CN103349007A - Agricultural composition containing antibiotics and plant source materials and application thereof - Google Patents

Agricultural composition containing antibiotics and plant source materials and application thereof Download PDF

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Publication number
CN103349007A
CN103349007A CN2013103211300A CN201310321130A CN103349007A CN 103349007 A CN103349007 A CN 103349007A CN 2013103211300 A CN2013103211300 A CN 2013103211300A CN 201310321130 A CN201310321130 A CN 201310321130A CN 103349007 A CN103349007 A CN 103349007A
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China
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chinese
plant
composition
botanical components
antibiotic
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CN2013103211300A
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CN103349007B (en
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侯华民
张善学
王少龙
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Hainan Zhengye Biotechnology Co ltd
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Hainan Zhengye Zhongnong Hi Tech Co Ltd
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Priority to CN201510287336.5A priority Critical patent/CN104920395B/en
Priority to CN201310321130.0A priority patent/CN103349007B/en
Priority to CN201510652417.0A priority patent/CN105265501B/en
Priority to CN201510652419.XA priority patent/CN105191995B/en
Priority to CN201510652057.4A priority patent/CN105379779B/en
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/48—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with two nitrogen atoms as the only ring hetero atoms
    • A01N43/54—1,3-Diazines; Hydrogenated 1,3-diazines
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Abstract

The invention belongs to the field of plant protection, and relates to an agricultural composition containing antibiotics and plant source materials, wherein antibiotic is one or several selected from abamectin, ivermectin, milbemectin, pleocidin, nikkomycin, liuyangmycin, streptomycin, polyoxins, chunleimeisu, jinggangmeisu, ningnanmycin and the like; the plant source material is one or several of smashing material, crude extract, or active ingredient of derris, thunder god vine, tobacco, pyrethrum, tagetes, crofton weed, radix stemonae, cayenne, macleaya cordata, radix sophorae flavescentis and the like. The composition provided by the invention expresses well synergism in a certain matching range, and has excellent control efficiency for crop diseases and pests.

Description

Contain agriculturally useful compositions and the application of antibiotic and botanical components
Technical field
The invention belongs to the plant protection field, particularly relate to the agriculturally useful compositions and the application that contain antibiotic and botanical components, the present composition can effectively be prevented and treated diseases and pests of agronomic crop.
Background technology
In recent years, because single and Scientific Usage of Drugs not, damage by disease and insect has produced pesticide resistance in various degree, and agriculture and forestry are produced still with chemical pesticide as mainly preventing and treating kind, causes the seriously destruction increasingly of environmental pollution and ecotope.Along with the raising of people's living standard and the enhancing of health perception, the development of biopesticide and exploitation progressively receive agricultural chemicals R﹠D worker's concern, becoming the focus of agriculture and forestry sustainable development, is the effective way of improving environment, minimizing or delaying drug resistance and raising drug effect.Wherein, farm antibiotics and botanical components become one of focus of biopesticide research.
Farm antibiotics refers to be produced, have the agricultural chemicals function, be used for the upward secondary metabolite of the anti-pests such as Chinese caterpillar fungus mouse of curing the disease of agricultural by microbial fermentation.The microorganisms such as actinomycetes, fungi, bacterium all can produce farm antibiotics, and wherein the farm antibiotics of actinomycetes generation is maximum.The many important farm antibiotics of at present extensive use all is to separate the actinomycetes that obtain to produce from streptomyces.Farm antibiotics the earliest is streptomycin, and has promoted thus the application of antibiotic on agricultural, has obtained rapidly development behind 20 century 70s.At present, farm antibiotics almost spreads all over the agricultural chemicals all spectras such as insecticide, bactericide, weed killer herbicide, plant growth regulator.Such as the Avermectin of Insecticiding-miticiding effect, ivermectin, milbemectin, pleocidin, macro tetrolide, nikkomycin etc., the polyoxin of control fungal disease, kasugarnycin, jinggangmycin, Ningnanmycin, mildiomycin, cycloheximide, blasticidin, valida, blasticidin-S, Qinlingmycin etc., prevent and treat streptomycin sulphate, terramycin of bacteriosis etc., bialaphos with herbicidal effect has the gibberellin of coordinate plant growth etc.
The plant that the agricultural use future of tool and exploitation are worth mainly contains Meliaceae, composite family, pulse family, Rutaceae, aster section, Labiatae, Annonaceae, Ranunculaceae, Euphorbiaceae, Araeceae, Myrsinacea, the certain plants of Papilionaceae etc. is studied the more trifoliate jewelvine that has, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, the India red sandalwood, erythrina indica, plant iron son or frutus cnidii etc.
Have desinsection, sterilization, fertilizer, fresh-keeping etc. botanical components, comprise crushed material or the crude extract such as the root that can directly utilize plant, stem, leaf, flower, fruit, seed or extract the active component of plant.The plant resource active component is divided into alkaloids, terpenes, flavonoids, essential oil class, photoactivation endotoxin and other class active components by chemical constitution.
Contain the more section of alkaloid Cephalotaxaceae, Ranunculaceae, Berberidaceae, Papaveraceae, pulse family, Loganiaceae, Apocynaceae, Solanaceae, composite family, Liliaceae, Amaryllidaceae, Loganiaceae, Rutaceae, Lauraceae etc. are arranged.
The terpenes active component mainly contains monoterpenes, sesquiterpenoids, Diterpenes and triterpene compound.Monoterpene is modal terpene, it is the key component of plant volatile oil, content is relatively high in the Cupressaceae plant, sesquiterpenoids is more in Coriariaceae plant, Celastraceae plant Celastrus angulatus etc., diterpene-kind compound is more in Euphorbiaceae, Isolated From Thymelaeaceae Species, and the important representative of triterpene compound has insect anti-feedant nimbin.
Flavonoids also claims the flavone class, the form that most of and sugar are combined into glycoside or carbon glycosyl in plant corpus exists, and also has to exist with free form.Mainly be distributed in the plants such as pulse family, Papilionaceae, Rutaceae, Umbelliferae, Labiatae.The rotenone that extracts from Derris and Baptisia plant has powerful tagging and stomach poison function to insect, and insecticidal spectrum is wide, and insect is difficult for developing immunity to drugs.The pterocarpoid chromocor compound that extracts from Pterocarpus, Erythrina, reticulate millettia platymiscium has very strong antimycotic and bacterial activity effect, can be used as important plant defense element.
Plants essential oil often is present in the oil droplet or the empty resin of organizing of plant of plant.Most of essential oil components are complicated, and chemical constituent can be divided into four classes substantially, and a class is terpene compound, is the key component of essential oil, is divided into monoterpene derivative, sesquiterpene derivative, forskolin.Equations of The Second Kind is aromatic compound, is only second to terpene compound in essential oil.The 3rd class is aliphatic compound.The 4th class is the sulfur-bearing nitrogen-containing compound.Essential oil is volatile at normal temperatures, and strong peat-reek is arranged, and is oily liquids at normal temperatures, dissolves in the multiple organic solvents such as methyl alcohol, ethanol.
Plant Light activation toxin mainly is some natural productss that derive from Rutaceae composite family, samphire, in the situation that unglazed not high to the insect activity, very strong activity is arranged illumination is next.Plant Light activation toxin main Types has polyyne class, thiophene phenols and quinones etc., and its mechanism of action is very unique, is different from traditional any insecticides, therefore can not produce the problem of cross tolerance.
Research report about the agriculturally useful compositions of antibiotics material and botanical components is less.
Summary of the invention
The objective of the invention is to improve environment, enlarge action spectrum, minimizing or delaying drug resistance, raising drug effect, the agriculturally useful compositions of a kind of antibiotics and botanical components is provided.
The present invention is achieved through the following technical solutions:
Contain antibiotics and botanical components agriculturally useful compositions, it is characterized in that said composition comprises A and the B of effective dose, A is selected from Avermectin, ivermectin, milbemectin, pleocidin, nikkomycin, macro tetrolide, polyoxin, kasugarnycin, jinggangmycin, Ningnanmycin, mildiomycin, cycloheximide, blasticidin, valida, blasticidin-S, Qinlingmycin, bialaphos, gibberellin, streptomycin sulphate, in the terramycin one or more, B is selected from trifoliate jewelvine, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, the India red sandalwood, erythrina indica, one or more meal of the young and frutus cnidii of plant iron.Preferably, botanical components is selected from Aztec marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia.
In the present composition, A is selected from Avermectin, ivermectin, milbemectin, pleocidin, nikkomycin, macro tetrolide, polyoxin, kasugarnycin, jinggangmycin, Ningnanmycin, mildiomycin, cycloheximide, blasticidin, valida, blasticidin-S, Qinlingmycin, bialaphos, gibberellin, streptomycin sulphate, in the terramycin one or more, B is selected from trifoliate jewelvine, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, the India red sandalwood, erythrina indica, alkaloids in the crude extract of one or more in plant iron son and the frutus cnidii or the active component, terpenes, flavonoids, the essential oil class, in the photoactivation endotoxin one or more.
The agriculturally useful compositions that contains antibiotics and botanical components of the present invention is characterized in that the feverfew in the botanical components is selected from Aztec marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia.
Alkaloids in the botanical components in the present composition is the datura total alkali, Chelidonine, the total alkaloids, camptothecine, aconitine, strychnia, total alkaloid of sophora alopecuroide, the thunder godvine alkaloid, oxymatrine, nicotine, the black false hellebore total alkali, capsaicine, matrine, sanguinarine, jamaicin, stemonine, papaverine, quinoline is peaceful, tomatin, lupinine, sparteine, the numb rope in ground, donaxine, morphine, kind art soft-shelled turtle alkali, gelsemium henbane amine, mufangchine, magnoflorine, aconitine, eulexine, atropine, the black nightshade alkaloid, one or more alkaloids in the dandelion alkaloid etc. or one or more components in the above-mentioned total alkali.One or more components in one or more alkaloids in datura total alkali, Chelidonine, the total alkaloids, camptothecine, aconitine, strychnia, Cynanchum Komarovii alkali, solanine or the dandelion alkali or the biology total alkali preferably.
Terpenes in the botanical components in the present composition is in the diterpene-kind compound in the Celastrus angulatus of the coriamyrtin of the monoterpene in the Chinese azalea extract in the Ericaceae, the menthol, peppermint aldehyde, Cupressaceae plant in the Labiatae, Coriariaceae plant, Celastraceae plant, Euphorbiaceae, the Isolated From Thymelaeaceae Species and the triterpene compound in the Meliaceae etc. one or more.Preferred terpenes is a kind of in Chinese azalea extract and the coriamyrtin or two kinds.
Flavonoids in the botanical components in the present composition is one or more in the young flavones of chamaejasmine, rotenone, pterocarpoid, kuh-seng flavones and plant iron.Preferred flavonoids is a kind of in chamaejasmine, the pterocarpoid or two kinds.
Essential oil class in the botanical components in the present composition is in the terpene compound in thyme, Chinese cassia tree, lemongrass, cloves, Chinese anise, orange peel, tree-of-heaven bark, chilli powder, Siberian cocklebur, lavender, the fruit of a cubeb litsea tree, garlic, peppermint, cypress, Chinese prickly ash, the Artemisia scoparia etc., aromatic compound, aliphatic compound, the sulfur-bearing nitrogen-containing compound one or more.Preferred essential oil is a kind of in thymol and the cinnamic acid or two kinds.
Plant Light activation endotoxin in the botanical components in the present composition is one or more in furocoumarin class, polyyne class, thiophene phenols and the quinones etc.
In the present composition, the ratio of quality and the number of copies of antibiotics and botanical components is 50:1-1:200.Preferably, the ratio of quality and the number of copies of antibiotics and botanical components is 30:1-1:20.
Above-mentioned composition process preparation of the present invention is wetting powder, water dispersible granules, aqueous emulsion, microemulsion, suspending agent, and the percentage that antibiotics and botanical components quality sum account for the preparation gross mass is 0.05-80%.Preferably, to account for the percentage of preparation gross mass be 0.1-40% for antibiotics and botanical components quality sum
The preparation of above-mentioned composition processing of the present invention is used with base manure, spraying, filling root, seed dressing, impregnating, shows the purposes of preventing and treating the various crop damage by disease and insect.
The present invention also provides the composition of antibiotic and several composite family components and antibiotic and several alkaloid composition effect to citrus pest, cotton-plant pest-insects, antibiotic and several alkaloidal composition are to the effect of tomato disease, rice disease, several compositions of antibiotic and botanical components that contain are to the effect of cotton nematode, the composition of antibiotic and terpenes component and antibiotic and flavones is to the effect of wild cabbage insect, cotton-plant pest-insects, and the composition of antibiotic and plants essential oil is to the effect of rice sheath blight disease.
Composition of the present invention compared with prior art produces following beneficial effect:
1, purposes is widened: composition can be prevented and treated the Various Diseases insect pest of crops.
2, reduce use cost: because composition has the preventive effect of raising, the control spectrum increases, reduced the agricultural chemicals access times, reduced use cost.
3, delay pesticide resistance: the component that contains antibiotic and the composition of botanical components and be different mechanism of action is composite, and damage by disease and insect is difficult for developing immunity to drugs.
4, environmental friendliness: low to people and animals and non-target organism toxicity, in environment, degrade fast, low-residual, free from environmental pollution.
Embodiment
Following embodiment is described only for explaining the present invention, for not departing from modification, replacement or the improvement that the present invention is spiritual and principle is made, all belongs to the scope of protection of present invention.Antibiotic in following examples and botanical components are from commercial channel or voluntarily preparation.
The alkaloidal preparation method of embodiment 1 plant resource
Get respectively the plant material trifoliate jewelvine, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, the India red sandalwood, erythrina indica, one or more vegetable materials in plant iron son and the frutus cnidii, clean, dry, pulverize, adding 43 ℃ of 95% ethanol refluxes 2 * 1h/ time, Recycled ethanol is to concentrate, with the acidifying of 0.4mol/L aqueous sulfuric acid, rear with chloroform eccysis oil-soluble impurities, the acid liquid that obtains is neutralized to pH8.5 with sodium carbonate and uses chloroform extraction again, reclaim organic solvent, obtain the biology total alkali of botanical components.
The preparation of embodiment 2 botanical components flavonoids
Get respectively the plant trifoliate jewelvine, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, the India red sandalwood, erythrina indica, one or more vegetable materials in plant iron son and the frutus cnidii, clean, dry, pulverize, with crushed material and the solvent mixing in the extractor of packing into, place ultrasonoscope, 75-85 ℃ is extracted at least 25min, obtain suspension, filter to get filtrate and filter residue for the first time; With filter residue and the solvent mixing in the extractor of packing into, place ultrasonoscope, 82-94 ℃ is extracted at least 40min, obtains suspension, filters to get filtrate and filter residue for the second time; The filtrate mixing of above-mentioned secondary is adopted decompression distillation, and the concentrate that obtains is the plant resource Flavonoid substances.Above-mentioned solvent adopts one or more in water, ethyl acetate, acetone, ethanol, the methyl alcohol.
The preparation of embodiment 3 plant resource terpenes, essential oil material
Get respectively one or more vegetable materials in plant trifoliate jewelvine, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, India red sandalwood, erythrina indica, plant iron son and the frutus cnidii, clean, dry, pulverizing.Adopt steam distillation, ethonal extraction method or acetone and the water mixed solvent extraction method of this area routine to be prepared terpenes, essential oil class.Also can adopt the steam distillation of this area routine to prepare essential oil.
Embodiment 45% Avermectin Aztec marigold aqueous emulsion
With 5g dimethyl formamide dissolving 0.5g Avermectin, get Aztec marigold through the concentrate 4.5g of alcohol extract, distillation, 10g fully dissolves with ethanol, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, and water complements to 100g, has both got 5% Avermectin Aztec marigold aqueous emulsion.
Embodiment 55% ivermectin Eupatorium adenophorum aqueous emulsion
With 5g acetic acid dissolving 0.5g ivermectin, get Eupatorium adenophorum through the concentrate 4.5g of alcohol extract, distillation, 10g fully dissolves with ethanol, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, and water complements to 100g, has both got 5% ivermectin Eupatorium adenophorum aqueous emulsion.
Embodiment 65% milbemectin Dalmatian chrysanthemum aqueous emulsion
With 5g dimethyl formamide dissolving 0.5g milbemectin, get Dalmatian chrysanthemum through the concentrate 4.5g of alcohol extract, distillation, with fully dissolving with ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, and water complements to 100g, has both got 5% milbemectin Dalmatian chrysanthemum aqueous emulsion.
Embodiment 75% pleocidin Artemisia scoparia aqueous emulsion
With 5g dimethyl formamide dissolving 0.5g pleocidin, get Artemisia scoparia through the concentrate 4.5g of alcohol extract, distillation, 10g fully dissolves with ethanol, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, and water complements to 100g, has both got 5% pleocidin Artemisia scoparia aqueous emulsion.
Embodiment 85% nikkomycin Dalmatian chrysanthemum aqueous emulsion
With 5g dimethyl formamide dissolving 0.5g nikkomycin, get Dalmatian chrysanthemum through the concentrate 4.5g of alcohol extract, distillation, with fully dissolving with ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, and water complements to 100g, has both got 5% nikkomycin Dalmatian chrysanthemum aqueous emulsion.
Embodiment 95% macro tetrolide fennel wormwood artemisia aqueous emulsion
With 5g dimethyl formamide dissolving 0.5g macro tetrolide, get the fennel wormwood artemisia through the concentrate 4.5g of alcohol extract, distillation, 10g fully dissolves with ethanol, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, and water complements to 100g, has both got 5% macro tetrolide fennel wormwood artemisia aqueous emulsion.
Embodiment 101% Avermectin datura total alkali water dispersible granules
With Avermectin 0.5g, datura total alkali 0.5g, naphthalenesulfonate formaldehyde condensation compound 4g, sodium alkyl benzene sulfonate 1.5g, gum Arabic 0.5g, white carbon is supplied 100g and is mixed, mixture is carried out granulation after the ultra-fine grinding, drying, screening, both 1% Avermectin datura total alkali water dispersible granules.
Embodiment 111% ivermectin Chelidonine water dispersible granules
Ivermectin 0.5g, Chelidonine 0.5g, naphthalenesulfonate formaldehyde condensation compound 10g, sodium alkyl benzene sulfonate 5g, white carbon are supplied 100g to be mixed, mixture is carried out granulation after the ultra-fine grinding, drying, screening, both made 1% ivermectin Chelidonine water dispersible granules.
Embodiment 121% milbemectin the total alkaloids microemulsion
Milbemectin 0.5g is dissolved with dimethylbenzene 5g, the total alkaloids 0.5g fully dissolves with chloroform 3g and methyl alcohol 5g, adds phenethyl phenol polyethenoxy ether 5g and agricultural newborn 500#5g, and mixture is stirred in agitator, water complements to 100g, has both got 1% milbemectin the total alkaloids microemulsion.
Embodiment 131% pleocidin camptothecine aqueous emulsion
Pleocidin 0.5g is dissolved with dimethylbenzene 5g, camptothecine 0.5g fully dissolves with ethyl acetate 3g and ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, water complements to 100g, has both got 1% pleocidin camptothecine aqueous emulsion.
Embodiment 141% nikkomycin aconitine wetting powder
Nikkomycin 0.5g, aconitine 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 1% nikkomycin aconitine wetting powder.
Embodiment 151% macro tetrolide strychnia wetting powder
Macro tetrolide 0.5g, strychnia 0.5g, sodium lignin sulfonate 2g, white carbon are supplied 100g mix, with each component drying, cooling, levigate, both must be mixed with 1% macro tetrolide strychnia wetting powder.
Embodiment 161.5% Ningnanmycin Cynanchum Komarovii alkali wetting powder
Ningnanmycin 1g, Cynanchum Komarovii alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 1.5% Ningnanmycin Cynanchum Komarovii alkali wetting powder.
Embodiment 171.5% Ningnanmycin solanine microemulsion
Ningnanmycin 1g water 10g is dissolved, solanine 0.5g fully dissolves with chloroform 3g and methyl alcohol 5g, adds phenethyl phenol polyethenoxy ether 5g and agricultural newborn 500#5g, and mixture is stirred in agitator, water complements to 100g, has both got 1.5% Ningnanmycin solanine microemulsion.
Embodiment 181.5% Ningnanmycin dandelion buck emulsion
With Ningnanmycin element 1g water 10g dissolving, dandelion alkali 0.5g fully dissolves with ethyl acetate 3g and ethanol 10g, mix the first two dissolved matter, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, water complements to 100g, has both got 1.5% Ningnanmycin dandelion buck emulsion.
Embodiment 192.5% jinggangmycin Cynanchum Komarovii alkali wetting powder
Jinggangmycin 2g, Cynanchum Komarovii alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 2.5% jinggangmycin Cynanchum Komarovii alkali wetting powder.
Embodiment 202.5% jinggangmycin solanine wetting powder
Jinggangmycin 2g, solanine 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 2.5% jinggangmycin solanine wetting powder.
Embodiment 212.5% jinggangmycin dandelion alkali wetting powder
Jinggangmycin 2g, dandelion alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 2.5% jinggangmycin dandelion alkali wetting powder.
Embodiment 223% kasugarnycin Cynanchum Komarovii alkali wetting powder
Kasugarnycin 2.5g, Cynanchum Komarovii alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 3% kasugarnycin Cynanchum Komarovii alkali wetting powder.
Embodiment 233% kasugarnycin solanine wetting powder
Kasugarnycin 2.5g, solanine 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 3% kasugarnycin solanine wetting powder.
Embodiment 243% kasugarnycin dandelion alkali wetting powder
Kasugarnycin 2.5g, dandelion alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 3% kasugarnycin dandelion alkali wetting powder.
Embodiment 2536% streptomycin sulphate Cynanchum Komarovii alkali wetting powder
Streptomycin sulphate 35g, Cynanchum Komarovii alkali 1g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 36% streptomycin sulphate Cynanchum Komarovii alkali wetting powder.
Embodiment 263.5% polyoxin Cynanchum Komarovii alkali wetting powder
Polyoxin 3g, Cynanchum Komarovii alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 3.5% polyoxin Cynanchum Komarovii alkali wetting powder.
Embodiment 273.5% polyoxin solanine wetting powder
Polyoxin 3g, solanine 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 3.5% polyoxin solanine wetting powder.
Embodiment 283.5% polyoxin dandelion alkali wetting powder
Polyoxin 3g, dandelion alkali 0.5g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 3.5% polyoxin dandelion alkali wetting powder.
Embodiment 2936% streptomycin sulphate solanine wetting powder
Streptomycin sulphate 35g, solanine 1g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 36% streptomycin sulphate Cynanchum Komarovii alkali wetting powder.
Embodiment 3036% streptomycin sulphate dandelion alkali wetting powder
Streptomycin sulphate 35g, dandelion alkali 1g, sodium alkyl benzene sulfonate 2g, kaolin are supplied 100g mix, with each component drying, cooling, levigate, both be mixed with 36% streptomycin sulphate dandelion alkali wetting powder.
Embodiment 311% Avermectin Chinese azalea extract aqueous emulsion
Avermectin 0.5g is fully dissolved with dimethylbenzene 4g, Chinese azalea extract 0.5g fully dissolves with ethyl acetate 1g, chloroform 1g, mix the first two solution, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, water complements to 100g, has both got 1% Avermectin Chinese azalea extract aqueous emulsion.
Embodiment 321.5% pleocidin coriamyrtin aqueous emulsion
Pleocidin 0.5g is fully dissolved with dimethylbenzene 4g, coriamyrtin 1g fully dissolves with ethyl acetate 1g, chloroform 1g, mix the first two solution, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, water complements to 100g, has both got 1.5% pleocidin coriamyrtin aqueous emulsion.
Embodiment 331.5% Avermectin chamaejasmine suspending agent
Avermectin 0.5g, chamaejasmine 1g, sodium lignin sulfonate 3g, the withered powder 5g of tea, bentonite 5g, Magnesiumaluminumsilicate 2g, ethylene glycol 10g are fully mixed, add water 25g and fully grind, water complements to 100g, is mixed with 1.5% Avermectin chamaejasmine suspending agent.
Embodiment 341.5% pleocidin chamaejasmine suspending agent
Pleocidin 0.5g, chamaejasmine 1g, sodium lignin sulfonate 3g, the withered powder 5g of tea, bentonite 5g, Magnesiumaluminumsilicate 2g, ethylene glycol 10g are fully mixed, add water 25g and fully grind, water complements to 100g, is mixed with 1.5% pleocidin chamaejasmine suspending agent.
Embodiment 351.5% magnificent light rhzomorph pterocarpin suspending agent
Magnificent light rhzomorph 0.5g, pterocarpin 1g, sodium lignin sulfonate 3g, the withered powder 5g of tea, bentonite 5g, Magnesiumaluminumsilicate 2g, ethylene glycol 10g are fully mixed, add water 25g and fully grind, water complements to 100g, is mixed with 1.5% magnificent light rhzomorph pterocarpin suspending agent.
Embodiment 361.5% macro tetrolide pterocarpin suspending agent
Macro tetrolide 0.5g, pterocarpin 1g, sodium lignin sulfonate 3g, the withered powder 5g of tea, bentonite 5g, Magnesiumaluminumsilicate 2g, ethylene glycol 10g are fully mixed, add water 25g and fully grind, water complements to 100g, is mixed with 1.5% macro tetrolide pterocarpin suspending agent.
Embodiment 372% polyoxin thymol aqueous emulsion
Polyoxin 1.5g water is fully dissolved, and thymol 0.5g fully dissolves with ethanol 5g, mixes the first two solution, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, and water complements to 100g, has both got 2% polyoxin thymol aqueous emulsion.
Embodiment 3810% jinggangmycin thymol aqueous emulsion
Jinggangmycin 9.5g water is fully dissolved, and thymol 0.5g fully dissolves with ethanol 5g, mixes the first two solution, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, and water complements to 100g, has both got 10% jinggangmycin thymol aqueous emulsion.
Embodiment 392% polyoxin cinnamic acid aqueous emulsion
Polyoxin 1.5g water is fully dissolved, and cinnamic acid 0.5g fully dissolves with ethanol 5g, mixes the first two solution, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, and water complements to 100g, has both got 2% polyoxin cinnamic acid aqueous emulsion.
Embodiment 4010% jinggangmycin cinnamic acid aqueous emulsion
Jinggangmycin 9.5g water is fully dissolved, and cinnamic acid 0.5g fully dissolves with ethanol 5g, mixes the first two solution, add phenethyl phenol polyethenoxy ether 5g, agricultural newborn 500#5g, water slowly adds and stirs, and water complements to 100g, has both got 10% jinggangmycin cinnamic acid aqueous emulsion.
Embodiment 41 contains the composition of antibiotic and botanical components to the effect of cotton nematode
The dissolving of quantitative antibiotic is mixed with Aztec marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, the fennel wormwood artemisia of crushing screening respectively, add respectively auxiliary agent and be made into and treat articles for use.The dissolving of quantitative antibiotic is mixed with alkaloid respectively, add respectively auxiliary agent and be made into and treat articles for use.The above-mentioned articles for use for the treatment of are mixed into compost with sterilization soil and sterilization river sand respectively, get quantitative culture soil and sneak into quantitative compositions or single dose, fully mix thoroughly, add clear water and make water content 40%, the basin alms bowl of packing into, there is the cotton seedling of 10d to be transplanted in the basin growth, every pot transplanting 10 strains, 7d after transplanting, 100 of every basin access Meloidogyne incognita 2 instar larvaes, place the greenhouse, the quantitative watering management.If every chemicals treatment 6 basins, and establish that not sneak into chemicals treatment be blank.Behind the 20d, when blank plant rhizosphere has a large amount of root knot, investigate plant height and the root knot number of 3 basin cottons, and carry out classification by Liu Weizhi (1995): 0 grade, without root knot; 1 grade, the 1-2 root knot; 2 grades, 3-10 root knot; 3 grades, 11-30 root knot; 4 grades, 31-100 root knot; 5 grades, 100 above root knots.The every processing of 20d " Invest, Then Investigate " is the incidence of 3 basin cotton verticillium wilts in addition.The results are shown in Table 1.
Several compositions of antibiotic and botanical components that contain of table 1 are to the effect of cotton nematode
Figure BDA00003573205000091
Figure BDA00003573205000101
Table 1 shows, compare with corresponding single dose processing, contain the antibiotic Avermectin, ivermectin, milbemectin, pleocidin, nikkomycin, the compositions-treated of macro tetrolide and several feverfew components, the antibiotic Ningnanmycin, jinggangmycin, kasugarnycin, polyoxin, the processing root knot number of streptomycin sulphate and several alkaloidal compositions still less, plant height is higher, and the blade verticillium wilt incidence of disease is lower, the composition of antibiotic and several composite family components is described, antibiotic and several alkaloidal composition can effectively be prevented and treated nematode, reduce the generation of verticillium wilt.
The composition of embodiment 42 antibiotic and several composite family components and antibiotic and several alkaloidal composition are to the effect of oranges and tangerines, cotton
According to scheme, preparation built agent and single dose, and carry out active preliminary experiment.According to the determination of activity trial test, preparation is mixed with the concentration that needs.Before the test, the residential quarter is set, lists at citrus orchard and Cotton Fields respectively, investigation two spotted spider mite, aphid radix, and establish corresponding single dose and blank, adopt the conventional conventional spray of manual sprayer.The 7d investigation is listed and is processed the quantity of two spotted spider mite and aphid behind the medicine.Use the Abbot formula, convert percentage to preventive effect.
Figure BDA00003573205000111
Figure BDA00003573205000112
In the theoretical effect, x is the effect of the substance A of concentration when being a, and y is the effect of the substance B of concentration when being b, and relatively theoretical effect and actual effect are estimated the synergy of composition.The results are shown in Table 2, table 3.
The composition of table 2 antibiotic and several composite family components and antibiotic and several alkaloid composition are to the field efficacy of citrus pest
Figure BDA00003573205000113
Figure BDA00003573205000121
Annotate: in the table 2, Aztec marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia are through the concentrate after the extractive distillation.
The composition of table 3 antibiotic and several composite family components and antibiotic and several alkaloid composition are to the field efficacy of cotton-plant pest-insects
Figure BDA00003573205000122
Figure BDA00003573205000131
Annotate: in the table 3, Aztec marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia are through the concentrate after the extractive distillation.
Find out from table 2, table 3, antibiotic Avermectin, ivermectin, milbemectin, pleocidin, nikkomycin, macro tetrolide and several Asteraceae plants and with several alkaloidal compositions to citrus red mite and aphid, the actual effect of cotton red spider and aphid is higher than theoretical effect, show that composition has obvious synergistic function.
Embodiment 43 antibiotic and several alkaloidal composition are to the effect of tomato disease and rice disease
According to scheme, preparation built agent and single dose preparation, and carry out active preliminary experiment.According to the determination of activity trial test, preparation is mixed with the concentration that needs.Before the test in the tomato field and paddy field establish corresponding single dose and blank, adopt the conventional conventional spray of manual sprayer, every medicament sprays 50 strains.Again dispenser 1 time of 7-10d after the 1st dispenser.10-20d after the 2nd dispenser investigates tomato plant disease and the rice plant disease situation of listing.Use the Abbot formula, convert percentage to preventive effect.
Figure BDA00003573205000132
Figure BDA00003573205000133
In the theoretical effect, x is the effect of the substance A of concentration when being a, and y is the effect of the substance B of concentration when being b, and relatively theoretical effect and actual effect are estimated the synergy of composition.Composition sees Table respectively 4 and table 5 to the result of tomato plant disease and rice plant disease.
Table 4 antibiotic and several alkaloidal composition are to the field effect of tomato disease
Figure BDA00003573205000134
Figure BDA00003573205000141
Table 5 antibiotic and several alkaloidal composition are to the field effect of rice disease
Figure BDA00003573205000142
As seen from Table 4, antibiotic Ningnanmycin, jinggangmycin, kasugarnycin, polyoxin, streptomycin sulphate and several alkaloidal composition are higher than theoretical effect to the actual effect of tomato virus disease, graw mold of tomato and bacterial wilt of tomato, show that composition has obvious synergistic function.
As seen from Table 5, antibiotic Ningnanmycin, jinggangmycin, kasugarnycin, polyoxin, streptomycin sulphate and several alkaloidal composition are higher than the theoretical effect of corresponding medicament to the actual effect of stripe disease, rice blast and banded sclerotial blight, show that composition has obvious synergistic function.
The composition of composition, antibiotic and the flavones of embodiment 44 antibiotic and terpenes component is to the effect of wild cabbage, cotton-plant pest-insects
According to testing program, preparation built agent and single dose, and carry out active trial test.According to the determination of activity trial test, preparation is mixed with the concentration that needs.Before the test, the residential quarter is set, lists at cabbage field and Cotton Fields, investigation cabbage field diamond-back moth, cabbage caterpillar and Cotton Fields prodenia litura radix, and establish corresponding single dose and blank, adopt the conventional conventional spray of manual sprayer.7d investigation medicament is to the effect of diamond-back moth, cabbage caterpillar and prodenia litura behind the medicine.Use the Abbot formula, convert percentage to preventive effect.
Figure BDA00003573205000151
In the theoretical effect, x is the effect of the substance A of concentration when being a, and y is the effect of the substance B of concentration when being b, and relatively theoretical effect and actual effect are estimated the synergy of composition.The results are shown in Table 6, table 7.
Table 6 contains antibiotic composition to the field effect of wild cabbage insect
Figure BDA00003573205000153
Figure BDA00003573205000161
Table 7 contains antibiotic composition to the field effect of cotton prodenia litura
Figure BDA00003573205000162
Figure BDA00003573205000171
Find out from table 6, table 7, Avermectin in the antibiotic, ivermectin, pleocidin, milbemectin, nikkomycin, macro tetrolide respectively with the composition of the Chinese azalea extract of terpenes, with the composition of coriamyrtin and with the composition of the chamaejasmine of flavonoids, and and the composition of pterocarpin, preventive effect to wild cabbage diamond-back moth, cabbage caterpillar and cotton prodenia litura is remarkable, actual effect to insect all is higher than theoretical effect, shows obvious synergistic function.
The composition of embodiment 45 antibiotic and plants essential oil is to the effect of rice sheath blight disease
According to scheme, preparation built agent and single dose preparation, and carry out active trial test.According to active trial test result, preparation is mixed with the concentration that needs.Adopt the conventional conventional spray of manual sprayer at paddy field before the test, every medicament sprays 50 strains, and corresponding single dose and blank are set, again dispenser 1 time of 7-10d after the 1st dispenser, 10-20d after the 2nd dispenser, the investigation rice plant banded sclerotial blight incidence of listing.Use the Abbot formula, convert percentage to preventive effect.
Figure BDA00003573205000172
In the theoretical effect, x is the effect of the substance A of concentration when being a, and y is the effect of the substance B of concentration when being b, and relatively theoretical effect and actual effect are estimated the synergy of composition.Rice plant banded sclerotial blight situation the results are shown in Table 8.
Table 8 contains antibiotic composition to the field effect of rice sheath blight disease
Figure BDA00003573205000174
Figure BDA00003573205000181
As seen from Table 8, Ningnanmycin in the antibiotic, jinggangmycin, kasugarnycin, polyoxin, streptomycin sulphate respectively with the composition of the thymol of plants essential oil class and remarkable to the preventive effect of rice sheath blight disease with the composition of the cinnamic acid of plants essential oil class, actual effect to banded sclerotial blight all is higher than theoretical effect, shows obvious synergistic function.

Claims (10)

1. the agriculturally useful compositions that contains antibiotics and botanical components, it is characterized in that said composition comprises A and the B of effective dose, A is selected from Avermectin, ivermectin, milbemectin, pleocidin, nikkomycin, macro tetrolide, Ningnanmycin, jinggangmycin, kasugarnycin, polyoxin, mildiomycin, cycloheximide, blasticidin, valida, blasticidin-S, Qinlingmycin, bialaphos, gibberellin, streptomycin sulphate, in the terramycin one or more, B is selected from trifoliate jewelvine, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, the India red sandalwood, erythrina indica, one or more meal of the young and frutus cnidii of plant iron.
2. the agriculturally useful compositions that contains antibiotics and botanical components according to claim 1 is characterized in that botanical components is selected from Aztec marigold, Eupatorium adenophorum, Dalmatian chrysanthemum, Artemisia scoparia, fennel wormwood artemisia.
3. the agriculturally useful compositions that contains antibiotics and botanical components, it is characterized in that said composition comprises A and the B of effective dose, A is selected from Avermectin, ivermectin, milbemectin, pleocidin, nikkomycin, macro tetrolide, Ningnanmycin, jinggangmycin, kasugarnycin, polyoxin, mildiomycin, cycloheximide, blasticidin, valida, blasticidin-S, Qinlingmycin, bialaphos, gibberellin, streptomycin sulphate, in the terramycin one or more, B is botanical components, and B is selected from trifoliate jewelvine, thunder godvine, tobacco, Dalmatian chrysanthemum, Aztec marigold, Eupatorium adenophorum, the tuber of stemona, capsicum, macleaya cordata, kuh-seng, chinaberry, Chinese tallow tree, black nightshade, Rhododendron molle, Coriaria sinica, garlic, the fruit of a cubeb litsea tree, Rhododendron molle flowers, winter daphne, the root of langdu, Lysimachia foenum-graecum, peppermint, calamus, Chinese cassia tree, black pepper, Artemisia scoparia, galangal, argy wormwood, Chinese prickly ash, Cynanchum Komarovii, Chinese honey locust, datura, ginkgo, camphor tree, reticulate millettia, elscholtiza, the root of Chinese wild ginger, the India red sandalwood, erythrina indica, alkaloids in the crude extract of one or more in plant iron son and the frutus cnidii or the active component, terpenes, flavonoids, the essential oil class, in the photoactivation endotoxin one or more.
4. the agriculturally useful compositions that contains antibiotics and botanical components according to claim 3 is characterized in that botanical components is datura total alkali in the alkaloids, Chelidonine, the total alkaloids, camptothecine, aconitine, strychnia, total alkaloid of sophora alopecuroide, the thunder godvine alkaloid, oxymatrine, nicotine, the black false hellebore total alkali, capsaicine, matrine, sanguinarine, jamaicin, stemonine, papaverine, quinoline is peaceful, tomatin, lupinine, sparteine, the numb rope in ground, donaxine, morphine, kind art soft-shelled turtle alkali, gelsemium henbane amine, mufangchine, magnoflorine, aconitine, eulexine, atropine, the black nightshade alkaloid, one or more alkaloids in the dandelion alkaloid or one or more components in the above-mentioned total alkali; Or be diterpene-kind compound in the Celastrus angulatus, Euphorbiaceae, Isolated From Thymelaeaceae Species of coriamyrtin, the Celastraceae plant of monoterpene, Coriariaceae plant in the Chinese azalea extract, the menthol in the Labiatae, peppermint aldehyde, Cupressaceae plant in the Ericaceae and one or more in the triterpene compound in the Meliaceae; Or for flavonoids in the flavonoids be in the young flavones of chamaejasmine, rotenone, pterocarpoid, kuh-seng flavones and plant iron one or more; Or be to be in the terpene compound in the thyme, Chinese cassia tree, lemongrass, cloves, Chinese anise, orange peel, tree-of-heaven bark, chilli powder, Siberian cocklebur, lavender, the fruit of a cubeb litsea tree, garlic, peppermint, cypress, Chinese prickly ash, Artemisia scoparia, aromatic compound, aliphatic compound, the sulfur-bearing nitrogen-containing compound one or more in the essential oil; Or in the Plant Light activation endotoxin being one or more in furocoumarin class, polyyne class, thiophene phenols and the quinones.
5. the agriculturally useful compositions that contains antibiotics and botanical components according to claim 4, it is characterized in that botanical components is the datura total alkali in the alkaloids, Chelidonine, the total alkaloids, camptothecine, aconitine, strychnia, Cynanchum Komarovii alkali, one or more components in one or more alkaloids in solanine or the dandelion alkali or the biology total alkali, or a kind of in the Chinese azalea extract in the terpenes and the coriamyrtin or two kinds, or the chamaejasmine in the flavonoids, a kind of in the pterocarpoid or two kinds, or a kind of in the thymol in the essential oil and the cinnamic acid or two kinds.
6. each the agriculturally useful compositions that contains antibiotics and botanical components according to claim 1-5, the ratio of quality and the number of copies of antibiotics and botanical components is 50:1-1:200.
7. the agriculturally useful compositions that contains antibiotics and botanical components according to claim 6, the preparation that it is characterized in that composition processing is wetting powder, water dispersible granules, aqueous emulsion, microemulsion, suspending agent, and the percentage that antibiotics and botanical components quality sum account for the preparation gross mass is 0.05-80%.
8. the preparation of the agriculturally useful compositions processing that contains antibiotics and botanical components according to claim 7, the percentage that the quality sum that it is characterized in that antibiotics and botanical components accounts for the preparation gross mass is 0.1-40%.
9. according to claim 7 or the preparations of the 8 described agriculturally useful compositions processing that contain antibiotics and botanical components, it is characterized in that showing the purposes of preventing and treating the various crop damage by disease and insect with base manure, spraying, filling root, seed dressing, immersion applications.
10. the agriculturally useful compositions that contains antibiotics and botanical components according to claim 9, it is characterized in that the Avermectin in the antibiotic, ivermectin, milbemectin, pleocidin, nikkomycin, the compositions-treated of macro tetrolide and several feverfew components and the Ningnanmycin in the antibiotic, jinggangmycin, kasugarnycin, polyoxin, the processing of streptomycin sulphate and several alkaloidal compositions has positive effect to cotton nematode and verticillium wilt, Avermectin in the antibiotic, ivermectin, milbemectin, pleocidin, nikkomycin, the composition of macro tetrolide and several composite family components reaches with several alkaloid compositions citrus pest, cotton-plant pest-insects have synergistic effect, Ningnanmycin in the antibiotic, jinggangmycin, kasugarnycin, polyoxin, streptomycin sulphate and several alkaloidal composition are to tomato disease, rice disease has synergistic effect, Avermectin in the antibiotic, ivermectin, pleocidin, milbemectin, nikkomycin, macro tetrolide respectively with the composition of the Chinese azalea extract of terpenes and with the composition of coriamyrtin and with the composition of the chamaejasmine of flavonoids and with the composition of pterocarpin to the wild cabbage insect, cotton-plant pest-insects have synergistic effect, the antibiotic Ningnanmycin, jinggangmycin, kasugarnycin, polyoxin, the composition of streptomycin sulphate and plants essential oil has synergistic effect to rice sheath blight disease.
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CN109006844A (en) * 2018-08-24 2018-12-18 广西田园生化股份有限公司 A kind of agricultural insecticide composition of the derivative containing sparteine and its utilization
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CN112493237A (en) * 2019-09-16 2021-03-16 山东省联合农药工业有限公司 Pesticide composition containing cinnamaldehyde and preparation method and application thereof
CN110720275B (en) * 2019-09-24 2021-11-12 湖南农业大学 Cultivation method for improving salt resistance of macleaya cordata
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CN111149815A (en) * 2020-01-07 2020-05-15 湖北中医药大学 Bacteriostatic agent for efficiently preventing and treating cotton verticillium wilt and preparation method and application thereof
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CN115039781A (en) * 2022-06-14 2022-09-13 沈阳化工大学 Insecticidal composition containing spinosad and matrine and application thereof
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CN116686848B (en) * 2023-07-31 2023-10-10 山东浏园生态农业股份有限公司 Pesticide preparation for tea plant diseases and application thereof

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CN105265501A (en) 2016-01-27
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