CN103229786B - Complex organic plant pesticide and preparation method thereof - Google Patents
Complex organic plant pesticide and preparation method thereof Download PDFInfo
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- CN103229786B CN103229786B CN201210114361.XA CN201210114361A CN103229786B CN 103229786 B CN103229786 B CN 103229786B CN 201210114361 A CN201210114361 A CN 201210114361A CN 103229786 B CN103229786 B CN 103229786B
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- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 239000000575 pesticide Substances 0.000 title abstract description 23
- 241000196324 Embryophyta Species 0.000 claims abstract description 28
- 239000007788 liquid Substances 0.000 claims abstract description 24
- 241000931143 Gleditsia sinensis Species 0.000 claims abstract description 22
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 22
- 240000000275 Persicaria hydropiper Species 0.000 claims abstract description 22
- 235000017337 Persicaria hydropiper Nutrition 0.000 claims abstract description 22
- 241001251949 Xanthium sibiricum Species 0.000 claims abstract description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 22
- 235000011389 fruit/vegetable juice Nutrition 0.000 claims abstract description 11
- 239000002994 raw material Substances 0.000 claims abstract description 8
- 244000061176 Nicotiana tabacum Species 0.000 claims abstract 3
- 239000000706 filtrate Substances 0.000 claims description 35
- 238000010298 pulverizing process Methods 0.000 claims description 30
- 238000001914 filtration Methods 0.000 claims description 25
- 241001233914 Chelidonium majus Species 0.000 claims description 20
- 241000723346 Cinnamomum camphora Species 0.000 claims description 20
- 239000003905 agrochemical Substances 0.000 claims description 20
- 241000208125 Nicotiana Species 0.000 claims description 19
- 235000020072 grain neutral spirit Nutrition 0.000 claims description 19
- 239000002131 composite material Substances 0.000 claims description 14
- 230000001476 alcoholic effect Effects 0.000 claims description 5
- 238000005538 encapsulation Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- 239000002245 particle Substances 0.000 claims description 5
- 241000607479 Yersinia pestis Species 0.000 abstract description 10
- 230000000694 effects Effects 0.000 abstract description 6
- 201000010099 disease Diseases 0.000 abstract description 5
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 abstract description 5
- 150000001875 compounds Chemical class 0.000 abstract description 3
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 abstract 2
- 206010059866 Drug resistance Diseases 0.000 abstract 2
- 240000005636 Dryobalanops aromatica Species 0.000 abstract 2
- 241000221079 Euphorbia <genus> Species 0.000 abstract 2
- 235000012629 Mentha aquatica Nutrition 0.000 abstract 2
- 235000004442 Polygonum persicaria Nutrition 0.000 abstract 2
- 235000013399 edible fruits Nutrition 0.000 abstract 2
- 235000015203 fruit juice Nutrition 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 abstract 1
- 230000001276 controlling effect Effects 0.000 abstract 1
- 244000144972 livestock Species 0.000 abstract 1
- 230000002195 synergetic effect Effects 0.000 abstract 1
- 238000009461 vacuum packaging Methods 0.000 abstract 1
- 238000012360 testing method Methods 0.000 description 7
- 241000238631 Hexapoda Species 0.000 description 5
- 241000209094 Oryza Species 0.000 description 4
- 235000007164 Oryza sativa Nutrition 0.000 description 4
- 239000003814 drug Substances 0.000 description 4
- 235000009566 rice Nutrition 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 241000209140 Triticum Species 0.000 description 3
- 235000021307 Triticum Nutrition 0.000 description 3
- 240000008042 Zea mays Species 0.000 description 3
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 3
- 241000346285 Ostrinia furnacalis Species 0.000 description 2
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 description 2
- 230000006378 damage Effects 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 230000035558 fertility Effects 0.000 description 2
- 230000036039 immunity Effects 0.000 description 2
- 235000009973 maize Nutrition 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 210000004894 snout Anatomy 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical compound CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 1
- 241000426497 Chilo suppressalis Species 0.000 description 1
- 241000008892 Cnaphalocrocis patnalis Species 0.000 description 1
- 241000176086 Sogatella furcifera Species 0.000 description 1
- 208000031320 Teratogenesis Diseases 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 230000009418 agronomic effect Effects 0.000 description 1
- 230000000853 biopesticidal effect Effects 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 230000000857 drug effect Effects 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002703 mutagenesis Methods 0.000 description 1
- 231100000350 mutagenesis Toxicity 0.000 description 1
- 238000010899 nucleation Methods 0.000 description 1
- 244000144977 poultry Species 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 238000009331 sowing Methods 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
The invention relates to a compound organic plant pesticide and a preparation method thereof. The pesticide is composed of 2-20 parts of cinnamomum camphora, 1-15 parts to tobacco, 2-18 parts of Siberian cocklebur fruit, 1-7 parts of sun euphorbia herb, 0.5-5 parts of Chinese honeylocust fruit, 3-9 parts of marshpeper smartweed herb, limewater, grain distillate spirit, and a proper amount of water. According to the invention, cinnamomum camphora liquid, tobacco juice, Siberian cocklebur fruit juice, sun euphorbia herb liquid, Chinese honeylocust fruit juice, and marshpeper smartweed herb liquid are mixed; the mixture is heated, such that water is evaporated and the mixture is concentrated; and the concentrated liquid is subjected to vacuum packaging. The raw materials of the pesticide are sourced from natural plants, such that the pesticide is safe to human and livestock, and drug resistance is prevented. The raw materials are widely distributed in our nation, and the cost is low. With the pesticide, pest diseases can be effectively controlled, and an advantage for developing plant pesticide is shown. According to the invention, various plants are complexed. With the synergetic effect of the various effective components, the effect is fast, and the effective period is long, such that a comprehensive controlling effect against various pests is improved. The pesticide is safe to use, and pest drug resistance is prevented. The pesticide is a safe and environment-friendly pesticide.
Description
Technical field
The present invention relates to biological pesticide technical field, is a kind of composite organic plant agricultural chemicals and preparation method thereof specifically.
Background technology
At present, pesticide market is still taking chemical pesticide as main both at home and abroad, although can effectively kill disease and insect, but there are many problems in chemical pesticide, as caused " 3R " problem of pest resistance to insecticide, medicament residue and the mutagenesis of medicine, teratogenesis and carcinogenic " three cause " problem, serious environment pollution and agricultural product, cause very big harm to human health and the ecological balance.Therefore, the plant pesticide instead of chemical agricultural chemicals of development health environment-friendly, high-efficiency low-toxicity becomes the certainty of novel agrochemical development.
Along with agrotechnical progress, China Development and Production goes out some biopesticides, but restricted by agrotechnique, laboratory facilities, makes progress hysteresis as the same.These action of agricultural chemicals are slow in the effect of diseases and pests of agronomic crop, and quick-acting is not strong, limited it and promoted the use of.Carrying out science collocation but how reasonably to choose plant, obtain effect and fill a prescription significantly, to improve the control efficiency of damage by disease and insect, is development botanical pesticide problem in the urgent need to address.
Summary of the invention
For overcoming the deficiencies in the prior art, goal of the invention of the present invention is to provide a kind of composite organic plant agricultural chemicals and preparation method thereof, and the preparation taking natural plants as raw material, to realize the effect of safety comprehensive pest control.
For achieving the above object, the present invention is formulated by the raw material of following weight parts: fragrant camphor tree 2-20 part, tobacco 1-15 part, achene of Siberian cocklebur 2-18 part, wartwort 1-7 part, Chinese honey locust 0.5-5 part, polygonum flaccidum 3-9 part, all the other are limewash, grain neutral spirit and water.
The raw material of preferred weight part of the present invention is formulated as: fragrant camphor tree 3-5 part, tobacco 6-8 part, achene of Siberian cocklebur 6-10 part, wartwort 4-6 part, Chinese honey locust 1-3 part, polygonum flaccidum 5-7 part, all the other are limewash, grain neutral spirit and water.
The preparation method of composite organic plant agricultural chemicals of the present invention is: fragrant camphor tree, tobacco, the achene of Siberian cocklebur, wartwort, Chinese honey locust, polygonum flaccidum are ground into respectively to 20-40 order particle; It is that the grain neutral spirit of 52 degree soaks 24-48 hour, filtering and collecting filter liquid that the fragrant camphor tree 2-20 part of pulverizing is put into 10-20 alcoholic strength doubly; Tobacco 1-15 part of pulverizing is put into the limewash soak at room temperature 24-48 hour that 6-15 times of pH value is 7-8, filtering and collecting filter liquid; It is that more than 52 degree grain neutral spirit soaks 24-72 hour, filtering and collecting filter liquid that achene of Siberian cocklebur 2-18 part of pulverizing is put into 5-8 times of concentration; It is that more than 52 degree grain neutral spirit soaks 24-72 hour, filtering and collecting filter liquid that wartwort 1-7 part of pulverizing is put into 6-10 times of concentration; Chinese honey locust 0.5-5 part of pulverizing is added water to 1-15 doubly, under normal temperature, soak 12-24 hour, after filtration, obtain filtrate; Polygonum flaccidum 3-9 part of pulverizing 4-13 that adds water is doubly taken to juice; Described fragrant camphor tree filtrate, tobacco filtrate, achene of Siberian cocklebur filtrate, wartwort filtrate, Chinese honey locust filtrate, polygonum flaccidum filtrate are mixed, and heating makes water evaporates concentrated; After being vacuumized to encapsulation, juice after concentrated obtains composite organic plant agricultural chemicals.
The present invention, because its raw material sources are in natural plants, is difficult for developing immunity to drugs to person poultry safety, insect, is a kind of safe environment protection type agricultural chemicals.Fragrant camphor tree, tobacco, the achene of Siberian cocklebur, wartwort, Chinese honey locust, polygonum flaccidum are widely distributed, and cost is lower, and effectively prevention and elimination of disease and pests, has the advantage that develops plant pesticide.The present invention is composite by several plants, utilizes the synergy of various effective ingredients, and rapid-action, the drug effect phase is long, has improved the effect to various pests integrated control, uses safety and insect to be difficult for developing immunity to drugs, and is a kind of safe environment protection type agricultural chemicals.
embodiment
Below in conjunction with specific embodiment, the invention will be further described.
Embodiment 1
Fragrant camphor tree, tobacco, the achene of Siberian cocklebur, wartwort, Chinese honey locust, polygonum flaccidum are ground into respectively to 20-40 order particle; It is that the grain neutral spirit of 52 degree soaks 24 hours that 20 parts of the fragrant camphor trees of pulverizing are put into the alcoholic strength of 20 times, filtering and collecting filter liquid; 10 parts of the tobaccos of pulverizing are put into the limewash normal temperature that 6 times of pH values are 7 and soak 24 hours, filtering and collecting filter liquid; It is that more than 52 degree grain neutral spirit soaks 24 hours that 2 parts of the achenes of Siberian cocklebur of pulverizing are put into 5 times of concentration, filtering and collecting filter liquid; It is that more than 52 degree grain neutral spirit soaks 24 hours that 5 parts of the wartwort of pulverizing are put into 6 times of concentration, filtering and collecting filter liquid; 0.5 part of the Chinese honey locust of pulverizing is added water to 3 times, under normal temperature, soak 24 hours, after filtration, obtain filtrate; 6 parts of the polygonum flaccidums of pulverizing are added water 4 times and take juice; Described fragrant camphor tree filtrate, tobacco filtrate, achene of Siberian cocklebur filtrate, wartwort filtrate, Chinese honey locust filtrate, polygonum flaccidum filtrate are mixed, and heating makes water evaporates concentrated; After being vacuumized to encapsulation, juice after concentrated obtains composite organic plant agricultural chemicals.
Embodiment 2
Fragrant camphor tree, tobacco, the achene of Siberian cocklebur, wartwort, Chinese honey locust, polygonum flaccidum are ground into respectively to 20-40 order particle; It is that the grain neutral spirit of 52 degree soaks 48 hours that 10 parts of the fragrant camphor trees of pulverizing are put into the alcoholic strength of 20 times, filtering and collecting filter liquid; 15 parts of the tobaccos of pulverizing are put into the limewash normal temperature that 15 times of pH values are 8 and soak 48 hours, filtering and collecting filter liquid; It is that more than 52 degree grain neutral spirit soaks 72 hours that 12 parts of the achenes of Siberian cocklebur of pulverizing are put into 8 times of concentration, filtering and collecting filter liquid; It is that more than 52 degree grain neutral spirit soaks 72 hours that 7 parts of the wartwort of pulverizing are put into 10 times of concentration, filtering and collecting filter liquid; 3 parts of the Chinese honey locusts of pulverizing are added water to 15 times, under normal temperature, soak 24 hours, after filtration, obtain filtrate; 9 parts of the polygonum flaccidums of pulverizing are added water 13 times and take juice; Described fragrant camphor tree filtrate, tobacco filtrate, achene of Siberian cocklebur filtrate, wartwort filtrate, Chinese honey locust filtrate, polygonum flaccidum filtrate are mixed, and heating makes water evaporates concentrated; After being vacuumized to encapsulation, juice after concentrated obtains composite organic plant agricultural chemicals.
Embodiment 3
Fragrant camphor tree, tobacco, the achene of Siberian cocklebur, wartwort, Chinese honey locust, polygonum flaccidum are ground into respectively to 20-40 order particle; It is that the grain neutral spirit of 52 degree soaks 72 hours that 2 parts of the fragrant camphor trees of pulverizing are put into the alcoholic strength of 9 times, filtering and collecting filter liquid; 1 part of the tobacco of pulverizing is put into the limewash normal temperature that 10 times of pH values are 7.5 and soak 12 hours, filtering and collecting filter liquid; It is that more than 52 degree grain neutral spirit soaks 10 hours that 18 parts of the achenes of Siberian cocklebur of pulverizing are put into 6 times of concentration, filtering and collecting filter liquid; It is that more than 52 degree grain neutral spirit soaks 72 hours that 1 part of the wartwort of pulverizing is put into 4 times of concentration, filtering and collecting filter liquid; 5 parts of the Chinese honey locusts of pulverizing are added water to 20 times, under normal temperature, soak 10 hours, after filtration, obtain filtrate; 3 parts of the polygonum flaccidums of pulverizing are added water 10 times and take juice; Described fragrant camphor tree filtrate, tobacco filtrate, achene of Siberian cocklebur filtrate, wartwort filtrate, Chinese honey locust filtrate, polygonum flaccidum filtrate are mixed, and heating makes water evaporates concentrated; After being vacuumized to encapsulation, juice after concentrated obtains composite organic plant agricultural chemicals.
As follows by experimentation and the experimental data of above-mentioned example gained highly efficiency compositional organic plant agricultural chemicals:
One, the field trial of control rice insect pest.
1, control crop: late rice.
2, controlling object: rice leaf roller, striped rice borer, rice fulgorid etc.
3, test site: eight groups, Tao Jia village, yellow market town.
4, examination model point overview: field, 7, totally 6 family adds up to 19.3 mu of areas, and kind is hybrid rice, and soil type is hillock loess pH value 5.7, and before middle fertility, stubble is wheat, sowing in-10 days on the 7th June, adopts twice seedling raising method.
5, application method: spraying equipment is that back of the body person's formula sprayer is provided at each family for oneself, 30 kilograms of mu waters, mu dosage is not less than 500g.
Result of the test sees the following form one.
Table one: eight groups, Tao Jia village, yellow market town plant pesticide control late rice primary pest demonstration test table
Two, the field trial of compound botanical pesticide control of maize snout moth's larva
1, control crop: Corn after wheat.
2, controlling object: corn borer.
3, test site: 4 groups, Taishan village, corn borer district occurred frequently, Shu Xiang backlands district.
4, test site overview: field, 5, totally 5 family all belongs to Xiang Bei hillock, and preceding crop is wheat, physical features, fertility, date of seeding are basically identical.
5, testing program: 16 mu of areas of demonstration, mu is executed the compound botanical pesticide 500g 30kg that adds water, even spraying, in dispenser on the-20th on July 15, peasant's routine administration, 15 mu of areas, by peasant habit dispenser.
Test examination model the results are shown in following table two.
Table two: four groups, Taishan village, yellow market town plant pesticide control of maize snout moth's larva demonstration test table
| ? | Look into strain (strain) | Worm strain number alive | There is worm rate % | Relative control effect % |
| Use plant pesticide | 540 | 13 | 2.4 | 87.2 |
| Peasant is from anti- | 620 | 41 | 6.6 | 64.9 |
It is as shown in the table, and the present invention's control efficiency compared with chemical pesticide is more satisfactory, embodied the advantage of organic plant agricultural chemicals.
Claims (2)
1. a composite organic plant agricultural chemicals, it is characterized in that: composite organic plant agricultural chemicals is formulated by the raw material of following weight parts: fragrant camphor tree 2-20 part, tobacco 1-15 part, achene of Siberian cocklebur 2-18 part, wartwort 1-7 part, Chinese honey locust 0.5-5 part, polygonum flaccidum 3-9 part, all the other are limewash, grain neutral spirit and water;
The preparation method of described composite organic plant agricultural chemicals is: fragrant camphor tree, tobacco, the achene of Siberian cocklebur, wartwort, Chinese honey locust, polygonum flaccidum are ground into respectively to 20-40 order particle; It is that the grain neutral spirit of 52 degree soaks 24-48 hour, filtering and collecting filter liquid that the fragrant camphor tree 2-20 part of pulverizing is put into 10-20 alcoholic strength doubly; Tobacco 1-15 part of pulverizing is put into the limewash soak at room temperature 24-48 hour that 6-15 times of pH value is 7.5-8, filtering and collecting filter liquid; It is that more than 52 degree grain neutral spirit soaks 24-72 hour, filtering and collecting filter liquid that achene of Siberian cocklebur 2-18 part of pulverizing is put into 5-8 times of concentration; It is that more than 52 degree grain neutral spirit soaks 24-72 hour, filtering and collecting filter liquid that wartwort 1-7 part of pulverizing is put into 6-10 times of concentration; Chinese honey locust 0.5-5 part of pulverizing is added water to 1-15 doubly, under normal temperature, soak 12-24 hour, after filtration, obtain filtrate; Polygonum flaccidum 3-9 part of pulverizing 4-13 that adds water is doubly taken to juice; Described fragrant camphor tree filtrate, tobacco filtrate, achene of Siberian cocklebur filtrate, wartwort filtrate, Chinese honey locust filtrate, polygonum flaccidum filtrate are mixed, and heating makes water evaporates then concentrated; After being vacuumized to encapsulation, juice after concentrated obtains composite organic plant agricultural chemicals.
2. the composite organic plant agricultural chemicals of one according to claim 1, it is characterized in that: the raw material of preferred weight part is formulated as: fragrant camphor tree 3-5 part, tobacco 6-8 part, achene of Siberian cocklebur 6-10 part, wartwort 4-6 part, Chinese honey locust 1-3 part, polygonum flaccidum 5-7 part, all the other are limewash, grain neutral spirit and water.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201210114361.XA CN103229786B (en) | 2012-04-18 | 2012-04-18 | Complex organic plant pesticide and preparation method thereof |
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| CN201210114361.XA CN103229786B (en) | 2012-04-18 | 2012-04-18 | Complex organic plant pesticide and preparation method thereof |
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| CN103229786A CN103229786A (en) | 2013-08-07 |
| CN103229786B true CN103229786B (en) | 2014-07-09 |
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Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103694058B (en) * | 2013-12-03 | 2015-09-30 | 山东裕利蔬菜股份有限公司 | Pest control compound formulation and preparation technology thereof |
| CN105145683A (en) * | 2015-08-25 | 2015-12-16 | 蚌埠海上明珠农业科技发展有限公司 | Efficient natural biological pesticide and preparation method thereof |
| CN105123809A (en) * | 2015-08-27 | 2015-12-09 | 蚌埠龙达农业专业合作社 | Biological insecticide for floriculture and preparation method thereof |
| CN105815345A (en) * | 2016-04-12 | 2016-08-03 | 安徽林海园林绿化股份有限公司 | Nursery stock pest control agent prepared from schima superba leaves |
| CN106135315A (en) * | 2016-06-29 | 2016-11-23 | 辽宁科技学院 | A kind of natural botanical insecticide |
| CN106614782A (en) * | 2016-10-29 | 2017-05-10 | 蚌埠市涂山绿园蔬菜科研专业合作社 | Method for preventing and treating plant diseases and insect pests of sweet corn |
| CN106922762A (en) * | 2017-03-24 | 2017-07-07 | 合肥慧谷农业科技有限公司 | A kind of novel corn insecticide and preparation method thereof |
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