DE2630742C3 - Verfahren zur Gewinnung und Reinigung von Germanium aus Zinkerzen - Google Patents

Verfahren zur Gewinnung und Reinigung von Germanium aus Zinkerzen

Info

Publication number
DE2630742C3
DE2630742C3 DE2630742A DE2630742A DE2630742C3 DE 2630742 C3 DE2630742 C3 DE 2630742C3 DE 2630742 A DE2630742 A DE 2630742A DE 2630742 A DE2630742 A DE 2630742A DE 2630742 C3 DE2630742 C3 DE 2630742C3
Authority
DE
Germany
Prior art keywords
germanium
distillation
zinc
solution
extraction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE2630742A
Other languages
German (de)
English (en)
Other versions
DE2630742A1 (de
DE2630742B2 (de
Inventor
Jean-Michel Viroflay Demarthe
Paul Elancourt Fossi
Albert Courscelles-Les- Lens Lebleu
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
MINIERE ET METALLURGIQUE DE PENARROYA PARIS Ste
Original Assignee
MINIERE ET METALLURGIQUE DE PENARROYA PARIS Ste
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by MINIERE ET METALLURGIQUE DE PENARROYA PARIS Ste filed Critical MINIERE ET METALLURGIQUE DE PENARROYA PARIS Ste
Publication of DE2630742A1 publication Critical patent/DE2630742A1/de
Publication of DE2630742B2 publication Critical patent/DE2630742B2/de
Application granted granted Critical
Publication of DE2630742C3 publication Critical patent/DE2630742C3/de
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G17/00—Compounds of germanium
    • C01G17/04—Halides of germanium
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G17/00—Compounds of germanium
    • C01G17/003—Preparation involving a liquid-liquid extraction, an adsorption or an ion-exchange
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
    • C01G17/00—Compounds of germanium
    • C01G17/02—Germanium dioxide
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)
DE2630742A 1975-07-08 1976-07-08 Verfahren zur Gewinnung und Reinigung von Germanium aus Zinkerzen Expired DE2630742C3 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR7521327A FR2317366A1 (fr) 1975-07-08 1975-07-08 Procede pour la recuperation et la purification de germanium a partir de minerais de zinc

Publications (3)

Publication Number Publication Date
DE2630742A1 DE2630742A1 (de) 1977-01-20
DE2630742B2 DE2630742B2 (de) 1977-07-28
DE2630742C3 true DE2630742C3 (de) 1978-03-23

Family

ID=9157637

Family Applications (1)

Application Number Title Priority Date Filing Date
DE2630742A Expired DE2630742C3 (de) 1975-07-08 1976-07-08 Verfahren zur Gewinnung und Reinigung von Germanium aus Zinkerzen

Country Status (12)

Country Link
US (1) US4090871A (US20080094685A1-20080424-C00004.png)
JP (1) JPS6034498B2 (US20080094685A1-20080424-C00004.png)
AU (1) AU497928B2 (US20080094685A1-20080424-C00004.png)
BE (1) BE843453A (US20080094685A1-20080424-C00004.png)
CA (1) CA1083358A (US20080094685A1-20080424-C00004.png)
DE (1) DE2630742C3 (US20080094685A1-20080424-C00004.png)
FR (1) FR2317366A1 (US20080094685A1-20080424-C00004.png)
GB (1) GB1526115A (US20080094685A1-20080424-C00004.png)
IT (1) IT1069436B (US20080094685A1-20080424-C00004.png)
PL (1) PL110332B1 (US20080094685A1-20080424-C00004.png)
YU (1) YU39214B (US20080094685A1-20080424-C00004.png)
ZM (1) ZM9176A1 (US20080094685A1-20080424-C00004.png)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4389379A (en) * 1980-08-15 1983-06-21 Societe Miniere Et Metallurgique De Penarroya Process for selective liquid-liquid extraction of germanium
DE3635450A1 (de) * 1986-10-18 1988-04-21 Metallgesellschaft Ag Verfahren zur selektiven gewinnung von germanium und/oder arsen aus waessrigen loesungen
FR2623522B1 (fr) * 1987-11-24 1990-04-20 Metaleurop Sa Procede de traitement hydrometallurgique d'une solution de chlorure d'indium
US6337057B1 (en) * 1999-06-23 2002-01-08 Lucent Technologies, Inc. Process for the direct production of germanium tetrachloride from hydrated germanate-containing solids using gaseous hydrogen chloride
US6238462B1 (en) * 1999-07-14 2001-05-29 Corning Incorporated Methods for the separation of compounds from acidic aqueous solutions
KR20030005722A (ko) * 2001-07-10 2003-01-23 (주)나인디지트 건식 금속 게르마늄 제조방법과 그 정제장치
ZA200702593B (en) * 2004-09-29 2008-09-25 Umicore Nv Process for the production of Ge by reduction of GeCl4 with liquid metal
US8585797B2 (en) * 2007-06-15 2013-11-19 The Governors Of The University Of Alberta Method for preparing nanocrystalline germanium in GeO2 and freestanding germanium nanoparticles
US20100183500A1 (en) * 2009-01-17 2010-07-22 Henry Lee Germane gas production from germanium byproducts or impure germanium compounds
JP5676206B2 (ja) * 2010-10-27 2015-02-25 Ｄｏｗａメタルマイン株式会社 四塩化ゲルマニウムの回収方法
JP6141651B2 (ja) * 2013-02-21 2017-06-07 Ｄｏｗａメタルマイン株式会社 ゲルマニウム酸化物の製造方法
CN104911363A (zh) * 2015-06-24 2015-09-16 上海交通大学 一种回收褐煤烟尘中锗的方法
EP3401283B1 (en) 2017-05-10 2019-11-06 ITM Isotopen Technologien München AG Method for the manufacture of highly purified 68ge material for radiopharmaceutical purposes
CN107723467A (zh) * 2017-09-20 2018-02-23 郴州丰越环保科技有限公司 一种高效回收锗的方法
JP7281288B2 (ja) * 2019-01-30 2023-05-25 Ｄｏｗａメタルマイン株式会社 ゲルマニウム酸化物粉末およびその製造方法
CN110938752A (zh) * 2019-11-07 2020-03-31 深圳市中金岭南有色金属股份有限公司丹霞冶炼厂 一种提高锗回收率的萃取工艺
CN114277264B (zh) * 2021-12-28 2023-10-24 广东先导稀材股份有限公司 一种萃取回收锗的方法
CN115477322A (zh) * 2022-09-29 2022-12-16 云南驰宏国际锗业有限公司 一种超高纯GeCl4制备方法
CN116640928B (zh) * 2023-07-27 2023-10-20 昆明理工大学 一种氯化蒸馏锗残渣与铅锌冶炼酸性废水协同处置的方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1905460A (en) * 1930-06-17 1933-04-25 Gamichon Paul Process for converting into soluble salts lead and other metals contained in lead bearing ores
ES207331A1 (es) * 1952-01-21 1953-03-01 Sogo Kenkyujo Zh Sekitan Un método de recuperar germanio desde carbones
US2767052A (en) * 1952-06-26 1956-10-16 Eagle Picher Co Recovery of germanium from scrap materials
GB785751A (en) * 1952-08-15 1957-11-06 Nat Res Dev Improvements in and relating to the purification of germanium
US2920951A (en) * 1955-06-23 1960-01-12 Knapsack Ag Process for the continuous production of easily vaporizable metals
US2835569A (en) * 1956-04-19 1958-05-20 Electro Chimie Metal Process of extracting gold and other metals from ores, concentrates, residues and the like containing principally cobalt, nickel, iron, arsenic and gold
FR1324877A (fr) * 1962-06-14 1963-04-19 American Metal Climax Inc Procédé de purification de tétra chlorure de germanium, installation pour la réalisation du procédé, et produit conforme à ceux obtenus par le présent procédé ou procédé similaire
US3981962A (en) * 1975-06-30 1976-09-21 The United States Of America As Represented By The Secretary Of The Interior Decomposition leach of sulfide ores with chlorine and oxygen

Also Published As

Publication number Publication date
DE2630742A1 (de) 1977-01-20
GB1526115A (en) 1978-09-27
AU1547676A (en) 1978-01-05
YU164376A (en) 1982-05-31
JPS6034498B2 (ja) 1985-08-09
CA1083358A (en) 1980-08-12
DE2630742B2 (de) 1977-07-28
BE843453A (fr) 1976-12-27
PL110332B1 (en) 1980-07-31
FR2317366B1 (US20080094685A1-20080424-C00004.png) 1977-12-16
JPS529000A (en) 1977-01-24
YU39214B (en) 1984-08-31
AU497928B2 (en) 1979-01-25
ZM9176A1 (en) 1977-10-21
FR2317366A1 (fr) 1977-02-04
IT1069436B (it) 1985-03-25
US4090871A (en) 1978-05-23

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Legal Events

Date Code Title Description
C3 Grant after two publication steps (3rd publication)
8339 Ceased/non-payment of the annual fee