CN107440965A - A kind of deep layer purifies mildy wash - Google Patents

A kind of deep layer purifies mildy wash Download PDF

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Publication number
CN107440965A
CN107440965A CN201710747432.2A CN201710747432A CN107440965A CN 107440965 A CN107440965 A CN 107440965A CN 201710747432 A CN201710747432 A CN 201710747432A CN 107440965 A CN107440965 A CN 107440965A
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CN
China
Prior art keywords
deep layer
mildy wash
extract
butterflybush flower
radix stellariae
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CN201710747432.2A
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Chinese (zh)
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不公告发明人
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Foshan Sanshui Jiahua Chemical Research Institute (general Partnership)
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Foshan Sanshui Jiahua Chemical Research Institute (general Partnership)
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Priority to CN201710747432.2A priority Critical patent/CN107440965A/en
Publication of CN107440965A publication Critical patent/CN107440965A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/965Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of inanimate origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Cosmetics (AREA)

Abstract

The invention discloses a kind of deep layer to purify mildy wash, and it includes the composition of following mass percent:Fulvic acid 0.4~2.5%, butterflybush flower volatile oil 1~10%, Radix Stellariae extract 0.5~8%, butanediol 2~8%, stearic acid 2~8%, glycerine 2~8%, myristic acid 5~15%, laurate 5~15%, hyaluronic acid 0.01~0.05%, Cocoamidopropyl betaine 5~10%, laruyl alcohol sulfosuccinate disodium 5~10%, sodium benzoate 0.1~0.3%, Phenoxyethanol 0.2~0.6%, deionized water surplus.Long-term use of mildy wash can reduce the deposition of heavy metal in skin, slow down skin heavy metal poisoning symptom, at the same can also be in deep layer cleaning pore dirt, suppress scytitis reaction, there is no tight feeling, and persistently skin can be kept to moisten, allow wash one's face and become a kind of enjoyment yet.

Description

A kind of deep layer purifies mildy wash
Technical field
The present invention relates to cosmetic field, and in particular to a kind of deep layer purifies mildy wash.
Background technology
Mildy wash is also mildy wash, is the cleaning supplies for cleaning facial dirt such as sweat, dust color make-up etc..Compared with making Face is cleaned with soap, stimulation of the mildy wash to skin is smaller, and flushing is also more prone to, also can be clean even if the concavo-convex position of face Only.At present, most of commercially available mildy wash is mainly to clean the dirt on human body face surface, thus its composition mainly with water and Surfactant, and some additional auxiliary materials.But in fact, the human body face rested on not only only has dirt, it is also With substantial amounts of pathogenic microorganism, the heavy metal of air and cosmetics residual, the attractive in appearance of human body face is not only had influence on, and very Inside of human body may be brought into so as to be threatened to health.Only played clearly if used when cleaning human body face If the mildy wash of clean dirt digestion, that does not just reach real cleaning action.Therefore, development is a kind of can both be carried out to skin Deep layer cleaning, the mildy wash that can adsorb the harmful substances such as heavy metal again will be more welcomed by the people.
The content of the invention
Based on this, it is an object of the invention to provide a kind of deep layer to purify mildy wash.
To achieve the above object, the present invention adopts the following technical scheme that:
A kind of mass percent of deep layer purification each composition of mildy wash is:Fulvic acid 0.4~2.5%, butterflybush flower volatile oil 1 ~10%, Radix Stellariae extract 0.5~8%.
Preferably, the mass percent of described deep layer purification each composition of mildy wash is:Fulvic acid 0.8~1.8%, close illiteracy Flowers volatile oil 3.3~8.4%, Radix Stellariae extract 2.3~6.5%.
Optimal, the mass percent of described deep layer purification each composition of mildy wash is:Fulvic acid 1.3%, butterflybush flower are waved Hair oil 4.6%, Radix Stellariae extract 4.6%.
Further, described butterflybush flower volatile oil is prepared as follows:The dry butterflybush flower of natural drying is taken to carry out clear Wash;Crush the butterflybush flower after cleaning and drying;After butterflybush flower crushing is soaked into 4 hours with deionized water, connect immersion water one And after being transferred to the immersion 3 days of 80 DEG C~90 DEG C of hermetically sealed can constant temperature, 90~100 DEG C of heating stirrings for carrying out 3 hours are warming up to, are obtained Extract mixed liquor;Extract mixed liquor is finally evaporated concentration, obtained concentrate is required butterflybush flower volatile oil.
Further, described Radix Stellariae extract is prepared as follows:Radix stellariae dichotomae is put into 60~70 DEG C of water 1~2h is extracted, separates supernatant, Radix Stellariae extract is obtained after concentration.
A kind of deep layer purification mildy wash also includes the composition of following mass percent:Butanediol 2~8%, stearic acid 2~ 8%th, glycerine 2~8%, myristic acid 5~15%, laurate 5~15%, hyaluronic acid 0.01~0.05%, coconut oleoyl amine third Base glycine betaine 5~10%, laruyl alcohol sulfosuccinate disodium 5~10%, sodium benzoate 0.1~0.3%, Phenoxyethanol 0.2 ~0.6%, deionized water surplus.
Several compositions in the present invention are introduced below:
Humic acid material is a kind of natural macromolecular organic matter, including fulvic acid, humic acid or humic acid, humic acid, It is widely present in water body and soil.Humus accounts for half of contained total amount of organic or so in general water body, and what is had is reachable 80%, wherein fulvic acid accounts for 83-90%, and humic acid or humic acid account for 3-4%, and humic acid accounts for 7-13%.Thus fulvic acid is water The main body of humus in body.Fulvic acid surface includes substantial amounts of active group, and fulvic acid is based on aromatic group, containing a large amount of Hydroxyl, carboxyl, carbonyl.These functional structures contribute to fulvic acid to be complexed with heavy metal ion.In addition, fulvic acid surface band There is larger elecrtonegativity, the series reaction between fulvic acid and heavy metal ion can be promoted.
Butterflybush flower is the drying flower or bud of loganiaceae plant butterflybush flower, also known as sheep ear, worm see dead grass;It is mainly distributed on The ground such as Fujian, Guangdong, Guangxi, Yunnan;Property it is sweet, cool, have wind-dispelling, cool blood, profit liver, improving eyesight the effect of.So far, from Isolated a variety of chemical compositions in butterflybush flower, including flavonoids, benzyl carbinol glycoside, triterpene and its saponin(e, monoterpene, iridoid With volatile oil etc..46 peaks are isolated from butterflybush flower volatile oil, wherein 27 compositions is identified, accounts for volatile oil total amount 72.41%, main component is palmitic acid (14.07%), 6,10,14- trimethyl -2- pentadecanones (12.92%), heneicosane (6.15%), heptacosane (3.28%).Wherein, alkane compound content highest, next to that ester, also changes containing some alcohols etc. Compound.Research shows that the alkanes such as eicosane, heneicosane and heptacosane have skin care effect;6,10,14- front threes Base -2- pentadecanones have certain antifungal activity.
Radix stellariae dichotomae is the dry root of pinkwort radix stellariae dichotomae, is slightly cold, sweet, has clearind deficient heat, the function for the treatment of infantile malnutrition wide fever, is used In diseases such as fever due to yin deficiency, steaming bone and consumptive fever, children's infantile malnutrition due to digestive disturbances or intestinalparasites heat.Clinic is commonly applied to treat infantile malnutrition generates heat, prolonged illness heating, deficiency of Yin tide The diseases such as heat, flu high fever.Research in recent years finds that radix stellariae dichotomae not only has clearing heat and cooling blood function, also have anti-inflammatory, treated The effects such as quick property disease, anticancer, expansion blood vessel.Radix stellariae dichotomae is traditional Chinese medicine, has good antibacterial and anti-inflammation functions.In recent years with The further investigation to its active component steroid, alkaloids, cyclic peptide, it is found that Radix Stellariae extract also has good solution Heat, antibacterial, anti-inflammatory etc. act on.
It is the device have the advantages that as follows:Mildy wash of the present invention is mainly by fulvic acid, butterflybush flower volatile oil, radix stellariae dichotomae Extract is formed in specific proportions, and toxin expelling is carried out by fulvic acid, and absorption heavy metal is carried out when cleaning face skin, is removed The dirt of pore depths, remove skin tough stains, deep layer cleaning;Radix Stellariae extract anti-inflammatory, antibacterial effect simultaneously, effectively side Skin microbial balance is helped, suppresses inflammation radical response;Butterflybush flower volatile oil Glycerin, make skin not tight after cleaning, temperature With it is moist.Long-term use of mildy wash can reduce the deposition of heavy metal in skin, slow down skin heavy metal poisoning symptom, simultaneously Dirt that can also be in deep layer cleaning pore, suppresses scytitis reaction, without tight feeling, and persistently skin can be kept to moisten, Allow wash one's face and also become a kind of enjoyment.
Embodiment
Below in conjunction with specific embodiment, the present invention is further elaborated:
The mildy wash embodiment 1~5 of the present invention is formulated, and is shown in Table 1.
Table 1
1st, butterflybush flower volatile oil of the present invention is prepared as follows:
The butterflybush flower for taking natural drying dry is cleaned;Crush the butterflybush flower after cleaning and drying;Spend butterflybush flower is broken After ionized water soaks 4 hours, after even immersion is transferred to the immersion 3 days of 80 DEG C~90 DEG C of hermetically sealed can constant temperature with water in the lump, it is warming up to 90~100 DEG C of heating stirrings for carrying out 3 hours, obtain extract mixed liquor;Extract mixed liquor is finally evaporated concentration, Obtained concentrate is required butterflybush flower volatile oil.
2nd, Radix Stellariae extract of the present invention is prepared as follows:
Radix stellariae dichotomae is put into 1~2h of extraction in 60~70 DEG C of water, supernatant is separated, radix stellariae dichotomae extract solution is obtained after concentration.
Comparative example 1:
Difference with embodiment 3 is only to be free of fulvic acid, and remaining each group material addition, preparation does not change with technique.
Comparative example 2:
Difference with embodiment 3 is only to be free of butterflybush flower volatile oil, and remaining each group material addition, preparation does not occur with technique Change.
Comparative example 3:
Difference with embodiment 3 is only to be free of Radix Stellariae extract, and remaining each group material addition, preparation does not occur with technique Change.
Comparative example 4:
Difference with embodiment 3 is only to be free of 3 kinds of fulvic acid, butterflybush flower volatile oil and Radix Stellariae extract compositions, remaining Each group material adds, and preparation does not change with technique.
Efficacy validation
In order to verify absorption heavy metal effect of mildy wash of the present invention, choose embodiment 1~5 and comparative example 1~4 is tried Use evaluation test.
1st, object is tried out:Trier's health is all right, without lactation or pregnancy period, shows as the poisoning of heavy metal skin Crowd, and show skin inflammation.
2nd, embodiment is as follows:Every group of 25 people are chosen to be tested.Product 22- every night corresponding to experimenter's use Using corresponding trial target between 24 points, each sampling phase is one month, and at the 30th day, experimenter was to adsorbing heavy metal Effect carries out self-appraisal, and self-appraisal is carried out to the cleannes of adsorbed film, before on probation with skinanalysis apparatus detect skin content of beary metal, Skin water content and content of beary metal, skin water content are detected at the 30th day;Whole people complete whole experiment during experiment, And require that everyone is honest and report result of the test, it must not use other any skin-protection products in experimentation.
3rd, test event:Heavy metal poisoning inflammation skin, the cleannes of skin.
4th, evaluation criterion:It is effective to refer to that heavy metal inflammation skin is cured;Effectively refer to that heavy metal inflammation skin improves;It is invalid Refer to that skin condition cannot improve, or even aggravate.
5th, using the clinical evaluation of skin quality, the result of the test such as table 2 below of heavy metal is adsorbed;
Product beta test evaluation test result such as table 3 below.
Table 2
As shown in Table 2, after product of the invention is used 30 days, the test of skin detection instrument substantially subtracts to skin heavy metal Few, embodiment 1-5 product has the absorption heavy metal characteristic of conspicuousness relative to comparative example 1-4, and with the absorption of embodiment 3 Best results;Trying out product of the invention 30 days, the water content of experimenter's skin increases considerably, and illustrates the product of the present invention Energy Glycerin, skin of releiving is without tight.
Table 3
As can be seen from Table 3, product of the present invention can slow down skin heavy metal poisoning symptom, suppress skin inflammation, so as to promote The reparation of inflammation skin is entered;The experimenter for having more than 95% thinks that the mildy wash of the present invention has excellent deep layer cleaning skin Effect, the dirt of pore depths is effectively removed, maintain the health status of skin.
Bacteriostasis efficacy is verified
For trying strain:Salmonella, enterococcus faecalis, staphylococcus aureus, Escherichia coli culture medium and condition of culture:It is general Logical nutrient agar (37 DEG C, 48h cultures, for staphylococcus aureus, enterococcus faecalis, Escherichia coli culture);Sharpe Agar medium (30 DEG C, 3 days are cultivated, for salmonella).
Test method:With reference to National Standard of the People's Republic of China GB15797-2002, " Disposable Sanitary Accessory is defended Appendix C 4 " stripping property resists (suppression) bacterium product bacteriostasis property test method " in raw standard ".
Operating procedure:
(1) test organisms 24h (bacterium) and 5 days (fungi) cultures are washed down with 0.03mol/L PBS, are made 106cfu/mL Bacteria suspension.
(2) each 1g of product made from Example 1-5 and comparative example 1-4 adds above-mentioned bacteria suspension 0.1mL even spreads and mixed Close, after starting timing 20min, add 9mL 0.03mol/L PBS and fully mix, after making appropriate dilution, take wherein 2-3 dilution Degree, takes 1mL to be placed in two parallel plates respectively, adds corresponding culture medium difference Hybrid NC machine tool.Make colony count.Try above Test and be repeated 3 times, take its average, while set blank control.
Calculate:X=(A-B)/A × 100%
In formula:X --- bacteriostasis rate, %
A --- control sample averagely reclaims bacterium colony;
B --- test specimen averagely reclaims bacterium colony.
Bacteriostasis efficacy is evaluated:
Efficacy assessments divide three-level:It is effective, effective and invalid, such as table 4 below.
Table 4
Bacteriostatic test result:
According to above-mentioned test method, 20min bacteriostatic test is carried out, the results are shown in Table 5.
Table 5
Shown by the bacteriostatic test result of table 5, the bacteriostasis rate of product made from embodiment 1-5 apparently higher than comparative example 1-4, Illustrating the product of the present invention has bacteriostasis.
Above example is merely to illustrate embodiment of the present invention, does not have any formal limit to the present invention System;It is any to be engaged in professional and technical personnel, all have the ability using the technology contents having revealed that, some are made to it and changes or repaiies Decorations, turn into the equivalent embodiment of equivalent variations.According to the technology of the present invention essence, simply modification, equivalent variations are carried out to the present invention With modification, belong in the range of technical solution of the present invention.

Claims (6)

1. a kind of deep layer purifies mildy wash, it is characterised in that the mass percent of described deep layer purification each composition of mildy wash is: Fulvic acid 0.4~2.5%, butterflybush flower volatile oil 1~10%, Radix Stellariae extract 0.5~8%.
2. a kind of deep layer purification mildy wash according to claim 1, it is characterised in that described deep layer purification mildy wash is each The mass percent of composition is:Fulvic acid 0.8~1.8%, butterflybush flower volatile oil 3.3~8.4%, Radix Stellariae extract 2.3~ 6.5%.
3. a kind of deep layer purification mildy wash according to claim 2, it is characterised in that described deep layer purification mildy wash is each The mass percent of composition is:Fulvic acid 1.3%, butterflybush flower volatile oil 4.6%, Radix Stellariae extract 4.6%.
A kind of 4. deep layer purification mildy wash according to any one of claims 1 to 3, it is characterised in that described butterflybush flower Volatile oil is prepared as follows:The butterflybush flower for taking natural drying dry is cleaned;Crush the butterflybush flower after cleaning and drying;Will After butterflybush flower crushing soaks 4 hours with deionized water, even immersion is transferred to 80 DEG C~90 DEG C leachings of hermetically sealed can constant temperature with water in the lump Bubble is warming up to 90~100 DEG C of heating stirrings for carrying out 3 hours, obtains extract mixed liquor after 3 days;Finally extract is mixed Liquid is evaporated concentration, and obtained concentrate is required butterflybush flower volatile oil.
A kind of 5. deep layer purification mildy wash according to any one of claims 1 to 3, it is characterised in that described radix stellariae dichotomae Extract is prepared as follows:Radix stellariae dichotomae is put into 1~2h of extraction in 60~70 DEG C of water, separates supernatant, after concentration Radix Stellariae extract.
6. a kind of deep layer purification mildy wash according to any one of Claims 1 to 5, it is characterised in that described deep layer is net Changing mildy wash also includes the composition of following mass percent:Butanediol 2~8%, stearic acid 2~8%, glycerine 2~8%, Pork and beans Cool sour 5~15%, laurate 5~15%, hyaluronic acid 0.01~0.05%, Cocoamidopropyl betaine 5~10%, bay Alcohol sulfosuccinate disodium 5~10%, sodium benzoate 0.1~0.3%, Phenoxyethanol 0.2~0.6%, deionized water surplus.
CN201710747432.2A 2017-08-25 2017-08-25 A kind of deep layer purifies mildy wash Pending CN107440965A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107854341A (en) * 2017-12-11 2018-03-30 广州市汇吉科技企业孵化器有限公司 A kind of nose patch adsorbed film for adsorbing heavy metal
CN111888298A (en) * 2020-08-28 2020-11-06 广州市妆妍生物技术有限公司 Shower gel and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107854341A (en) * 2017-12-11 2018-03-30 广州市汇吉科技企业孵化器有限公司 A kind of nose patch adsorbed film for adsorbing heavy metal
CN111888298A (en) * 2020-08-28 2020-11-06 广州市妆妍生物技术有限公司 Shower gel and preparation method thereof

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