CN103687908B - 成型材料 - Google Patents
成型材料 Download PDFInfo
- Publication number
- CN103687908B CN103687908B CN201280035339.4A CN201280035339A CN103687908B CN 103687908 B CN103687908 B CN 103687908B CN 201280035339 A CN201280035339 A CN 201280035339A CN 103687908 B CN103687908 B CN 103687908B
- Authority
- CN
- China
- Prior art keywords
- methyl
- molded body
- film
- acrylate
- moulding material
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- 239000000463 material Substances 0.000 title claims abstract description 395
- 238000000465 moulding Methods 0.000 title claims abstract description 198
- 238000007493 shaping process Methods 0.000 claims abstract description 130
- 239000000839 emulsion Substances 0.000 claims abstract description 126
- 238000000034 method Methods 0.000 claims abstract description 114
- 239000011347 resin Substances 0.000 claims abstract description 92
- 229920005989 resin Polymers 0.000 claims abstract description 92
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims abstract description 68
- BAPJBEWLBFYGME-UHFFFAOYSA-N Methyl acrylate Chemical compound COC(=O)C=C BAPJBEWLBFYGME-UHFFFAOYSA-N 0.000 claims abstract description 60
- 238000004519 manufacturing process Methods 0.000 claims abstract description 58
- 229920000178 Acrylic resin Polymers 0.000 claims abstract description 46
- 239000004925 Acrylic resin Substances 0.000 claims abstract description 46
- 239000003505 polymerization initiator Substances 0.000 claims abstract description 22
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 239000000758 substrate Substances 0.000 claims description 138
- -1 Alkyl diol Chemical class 0.000 claims description 133
- 229910052799 carbon Inorganic materials 0.000 claims description 21
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 16
- 125000000217 alkyl group Chemical group 0.000 claims description 9
- 230000008859 change Effects 0.000 claims description 9
- 239000012528 membrane Substances 0.000 claims description 7
- SSOONFBDIYMPEU-UHFFFAOYSA-N [3-hydroxy-2-[[3-hydroxy-2,2-bis(hydroxymethyl)propoxy]methyl]-2-(hydroxymethyl)propyl] prop-2-enoate Chemical compound OCC(CO)(CO)COCC(CO)(CO)COC(=O)C=C SSOONFBDIYMPEU-UHFFFAOYSA-N 0.000 claims description 6
- 239000007787 solid Substances 0.000 claims description 4
- 239000012778 molding material Substances 0.000 claims description 3
- 229920001296 polysiloxane Polymers 0.000 abstract description 10
- 239000010410 layer Substances 0.000 description 250
- 239000010408 film Substances 0.000 description 139
- 239000000178 monomer Substances 0.000 description 139
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 description 128
- 229920000642 polymer Polymers 0.000 description 104
- 239000002585 base Substances 0.000 description 94
- CERQOIWHTDAKMF-UHFFFAOYSA-N alpha-methacrylic acid Natural products CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 79
- 239000002245 particle Substances 0.000 description 70
- 230000009477 glass transition Effects 0.000 description 43
- 239000011521 glass Substances 0.000 description 36
- 230000015572 biosynthetic process Effects 0.000 description 35
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 32
- 150000001875 compounds Chemical class 0.000 description 31
- 239000003595 mist Substances 0.000 description 29
- 150000002148 esters Chemical class 0.000 description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 27
- 239000011248 coating agent Substances 0.000 description 25
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- 238000007720 emulsion polymerization reaction Methods 0.000 description 25
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- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 20
- 238000002360 preparation method Methods 0.000 description 20
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 19
- 239000003795 chemical substances by application Substances 0.000 description 19
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 18
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- 239000010959 steel Substances 0.000 description 15
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 14
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- LYCAIKOWRPUZTN-UHFFFAOYSA-N ethylene glycol Natural products OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 12
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- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 9
- 239000011247 coating layer Substances 0.000 description 9
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- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 8
- VVQNEPGJFQJSBK-UHFFFAOYSA-N Methyl methacrylate Chemical compound COC(=O)C(C)=C VVQNEPGJFQJSBK-UHFFFAOYSA-N 0.000 description 8
- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 8
- 229920001519 homopolymer Polymers 0.000 description 8
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 8
- 238000010422 painting Methods 0.000 description 8
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 description 8
- 229920001971 elastomer Polymers 0.000 description 7
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- 125000000524 functional group Chemical group 0.000 description 7
- 230000000873 masking effect Effects 0.000 description 7
- 239000002609 medium Substances 0.000 description 7
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 7
- KNCYXPMJDCCGSJ-UHFFFAOYSA-N piperidine-2,6-dione Chemical group O=C1CCCC(=O)N1 KNCYXPMJDCCGSJ-UHFFFAOYSA-N 0.000 description 7
- 239000013047 polymeric layer Substances 0.000 description 7
- 230000009257 reactivity Effects 0.000 description 7
- 239000005060 rubber Substances 0.000 description 7
- 238000007790 scraping Methods 0.000 description 7
- SAPGBCWOQLHKKZ-UHFFFAOYSA-N 6-(2-methylprop-2-enoyloxy)hexyl 2-methylprop-2-enoate Chemical compound CC(=C)C(=O)OCCCCCCOC(=O)C(C)=C SAPGBCWOQLHKKZ-UHFFFAOYSA-N 0.000 description 6
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 description 6
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 6
- 239000005977 Ethylene Substances 0.000 description 6
- 239000004793 Polystyrene Substances 0.000 description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- 230000033228 biological regulation Effects 0.000 description 6
- 238000005520 cutting process Methods 0.000 description 6
- 239000008367 deionised water Substances 0.000 description 6
- 229910021641 deionized water Inorganic materials 0.000 description 6
- 238000001035 drying Methods 0.000 description 6
- 238000002844 melting Methods 0.000 description 6
- 230000008018 melting Effects 0.000 description 6
- 230000035515 penetration Effects 0.000 description 6
- 229920002223 polystyrene Polymers 0.000 description 6
- 229920002451 polyvinyl alcohol Polymers 0.000 description 6
- 239000002904 solvent Substances 0.000 description 6
- 229920001169 thermoplastic Polymers 0.000 description 6
- 229920002554 vinyl polymer Polymers 0.000 description 6
- IMSODMZESSGVBE-UHFFFAOYSA-N 2-Oxazoline Chemical compound C1CN=CO1 IMSODMZESSGVBE-UHFFFAOYSA-N 0.000 description 5
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 5
- 239000007864 aqueous solution Substances 0.000 description 5
- RWCCWEUUXYIKHB-UHFFFAOYSA-N benzophenone Chemical compound C=1C=CC=CC=1C(=O)C1=CC=CC=C1 RWCCWEUUXYIKHB-UHFFFAOYSA-N 0.000 description 5
- 239000012965 benzophenone Substances 0.000 description 5
- 210000000481 breast Anatomy 0.000 description 5
- IAQRGUVFOMOMEM-UHFFFAOYSA-N but-2-ene Chemical group CC=CC IAQRGUVFOMOMEM-UHFFFAOYSA-N 0.000 description 5
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 description 5
- 239000008199 coating composition Substances 0.000 description 5
- 230000006835 compression Effects 0.000 description 5
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- 239000006185 dispersion Substances 0.000 description 5
- 239000000975 dye Substances 0.000 description 5
- 125000004185 ester group Chemical group 0.000 description 5
- VANNPISTIUFMLH-UHFFFAOYSA-N glutaric anhydride Chemical group O=C1CCCC(=O)O1 VANNPISTIUFMLH-UHFFFAOYSA-N 0.000 description 5
- 238000010438 heat treatment Methods 0.000 description 5
- 230000004048 modification Effects 0.000 description 5
- 238000012986 modification Methods 0.000 description 5
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 5
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 5
- 239000010453 quartz Substances 0.000 description 5
- 230000006641 stabilisation Effects 0.000 description 5
- 238000011105 stabilization Methods 0.000 description 5
- 238000012719 thermal polymerization Methods 0.000 description 5
- 239000012956 1-hydroxycyclohexylphenyl-ketone Substances 0.000 description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
- KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 description 4
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 4
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 4
- 239000004372 Polyvinyl alcohol Substances 0.000 description 4
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
- SMWDFEZZVXVKRB-UHFFFAOYSA-N Quinoline Chemical compound N1=CC=CC2=CC=CC=C21 SMWDFEZZVXVKRB-UHFFFAOYSA-N 0.000 description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Polymers OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 239000007983 Tris buffer Substances 0.000 description 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N acetone Substances CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 4
- 229920000122 acrylonitrile butadiene styrene Polymers 0.000 description 4
- 125000005250 alkyl acrylate group Chemical group 0.000 description 4
- 239000012964 benzotriazole Substances 0.000 description 4
- MQDJYUACMFCOFT-UHFFFAOYSA-N bis[2-(1-hydroxycyclohexyl)phenyl]methanone Chemical compound C=1C=CC=C(C(=O)C=2C(=CC=CC=2)C2(O)CCCCC2)C=1C1(O)CCCCC1 MQDJYUACMFCOFT-UHFFFAOYSA-N 0.000 description 4
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- 125000004433 nitrogen atom Chemical group N* 0.000 description 4
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- JRKICGRDRMAZLK-UHFFFAOYSA-L persulfate group Chemical group S(=O)(=O)([O-])OOS(=O)(=O)[O-] JRKICGRDRMAZLK-UHFFFAOYSA-L 0.000 description 4
- 239000004014 plasticizer Substances 0.000 description 4
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- RKMGAJGJIURJSJ-UHFFFAOYSA-N 2,2,6,6-Tetramethylpiperidine Substances CC1(C)CCCC(C)(C)N1 RKMGAJGJIURJSJ-UHFFFAOYSA-N 0.000 description 3
- JAHNSTQSQJOJLO-UHFFFAOYSA-N 2-(3-fluorophenyl)-1h-imidazole Chemical compound FC1=CC=CC(C=2NC=CN=2)=C1 JAHNSTQSQJOJLO-UHFFFAOYSA-N 0.000 description 3
- AAMTXHVZOHPPQR-UHFFFAOYSA-N 2-(hydroxymethyl)prop-2-enoic acid Chemical compound OCC(=C)C(O)=O AAMTXHVZOHPPQR-UHFFFAOYSA-N 0.000 description 3
- FXRQXYSJYZPGJZ-UHFFFAOYSA-N 2-[(2-methylpropan-2-yl)oxy]ethenylbenzene Chemical group CC(C)(C)OC=CC1=CC=CC=C1 FXRQXYSJYZPGJZ-UHFFFAOYSA-N 0.000 description 3
- TXBCBTDQIULDIA-UHFFFAOYSA-N 2-[[3-hydroxy-2,2-bis(hydroxymethyl)propoxy]methyl]-2-(hydroxymethyl)propane-1,3-diol Chemical compound OCC(CO)(CO)COCC(CO)(CO)CO TXBCBTDQIULDIA-UHFFFAOYSA-N 0.000 description 3
- JLBJTVDPSNHSKJ-UHFFFAOYSA-N 4-Methylstyrene Chemical compound CC1=CC=C(C=C)C=C1 JLBJTVDPSNHSKJ-UHFFFAOYSA-N 0.000 description 3
- 229920008347 Cellulose acetate propionate Polymers 0.000 description 3
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- VPJOGDPLXNTKAZ-UHFFFAOYSA-N 2-methylpropanoic acid;2,2,4-trimethylpentane-1,3-diol Chemical compound CC(C)C(O)=O.CC(C)C(O)C(C)(C)CO VPJOGDPLXNTKAZ-UHFFFAOYSA-N 0.000 description 2
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- YYPNJNDODFVZLE-UHFFFAOYSA-N 3-methylbut-2-enoic acid Chemical compound CC(C)=CC(O)=O YYPNJNDODFVZLE-UHFFFAOYSA-N 0.000 description 2
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
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CN103687908B (zh) * | 2011-07-20 | 2016-11-02 | 株式会社日本触媒 | 成型材料 |
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KR20150119024A (ko) * | 2013-03-12 | 2015-10-23 | 코니카 미놀타 가부시키가이샤 | 유기 일렉트로루미네센스 표시 장치 및 그 제조 방법 |
JP2015038978A (ja) * | 2013-07-17 | 2015-02-26 | 日本電気硝子株式会社 | 波長変換部材 |
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US10174191B2 (en) * | 2013-11-22 | 2019-01-08 | Kaneka Corporation | Resin material and film thereof |
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WO2015079694A1 (ja) | 2013-11-29 | 2015-06-04 | 株式会社カネカ | 光学用樹脂組成物、およびフィルム |
JP6691778B2 (ja) | 2013-12-25 | 2020-05-13 | 株式会社カネカ | 光学用樹脂組成物、および成形体 |
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WO2015128995A1 (ja) * | 2014-02-27 | 2015-09-03 | コニカミノルタ株式会社 | 偏光板保護フィルム、その製造方法、偏光板及び液晶表示装置 |
JP2016115779A (ja) * | 2014-12-13 | 2016-06-23 | 株式会社ダイセル | ナノインプリント用光硬化性組成物 |
KR20160096368A (ko) | 2015-02-05 | 2016-08-16 | 삼성전자주식회사 | 반사 방지 구조물 제조 장치 및 이를 이용한 반사 방지 구조물 제조 방법 |
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JP7061930B2 (ja) * | 2018-06-01 | 2022-05-02 | 株式会社クレハ | 熱収縮性多層フィルム |
CN111175859B (zh) * | 2018-11-13 | 2021-10-22 | 株式会社小糸制作所 | 2色成形透镜 |
JP2020093472A (ja) * | 2018-12-13 | 2020-06-18 | スリーエム イノベイティブ プロパティズ カンパニー | 熱伝導性成形体、その製造方法、構造体及び多層フィルム |
JP7177724B2 (ja) * | 2019-02-22 | 2022-11-24 | 旭化成株式会社 | 成形体の製造方法 |
JP7099414B2 (ja) * | 2019-08-02 | 2022-07-12 | 三菱ケミカル株式会社 | 積層体 |
CN115363302B (zh) * | 2022-09-23 | 2023-10-03 | 淮阴工学院 | 一种适用于绒花制作的织造工具 |
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JP2013040325A (ja) | 2013-02-28 |
KR20140047662A (ko) | 2014-04-22 |
US20140221568A1 (en) | 2014-08-07 |
CN103687908A (zh) | 2014-03-26 |
EP2735588A1 (en) | 2014-05-28 |
EP2735588A4 (en) | 2015-07-15 |
WO2013011828A1 (ja) | 2013-01-24 |
JP6386506B2 (ja) | 2018-09-05 |
JP2017001399A (ja) | 2017-01-05 |
JP6085108B2 (ja) | 2017-02-22 |
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