CN103689017A - Composite plant source pesticide and preparation method thereof - Google Patents
Composite plant source pesticide and preparation method thereof Download PDFInfo
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- CN103689017A CN103689017A CN201310612888.XA CN201310612888A CN103689017A CN 103689017 A CN103689017 A CN 103689017A CN 201310612888 A CN201310612888 A CN 201310612888A CN 103689017 A CN103689017 A CN 103689017A
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- mother liquor
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention relates to a composite plant source pesticide, which is characterized by including a mother liquid and an additive. The mother liquor comprises the following raw materials by weight: 35% of a Sophora flavescens extract, 35% of a resveratrol extract, 10% of a radix stemonae extract, 10% of a Melia azedarach extract, 5% of a Chinese azalea flower extract and 5% of a folium artemisiae argyi extract. A preparation method provided by the invention comprises the steps of: weighing the Sophora flavescens, resveratrol, radix stemonae, tobacco, Melia azedarach and folium artemisiae argyi according to the proportion; conducting screening, boiling extraction and purification to prepare an extract containing active ingredients of each component; and then mixing the mother liquor and the additive to obtain the product. Through various tests, the product has no adverse excitant smell, no drug residue, no damage to human, livestock, agricultural products, air and soil, has insecticidal and antimicrobial effects, and is suitable for usage in field, greenhouse, nursery, golf course, tea garden and forestry greening.
Description
Technical field
The invention belongs to vegetable insecticide technical field, especially a kind of composite plant source pesticide and preparation method thereof.
Background technology
Insecticide is mainly used in preventing and treating the medicine of pest and urban health insect, it uses long history, consumption large, wide in variety, in today of agriculture fast development, various utilizations of pesticides, farm output is increased, it can be divided into stomach poison, contact insecticide, fumigant and systemic insecticide by mode of action classification, it can be divided into never poison, respiratory poison, physical property toxic agent and specificity insecticide by toxicological effect classification, but the change ecosystem that nearly all insecticide all can be serious is most of harmful to people and animals.
Along with social progress, food-safety problem has received people's concern just day by day, and Pesticide Residue during as planting is the problem that people are concerned about most, through people, constantly study, developed various plants insecticide, it is by effective component extracting from possess the plant of desinsection special efficacy, the medicament of making after adding auxiliary agent to dissolve, it is generally acknowledged wide spectrum, efficient, low toxicity, the easy insecticide of degraded, noresidue, to people and animals and surrounding environment less pollution.But the vegetable insecticide of each manufacturer production all has own consideration on the determining of the selection of component, consumption, but in the effect of actual use, can not meet the needs of growing agriculture deinsectization.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, provide proportioning science, environmental protection, to harmless, the efficient a kind of composite plant source pesticide of people livestock and poultry.
The technical scheme that the present invention takes is:
A composite plant source pesticide, is characterized in that: comprise mother liquor and auxiliary agent, the raw material of described mother liquor comprises the following component of mixing by weight percentage:
And described auxiliary agent comprises emulsifier, bleeding agent, ethanol, phase solvent and turpentine oil, the percentage by weight that each component accounts for mother liquor is respectively 15%, 13%, 10%, 12% and 4%.
And described emulsifier is the mixture of sheep oil, fatty alcohol-polyoxyethylene ether, castor oil polyoxyethylene ether and absolute ethyl alcohol, the weight ratio of each component is 3:3:2:2.
And described bleeding agent is a kind of in dimethyl sulfoxide (DMSO), azone or thiophene ketone.
And described concentration of alcohol is 95%.
And described phase solvent is cyclohexanone.
And described mother liquor and auxiliary agent add synergist after mixing, this synergist is the Affirm (Merck Co.) of mother liquor weight 2～3 ‰, at least one in 9 ‰ Avermectin.
Another object of the present invention is to provide a kind of preparation method of composite plant source pesticide, it is characterized in that: comprise the following steps:
(1) take without going mouldy, the kuh-seng without rotten, black false hellebore, the tuber of stemona, China tree, Rhododendron molle and tarragon, clean up, standby;
(2) step individual component is (1) added respectively in the cold water of 8 times of weight and decoct;
(3) the filtering dregs of a decoction, the concentrated liquid extract that forms of the independent low temperature of each liquid;
(4) in proportion each liquid extract is mixed, form mother liquor after adding water;
(5) mother liquor (4) of step is further processed to then in storage tank standing 72 hours through colloid mill and homogenizer;
(6) the supernatant of getting after standing adds auxiliary agent and synergist in proportion, after then stirring in Chinese medicine emulsification pot, makes finished product.
The process for preparation of described auxiliary agent is:
Use phase solvent dilution turpentine oil, continue to add emulsifier, bleeding agent, ethanol, stir.
Another object of the present invention is to provide a kind of using method of composite plant source pesticide, it is characterized in that: in finished product, add the water dilution of 800～3000 times, then spray.
Advantage of the present invention and good effect are:
In the present invention, by metering, take kuh-seng, black false hellebore, the tuber of stemona, tobacco leaf, Rhododendron molle and tarragon, after screening, boiling are extracted, are purified, make the extract that contains each component active ingredient, then will after mother liquor and additive compound, make finished product, this finished product is tested through many-side, without bad penetrating odor, drug residue free, people and animals, agricultural product, air, soil are not all had to poisoning, possess desinsection, antibacterial effect, be applicable to the ground such as land for growing field crops, booth, nursery, golf course, tea place and forestry greening and use.
Embodiment
Below in conjunction with embodiment, the present invention is further described, and following embodiment is illustrative, is not determinate, can not limit protection scope of the present invention with following embodiment.
A composite plant source pesticide, innovation of the present invention is: comprise mother liquor and auxiliary agent, the raw material of described mother liquor comprises the following component of mixing by weight percentage:
Described auxiliary agent comprises emulsifier, bleeding agent, 95% ethanol, phase solvent and turpentine oil, and the percentage by weight that each component accounts for mother liquor is respectively 15%, 13%, 10%, 12% and 4%.Described emulsifier is the mixture of sheep oil, fatty alcohol-polyoxyethylene ether, castor oil polyoxyethylene ether and absolute ethyl alcohol, and the weight ratio of each component is 3:3:2:2.Described bleeding agent is a kind of in dimethyl sulfoxide (DMSO), azone or thiophene ketone.Described phase solvent is cyclohexanone.Described mother liquor and auxiliary agent add synergist after mixing, and this synergist is the Affirm (Merck Co.) of mother liquor weight 2～3 ‰, at least one in 9 ‰ Avermectin.
The preparation method of above-mentioned composite plant source pesticide comprises the following steps:
(2) get without going mouldy, the kuh-seng without rotten, black false hellebore, the tuber of stemona, China tree, Rhododendron molle and tarragon, clean up, standby;
(2) step individual component is (1) added respectively in the cold water of 8 times of weight and decoct, 120 ℃ of temperature, decoct 2 hours;
(3) the filtering dregs of a decoction, the concentrated liquid extract that forms of the independent low temperature of each liquid;
(4) in proportion each liquid extract is mixed, form mother liquor after adding water;
(5) mother liquor (4) of step is further processed to then in storage tank standing 72 hours through colloid mill and homogenizer;
(6) the supernatant of getting after standing adds auxiliary agent and synergist in proportion, after then stirring in Chinese medicine emulsification pot, makes finished product.
The process for preparation of described auxiliary agent is:
Use phase solvent dilution turpentine oil, continue to add emulsifier, bleeding agent, ethanol, stir.
In the present invention, in kuh-seng, extract oxymatrine, in black false hellebore, extract jervine, in the tuber of stemona, extract stemonine, in China tree, extract margosine, in Rhododendron molle, extract Andromedotoxin and Chinese photinia element, from tarragon, extract Blumea oil, each active ingredient cooperatively interacts, by auxiliary agents such as emulsifier, form liquid, wherein utilize all ginsengs (ginseng, Radix Codonopsis, the root of straight ladybell, radix scrophulariae, kuh-seng, the red sage root) pungent (root of Chinese wild ginger) Chinese herbaceous peony (radix paeoniae rubrathe root of herbaceous peony) black false hellebore of betraing in the traditional eighteen incompatibilities theory of Chinese medicine, be to mutually promote after oxymatrine and jervine combination, increase insecticidal activity.
During use, by the multiple dilution by weight of liquid water, in the prevention stage, can be diluted to 3000 times, in the stage occurred frequently, can be diluted to 800 times, carry out complete stool sprinkling, do not mix with strong alkaline substance, the morning, 10 left and right medications were best, avoided rainwater, and it will be tagged, stomach kills and combines, after spraying, make insect death by suffocation, before medication, this product is fully shaken up, inside have a small amount of sediment not affect desinsection quality, be applicable to land for growing field crops, booth, flowers, golf course, tea place, forestry greenery patches etc., nontoxic to people and animals, can contaminated air, environment, soil etc.
Each component adopts flooding to carry out effective component extracting, avoided water boiling and precipitation with ethanol method by nutriment precipitations such as polysaccharide, protein, by the effect of bleeding agent, these nutrients mass-energy rapid osmotic enter in plant cell, and insecticide sterilization component also can rapid osmotic, wherein dimethyl sulfoxide (DMSO) effect is better, but cost is low, azone and thiophene ketone better effects if, but cost is higher.
95% ethanol has played preservation, can make drug effect keep the longer time.Emulsifier makes liquid more even.Turpentine oil increases the adhesive force of liquid.
Toxicity test 1
Inspection Unit: Environmental Sanitation Inst., China Preventive Medical Science Academy
Interventions Requested: acute oral toxicity test, acute dermal toxicity test, eye irritant test
Assay:
1. acute oral toxicity test: this medicine is all greater than 5000mg/kg body weight to female male white mouse LD50 of passing through mouth, belongs to hypotoxicity.
2. acute dermal toxicity test: this medicine is all greater than 2000mg/kg body weight to female male rabbit through skin LD50, belongs to hypotoxicity.
3. eye irritant test: this medicine animal eyes is contaminated under washing condition not 4 second afterflush and 30 seconds afterflush of contamination all present slight excitant.
Toxicity test 2
Inspection Unit: Hong Kong China manufacturer's association
Interventions Requested: whether contain chemical pesticide
Assay: not containing any chemical pesticide
Toxicity test 3
Inspection Unit: Chinese Academy of Agricultural Sciences's quality testing center
Interventions Requested: the harmful substance that whether contains organic tea garden forbidding
Assay: after spray in tea place, sampling Detection does not contain the harmful substance of any forbidding
Embodiment 1
Be below concrete example, please fill in red blank space, the consumption of filling out should be identical with the ratio in claims.
(1) take without the 400 kilograms of kuh-sengs, 400 kilograms of black false hellebores, 150 kilograms of tubers of stemona, 150 kilograms of China trees, 80 kilograms of Rhododendron molles and the 80 kilograms of tarragons that go mouldy, nothing is rotten, clean up, standby;
(2) step individual component is (1) added respectively in the cold water of 8 times of weight and decoct;
(3) the filtering dregs of a decoction, the concentrated liquid extract that forms of the independent low temperature of each liquid;
(4) in proportion each liquid extract is mixed, form mother liquor after adding water;
(5) mother liquor (4) of step is further processed to then in storage tank standing 72 hours through colloid mill and homogenizer;
(6) the supernatant of getting after standing adds auxiliary agent in proportion, after then stirring in Chinese medicine emulsification pot, makes finished product.
Embodiment 2
Be below concrete example, please fill in red blank space, the consumption of filling out should be identical with the ratio in claims.
(1) take without the 400 kilograms of kuh-sengs, 400 kilograms of black false hellebores, 150 kilograms of tubers of stemona, 150 kilograms of China trees, 80 kilograms of Rhododendron molles and the 80 kilograms of tarragons that go mouldy, nothing is rotten, clean up, standby;
(2) step individual component is (1) added respectively in the cold water of 8 times of weight and decoct;
(3) the filtering dregs of a decoction, the concentrated liquid extract that forms of the independent low temperature of each liquid;
(4) ratio is mixed each liquid extract, forms mother liquor after adding water;
(5) mother liquor (4) of step is further processed to then in storage tank standing 72 hours through colloid mill and homogenizer;
(6) the supernatant of getting after standing adds auxiliary agent and Affirm (Merck Co.) in proportion, after then stirring in Chinese medicine emulsification pot, makes finished product.
Embodiment 3
Be below concrete example, please fill in red blank space, the consumption of filling out should be identical with the ratio in claims.
(1) take without the 400 kilograms of kuh-sengs, 400 kilograms of black false hellebores, 150 kilograms of tubers of stemona, 150 kilograms of China trees, 80 kilograms of Rhododendron molles and the 80 kilograms of tarragons that go mouldy, nothing is rotten, clean up, standby;
(2) step individual component is (1) added respectively in the cold water of 8 times of weight and decoct;
(3) the filtering dregs of a decoction, the concentrated liquid extract that forms of the independent low temperature of each liquid;
(4) ratio is mixed each liquid extract, forms mother liquor after adding water;
(5) mother liquor (4) of step is further processed to then in storage tank standing 72 hours through colloid mill and homogenizer;
The supernatant of getting after standing adds auxiliary agent and Avermectin in proportion, after then stirring in Chinese medicine emulsification pot, makes finished product.
Embodiment 4
Be below concrete example, please fill in red blank space, the consumption of filling out should be identical with the ratio in claims.
(1) take without the 400 kilograms of kuh-sengs, 400 kilograms of black false hellebores, 150 kilograms of tubers of stemona, 150 kilograms of China trees, 80 kilograms of Rhododendron molles and the 80 kilograms of tarragons that go mouldy, nothing is rotten, clean up, standby;
(2) step individual component is (1) added respectively in the cold water of 8 times of weight and decoct;
(3) the filtering dregs of a decoction, the concentrated liquid extract that forms of the independent low temperature of each liquid;
(4) ratio is mixed each liquid extract, forms mother liquor after adding water;
(5) mother liquor (4) of step is further processed to then in storage tank standing 72 hours through colloid mill and homogenizer;
The supernatant of getting after standing adds auxiliary agent, Affirm (Merck Co.) and Avermectin in proportion, after then stirring in Chinese medicine emulsification pot, makes finished product.
Application Example 1
Inspection Unit: entomology research institute of Zhongshan University
Interventions Requested: virulence test
The LC50 of Interventions Requested: embodiment 1 pair of beet armyworm, cotton bollworm and prodenia litura measures
Assay: test data is inputted to calculator, measure embodiment medicament the diluted concentration of the LC50 of beet armyworm, cotton bollworm and prodenia litura third-instar larvae is respectively to 24000,25000 and 5600.
Application Example 2
Inspection Unit: tea place, You Long village, Xiuning County
Interventions Requested: tea caterpillar, tea aleyrodid, tea geometrid, tea aphid, tea olethreutid, cluster caterpillar that tea place is common
3000 times of assay: embodiment 2 medicaments dilutions, in medication 1～3 day, dead rate of knockdown 95% left and right.
Application Example 3
Inspection Unit: the Chinese Academy of Agricultural Sciences's Plant Protection Institute
Interventions Requested: cotton bollworm, beet armyworm, striped rice borer, aphid, oriental tobacco budworm, two spotted spider mite
The dead rate of knockdown that assay: embodiment 3 medicament dilution is 2000 times is more than 90%.
Application Example 4
Inspection Unit: proving ground, drug effect Changping, national agricultural chemicals land for growing field crops
Interventions Requested: Chinese scholar tree looper
The dead rate of knockdown that assay: embodiment 4 medicament dilution is 1500 times is more than 95%.
Application Example 5
Inspection Unit: Hubei Province agriculture chemical examination administrative institute
Interventions Requested: Chinese cabbage cabbage caterpillar
The dead rate of knockdown that assay: embodiment 1 medicament dilution is 1200 times is more than 96%.
Application Example 6
Inspection Unit: the Production and Construction Corps of Xinjiang
Interventions Requested: cotten aphid, trialeurodes vaporariorum, cotton thrips, cotton spider mites, cotton bollworm
The dead rate of knockdown that assay: embodiment 1 medicament dilution is 1000 times is more than 97%.
Application Example 7
Inspection Unit: Hubei Province agriculture chemical examination administrative institute
Interventions Requested: wild cabbage diamond-back moth
The dead rate of knockdown that assay: embodiment 1 medicament dilution is 800 times is more than 93%.
Application Example 8
Inspection Unit: Sanya State Forestry Administration, P.R. China
Interventions Requested: Brontispa longissima worm
After assay: embodiment 1 medicament dilutes 900 times, complete stool is sprayed, and Brontispa longissima worm climbs out of rear death by suffocation in pith, and dead rate of knockdown is more than 95%.
Application Example 9
Inspection Unit: Jiangsu pesticide research institute
Interventions Requested: wheat powdery mildew
The control rate that assay: embodiment 1 medicament dilution is 1600 times is more than 94%.
Application Example 10
Inspection Unit: Henan agriculture chemical examination administrative institute
Interventions Requested: tomato spot disease
The control rate that assay: embodiment 1 medicament dilution is 2000 times is more than 92%.
Application Example 11
Inspection Unit: Hebei Agricultural Product quality testing center
Interventions Requested: watermelon blight
The control rate that assay: embodiment 1 medicament dilution is 1000 times is more than 94%.
Application Example 12
Inspection Unit: agricultural chemicals supervision and management station, Jixian Tianjin
Interventions Requested: walnut rot
The control rate that assay: embodiment 1 medicament dilution is 2000 times is more than 91%.
Application Example 13
Inspection Unit: guesthouse management office garden management place, fishing platform
Interventions Requested: ornamental plants anthracnose, greening seedling downy mildew
After 1200 times of assay: embodiment 1 medicament dilutions, above-mentioned two kinds of sick control rates are more than 92%.
Application Example 14
Inspection Unit: Shanghai golf course
Interventions Requested: expelling parasite, smell
After assay: embodiment 1 medicament dilutes 900 times, the control rate of common insect pest and disease is more than 92%, after spraying the morning, place can be opened afternoon, and nonirritant taste is harmless.
In the present invention, by metering, take kuh-seng, black false hellebore, the tuber of stemona, tobacco leaf, Rhododendron molle and tarragon, after screening, boiling are extracted, are purified, make the extract that contains each component active ingredient, then will after mother liquor and additive compound, make finished product, this finished product is tested through many-side, without bad penetrating odor, drug residue free, people and animals, agricultural product, air, soil are not all had to poisoning, possess desinsection, antibacterial effect, be applicable to the ground such as land for growing field crops, booth, nursery, golf course, tea place and forestry greening and use.
Claims (9)
1. a composite plant source pesticide, is characterized in that: comprise mother liquor and auxiliary agent, the raw material of described mother liquor comprises the following component of mixing by weight percentage:
2. a kind of composite plant source pesticide according to claim 1, is characterized in that: described auxiliary agent comprises emulsifier, bleeding agent, ethanol, phase solvent and turpentine oil, and the percentage by weight that each component accounts for mother liquor is respectively 15%, 13%, 10%, 12% and 4%.
3. a kind of composite plant source pesticide according to claim 2, is characterized in that: described emulsifier is the mixture of sheep oil, fatty alcohol-polyoxyethylene ether, castor oil polyoxyethylene ether and absolute ethyl alcohol, and the weight ratio of each component is 3:3:2:2.
4. a kind of composite plant source pesticide according to claim 3, is characterized in that: described bleeding agent is a kind of in dimethyl sulfoxide (DMSO), azone or thiophene ketone.
5. a kind of composite plant source pesticide according to claim 2, is characterized in that: described concentration of alcohol is 95%.
6. a kind of composite plant source pesticide according to claim 4, is characterized in that: described phase solvent is cyclohexanone.
7. a kind of composite plant source pesticide according to claim 6, is characterized in that: described mother liquor and auxiliary agent add synergist after mixing, and this synergist is the Affirm (Merck Co.) of mother liquor weight 2～3 ‰, at least one in 9 ‰ Avermectin.
8. the preparation method of a kind of composite plant source pesticide according to claim 7, is characterized in that: comprise the following steps:
(1) take without going mouldy, the kuh-seng without rotten, black false hellebore, the tuber of stemona, China tree, Rhododendron molle and tarragon, clean up, standby;
(2) step individual component is (1) added respectively in the cold water of 8 times of weight and decoct;
(3) the filtering dregs of a decoction, the concentrated liquid extract that forms of the independent low temperature of each liquid;
(4) in proportion each liquid extract is mixed, form mother liquor after adding water;
(5) mother liquor (4) of step is further processed to then in storage tank standing 72 hours through colloid mill and homogenizer;
(6) the supernatant of getting after standing adds auxiliary agent and synergist in proportion, after then stirring in Chinese medicine emulsification pot, makes finished product.
The process for preparation of described auxiliary agent is:
Use phase solvent dilution turpentine oil, continue to add emulsifier, bleeding agent, ethanol, stir.
9. the using method of a kind of composite plant source pesticide according to claim 8, is characterized in that: in finished product, add the water dilution of 800～3000 times, then spray.
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| CN103689017B CN103689017B (en) | 2016-04-13 |
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