抽出物からなる群より選択される１又は２以上の成分と混合し、次いで乾燥させる、請求項９に記載の方法。
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161437399P | 2011-01-28 | 2011-01-28 | |
| US61/437,399 | 2011-01-28 |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013551285A Division JP6014051B2 (ja) | 2011-01-28 | 2012-01-24 | レバウディオサイド−モグロサイドｖ混合物 |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017010434A Division JP6702897B2 (ja) | 2011-01-28 | 2017-01-24 | レバウディオサイド−モグロサイドｖ混合物 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2016041073A JP2016041073A (ja) | 2016-03-31 |
| JP2016041073A5 true JP2016041073A5 (ja) | 2018-06-07 |
| JP6430917B2 JP6430917B2 (ja) | 2018-11-28 |
Family
ID=45563586
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013551285A Active JP6014051B2 (ja) | 2011-01-28 | 2012-01-24 | レバウディオサイド−モグロサイドｖ混合物 |
| JP2015207779A Active JP6430917B2 (ja) | 2011-01-28 | 2015-10-22 | レバウディオサイド−モグロサイドｖ混合物 |
| JP2017010434A Active JP6702897B2 (ja) | 2011-01-28 | 2017-01-24 | レバウディオサイド−モグロサイドｖ混合物 |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2013551285A Active JP6014051B2 (ja) | 2011-01-28 | 2012-01-24 | レバウディオサイド−モグロサイドｖ混合物 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2017010434A Active JP6702897B2 (ja) | 2011-01-28 | 2017-01-24 | レバウディオサイド−モグロサイドｖ混合物 |
Country Status (14)
| Country | Link |
|---|---|
| US (3) | US8962698B2 (ja) |
| EP (2) | EP3111781B1 (ja) |
| JP (3) | JP6014051B2 (ja) |
| KR (1) | KR101809183B1 (ja) |
| CN (2) | CN105124520B (ja) |
| AR (2) | AR084936A1 (ja) |
| AU (1) | AU2012209241B2 (ja) |
| BR (2) | BR122021007625B1 (ja) |
| CA (2) | CA2989105C (ja) |
| ES (2) | ES2642351T3 (ja) |
| IL (1) | IL227514A (ja) |
| MX (1) | MX343289B (ja) |
| RU (1) | RU2596978C2 (ja) |
| WO (1) | WO2012103074A2 (ja) |
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| GB201310060D0 (en) | 2013-03-15 | 2013-07-17 | Tate & Lyle Americas Llc | Redistribution of mogrol glyoside contact |
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