CN108531319A - A kind of antibacterial cleaning products and preparation method thereof - Google Patents
A kind of antibacterial cleaning products and preparation method thereof Download PDFInfo
- Publication number
- CN108531319A CN108531319A CN201710122900.7A CN201710122900A CN108531319A CN 108531319 A CN108531319 A CN 108531319A CN 201710122900 A CN201710122900 A CN 201710122900A CN 108531319 A CN108531319 A CN 108531319A
- Authority
- CN
- China
- Prior art keywords
- cleaning products
- antibacterial cleaning
- antibacterial
- mass percent
- agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/042—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on anionic surface-active compounds and soap
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D10/00—Compositions of detergents, not provided for by one single preceding group
- C11D10/04—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap
- C11D10/045—Compositions of detergents, not provided for by one single preceding group based on mixtures of surface-active non-soap compounds and soap based on non-ionic surface-active compounds and soap
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/06—Inorganic compounds
- C11D9/08—Water-soluble compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/30—Organic compounds, e.g. vitamins containing nitrogen
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/04—Carboxylic acids or salts thereof
- C11D1/10—Amino carboxylic acids; Imino carboxylic acids; Fatty acid condensates thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/14—Sulfonic acids or sulfuric acid esters; Salts thereof derived from aliphatic hydrocarbons or mono-alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/16—Sulfonic acids or sulfuric acid esters; Salts thereof derived from divalent or polyvalent alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/02—Anionic compounds
- C11D1/12—Sulfonic acids or sulfuric acid esters; Salts thereof
- C11D1/29—Sulfates of polyoxyalkylene ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/75—Amino oxides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/88—Ampholytes; Electroneutral compounds
- C11D1/90—Betaines
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
Abstract
The invention discloses a kind of antibacterial cleaning products and preparation method thereof, the Cannador of Optimum is added in the antibacterial cleaning products, especially hemp leaf extract, bacteriostatic activity is high, can effectively inhibit various pathogens, clean effect is good, it is safe and non-toxic, there is not the problems such as coarse dry to no skin irritation, and using rear skin, it can be not only used for the washing of clothing etc., it can also be used to the cleaning of skin.The manufacture craft of above-mentioned antibacterial cleaning products provided by the invention is simple and safe, and production cost is relatively low, is easy to industrialize.
Description
Technical field
The present invention relates to field of hygiene products, and in particular to a kind of antibacterial cleaning products and preparation method thereof, especially one
Antibacterial cleansing soap of kind and preparation method thereof.
Background technology
There is a large amount of pathogenic bacteria and fungi, common bacteria and fungal infections to happen occasionally in the environment that we live,
Skin is the significant points of prevailing conditions pathogenic bacteria parasitism, the use of have the cleaning products of fungistatic effect is to prevent to infect the good of generation
One of good measure.The antibacterial product sold in the market includes perfumed soap, hand cleanser etc..Perfumed soap is greatly to utilize trichlorine card
The chemical substances such as class, triclosan are antibacterial, and safety needs to be probed into, and certain chemical substance is used for a long time and inhibits bacterial growth
Microorganism can be caused to generate drug resistance.Some manufacturers are to make perfume as primary raw material using sodium soap and other surfaces activating agent
Soap, add quality improver and appearance modifying agents, the manufactured product after machine-shaping, due to the pH of these perfumed soap products
Value is higher, and skin can not be resistant to for a long time, can only be used for cleaning clothing.And the natural bacteriostatic activity contained in some plant extracts
Substance not will produce adverse reaction and side effect to human body, not damage the health of user.Many researchers are by plant in recent years
The natural active matter of middle extraction be added in cleaning products realize it is antibacterial, as patent CN201310577658.4 discloses a kind of U.S.
Hold antibacterial toilet soap, wherein antibacterial raw material components include：Bighead atractylodes rhizome decocting liquid, root of Dahurain angelica ultrasound alcohol extract, lucid asparagus decocting liquid, tea tree essence
Oil, antipathogenic composition is more, and antibacterial toilet soap preparation process is more complex, and total preparation cost is higher.
Related document report both at home and abroad, Cannador has bacteriostatic activity, but yet there are no and apply it to daily chemical products
In report.
Invention content
In consideration of it, the present invention provides a kind of antibacterial cleaning products, material composition includes：Solvent, thickener, surface are lived
Property agent, Cannador；The bacteriostatic activity of the antibacterial cleaning products is high, can effectively inhibit various pathogens, and clean effect is good, and
It is safe and non-toxic, to no skin irritation, there is not the problems such as coarse dry using rear skin.
Preferably, the extract part of the Cannador, hemp plant includes：One in stalk core, flower, leaf and root
The combination of kind or two or more arbitrary proportions；
Preferably, the Cannador can be the extract or extract that different plant parts are extracted to formation respectively
Combination, such as hemp stalk core extract, hemp flower extract, hemp leaf extract, hemp root extract, or, hemp stalk core carries
Take the combination of object, hemp flower extract, hemp leaf extract and two or more arbitrary proportions in hemp root extract；
Preferably, the Cannador can by different plant parts or combinations thereof while be extracted, obtained extract
Or the combination of extract, i.e. the combination of the extract or extract of the combination of one or more of stalk core, flower, leaf, root.
As the extract of the extract of cannabis and leaf, hemp stalk core and flower, the extract of leaf, hemp stalk core and flower, hemp stalk core and
The extract of leaf, the extract etc. of cannabis and root；
Plant extraction process conventional in the prior art can be used to prepare, such as solvent extraction method, water in the Cannador
Steam distillation method, sublimed method, supercritical fluid extraction, film extraction and separation technology etc.；Preferably, solvent extraction method can be used,
Extraction solvent can be：Low mass molecule alcohol（Such as methanol, ethyl alcohol, butanol or propyl alcohol）, acetic acid esters（Such as methyl acetate or acetic acid second
Ester）, ketone（Such as acetone）, ether（Such as methyl ether or ether）, low-boiling aliphatic hydrocarbon either aromatic hydrocarbon or chlorinated hydrocabon etc.；Extraction
Technique can be to be heated to reflux, may also be combined with other extraction separate modes such as extract, distill, crystallizing, one kind in chromatographic isolation
Or a variety of combinations carries out further purification ＆ isolation to extract.
Preferably, the Cannador in the antibacterial cleaning products is hemp leaf extract；
Preferably, the mass percent of Cannador is 0.1-30% in the antibacterial cleaning products；Preferably 0.1-20%, more
Preferably 0.1-10%；
Preferably, the mass percent of ropiness increasing agent is 0.01-1%, more preferably 0.05-0.8% in the antibacterial cleaning products；
Preferably, the mass percent of surfactant is 40-60%, more preferably 45-55% in the antibacterial cleaning products；
Preferably, the mass percent of solvent is 20-40%, more preferably 25-35% in the antibacterial cleaning products；
Preferably, the solvent is water, more preferably deionized water；
Preferably, the thickener is selected from：It is one or more in carragheen, gellan gum；
Preferably, the surfactant is selected from：Lauryl sodium sulfate, cetearyl glucoside, dodecanamide propyl
Glycine betaine, C12-20 alkyl glucosides, Sodium dodecylpolyoxyethylene sulfate, glucoside APG, empgen BB,
Alcohol ether sulfosuccinic acid monoesters disodium, alkyl amine-oxides, sodium N-lauroyl sarcosinate, one kind in alpha-alkene sulfonate or more
Kind.
Preferably, the raw material components of the antibacterial cleaning products further include：Chelating agent is assigned in ester agent, moisturizer, deodorant tune
It is one or more；
In a preferred embodiment of the invention, the raw material components of the antibacterial cleaning products include：Solvent, thickener, table
Face activating agent, chelating agent, assigns ester agent, moisturizer, deodorant tune at Cannador.
Preferably, the chelating agent is selected from：It is one or more in EDTA-2Na, EDTA-4Na；
Preferably, the tax ester agent is selected from：Jojoba oil, wheat-germ oil, Sweet Almond Oil, olive oil, methoxy cinnamic acid
It is one or more in ethylhexyl, hemp-seed oil, Avocado Oil, castor oil, sunflower oil, soybean oil；
Preferably, the moisturizer is selected from：1,3 butylene glycol, lactic acid, sorbierite, glycerin polyether -26, polyethylene glycol -401, β -
Glucan, sodium lactate, ethoxy urea element, Sodium Hyaluronate, 1,2- propylene glycol, glycerine, fucosan, trehalose, beta glucan,
It is one or more in allantoin, hydrolytic collagen；
Deodorant tune of the present invention can be conventional daily chemical essence in the prior art, and those skilled in the art can be according to manufacture
Technique and production and sales need to select suitable essence, to recall special odor type and effect, it is possible to use a variety of essence combinations, this
Invention is not specifically limited this；
In another preferred embodiment of the invention, the raw material components and its mass percent point of above-mentioned antibacterial cleaning products
It is not：Solvent 20-40%, thickener 0.01-1%, surfactant 40-60%, Cannador 0.1-30%, chelating agent 0.05-
1%, ester agent 0.1-5%, moisturizer 1-10%, deodorant tune 0.01-0.5% are assigned.
Preferably, mass percent of the above-mentioned chelating agent in above-mentioned antibacterial cleaning products is 0.05-1%, preferably
0.1-0.8%；
Preferably, mass percent of the above-mentioned tax ester agent in antibacterial cleaning products is 0.1-5%, preferably 0.5-2%；
Preferably, mass percent of the above-mentioned moisturizer in antibacterial cleaning products is 1-10%, preferably 2-10%；
Preferably, mass percent of the above-mentioned deodorant tune in antibacterial cleaning products is 0.01-0.5%, preferably 0.02-0.3%.
Those skilled in the art can also be added according to actual needs into above-mentioned antibacterial cleaning products：Colorant, preservative,
In the additives such as antioxidant, emulsifier, foaming agent, curing agent, solubilizer, nourishing additive agent, pH adjusting agent, natural flowers and plants
One or more, the antibacterial cleaning products of gained are also included in protection scope of the present invention.
Preferably, the antibacterial cleaning products can be liquid form such as liquid soap, solid form such as perfumed soap, facial soap
Deng preferably solid form, especially antibacterial toilet soap, facial soap.
Another aspect of the present invention also provides the preparation method of above-mentioned antibacterial cleaning products, and the method includes following step
Suddenly：
（1）Solvent, chelating agent, thickener are mixed, heating；
（2）Surfactant is added；
（3）It is added and assigns ester agent；
（4）After cooling obtained by abovementioned steps, Cannador, moisturizer, deodorant tune is added and stirs and evenly mixs；
Optionally,（5）By step（4）Obtained system drying.
Preferably, step（1）Described in be heated to temperature be 60-80 DEG C；
Preferably, step（4）Described in be cooled to temperature be 30-50 DEG C；
In one embodiment of the invention, the step（5）Including：By step（4）After obtained system pours into mold, lid
It is good, heat preservation；It is demoulded after solidification, natural drying is got product.
The present invention also provides a kind of application of above-mentioned antibacterial cleaning products in preparing cosmetics, bath article.
The present invention also provides a kind of application of above-mentioned antibacterial cleaning products in the cleaning of skin and clothing is antibacterial.
Preferably, above application is that skin cleaning is antibacterial.
The Cannador of Optimum, especially marihuana is added in antibacterial cleaning products provided by the invention to extract
Object, bacteriostatic activity is high, can effectively inhibit various pathogens, clean effect is good, and safe and non-toxic, to no skin irritation, and makes
There is not the problems such as coarse dry with rear skin, can be not only used for the washing of clothing etc., it can also be used to the cleaning of skin.The present invention
The manufacture craft of the above-mentioned antibacterial cleaning products provided is simple and safe, and production cost is relatively low, is easy to industrialize.
Specific implementation mode
The technical scheme in the embodiments of the invention will be clearly and completely described below, it is clear that described implementation
Example is only a part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiments of the present invention, the common skill in this field
The every other embodiment that art personnel are obtained without creative efforts belongs to the model that the present invention protects
It encloses.
The preparation of 1 Cannador of embodiment
Technique：
1, raw material hemp stalk core, cannabis, marihuana and/or cannabis root are cleaned and is air-dried；
2, the raw material after above-mentioned air-dry are crushed to 10-40 mesh；
3, it by gained powder, is extracted 1-3 times with the ethyl alcohol cold soaking of 4-8 times of amount, 30%-60%, it is 0.5-2 hours each；
4, merge extracting solution, decolourize through 0.1-1wt% activated carbon adsorptions；
5, under 70 DEG C of temperature conditions, it is concentrated under reduced pressure into relative density 1.01-1.03；
Up to Cannador medicinal extract, such as hemp stalk core extract, hemp flower extract, hemp leaf extract, cannabis root extraction
The combination of object or in which two kinds, three kinds, four kinds extracts.
Cannador used in following embodiments can be made for 1 method of embodiment, or public in the prior art
Other extracting methods opened are made.
The preparation of 2 product of the present invention of embodiment
Technique：
1, by A phase cold water mix it is uniform after be heated to 70 DEG C, B is added in A phases, is stirred evenly.
2 and then addition C is mixed uniformly.
3, D phases are added after 40 DEG C of cooling to stir evenly to get soap lye
4, it dips a small amount of olive oil with brush and applies die inside, after mixing soap lye is then poured into mold, with plastic film mould
Tool covers, and 35 DEG C of incubators place 24-48h；After its solidification after air-dry demoulding, be then placed within normal temperature environment ventilation allow its from
Right dry 4 weeks to obtain the final product.
Wherein the ingredient of A, B, C, D phase and quality proportioning are as shown in table 1.
The preparation of 3 product of the present invention of embodiment
Technique：
1, by A phase cold water mix it is uniform after be heated to 60 DEG C, B is added in A phases, is stirred evenly.
2 and then addition C is mixed uniformly.
3, D phases are added after 30 DEG C of cooling to stir evenly to get soap lye
4, it dips a small amount of olive oil with brush and applies die inside, after mixing soap lye is then poured into mold, with plastic film mould
Tool covers, and 35 DEG C of incubators place 24-48h；After its solidification after air-dry demoulding, be then placed within normal temperature environment ventilation allow its from
Right dry 4 weeks to obtain the final product.
Wherein the ingredient of A, B, C, D phase and quality proportioning are as shown in table 2.
The preparation of 4 product of the present invention of embodiment
Technique：
1, by A phase cold water mix it is uniform after be heated to 80 DEG C, B is added in A phases, is stirred evenly.
2 and then addition C is mixed uniformly.
3, D phases are added after 50 DEG C of cooling to stir evenly to get soap lye
Wherein the ingredient of A, B, C, D phase and quality proportioning are as shown in table 3.
The preparation of 5 product of the present invention of embodiment
Technique：
1, by A phase cold water mix it is uniform after be heated to 70 DEG C, B is added in A phases, is stirred evenly.
2, D phases are added after 40 DEG C of cooling to stir evenly to get soap lye
3, it dips a small amount of olive oil with brush and applies die inside, after mixing soap lye is then poured into mold, with plastic film mould
Tool covers, and 35 DEG C of incubators place 24-48h；After its solidification after air-dry demoulding, be then placed within normal temperature environment ventilation allow its from
Right dry 4 weeks to obtain the final product.
Wherein the ingredient of A, B, D phase and quality proportioning are as shown in table 4.
The preparation of 6 product of the present invention of embodiment
Technique：
1, by A phase cold water mix it is uniform after be heated to 70 DEG C, B is added in A phases, is stirred evenly.
2, D phases are added after 40 DEG C of cooling to stir evenly to get soap lye.
Wherein the ingredient of A, B, D phase and quality proportioning are as shown in table 5.
The preparation of 7 product of the present invention of embodiment
Technique：
1, by A phase cold water mix it is uniform after be heated to 70 DEG C, B is added in A phases, is stirred evenly.
2, D phases are added after 40 DEG C of cooling to stir evenly to get soap lye.
3, it dips a small amount of olive oil with brush and applies die inside, after mixing soap lye is then poured into mold, use plastic film
Mold is covered, 35 DEG C of incubators place 24-48h；Demoulding is air-dried after its solidification, normal temperature environment ventilation is then placed within and allows
It spontaneously dries 4 weeks to obtain the final product.
Wherein the ingredient of A, B, D phase and quality proportioning are as shown in table 6.
The preparation of 8 product of the present invention of embodiment
Technique：
1, by A phase cold water mix it is uniform after be heated to 70 DEG C, B is added in A phases, is stirred evenly.
2 and then addition C is mixed uniformly.
3, D phases are added after 40 DEG C of cooling to stir evenly to get soap lye.
Wherein the ingredient of A, B, C, D phase and quality proportioning are as shown in table 7.
9 cleansing soap bacteriostatic test of embodiment
One, experiment material
1, bacterial strain：Staphylococcus aureus, Escherichia coli, Pseudomonas aeruginosa, Candida albicans；
2, test specimen：Cleaning products prepared by embodiment 2-8.
Two, experimental method
1, GB15979-2002 is pressed in experiment《Disposable Sanitary Accessory sanitary standard》" stripping property is anti-for appendix C 4（Suppression）Bacterium produces
Product bacteriostasis property test method " carries out.
2, with sample 1：1 solution acts on 2min to test organisms, and experiment is repeated 3 times under the conditions of 20 ± 1 DEG C, is averaged.
Three, evaluation criterion
Bacteriostasis rate >=50%-90%, product have bacteriostasis；Bacteriostasis rate>90%, product has stronger bacteriostasis.
Four, experimental result
Experimental result is as shown in table 8.By result in table 8 it is found that various cleansing soaps provided by the present invention are to Staphylococcus aureus
Bacterium, Escherichia coli, Pseudomonas aeruginosa, Candida albicans all have stronger inhibiting effect.
The bacteriostatic experiment result of 8 cleansing soap of table
10 cleansing soap sterilization test of embodiment
One, experiment material
1, bacterial strain：Staphylococcus aureus, Escherichia coli, Pseudomonas aeruginosa, Candida albicans；
2, test specimen：Cleansing soap prepared by embodiment 2-8.
Two, experimental method
1, QB/T2738 is pressed in experiment《The evaluation method of daily chemical products antibacterial bacteriostatic effect》In 7.2 antimicrobial form daily chemical products sterilization
Validity check method（Suspension quantitative method）It carries out.
2, with sample 1：1（v/v）Solution acts on 2min to test organisms, and experiment is repeated 3 times under the conditions of 20 ± 1 DEG C, makes even
Mean value.
Three, effect assessment
Sterilizing rate >=90% of product shows that product has stronger antibacterial action, reaches A1 grades of levels.
Four, experimental result
Experimental result is as shown in table 9.
As shown in Table 9, various cleansing soaps provided by the present invention to staphylococcus aureus, Escherichia coli, Pseudomonas aeruginosa,
Candida albicans all has stronger bactericidal effect.
11 cleansing soap skin irritation test of embodiment
One, experimental method
According to the Ministry of Public Health《Disinfection technology standard》2002 editions, toxicological experiment is carried out to sample prepared by 2-8 of the embodiment of the present invention,
An intact skin irritant test including cavy and multiple intact skin irritation test.
1, an intact skin irritant test
(1) before the test for 24 hours, the hair of guinea pig back backbone both sides is removed with depilatory agent, skin must not be damaged.Unhairing range,
Left and right each about 3cm × 3cm.
(2) next day is by tested material（Cleansing soap a concentration of 1：5 water diluents）0.5g directly drip in area be 2.5cm ×
On the side unhairing intact skin of 2.5cm, or drop on an equal amount of 2 layers of -4 layers of gauze and apply in side skin of unhairing
Then surface is covered with one layer of non-stimulated plastic foil or oilpaper, then with non-stimulated immobilization with adhesive tape.Other side skin of unhairing is as empty
White control (or solvent control).The application time is 4h.After the test, tested with warm water or nonirritant solvent removing residual
Object.
(3) after removing tested material 1h, for 24 hours with 48h observation local skin reaction, and by table 10 carry out stimulate the reaction
Scoring.
2, multiple intact skin irritant test
（1）Before the test for 24 hours, the hair of guinea pig back backbone both sides is removed with depilatory agent, skin must not be damaged.Unhairing range,
Left and right each about 3cm × 3cm.
（2）Next day is by tested material（Cleansing soap a concentration of 1：5 water diluents）0.5g is coated on the skin of side, and the other side applies molten
As a contrast, the 4h after smearing is cleaned with water or non-stimulated suitable solvent for agent, removes residue.It smears daily once, continuously
Smear 14d.Observation for 24 hours by table 10 as a result, score after each smear.It is seen for the ease of the smearing and result of tested material
It examines, answers cropping when necessary.The same trial zone of processing method of check plot.
Two, evaluation regulation
1, a Skin Irritation Test
In each observing time point, scored with oedema formational situation the erythema of animal according to table 10, and press respectively
Time point is added the scoring of 3 animals divided by number of animals, the skin wound repair integral mean value for obtaining different time points (pierce
Swash index).Wherein highest skin irritation index is taken, rank of the tested material to animal skin stimulus intensity is evaluated by table 11.
2, multiple Skin Irritation Test
Daily every animal average integral is calculated according to the following formula（Stimulus index）, and skin irritatin intensity is judged with table 11.
Three, evaluation result
According to above-mentioned experimental method, for given the test agent in skin irritation test, the integral of assessment result is the sections 0-0.5, table
Bright cleansing soap of the present invention is suitably applied personal cleanliness and article cleaning without skin irritation.
12 cleansing soap detergency of embodiment detects
One, experiment material
Test soiled cotton：Carbon black greasy dirt cloth, albumen soiled cotton, sebum soiled cotton；
Given the test agent：Cleansing soap prepared by embodiment 2-8.
Two, experimental method
Test basis GB/T13174《Dress material detergent detergency and the measurement for recycling scourability》And QB/T1224《Dress material
Wash agent by liquid》Relevant regulations carry out.
Experimental condition：Standard liquid detergent and given the test agent solution concentration are all 0.2%, i.e. 2g cleansing soaps grinds are dissolved in 1L
Dissolving is entirely sample solution in hard water, and experiment is repeated 3 times.
The decontamination ratio of three kinds of soiled cottons test is all higher than 1 and meets QB/T1224《Dress material washes agent by liquid》Regulation.
Three, experimental result
Test result shows that three kinds of soiled cotton detergencies of cleansing soap pair of the present invention are better than standard liquid detergent.
The dry and astringent degree evaluation of pachylosis of 13 cleansing soap of embodiment
One, experiment material
Given the test agent：Cleansing soap prepared by embodiment 2-8.
Two, experimental method
Experiment is divided into 7 groups, 10 personnel of every group of random selection（Male to female ratio is 1：1）Cleansing soap washs obtained by embodiment 2-8
An equal amount of towel 3min is rinsed 1 minute, and wash hands are dried, evaluation.
5 are denoted as with the dry and astringent degree of pachylosis, with 0-5 points of system evaluations, score value is higher to show that degree of drying is higher.
Three, experimental result
According to above-mentioned experimental method, for given the test agent in the dry and astringent degree evaluation experiment of pachylosis, the integral of assessment result is basic
It is 0, is partly 1, show that cleansing soap of the present invention will not cause skin the problems such as coarse dry and astringent, there are moisture-keeping functions.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
Within god and principle, made by any modification, equivalent replacement etc., should all be included in the protection scope of the present invention.
Claims (12)
1. a kind of antibacterial cleaning products, the antibacterial cleaning products material composition include：It is solvent, thickener, surfactant, big
Nettle extract；The extract part of the Cannador, hemp plant includes：One kind in stalk core, flower, leaf and root or two
The combination of kind any of the above ratio.
2. antibacterial cleaning products as described in claim 1, which is characterized in that hemp in the antibacterial cleaning products material composition
The mass percent of extract is 0.1-30%, and the mass percent of thickener is 0.01-1%, the quality percentage of surfactant
Than being 20-40% for the mass percent of 40-60%, solvent.
3. antibacterial cleaning products as claimed in claim 2, which is characterized in that hemp in the antibacterial cleaning products material composition
The mass percent of extract is 0.1-20%, and the mass percent of the thickener is 0.05-0.8%, the surfactant
Mass percent be 45-55%, the mass percent of the solvent is 25-35%.
4. the antibacterial cleaning products as described in claim 1-3 any one, which is characterized in that the solvent is deionization
Water；The thickener is one or more in carragheen, gellan gum；The surfactant is dodecyl sulphate
Sodium, cetearyl glucoside, lauroylamidopropyl betaine, C12-20 alkyl glucosides, dodecyl polyoxyethylene ether sulphur
Hydrochlorate, glucoside APG, empgen BB, alcohol ether sulfosuccinic acid monoesters disodium, alkyl amine-oxides, lauroyl flesh
It is one or more in propylhomoserin sodium, alpha-alkene sulfonate.
5. antibacterial cleaning products as described in claim 1, which is characterized in that the material composition of the antibacterial cleaning products also wraps
It includes：It is one or more in chelating agent, the agent of tax ester, moisturizer, deodorant tune.
6. antibacterial cleaning products as claimed in claim 5, which is characterized in that the chelating agent is selected from：EDTA-2Na、
It is one or more in EDTA-4Na；The tax ester agent is selected from：Jojoba oil, wheat-germ oil, Sweet Almond Oil, olive oil,
It is one or more in ethylhexyl methoxy cinnamate, hemp-seed oil, Avocado Oil, castor oil, sunflower oil, soybean oil；Institute
Moisturizer is stated to be selected from：1,3 butylene glycol, lactic acid, sorbierite, glycerin polyether -26, polyethylene glycol -401, beta glucan, sodium lactate,
Ethoxy urea element, Sodium Hyaluronate, 1,2- propylene glycol, glycerine, fucosan, trehalose, beta glucan, allantoin, hydrolysis glue
It is one or more in original；The deodorant tune is selected from：Essence.
7. antibacterial cleaning products as claimed in claim 6, which is characterized in that the chelating agent antibacterial cleaning products raw material at
Mass percent in point is 0.05-1%, preferably 0.1-0.8%；The quality hundred that ester agent is assigned in antibacterial cleaning products
Score is 0.1-5%, preferably 0.5-2%；Mass percent of the moisturizer in antibacterial cleaning products is 1-10%, preferably
For 2-10%；Mass percent of the deodorant tune in antibacterial cleaning products is 0.01-0.5%, preferably 0.02-0.3%.
8. antibacterial cleaning products as claimed in claim 5, which is characterized in that the material composition packet of the antibacterial cleaning products
It includes：Solvent, surfactant, Cannador, chelating agent, assigns ester agent, moisturizer, deodorant tune at thickener；The antibacterial cleaning
The material composition and its mass percent of product be respectively：Solvent 20-40%, thickener 0.01-1%, surfactant 40-60%,
Cannador 0.1-30%, chelating agent 0.05-1%, ester agent 0.1-5%, moisturizer 1-10%, deodorant tune 0.01-0.5% are assigned.
9. antibacterial cleaning products as described in claim 1, which is characterized in that the antibacterial cleaning products are liquid or solid.
10. a kind of preparation method of the antibacterial cleaning products of claim 1-9 any one of them, the method includes following step
Suddenly：
（1）Solvent, chelating agent, thickener are mixed, heating；
（2）Surfactant is added；
（3）It is added and assigns ester agent；
（4）After cooling obtained by abovementioned steps, Cannador, moisturizer, deodorant tune is added and stirs and evenly mixs；
Optionally,（5）By step（4）Obtained system drying.
11. the preparation method of antibacterial cleaning products according to any one of claims 10, the step（1）In be heated to temperature 60-80
℃；The step（4）In be cooled to 30-50 DEG C of temperature.
12. a kind of application of antibacterial cleaning products of claim 1-9 any one of them in the cleaning of skin and clothing is antibacterial.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710122900.7A CN108531319A (en) | 2017-03-03 | 2017-03-03 | A kind of antibacterial cleaning products and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710122900.7A CN108531319A (en) | 2017-03-03 | 2017-03-03 | A kind of antibacterial cleaning products and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108531319A true CN108531319A (en) | 2018-09-14 |
Family
ID=63489270
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710122900.7A Pending CN108531319A (en) | 2017-03-03 | 2017-03-03 | A kind of antibacterial cleaning products and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN108531319A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111187682A (en) * | 2018-12-05 | 2020-05-22 | 张红 | Laundry detergent with antibacterial and bacteriostatic effects of natural plants and preparation method thereof |
| CN113999737A (en) * | 2021-11-29 | 2022-02-01 | 云南人本生物科技有限公司 | Plant enzyme detergent and preparation method thereof |
| CN115491265A (en) * | 2022-08-24 | 2022-12-20 | 纳爱斯浙江科技有限公司 | Hand-protecting washing powder |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103589537A (en) * | 2013-11-19 | 2014-02-19 | 淮阴工学院 | Beautifying and antibacterial toilet soap |
| CN105838522A (en) * | 2016-04-29 | 2016-08-10 | 贾志军 | Safe and environment-friendly detergent |
| CN106265364A (en) * | 2016-09-30 | 2017-01-04 | 汉义生物科技（北京）有限公司 | A kind of compositions containing Fructus Cannabis extract and the application in cleaning supplies thereof |
-
2017
- 2017-03-03 CN CN201710122900.7A patent/CN108531319A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103589537A (en) * | 2013-11-19 | 2014-02-19 | 淮阴工学院 | Beautifying and antibacterial toilet soap |
| CN105838522A (en) * | 2016-04-29 | 2016-08-10 | 贾志军 | Safe and environment-friendly detergent |
| CN106265364A (en) * | 2016-09-30 | 2017-01-04 | 汉义生物科技（北京）有限公司 | A kind of compositions containing Fructus Cannabis extract and the application in cleaning supplies thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111187682A (en) * | 2018-12-05 | 2020-05-22 | 张红 | Laundry detergent with antibacterial and bacteriostatic effects of natural plants and preparation method thereof |
| CN113999737A (en) * | 2021-11-29 | 2022-02-01 | 云南人本生物科技有限公司 | Plant enzyme detergent and preparation method thereof |
| CN115491265A (en) * | 2022-08-24 | 2022-12-20 | 纳爱斯浙江科技有限公司 | Hand-protecting washing powder |
| CN115491265B (en) * | 2022-08-24 | 2024-04-02 | 纳爱斯浙江科技有限公司 | Hand-protecting washing powder |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| KR101011191B1 (en) | A shampoo composite and making method thereof | |
| CN108203631A (en) | A kind of antibacterial cleaning products and preparation method thereof | |
| KR101592242B1 (en) | Multi-functional Cleansing Tissue containing vegetable collagen for removing makeup and skin care and preparation method thereof | |
| CN108186385A (en) | A kind of hair scalp cleaning compositions | |
| CN103830151A (en) | Application of blumea balsamifera oil in daily chemical product | |
| CN105779165A (en) | Washing composition as well as preparation method and application of washing composition | |
| KR102039638B1 (en) | Method for preparing extracts of Chamecyparis obutsa and a composition for life goods comprising the using the same | |
| CN106038422A (en) | Washing composition and preparation method and application thereof | |
| CN106727059A (en) | The formula and preparation technology of the mildy wash that a kind of suitable Dry is used | |
| CN108531319A (en) | A kind of antibacterial cleaning products and preparation method thereof | |
| CN103655432A (en) | Biological antiphlogistic and antibacterial moderate cleansing oil | |
| CN102961272B (en) | Salt mixed hair shampoo and preparation method thereof | |
| KR102226774B1 (en) | Detergent comprising the extract of astragalus membranaceus, polydonati rhizoma and pine leaf, and the method of manufacturing thereof | |
| CN110613632B (en) | Pet washing and caring composition rich in hyaluronic acid or salt thereof and preparation method thereof | |
| KR102252604B1 (en) | Natural shampoo-bar comprising coconut-extracted surfactant and manufacturing method thereof | |
| CN108553341A (en) | A kind of composition of suppression acne sterilization | |
| CN109010178B (en) | Shower gel and production process thereof | |
| CN103756813A (en) | Aesthetic health care perfumed soap and preparation method thereof | |
| CN102994278A (en) | Bee glue perfumed soap and making method thereof | |
| CN108703897A (en) | The purposes of agalloch eaglewood flower essential oil and its handmade soap of preparation | |
| CN109303742A (en) | A kind of antibacterial conditioning liquid and preparation method thereof | |
| JP2004323424A (en) | Moisture-keeping plant extract, and external preparation, cosmetic, bath agent and detergent all containing the extract | |
| KR102348162B1 (en) | Composition of anti bacterial containing Zophobas morio oil | |
| CN108300622A (en) | A kind of antibacterial cleaning products and preparation method thereof | |
| CN108324586A (en) | A kind of antibacterial anti-inflammatory composition and its application |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180914 |