CN109010178B

CN109010178B - Shower gel and production process thereof

Info

Publication number: CN109010178B
Application number: CN201811099045.3A
Authority: CN
Inventors: 钟代
Original assignee: Xiamen Wally Bath Manufacture Co ltd
Current assignee: Xiamen Wally Bath Manufacture Co ltd
Priority date: 2018-09-20
Filing date: 2018-09-20
Publication date: 2021-09-28
Anticipated expiration: 2038-09-20
Also published as: CN109010178A

Abstract

The invention discloses a shower gel and a production process thereof, and relates to the field of bath products, wherein the shower gel comprises the following components in parts by weight: 35-55% by weight of a surfactant, 4-12% by weight of a natural preservative, 2-8% by weight of a disinfectant, 15-20% by weight of a skin care agent and 22-32% by weight of a soothing agent, wherein the surfactant comprises any two of an amino acid surfactant, lecithin, dodecyl ethoxy sulfobetaine and octadecyl amidopropyl amine oxide; the natural antiseptic comprises two of protamine, propolis, pectin and citric acid; the disinfectant comprises any two of oleum folium Artemisiae Argyi, fructus Zanthoxyli extractive solution, Perillae herba and flos Chrysanthemi; the skin caring agent comprises two of Aloe extractive solution, emulsified silicone oil, and glycerol; the soothing agent comprises ginger powder, rice wine and frankincense, and the shower gel is good in decontamination capability, free of stimulation, mild, skin-friendly, capable of preserving moisture and locking water, antibacterial and disinfectant, long in shelf life and suitable for any skin type.

Description

Shower gel and production process thereof

Technical Field

The invention relates to the field of bath products, in particular to shower gel and a production process thereof.

Background

The liquid skin-cleaning product is a cosmetic used for cleaning skin and having a certain skin-care effect, and the liquid skin-cleaning cosmetic mainly comprises products such as shower gel, foam bath agent, hand cleanser, foot-bath liquid medicine and the like. The bath lotion is a liquid body-cleaning skin-care product prepared by taking a surfactant and skin-care components as main raw materials. The main functions of the shower gel are to clean excessive grease, dirt, sweat stain, human secretion and the like adhered to the skin of a human body, and keep the body clean and sanitary. Compared with the traditional bath soap, the bath lotion has the characteristics of convenience in use, easiness in cleaning, hard water resistance, abundant foam, good skin smoothness after use and the like, and particularly, flaky soap stains which are generated in the use process of the bath lotion and are not floated on the water surface like the soap are not generated, so that the production and marketing are continuously increased in recent years, and the bath soap becomes a mainstream product for bath cleaning. Most of the existing bath lotion products on the market only play basic cleaning and fragrance roles, partial moisturizing roles and the like, cannot well play a skin care role, and the components of the bath lotion are not suitable for infants.

In order to solve the problems, the Chinese patent with the granted publication number of CN103655415A discloses a bath cream for infants, which is prepared from the following raw materials in parts by weight: 15-30 parts of deionized water, 10-20 parts of cow milk, 1-4 parts of cocamidopropyl sweet acid base, 1-3 parts of salicylic acid, 2-6 parts of hydroxypropyl methyl cellulose, 3-6 parts of alkenyl sulfonate, 4-6 parts of tetrasodium ethylenediaminetetraacetate, 5-8 parts of cocoglyceride, 3-6 parts of sodium chloride, 6-12 parts of sodium laureth sulfate, 3-6 parts of citric acid, 1-4 parts of cocamidopropyl betaine, 2-5 parts of DMDM hydantoin and 4-9 parts of decyl glucoside, although the shower gel can supplement water, moisturize and moisten skin, the DMDM hydantoin serving as a preservative can create an environment unsuitable for the existence of microorganisms by releasing formaldehyde so as to achieve the preservative effect, the higher the temperature, the larger the release amount is, local irritation reaction is easy to cause when the shower gel is used, the formaldehyde can enter blood when the contact exceeds normal metabolic capacity, the health-care food is harmful to the body, and is especially harmful to people with low immunity, such as children, pregnant women, old people and the like.

Disclosure of Invention

The invention aims to provide shower gel which has the advantages of good decontamination capability, no stimulation, mildness and skin friendliness, moisture retention and water locking, skin moistening, bacteriostasis and disinfection, longer shelf life, blood circulation promotion, muscle and bone soothing, anti-allergy and suitability for any skin.

The technical purpose of the invention is realized by the following technical scheme:

the shower gel comprises the following components in parts by weight: 35-55 wt% of surfactant, 4-12 wt% of natural preservative, 2-8 wt% of disinfectant, 15-20 wt% of skin care agent and 22-32 wt% of soothing agent.

The surfactant comprises any two of amino acid surfactant, lecithin, dodecyl ethoxy sulfobetaine and octadecyl amido propyl amine oxide;

the natural preservative comprises any two of protamine, propolis, pectin and citric acid;

the disinfectant comprises any two of blumea oil, a zanthoxylum piperitum extract, perilla and chrysanthemum;

the skin care agent comprises any two of aloe extract, emulsified silicone oil and glycerin;

the soothing agent comprises ginger powder, rice wine and frankincense.

The surfactant is the main component of the shower gel, and the surfactant endows the product with excellent degreasing power, detergency and abundant foam by utilizing the functions of self adsorption, surface tension reduction, penetration, emulsification, solubilization, dispersion and the like. In the invention, the surfactant comprises any two of amino acid surfactant, lecithin, dodecyl ethoxy sulfobetaine and octadecyl amido propyl amine oxide; preferably, the surfactant is an amino acid surfactant and dodecyl ethoxy sulfobetaine, and the amino acid surfactant and the dodecyl ethoxy sulfobetaine respectively account for 15-20 wt% and 15-30 w% of the total amount of the shower gel; more preferably, the amino acid surface activity is 16-19 wt% and the dodecyl ethoxy sulfobetaine is 17-28 wt%.

The amino acid surfactant, lecithin, dodecyl ethoxy sulfobetaine and octadecyl amidopropyl amine oxide belong to amphoteric surfactants, can give protons and accept protons, and have good washing, dispersing, emulsifying and sterilizing capabilities when used in shower gel. The amino acid surfactant is amino acid (such as glutamic acid, glycine, etc.) salt (sodium salt, potassium salt, triethanolamine salt) of coconut oil (or laurel oil or palm oil) with foaming detergency. The pH value of the weakly acidic amino acid surfactant is close to that of human skin, and the amino acid is a basic substance for forming protein, so the amino acid surfactant is used in the shower gel, and the shower gel is mild and skin-friendly and can be used for sensitive skin safely. Lecithin is a natural amphoteric surfactant which generally has good washing, dispersing, emulsifying and sterilizing effects, and lecithin is a natural antidote which provides sufficient nutrients such as water and oxygen to the skin by adding heme, so that the skin becomes smooth and soft.

The dodecyl ethoxy sulfobetaine has the characteristics of no toxicity, small irritation, easy water solubility, stability to acid and alkali, more foams, strong detergency, excellent thickening property, antistatic property and hard water resistance, has excellent stability under acidic and alkaline conditions, respectively presents positive and negative ions, has good compatibility with an amino acid surfactant, is matched with each other, has strong decontamination capability, is mild and skin-friendly, has small irritation to the skin, is suitable for any skin, and has stable chemical property.

The natural preservative comprises any two of protamine, propolis, pectin and citric acid; preferably, the natural preservative is propolis and citric acid, and the propolis and the citric acid respectively account for 5-10 wt% and 3-7 wt% of the total amount of the shower gel; more preferably, propolis is 3-7 wt% and citric acid is 1-5 wt%. The natural preservative is selected from organism secretion substances or substances with bacteriostatic action existing in organisms and is prepared by artificial extraction or processing, and the preservative is a natural substance, and some of the preservatives are components of food, so that the preservative is harmless to human bodies and has no stimulation to skin.

Protamine is an alkaline protein, exists mainly in the form of nucleoprotein combined with DNA in the cell nucleus of mature sperm of fish (such as salmon, trout, herring and the like), has the advantages of high safety, good antiseptic property, high thermal stability and the like, and can prolong the shelf life of the shower gel; the bath foam has the functions of resisting thrombus, inhibiting blood coagulation and the like, and can promote blood circulation and relieve fatigue to a certain extent. The pectin substance is one of plant cell wall components, is a linear polysaccharide polymer essentially, has good gelling and emulsifying stabilization effects, and can prolong the shelf life of the bath lotion.

Natural citric acid is widely distributed in nature, and exists in fruits such as lemon, orange, pineapple, etc., bones, muscles and blood of animals, and artificially synthesized citric acid is prepared by fermenting sugar-containing substances such as granulated sugar, molasses, starch, grape, etc., and can be divided into anhydrous one and hydrate one. Many fruits and vegetables, especially citrus fruits, contain high levels of citric acid, especially lemon and lime, which contain high levels of citric acid, up to 8% after drying. The citric acid is widely available and is easy to obtain; citric acid is used as solubilizer, buffer, antioxidant, deodorizing agent, gelling agent, toner, etc., and further, citric acid has antibacterial and chelating effects.

The propolis Chinese medicinal material is named as a tawny or black brown viscous substance secreted by the insects of the family Apidae, such as Chinese honeybees and the like, the propolis contains a certain amount of benzoic acid, so the propolis has a certain antiseptic effect, has good gelling and emulsion stabilizing effects, can prolong the shelf life of the bath lotion, has the effects of moistening skin, promoting granulation, diminishing inflammation and relieving pain, can disinfect, inhibit bacteria, prevent mildew and prevent corrosion, solves the defect that antibiotics only act on a single microorganism, has no side effect, can decompose pigments, smooth wrinkles, slow aging and the like, and is frequently used as a bathing article containing the propolis, and has the effects of maintaining beauty and keeping young.

The citric acid and the propolis are matched with each other, so that the stability of the shower gel is maintained, the corrosion resistance is improved, the shelf life of the shower gel is prolonged, the pH of the shower gel can be adjusted mildly and approaches to the pH of a human body, and the shower gel disclosed by the invention is mild and skin-friendly, does not stimulate the skin and is suitable for different skin types; the citric acid and propolis are matched with each other, so that granulation tissues can be protected, the wound healing is facilitated, and the chapped skin is facilitated, and the skin is nourished; the interaction of the citric acid, the propolis and the amino acid surfactant enables the shower gel to have a certain antioxidation effect, can effectively remove wastes such as excessive active oxygen and free radicals generated by bad living habits such as overwork, environmental pollution and smoking and external factors, can inhibit bacteria, prevent mold and corrosion to a certain extent, has no side effect, and can not stimulate or harm the body.

The sterilization disinfectant comprises any two of blumea oil, a zanthoxylum piperitum extract, perilla and chrysanthemum; preferably, the sterilizing disinfectant is folium artemisiae argyi oil and a pericarpium zanthoxyli extracting solution, wherein the folium artemisiae argyi oil and the pericarpium zanthoxyli extracting solution respectively account for 2-5 wt% and 2-5 wt% of the total amount of the shower gel, and more preferably, the folium artemisiae argyi oil accounts for 1-4 wt% and the pericarpium zanthoxyli extracting solution accounts for 1-4 wt% of the total amount of the shower gel.

The oleum Artemisiae Argyi is volatile oil contained in dry or fresh folium Artemisiae Argyi of Compositae, has antiallergic effect, and contains dried mature pericarp of green pepper (pericarpium Zanthoxyli, green pepper, fructus Zanthoxyli, and fructus Zanthoxyli) or fructus Zanthoxyli (pericarpium Zanthoxyli, fructus Zanthoxyli, and radix Campylotropis) of Rutaceae, and can be used for treating eczema and pudendal pruritus. The shower gel and the preparation method are matched with each other, so that the shower gel can sterilize and disinfect, has a certain anti-allergic effect, is suitable for people with allergic constitution, is also suitable for people with different skin types, and is especially suitable for people with low immunity such as children, pregnant women, old people and the like.

The volatile oil, brass, phenolic acid, etc. contained in folium Perillae have antibacterial, antiinflammatory, and antiallergic effects; the wild chrysanthemum has the effects of clearing away heat and toxic materials, dispelling wind, calming the liver, diminishing inflammation and diminishing swelling, and the perilla and the chrysanthemum are added into the formula of the shower gel and matched with each other, so that the shower gel has certain antibacterial, anti-inflammatory and anti-allergic effects, is suitable for any skin, can promote blood circulation, refresh and restore consciousness, and can relieve pressure and relieve spirit to a certain extent.

In the invention, the skin care agent comprises any two of aloe extract, emulsified silicone oil and glycerin; preferably, the skin care agent is aloe extract and emulsified silicone oil, the aloe extract and the emulsified silicone oil respectively account for 5-10 wt% and 5-9 wt% of the total amount of the shower gel, and more preferably, the aloe extract accounts for 6-9 wt% and the emulsified silicone oil accounts for 6-7 wt%.

Aloe, a perennial evergreen plant with large and fleshy leaves, and the aloe extract, is the juice extracted from the leaves of aloe. The aloe contains anthraquinone derivatives, aloe rhubarb, saponin, amino acid and polysaccharide, has the functions of nutrition and moisture retention and sun protection, can form a layer of smooth moisture absorption film on the surface of skin, improves the gorgeous feeling and softness of the shower gel under the condition of not increasing the viscosity, and reduces the water loss through skin by the film forming function; because of being rich in polysaccharide, the health care tea has a relieving effect; contains biological enzyme, has anti-inflammatory and antibacterial effects by slowly hydrolyzing with skin, and can act with collagen in stratum corneum under the action of amino acid to heal wound.

The emulsified silicone oil, also called as silky element, is white viscous liquid, odorless, non-toxic and harmless to human bodies, has certain lubricity, hydrophobicity and low surface tension, is easy to wash when used in shower gel, is stable in chemical property, is non-volatile, is not easy to gel after being placed in the air for a long time, and can prolong the shelf life to a certain extent. The formula of the emulsified silicone oil is loose and not harsh, the emulsified silicone oil serving as an oil phase has good compatibility, various components can be fully dissolved, and the prepared shower gel is not easy to coagulate and gel and is convenient to use.

The soothing agent comprises ginger powder, rice wine and frankincense, and preferably the ginger powder, the rice wine and the frankincense respectively account for 5-12 wt%, 9-16 wt% and 3-9 wt% of the total weight of the shower gel; further preferably, 7-10 wt% of ginger powder, 10-15 wt% of rice wine and 5-7 wt% of frankincense.

Olibanum, a traditional Chinese medicine name, is resin exuded from bark of Boswellia carterii of Burseraceae and plants of the same genus, and can be used for treating rheumatalgia, muscular spasm, traumatic injury, carbuncle swelling, sore and ulcer. The rice wine is brewed by glutinous rice fermentation, contains a great amount of vitamins and amino acids, and trace alcohol not only can not cause people to be drunk, but also can accelerate blood circulation and metabolism, so that the internal circulation of a human body slowed down along with temperature is activated, the blood circulation of the human body is greatly enhanced, and fatigue can be relieved. The ginger powder is rich in gingerol, can disperse wind cold, can promote blood circulation and relieve fatigue while preventing and treating cold, combines the dual effects of the rice wine and the ginger powder, promotes metabolism and absorption due to the interaction of the ginger powder and the rice wine, and can promote the function of frankincense, promote blood circulation, relieve muscles and bones, relieve pain and relieve fatigue due to the addition of a certain temperature.

The invention aims to provide a production process of shower gel, which has the advantages of simple process, convenience in operation and easiness in implementation.

a production process of shower gel comprises the following steps:

the method comprises the following steps: taking emulsified silicone oil as an oil phase, heating and melting the emulsified silicone oil at 70-80 ℃ to form liquid, and keeping the temperature for later use;

step two: dissolving an amino acid surfactant, dodecyl ethoxy sulfobetaine, blumea oil, a pericarpium zanthoxyli extracting solution, ginger powder, rice wine, frankincense and deionized water in a weight ratio of 1: 4-6 in deionized water, heating to 60-80 ℃ to obtain a mixed solution, adding the standby oil phase obtained in the step one into the mixed solution, uniformly stirring to obtain a homogeneous stable emulsion, and cooling;

step three: adding the aloe extract, the propolis and the citric acid at 35-45 ℃, uniformly stirring, cooling to room temperature, and standing to obtain the bath foam.

Preferably, the preparation of the zanthoxylum piperitum extract is as follows:

crushing a Sichuan pepper raw material, sieving the ground Sichuan pepper raw material with 30-50 meshes, uniformly mixing Sichuan pepper powder and soybean oil according to a weight ratio of 1: 4-6, stirring and soaking at 85-95 ℃ for 2-3 h, then stirring and soaking at 110-130 ℃ for 50-70 min, cooling to room temperature, and filtering out material residues to obtain a Sichuan pepper oil extract.

Preferably, the aloe extract is prepared as follows:

peeling aloe, taking the middle bone and meat, cutting into pieces, heating the cut aloe bone and meat in water bath at 50-60 ℃, and collecting steam condensate to obtain aloe extract.

The bath cream is prepared and produced by adopting an emulsification process, the production process is simple, the operation is convenient, the preparation conditions are loose, and the energy consumption can be effectively reduced to a certain extent; the raw materials selected by the invention are renewable resources, have good biodegradability, do not harm the health of people, and do not cause pollution to the environment.

The preparation method of the zanthoxylum bungeanum maxim extract comprises the steps of crushing, dipping and filtering, has simple extraction process, convenient operation and easy implementation, belongs to a plant extraction method by dipping and extracting with soybean oil, is healthy and safe, and does not harm human bodies or environment.

The aloe extract is prepared by cutting aloe into blocks and collecting condensate during water bath heating, and has the advantages of simple preparation process, convenient operation, easy implementation, easy material acquisition, no addition of other substances in the preparation process, simple and effective property of keeping moisture and locking water of aloe.

In summary, compared with the prior art, the beneficial effects of the invention are as follows: the bath lotion has the advantages of good decontamination capability, no irritation, mild skin friendliness, moisture retention, skin moistening, antibacterial and disinfection, long shelf life, blood circulation promotion, muscle and bone soothing, anti-sensitivity and suitability for any skin type.

Detailed Description

The present invention will be described in further detail with reference to examples.

Example 1

The preparation method of the zanthoxylum piperitum extract comprises the following steps:

the method comprises the steps of treating a Sichuan pepper raw material, removing impurities such as prickly ash seeds and fruit stalks, crushing the treated Sichuan pepper raw material, sieving with a 30-mesh sieve, uniformly mixing Sichuan pepper powder and soybean oil according to a weight ratio of 1:4, stirring and soaking at 85 ℃ for 2h, stirring and soaking at 110 ℃ for 50min, cooling to room temperature, and filtering out Sichuan pepper residue to obtain a Sichuan pepper oil extract.

The aloe extract is prepared as follows:

picking fresh folium Aloe, washing with water to remove silt on the surface, draining, removing thorns and upper and lower epidermis on both sides of the folium Aloe, keeping pulp part, cutting into pieces, heating the cut Aloe bone and meat in water bath at 50 deg.C, and collecting steam condensate to obtain Aloe extractive solution.

The production process of the shower gel comprises the following steps:

the method comprises the following steps: taking emulsified silicone oil as an oil phase, heating and melting the emulsified silicone oil at 70 ℃ to form liquid, and keeping the temperature for later use;

step two: weighing 15g of amino acid surfactant, 15g of dodecyl ethoxy sulfobetaine, 3g of blumea oil, 4g of pericarpium zanthoxyli extracting solution, 7g of ginger powder, 15g of rice wine and 9g of frankincense, dissolving the weighed amino acid surfactant, dodecyl ethoxy sulfobetaine, blumea oil, pericarpium zanthoxyli extracting solution, ginger powder, rice wine, frankincense and deionized water in a weight ratio of 1:4 in deionized water, heating to 60 ℃ to obtain a mixed solution, adding the standby oil phase obtained in the step one into the mixed solution, stirring uniformly to obtain a homogeneous stable emulsion, and cooling;

step three: adding 19g of Aloe extractive solution, 7g of propolis and 6g of citric acid at 35 deg.C, stirring, cooling to room temperature, and standing to obtain bath lotion.

Example 2

the method comprises the steps of treating a pericarpium zanthoxyli raw material, removing impurities such as meshes and fruit stalks of the pericarpium zanthoxyli, crushing the treated pericarpium zanthoxyli raw material, sieving the crushed pericarpium zanthoxyli raw material with a 35-mesh sieve, uniformly mixing the pericarpium zanthoxyli powder and the soybean oil according to the weight ratio of 1:4.5, stirring and soaking the mixture at 90 ℃ for 2.2 hours, stirring and soaking the mixture at 120 ℃ for 55 minutes, cooling to room temperature, filtering out pericarpium zanthoxyli material residues, and obtaining the pericarpium zanthoxyli oil extract.

The aloe extract is prepared as follows:

picking fresh folium Aloe, washing with water to remove silt on the surface, draining, removing thorns and upper and lower epidermis on both sides of the folium Aloe, keeping pulp part, cutting into pieces, heating the cut Aloe bone and meat in water bath at 52 deg.C, and collecting steam condensate to obtain Aloe extractive solution.

The production process of the shower gel comprises the following steps:

the method comprises the following steps: taking emulsified silicone oil as an oil phase, heating and melting the emulsified silicone oil at 72 ℃ to form liquid, and keeping the temperature for later use;

step two: weighing 16g of amino acid surfactant, 17g of dodecyl ethoxy sulfobetaine, 5g of blumea oil, 5g of pericarpium zanthoxyli extract, 5g of ginger powder, 16g of rice wine and 7g of frankincense, dissolving the weighed amino acid surfactant, dodecyl ethoxy sulfobetaine, blumea oil, pericarpium zanthoxyli extract, ginger powder, rice wine, frankincense and deionized water in a weight ratio of 1:4.5 in deionized water, heating to 65 ℃ to obtain a mixed solution, adding the standby oil phase obtained in the step one into the mixed solution, stirring uniformly to obtain a homogeneous stable emulsion, and cooling;

step three: adding 12g of Aloe extractive solution, 10g of propolis and 7g of citric acid at 40 deg.C, stirring, cooling to room temperature, and standing to obtain bath lotion.

Example 3

the method comprises the steps of treating a Sichuan pepper raw material, removing impurities such as meshes and fruit stalks of the Sichuan pepper, crushing the treated Sichuan pepper raw material, sieving with a 40-mesh sieve, uniformly mixing Sichuan pepper powder and soybean oil according to a weight ratio of 1:5, stirring and soaking at 95 ℃ for 2.4h, stirring and soaking at 115 ℃ for 60min, cooling to room temperature, and filtering out Sichuan pepper residue to obtain a Sichuan pepper oil extract.

The aloe extract is prepared as follows:

picking fresh folium Aloe, washing with water to remove silt on the surface, draining, removing thorns and upper and lower epidermis on both sides of the folium Aloe, keeping pulp part, cutting into pieces, heating the cut Aloe bone and meat in water bath at 54 deg.C, and collecting steam condensate to obtain Aloe extractive solution.

The production process of the shower gel comprises the following steps:

the method comprises the following steps: taking emulsified silicone oil as an oil phase, heating and melting the emulsified silicone oil at 74 ℃ to form liquid, and keeping the temperature for later use;

step two: weighing 17g of amino acid surfactant, 28g of dodecyl ethoxy sulfobetaine, 4g of blumea oil, 1g of pericarpium zanthoxyli extracting solution, 10g of ginger powder, 10g of rice wine and 6g of frankincense, dissolving the weighed amino acid surfactant, dodecyl ethoxy sulfobetaine, blumea oil, pericarpium zanthoxyli extracting solution, ginger powder, rice wine, frankincense and deionized water in a weight ratio of 1:4.9 in deionized water, heating to 68 ℃ to obtain a mixed solution, adding the standby oil phase obtained in the step one into the mixed solution, stirring uniformly to obtain a homogeneous stable emulsion, and cooling;

step three: adding aloe extract 16g, propolis 5g and citric acid 3g at 45 deg.C, stirring, cooling to room temperature, and standing to obtain bath lotion.

Example 4

the method comprises the steps of treating a pericarpium zanthoxyli raw material, removing impurities such as meshes and fruit stalks of the pericarpium zanthoxyli, crushing the treated pericarpium zanthoxyli raw material, sieving the crushed pericarpium zanthoxyli raw material with a mesh of 45, uniformly mixing the pericarpium zanthoxyli powder and the soybean oil according to the weight ratio of 1:5.5, stirring and soaking the mixture at 87 ℃ for 2.6 hours, stirring and soaking the mixture at 130 ℃ for 65 minutes, cooling to room temperature, filtering out pericarpium zanthoxyli material residues, and obtaining the pericarpium zanthoxyli oil extract.

The aloe extract is prepared as follows:

picking fresh folium Aloe, washing with water to remove silt on the surface, draining, removing thorns and upper and lower epidermis on both sides of the folium Aloe, keeping pulp part, cutting into pieces, heating the cut Aloe bone and meat in water bath at 56 deg.C, and collecting steam condensate to obtain Aloe extractive solution.

The production process of the shower gel comprises the following steps:

the method comprises the following steps: taking emulsified silicone oil as an oil phase, heating and melting the emulsified silicone oil at 75 ℃ to form liquid, and keeping the temperature for later use;

step two: weighing 18g of amino acid surfactant, 22g of dodecyl ethoxy sulfobetaine, 3g of blumea oil, 3g of pericarpium zanthoxyli extract, 12g of ginger powder, 9g of rice wine and 8g of frankincense, dissolving the weighed amino acid surfactant, dodecyl ethoxy sulfobetaine, blumea oil, pericarpium zanthoxyli extract, ginger powder, rice wine, frankincense and deionized water in a weight ratio of 1:5 in deionized water, heating to 70 ℃ to obtain a mixed solution, adding the standby oil phase obtained in the step one into the mixed solution, stirring uniformly to obtain a homogeneous stable emulsion, and cooling;

step three: adding 17g Aloe extractive solution, 4g propolis and 4g citric acid at 37 deg.C, stirring, cooling to room temperature, and standing to obtain bath lotion.

Example 5

the method comprises the steps of treating a Sichuan pepper raw material, removing impurities such as meshes and fruit stalks of the Sichuan pepper, crushing the treated Sichuan pepper raw material, sieving with a 50-mesh sieve, uniformly mixing Sichuan pepper powder and soybean oil according to a weight ratio of 1:6, stirring and soaking at 89 ℃ for 2.8h, stirring and soaking at 125 ℃ for 70min, cooling to room temperature, and filtering out Sichuan pepper residue to obtain a Sichuan pepper oil extract.

The aloe extract is prepared as follows:

picking fresh folium Aloe, washing with water to remove silt on the surface, draining, removing thorns and upper and lower epidermis on both sides of the folium Aloe, keeping pulp part, cutting into pieces, heating the cut Aloe bone and meat in water bath at 58 deg.C, and collecting steam condensate to obtain Aloe extractive solution.

The production process of the shower gel comprises the following steps:

the method comprises the following steps: taking emulsified silicone oil as an oil phase, heating and melting the emulsified silicone oil at 76 ℃ to form liquid, and keeping the temperature for later use;

step two: weighing 19g of amino acid surfactant, 29g of dodecyl ethoxy sulfobetaine, 2g of blumea oil, 2g of pericarpium zanthoxyli extract, 8g of ginger powder, 12g of rice wine and 3g of frankincense, dissolving the weighed amino acid surfactant, dodecyl ethoxy sulfobetaine, blumea oil, pericarpium zanthoxyli extract, ginger powder, rice wine, frankincense and deionized water in a weight ratio of 1:5.1 in deionized water, heating to 71 ℃ to obtain a mixed solution, adding the standby oil phase obtained in the step one into the mixed solution, stirring uniformly to obtain a homogeneous stable emulsion, and cooling;

step three: adding aloe extract 14g, propolis 6g and citric acid 5g at 43 deg.C, stirring, cooling to room temperature, and standing to obtain bath lotion.

Example 6

the method comprises the steps of treating a Sichuan pepper raw material, removing impurities such as meshes and fruit stalks of the Sichuan pepper, crushing the treated Sichuan pepper raw material, sieving the raw material with a 42-mesh sieve, uniformly mixing Sichuan pepper powder and soybean oil according to a weight ratio of 1:4.8, stirring and soaking at 93 ℃ for 3 hours, stirring and soaking at 119 ℃ for 59 minutes, cooling to room temperature, and filtering out Sichuan pepper residue to obtain a Sichuan pepper oil extract.

The aloe extract is prepared as follows:

picking fresh folium Aloe, washing with water to remove silt on the surface, draining, removing thorns and upper and lower epidermis on both sides of the folium Aloe, keeping pulp part, cutting into pieces, heating the cut Aloe bone and meat in water bath at 60 deg.C, and collecting steam condensate to obtain Aloe extractive solution.

The production process of the shower gel comprises the following steps:

the method comprises the following steps: taking emulsified silicone oil as an oil phase, heating and melting the emulsified silicone oil at 78 ℃ to form liquid, and keeping the temperature for later use;

step two: weighing 20g of amino acid surfactant, 30g of dodecyl ethoxy sulfobetaine, 1g of blumea oil, 2g of zanthoxylum piperitum extract, 9g of ginger powder, 13g of rice wine and 5g of frankincense, dissolving the weighed amino acid surfactant, dodecyl ethoxy sulfobetaine, blumea oil, zanthoxylum piperitum extract, ginger powder, rice wine, frankincense and deionized water in a weight ratio of 1:5.5 in deionized water, heating to 75 ℃ to obtain a mixed solution, adding the standby oil phase obtained in the step one into the mixed solution, stirring uniformly to obtain a homogeneous stable emulsion, and cooling;

step three: adding 15g of Aloe extractive solution, 3g of propolis and 2g of citric acid at 39 deg.C, stirring, cooling to room temperature, and standing to obtain bath lotion.

Example 7

the method comprises the steps of treating a pericarpium zanthoxyli raw material, removing impurities such as meshes and fruit stalks of the pericarpium zanthoxyli, crushing the treated pericarpium zanthoxyli raw material, sieving the crushed pericarpium zanthoxyli raw material with a mesh of 38, uniformly mixing the pericarpium zanthoxyli powder and the soybean oil according to the weight ratio of 1:5.2, stirring and soaking the mixture at 91 ℃ for 2.5 hours, stirring and soaking the mixture at 121 ℃ for 61 minutes, cooling to room temperature, filtering out pericarpium zanthoxyli material residues, and obtaining the pericarpium zanthoxyli oil extract.

The aloe extract is prepared as follows:

picking fresh folium Aloe, washing with water to remove silt on the surface, draining, removing thorns and upper and lower epidermis on both sides of the folium Aloe, keeping pulp part, cutting into pieces, heating the cut Aloe bone and meat in water bath at 55 deg.C, and collecting steam condensate to obtain Aloe extractive solution.

The production process of the shower gel comprises the following steps:

the method comprises the following steps: taking emulsified silicone oil as an oil phase, heating and melting the emulsified silicone oil at 80 ℃ to form liquid, and keeping the temperature for later use;

step two: weighing 18g of amino acid surfactant, 23g of dodecyl ethoxy sulfobetaine, 5g of blumea oil, 3g of pericarpium zanthoxyli extract, 11g of ginger powder, 14g of rice wine and 6g of frankincense, dissolving the weighed amino acid surfactant, dodecyl ethoxy sulfobetaine, blumea oil, pericarpium zanthoxyli extract, ginger powder, rice wine, frankincense and deionized water in a weight ratio of 1:6 in deionized water, heating to 80 ℃ to obtain a mixed solution, adding the standby oil phase obtained in the step one into the mixed solution, stirring uniformly to obtain a homogeneous stable emulsion, and cooling;

step three: adding 10g of Aloe extractive solution, 9g of propolis and 1g of citric acid at 41 deg.C, stirring, cooling to room temperature, and standing to obtain bath lotion.

Reference group to example 1

Comparative example 1

Comparative example 1 differs from example 1 in that no propolis or citric acid was added to comparative example 1, and the rest was in agreement with example 1.

Comparative example 2

Comparative example 2 is different from example 1 in that the oil of mugwort leaf and the extract of zanthoxylum piperitum were not added in comparative example 2, and the rest was the same as example 1.

Comparative example 3

Comparative example 3 is different from example 1 in that ginger powder, rice wine and frankincense were not added to comparative example 3, and the rest was identical to example 1.

And (4) testing results:

appearance evaluation and basic physicochemical detection were performed on the shower gel samples prepared in examples 1 to 7 and comparative examples 1 to 3 according to the GB/T34857 to 2017 standard and the GB/T29680 to 2013 standard, and the results are shown in tables 1 and 2.

TABLE 1 sensory evaluation of samples

TABLE 2 basic physicochemical indices

As can be seen from the observation of the tables 1 and 2, the shower gel prepared by the method is uniform in color, stable in property and long in shelf life, particularly, after natural preservatives, namely propolis and citric acid are added, the shelf life of the shower gel can be prolonged to a certain extent on the premise of not damaging other basic properties of the shower gel, and the pH value of the shower gel is 6-7, is close to that of human skin, is non-irritant to human bodies, is mild and skin-friendly, is suitable for any skin type, and is suitable for any people.

Antibacterial disinfection and anti-sensitivity detection are carried out on the shower gel samples prepared in examples 1-7 and comparative examples 1-3 according to GB/T3485-2017 standards, and the detection results are shown in Table 3.

Bacteriostasis test

1) Strain:

escherichia coli ATCC24752

Staphylococcus aureus Staphylocouus aureus ATCC 6538

Moniliaalbican ATCC 10231 of Candida albicans

2) Method of producing a composite material

Recovering the strains of the strains, culturing to logarithmic phase, diluting to 105-106 CFU/ml with a culture medium, and uniformly coating the diluted bacterial liquid on a solid culture medium by using a coater.

3) Test of bacteriostatic Effect

The test is carried out on the arm, sampling is carried out before cleaning the arm according to the requirement of measuring the total number of bacteria, then the arm is cleaned by the shower gel according to the common bathing method, the cleaning duration is 40-60 s, and finally the cleaning is carried out under flowing water. After washing, sampling is carried out, the collected sample is diluted and mixed with a liquefied agar culture medium, and after the sample is cultured for 24 hours at 37 ℃, the total number of bacteria in the sample is calculated according to the number of colonies on the culture medium.

TABLE 3 statistical table of bacteriostatic test results

As can be seen from the observation of the table 3, the shower gel provided by the invention has excellent bacteriostatic and bactericidal functions, and particularly, after the blumea oil, the zanthoxylum piperitum extract, the ginger, the rice wine and the frankincense are added into the shower gel, various components in the shower gel interact and are matched with each other, so that the bactericidal effect is better.

Selecting 10 volunteers with common skin and 10 volunteers with sensitive skin, respectively taking the shower gel samples in the examples 1-7 and the comparative examples 1-3, cleaning the skin on the hands, respectively trying once in the morning and at the evening every day, and continuously trying for three days. The feedback structure is shown in table 4.

TABLE 4 sensitive test feedback Table

Sample (I)	General skin texture	Sensitive skin
			Example 1	Moist and not tight	No adverse reaction
Example 2	Moist and not tight	No adverse reaction
			Example 3	Moist and not tight	No adverse reaction
Example 4	Moist and not tight	No adverse reaction
			Example 5	Moist and not tight	No adverse reaction
Example 6	Moist and not tight	No adverse reaction
			Example 7	Moist and not tight	Without adverse reactionShould be taken
Comparative example 1	Not tight	No adverse reaction
			Comparative example 2	Not tight	Slight itching
Comparative example 3	Not tight	No adverse reaction

Observing the table 4, no matter the skin is a general volunteer or a sensitive skin volunteer, the shower gel has no adverse reaction when being used, which shows that the shower gel can sterilize, disinfect and resist allergy, and is suitable for any skin, and particularly, after the anti-allergic agent is added, all the components are matched with each other, so that the shower gel has an anti-allergic effect, can sterilize and disinfect, is suitable for people with allergic constitution, is also suitable for people with different skin types, and particularly suitable for people with low immunity such as children, pregnant women, old people, and the like, and can not cause irritation injury to the skin and relieve itching to a certain degree when being used.

Claims

1. A shower gel is characterized in that: the shower gel is prepared from the following components: 16-19 wt% of amino acid surfactant, 17-28 wt% of dodecyl ethoxy sulfobetaine, 3-7 wt% of propolis, 1-5 wt% of citric acid, 1-4 wt% of argy wormwood leaf oil, 1-4 wt% of pericarpium zanthoxyli extract, 6-9 wt% of aloe extract, 6-7 wt% of emulsified silicone oil, 7-10 wt% of ginger powder, 10-15 wt% of rice wine and 5-7 wt% of frankincense.

2. A method of producing a body wash according to claim 1, wherein: the production method comprises the following steps:

step three: adding the aloe extract, the propolis and the citric acid at 35-45 ℃, uniformly stirring, continuously cooling, cooling to room temperature, and standing to obtain the bath foam.

3. A method of producing a body wash according to claim 2, wherein: the preparation method of the zanthoxylum bungeanum extract comprises the following steps:

4. A method of producing a body wash according to claim 2, wherein: the aloe extract is prepared as follows: