CN106135315A - A kind of natural botanical insecticide - Google Patents

A kind of natural botanical insecticide Download PDF

Info

Publication number
CN106135315A
CN106135315A CN201610522705.9A CN201610522705A CN106135315A CN 106135315 A CN106135315 A CN 106135315A CN 201610522705 A CN201610522705 A CN 201610522705A CN 106135315 A CN106135315 A CN 106135315A
Authority
CN
China
Prior art keywords
gained
extract
folium
natural botanical
botanical insecticide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610522705.9A
Other languages
Chinese (zh)
Inventor
廉莲
贺凤伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Liaoning Institute of Science and Technology
Original Assignee
Liaoning Institute of Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Liaoning Institute of Science and Technology filed Critical Liaoning Institute of Science and Technology
Priority to CN201610522705.9A priority Critical patent/CN106135315A/en
Publication of CN106135315A publication Critical patent/CN106135315A/en
Pending legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/02—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms
    • A01N43/04—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom
    • A01N43/14—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings
    • A01N43/16—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one or more oxygen or sulfur atoms as the only ring hetero atoms with one hetero atom six-membered rings with oxygen as the ring hetero atom
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
    • A01N43/90—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having two or more relevant hetero rings, condensed among themselves or with a common carbocyclic ring system
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N63/00—Biocides, pest repellants or attractants, or plant growth regulators containing microorganisms, viruses, microbial fungi, animals or substances produced by, or obtained from, microorganisms, viruses, microbial fungi or animals, e.g. enzymes or fermentates
    • A01N63/10—Animals; Substances produced thereby or obtained therefrom
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/38—Solanaceae [Potato family], e.g. nightshade, tomato, tobacco or chilli pepper
    • A01N65/385—Tobacco
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Agronomy & Crop Science (AREA)
  • Microbiology (AREA)
  • Biotechnology (AREA)
  • Pest Control & Pesticides (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Mycology (AREA)
  • Virology (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The invention discloses a kind of natural botanical insecticide, the raw material of following mass percent be prepared from: Tsubaki-saponin 10%～15%；Folium Cucurbitae yeast powder 3%～7%；Flos Tagetis Erectae extract 0.5%～1.5%；Matrine 3%～5%；Nicotiana tabacum L. liquid 5%～9.4%；Herba polygoni hydropiperis grass meal 2.5%～5.5%；Lignum Aquilariae Resinatum leaf extract 2.5%～5.5%；Folium Cephalotaxi extract 5%～10%；Excess water.The material of the present invention derives from plant, uses safety, environmentally friendly, and pest controling effect is good, and does not affect the yield and quality of plant.

Description

A kind of natural botanical insecticide
Technical field
The present invention relates to field of pesticide preparation, be specifically related to a kind of natural botanical insecticide.
Background technology
In agricultural production, in order to ensure agricultural output and quality, it will usually use substantial amounts of chemical insecticide to agriculture Field is sprayed on a large scale, therefore brings chemical agent to pollute ecological environment, and causes some insect to develop immunity to drugs rapidly, Thus usually use the way strengthening insecticide consumption further, insect is killed, has thereby resulted in agricultural product pesticide residual Allowance severe overweight, brings significant damage to human food.In this context, develop with natural product as object, find raw Active substances has been the road of certainty.And although China kills the history of disease and insect at the secondary noxious substance utilizing plant to produce Long, but really carry out systematic study and start from the '30s of eighties of last century, but make slow progress, there is presently no non-convention The high efficacy pesticide for plant thought.Nowadays, botanical pesticide receives attention the most day by day, in the world before pesticide research Edge and focus, people wait in expectation and find the Novel high-efficient pesticide meeting ideals of human being from plant.
Summary of the invention
For solving the problems referred to above, the invention provides a kind of natural botanical insecticide, its material derives from plant, uses Safety, environmentally friendly, pest controling effect is good, and does not affect the yield and quality of plant.
For achieving the above object, the technical scheme that the present invention takes is:
A kind of natural botanical insecticide, is prepared from by the raw material of following mass percent:
Tsubaki-saponin 10%～15%；Folium Cucurbitae yeast powder 3%～7%；Flos Tagetis Erectae extract 0.5%～1.5%；Radix Sophorae Flavescentis Alkali 3%～5%；Nicotiana tabacum L. liquid 5%～9.4%；Herba polygoni hydropiperis grass meal 2.5%～5.5%；Lignum Aquilariae Resinatum leaf extract 2.5%～5.5%；Three Point Folium Cunninghamiae lanceolatae extract 5%～10%；Excess water.
Preferably, described Folium Cucurbitae yeast powder prepares gained by following steps:
After clean Folium Cucurbitae micronizing, after in proportion mixed bacteria liquid being diluted 3～7 times, spray into the Folium Cucurbitae of gained Powder mixes；Simultaneously by 1.3～2.2L/m3Carbamide is sprayed onto on Folium Cucurbitae powder and turns mix homogeneously, hereafter by the ratio of consumption Spray weekly 1 mixed bacteria liquid, turn and be formed uniformly stable bacterium colony body, vaccinization 4～make after 5 weeks raw material enter decompose rank Section, stops inoculation, then turned 1 raw material every 5 days, continues 4～5 weeks, keeps the aerobic conditions in stockpile, stockpile endogenous dampness Degree is maintained at 60%～70%, obtains Folium Cucurbitae yeast powder.
Preferably, described Flos Tagetis Erectae extract prepares gained by following steps:
Dry Pyrethrum is placed in percolation vat, adds the aqueous solutions of organic solvent soak extraction three times of appropriate 90%, 24h every time, filters, merging filtrate, is concentrated to give Flos Tagetis Erectae extract.
Preferably, described Herba polygoni hydropiperis grass meal prepares gained by following steps: dry Herba polygoni hydropiperis is placed in infrared ray light Under wither 20-50 minute, control fresh leaf blade face temperature and be 28-32 DEG C, be subsequently placed in steam-explosion jar, be first passed through nitrogen anti-to high pressure Answering pressure in still is 0.8MPa～1.8MPa, explosion treatment 8min～22min；It is passed through the most rapidly steam in autoclave Pressure is 1.8MPa～2.6MPa, after Steam explosion treatment 0.8min～2.4min, is spray-dried concentrated solution, obtains powder body.
Preferably, Lignum Aquilariae Resinatum leaf extract prepares gained by following steps:
Step one, the Lignum Aquilariae Resinatum leaf flash extracter process that will clean and be dried, gained extracting solution first heats with high heat, boiling Heating 1～1.5h with slow fire after rising, hollow fiber ultrafiltration membrane filters；Medicinal residues add 15～25 times of soak by water twice, and doughnut surpasses Membrane filtration, merges three filtrates, is concentrated into 1.5g/ml；
Step 2, by the concentrated solution that obtains with 5～7BV/h flow velocity by macroporous resin column, after dynamic adsorption is saturated, use Deionized water is colourless to effluent with the above-mentioned macroporous resin column of flow velocity drip washing of 7～13BV/h, then with volume fraction be 45%～ The organic solvent of 75% carries out eluting with the flow velocity of 9～13BV/h, collects organic solvent eluent, finally will collect gained eluting Liquid concentrating under reduced pressure, obtains extractum；
Step 3, by after extractum water dissolution with 5～6BV/h flow velocity by polyamide column, after dynamic adsorption is saturated, use 5～7BV deionized waters with 3～8BV/h the above-mentioned polyamide column of flow velocity drip washing, then be 20%～100% have by volume fraction Machine solvent aqueous solution carries out eluting with the flow velocity of 6～12BV/h, collects organic solvent eluent, is spray-dried, obtains Lignum Aquilariae Resinatum leaf and carry Take thing.
Preferably, described Folium Cephalotaxi extract prepares gained by following steps:
Clean Folium Cephalotaxi is carried out micronizing, by gained powder body through CO after three quick-freezings are thawed2Supercritical extracts Taking twice, each 3-6h, fluid extraction pressure is 20～40MPa, extraction temperature 35～40 DEG C, CO2Fluid flow be 700～ 800L/h, is spray-dried, obtains Folium Cephalotaxi extract.
Preferably, described mixed bacteria liquid is by Corynebacterium glutamicum, enterobacteria YC105C, Bacillus licheniformis in mass ratio 2: 3: 1 mixing gained.
Preferably, described organic solvent is the turpentine derivatives of natural origin, and described turpentine derivatives is pinene Isomery, disproportionation products.
The method have the advantages that
Preparation vermins-proof effect is stable, and after testing, effect is better than the chemical pesticides such as cyromazine；Medicament contains from plant simultaneously In extract substantial amounts of aminoacid, biological clamps, fatty acid etc., these several compounds can quickly be absorbed by plants, and supplements plant Nutrient, thus promote the growth promoter of plant, increase substantially the yield and quality of plant；Gained preparation of the present invention without Malicious, pollution-free, green, environmental protection, without chemical pesticide composition, from root, stop the generation of chemical pesticide residual.
Detailed description of the invention
In order to make objects and advantages of the present invention clearer, below in conjunction with embodiment, the present invention is carried out further Describe in detail.Should be appreciated that specific embodiment described herein, only in order to explain the present invention, is not used to limit this Bright.
In following example, the Folium Cucurbitae yeast powder used prepares gained by following steps:
After clean Folium Cucurbitae micronizing, after in proportion mixed bacteria liquid being diluted 3～7 times, spray into the Folium Cucurbitae of gained Powder mixes；Simultaneously by 1.3～2.2L/m3Carbamide is sprayed onto on Folium Cucurbitae powder and turns mix homogeneously, hereafter by the ratio of consumption Spray weekly 1 mixed bacteria liquid, turn and be formed uniformly stable bacterium colony body, vaccinization 4～make after 5 weeks raw material enter decompose rank Section, stops inoculation, then turned 1 raw material every 5 days, continues 4～5 weeks, keeps the aerobic conditions in stockpile, stockpile endogenous dampness Degree is maintained at 60%～70%, obtains Folium Cucurbitae yeast powder, and wherein, described mixed bacteria liquid is by Corynebacterium glutamicum, enterobacteria YC105C, Bacillus licheniformis in mass ratio 2: 3: 1 mixes gained.
The Flos Tagetis Erectae extract used prepares gained by following steps:
Dry Pyrethrum is placed in percolation vat, adds the aqueous solutions of organic solvent soak extraction three times of appropriate 90%, 24h every time, filters, merging filtrate, is concentrated to give Flos Tagetis Erectae extract.
Preferably, described Herba polygoni hydropiperis grass meal prepares gained by following steps: dry Herba polygoni hydropiperis is placed in infrared ray light Under wither 20-50 minute, control fresh leaf blade face temperature and be 28-32 DEG C, be subsequently placed in steam-explosion jar, be first passed through nitrogen anti-to high pressure Answering pressure in still is 0.8MPa～1.8MPa, explosion treatment 8min～22min；It is passed through the most rapidly steam in autoclave Pressure is 1.8MPa～2.6MPa, after Steam explosion treatment 0.8min～2.4min, is spray-dried concentrated solution, obtains powder body.
The Lignum Aquilariae Resinatum leaf extract used prepares gained by following steps:
Step one, the Lignum Aquilariae Resinatum leaf flash extracter process that will clean and be dried, gained extracting solution first heats with high heat, boiling Heating 1～1.5h with slow fire after rising, hollow fiber ultrafiltration membrane filters；Medicinal residues add 15～25 times of soak by water twice, and doughnut surpasses Membrane filtration, merges three filtrates, is concentrated into 1.5g/ml；
Step 2, by the concentrated solution that obtains with 5～7BV/h flow velocity by macroporous resin column, after dynamic adsorption is saturated, use Deionized water is colourless to effluent with the above-mentioned macroporous resin column of flow velocity drip washing of 7～13BV/h, then with volume fraction be 45%～ The organic solvent of 75% carries out eluting with the flow velocity of 9～13BV/h, collects organic solvent eluent, finally will collect gained eluting Liquid concentrating under reduced pressure, obtains extractum；
Step 3, by after extractum water dissolution with 5～6BV/h flow velocity by polyamide column, after dynamic adsorption is saturated, use 5～7BV deionized waters with 3～8BV/h the above-mentioned polyamide column of flow velocity drip washing, then be 20%～100% have by volume fraction Machine solvent aqueous solution carries out eluting with the flow velocity of 6～12BV/h, collects organic solvent eluent, is spray-dried, obtains Lignum Aquilariae Resinatum leaf and carry Taking thing, wherein, described organic solvent is the turpentine derivatives of natural origin, described turpentine derivatives be pinene isomery, Disproportionation products.
Preferably, described Folium Cephalotaxi extract prepares gained by following steps:
Clean Folium Cephalotaxi is carried out micronizing, by gained powder body through CO after three quick-freezings are thawed2Supercritical extracts Taking twice, each 3-6h, fluid extraction pressure is 20～40MPa, extraction temperature 35～40 DEG C, CO2Fluid flow be 700～ 800L/h, is spray-dried, obtains Folium Cephalotaxi extract.
Embodiment 1
A kind of natural botanical insecticide, is prepared from by the raw material of following mass percent:
Tsubaki-saponin 10%；Folium Cucurbitae yeast powder 3%；Flos Tagetis Erectae extract 0.5%；Matrine 3%；Nicotiana tabacum L. liquid 5%；Peppery Herba polygoni hydropiperis powder 2.5%；Lignum Aquilariae Resinatum leaf extract 2.5%；Folium Cephalotaxi extract 5%；Excess water.
Embodiment 2
A kind of natural botanical insecticide, is prepared from by the raw material of following mass percent:
Tsubaki-saponin 15%；Folium Cucurbitae yeast powder 7%；Flos Tagetis Erectae extract 1.5%；Matrine 5%；Nicotiana tabacum L. liquid 9.4%； Herba polygoni hydropiperis grass meal 5.5%；Lignum Aquilariae Resinatum leaf extract 5.5%；Folium Cephalotaxi extract 10%；Excess water.
Embodiment 3
A kind of natural botanical insecticide, is prepared from by the raw material of following mass percent:
Tsubaki-saponin 12.5%；Folium Cucurbitae yeast powder 5%；Flos Tagetis Erectae extract 1%；Matrine 4%；Nicotiana tabacum L. liquid 7.2%； Herba polygoni hydropiperis grass meal 4%；Lignum Aquilariae Resinatum leaf extract 4%；Folium Cephalotaxi extract 7.5%；Excess water.
The above is only the preferred embodiment of the present invention, it is noted that for the ordinary skill people of the art For Yuan, under the premise without departing from the principles of the invention, it is also possible to make some improvements and modifications, these improvements and modifications also should It is considered as protection scope of the present invention.

Claims (8)

1. a natural botanical insecticide, it is characterised in that be prepared from by the raw material of following mass percent:
Tsubaki-saponin 10%～15%；Folium Cucurbitae yeast powder 3%～7%；Flos Tagetis Erectae extract 0.5%～1.5%；Matrine 3%～5%；Nicotiana tabacum L. liquid 5%～9.4%；Herba polygoni hydropiperis grass meal 2.5%～5.5%；Lignum Aquilariae Resinatum leaf extract 2.5%～5.5%；Tricuspid Folium Cunninghamiae lanceolatae extract 5%～10%；Excess water.
A kind of natural botanical insecticide the most according to claim 1, it is characterised in that described Folium Cucurbitae yeast powder by with Lower step prepares gained:
After clean Folium Cucurbitae micronizing, spray into after in proportion mixed bacteria liquid being diluted 3～7 times in the Folium Cucurbitae powder of gained Mixing；Simultaneously by 1.3～2.2L/m3Carbamide is sprayed onto on Folium Cucurbitae powder and turns mix homogeneously, the most weekly by the ratio of consumption Spray 1 mixed bacteria liquid, turn and be formed uniformly stable bacterium colony body, vaccinization 4～make after 5 weeks raw material enter catabolic phase, stop Only inoculation, then 1 raw material was turned every 5 days, continuing 4～5 weeks, keep the aerobic conditions in stockpile, stockpile humidity is protected Hold 60%～70%, obtain Folium Cucurbitae yeast powder.
A kind of natural botanical insecticide the most according to claim 1, it is characterised in that described Flos Tagetis Erectae extract by with Lower step prepares gained:
Dry Pyrethrum is placed in percolation vat, adds the aqueous solutions of organic solvent soak extraction three times of appropriate 90%, every time 24h, filters, merging filtrate, is concentrated to give Flos Tagetis Erectae extract.
A kind of natural botanical insecticide the most according to claim 1, it is characterised in that described Herba polygoni hydropiperis grass meal is by following step Suddenly preparing gained: be placed under infrared ray light by dry Herba polygoni hydropiperis and wither 20-50 minute, controlling fresh leaf blade face temperature is 28- 32 DEG C, being subsequently placed in steam-explosion jar, being first passed through nitrogen to high pressure reacting kettle inner pressure is 0.8MPa～1.8MPa, explosion treatment 8min～22min；Being passed through the most rapidly steam to high pressure reacting kettle inner pressure is 1.8MPa～2.6MPa, Steam explosion treatment After 0.8min～2.4min, it is spray-dried concentrated solution, obtains powder body.
A kind of natural botanical insecticide the most according to claim 1, it is characterised in that Lignum Aquilariae Resinatum leaf extract is by following step Suddenly gained is prepared:
Step one, the Lignum Aquilariae Resinatum leaf flash extracter process that will clean and be dried, gained extracting solution first heats, after boiling with high heat Heating 1～1.5h with slow fire, hollow fiber ultrafiltration membrane filters；Medicinal residues add 15～25 times of soak by water twice, hollow fiber ultrafiltration membrane Filter, merge three filtrates, be concentrated into 1.5g/ml；
Step 2, by the concentrated solution that obtains with 5～7BV/h flow velocity by macroporous resin column, after dynamic adsorption is saturated, spend from Sub-water is colourless to effluent with the above-mentioned macroporous resin column of flow velocity drip washing of 7～13BV/h, then is 45%～75% by volume fraction Organic solvent carry out eluting with the flow velocity of 9～13BV/h, collect organic solvent eluent, finally collection gained eluent subtracted Pressure concentrates, and obtains extractum；
Step 3, by after extractum water dissolution with 5～6BV/h flow velocity by polyamide column, after dynamic adsorption is saturated, with 5～ 7BV deionized water with 3～8BV/h the above-mentioned polyamide column of flow velocity drip washing, then with volume fraction be 20%～100% organic molten Agent aqueous solution carries out eluting with the flow velocity of 6～12BV/h, collects organic solvent eluent, is spray-dried, obtains Lignum Aquilariae Resinatum leaf extract.
A kind of natural botanical insecticide the most according to claim 1, it is characterised in that described Folium Cephalotaxi extract passes through Following steps prepare gained:
Clean Folium Cephalotaxi is carried out micronizing, by gained powder body through CO after three quick-freezings are thawed2Supercritical extraction two Secondary, each 3-6h, fluid extraction pressure is 20～40MPa, extraction temperature 35～40 DEG C, CO2Fluid flow is 700～800L/ H, is spray-dried, obtains Folium Cephalotaxi extract.
A kind of natural botanical insecticide the most according to claim 2, it is characterised in that described mixed bacteria liquid is by glutamic acid rod Bacillus, enterobacteria YC105C, Bacillus licheniformis in mass ratio 2: 3: 1 mix gained.
A kind of natural botanical insecticide the most according to claim 5, it is characterised in that described organic solvent is natural origin Turpentine derivatives, described turpentine derivatives is the isomery of pinene, disproportionation products.
CN201610522705.9A 2016-06-29 2016-06-29 A kind of natural botanical insecticide Pending CN106135315A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610522705.9A CN106135315A (en) 2016-06-29 2016-06-29 A kind of natural botanical insecticide

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610522705.9A CN106135315A (en) 2016-06-29 2016-06-29 A kind of natural botanical insecticide

Publications (1)

Publication Number Publication Date
CN106135315A true CN106135315A (en) 2016-11-23

Family

ID=58062901

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610522705.9A Pending CN106135315A (en) 2016-06-29 2016-06-29 A kind of natural botanical insecticide

Country Status (1)

Country Link
CN (1) CN106135315A (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106721699A (en) * 2016-11-30 2017-05-31 江苏食品药品职业技术学院 A kind of sobering-up beverage and preparation method thereof
CN106962422A (en) * 2017-05-12 2017-07-21 还童（锦州）特殊医学用途配方食品有限公司 Vegetable insecticide and preparation method thereof
CN108812724A (en) * 2018-07-25 2018-11-16 周口师范学院 A kind of biological pesticide
CN108901551A (en) * 2018-07-05 2018-11-30 紫云自治县紫香源农林科技有限责任公司 A kind of high yield bamboo bamboo shoot planting technology
CN110200026A (en) * 2019-06-28 2019-09-06 湖南省烟草公司长沙市公司 A kind of plant and microorganism composite insecticide and preparation method thereof
CN110506762A (en) * 2019-09-16 2019-11-29 覃涛 The preparation method for preventing and treating the medical fluid of curcuma zedoary pest and disease damage
CN110771630A (en) * 2019-10-15 2020-02-11 汤怀信 Insecticide

Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1545888A (en) * 2003-12-03 2004-11-17 华南农业大学 Method for extracting Cephalotaxus fortunei genus plant nematode-killing alkaloid and application thereof
CN102295494A (en) * 2011-06-13 2011-12-28 北京融青生态农业有限公司 Melon-bean fermentation broth, fermentation fertilizer and its preparation method
CN103229786A (en) * 2012-04-18 2013-08-07 湖北省文东农业发展有限公司 Complex organic plant pesticide and preparation method thereof
CN103518784A (en) * 2013-09-30 2014-01-22 横县生产力促进中心 Pollution-free jasmine pesticide
CN103535389A (en) * 2013-10-27 2014-01-29 莫晟琼 Plant source fruit tree insecticide
CN103548895A (en) * 2013-10-27 2014-02-05 来光业 Botanical vegetable insecticide
CN103609756A (en) * 2013-10-30 2014-03-05 桂平市西山茶场 Organic tea processing method
CN104844357A (en) * 2015-04-29 2015-08-19 内蒙古自治区林业科学研究院 Sandy soil modifier and preparation method thereof
CN104872218A (en) * 2015-06-11 2015-09-02 福建春辉生物工程有限公司 Natural household insecticide containing camellia japonica saponin
CN105535116A (en) * 2015-12-23 2016-05-04 辽宁科技学院 Natural medicinal material extract and preparation method thereof

Patent Citations (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1545888A (en) * 2003-12-03 2004-11-17 华南农业大学 Method for extracting Cephalotaxus fortunei genus plant nematode-killing alkaloid and application thereof
CN102295494A (en) * 2011-06-13 2011-12-28 北京融青生态农业有限公司 Melon-bean fermentation broth, fermentation fertilizer and its preparation method
CN103229786A (en) * 2012-04-18 2013-08-07 湖北省文东农业发展有限公司 Complex organic plant pesticide and preparation method thereof
CN103518784A (en) * 2013-09-30 2014-01-22 横县生产力促进中心 Pollution-free jasmine pesticide
CN103535389A (en) * 2013-10-27 2014-01-29 莫晟琼 Plant source fruit tree insecticide
CN103548895A (en) * 2013-10-27 2014-02-05 来光业 Botanical vegetable insecticide
CN103609756A (en) * 2013-10-30 2014-03-05 桂平市西山茶场 Organic tea processing method
CN104844357A (en) * 2015-04-29 2015-08-19 内蒙古自治区林业科学研究院 Sandy soil modifier and preparation method thereof
CN104872218A (en) * 2015-06-11 2015-09-02 福建春辉生物工程有限公司 Natural household insecticide containing camellia japonica saponin
CN105535116A (en) * 2015-12-23 2016-05-04 辽宁科技学院 Natural medicinal material extract and preparation method thereof

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
李凯夫: "《三香宝典 降香·檀香·沉香树木栽培与应用》", 31 August 2015, 中国林业出版社 *
谭仁祥: "《植物成分功能》", 31 October 2003, 科学出版社 *

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106721699A (en) * 2016-11-30 2017-05-31 江苏食品药品职业技术学院 A kind of sobering-up beverage and preparation method thereof
CN106962422A (en) * 2017-05-12 2017-07-21 还童（锦州）特殊医学用途配方食品有限公司 Vegetable insecticide and preparation method thereof
CN108901551A (en) * 2018-07-05 2018-11-30 紫云自治县紫香源农林科技有限责任公司 A kind of high yield bamboo bamboo shoot planting technology
CN108812724A (en) * 2018-07-25 2018-11-16 周口师范学院 A kind of biological pesticide
CN110200026A (en) * 2019-06-28 2019-09-06 湖南省烟草公司长沙市公司 A kind of plant and microorganism composite insecticide and preparation method thereof
CN110506762A (en) * 2019-09-16 2019-11-29 覃涛 The preparation method for preventing and treating the medical fluid of curcuma zedoary pest and disease damage
CN110771630A (en) * 2019-10-15 2020-02-11 汤怀信 Insecticide

Similar Documents

Publication Publication Date Title
CN106135315A (en) A kind of natural botanical insecticide
CN104230405A (en) Method for preparing active algae extract foliar fertilizer
CN1111478A (en) Insectiside composed of Chinese herbal medicines and preparing method thereof
CN106221939A (en) A kind of plants essential oil with antibacterial effect and preparation method and application
CN104478568A (en) Novel method for preparing organic fertilizer from crop residual bodies by microbial fermentation technology
CN107518015A (en) A kind of environmental protection type agricultural seed coating agent
CN107805585A (en) A kind of preparation method of Chinese medicine distillers yeast assisted fermentation health white wine
CN101796968B (en) Method for preparing preparation for preventing plant aphids by utilizing tomato stem and leaf extract
CN110128222A (en) A kind of tea seed cake base bio-extract and preparation method thereof
CN105794867A (en) Compound botanical pesticide and preparing method thereof
CN107439897A (en) A kind of plant-based bacteriostat
CN106818946A (en) Vegetable insecticide and preparation method thereof
CN106982824A (en) A kind of flower antistaling agent and preparation method thereof
CN103622134B (en) Be that raw material preparation has anti-oxidant and method that is biocidal property food preservative with molasses
CN102585028A (en) Method for extracting natural polysaccharide humectant from love grass
CN105111003A (en) Liquid organic fertilizer and preparing method thereof
CN102204575A (en) Silktree-albizia-extract-based preparation for controlling tetranychus cinnabarinus, and preparation and application thereof
CN115769825A (en) Preparation method of high-content ginkgolic acid plant source pesticide
CN108935536A (en) A kind of natural drug and preparation method thereof inhibiting wawter bloom
CN105961460B (en) A kind of medicine based on herbs for preventing and treating bradysia odoriphaga
CN107788229A (en) A kind of purposes of plant-based bacteriostat
CN107440965A (en) A kind of deep layer purifies mildy wash
CN107494905A (en) A kind of preparation method of plant-based bacteriostat
CN106748236A (en) A kind of Snakegourd Fruit foliar fertilizer
CN107285818A (en) A kind of tea seed cake extract and preparation method thereof

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20161123

RJ01 Rejection of invention patent application after publication