CN104116681A - Hairdressing bath agent and preparation method thereof - Google Patents

Hairdressing bath agent and preparation method thereof Download PDF

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Publication number
CN104116681A
CN104116681A CN201410376357.XA CN201410376357A CN104116681A CN 104116681 A CN104116681 A CN 104116681A CN 201410376357 A CN201410376357 A CN 201410376357A CN 104116681 A CN104116681 A CN 104116681A
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extract
hair washing
washing bath
bath shampoo
radix
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CN201410376357.XA
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CN104116681B (en
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陈锐
舒士君
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LIUZHOU NUOXIN MEIDA SCIENCE & TECHNOLOGY Co Ltd
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LIUZHOU NUOXIN MEIDA SCIENCE & TECHNOLOGY Co Ltd
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Abstract

The invention discloses a hairdressing bath agent. The hairdressing bath agent is prepared by compounding plant traditional Chinese medicine components with effects of clearing damp, clearing heat and relieving itching such as wormwood extract, cortex dictamni extract, scutellaria baicalensis and cactus extract with mild surfactants. The hairdressing bath agent is safe, small in irritant and toxic and side effects, safe and reliable to use and easy and convenient to prepare and is particularly suitable for the skin allergy crowd and infants, and skin allergy and inflammation are difficultly caused. The anaphylactic reaction of diaper rash and eczema of baby skin caused by sweat and urine can be eliminated, and the hairdressing bath agent contributes to relieving pain and itch symptoms caused by mosquito bite and skin allergy.

Description

A kind of hair washing bath shampoo and preparation method thereof
Technical field
The present invention relates to a kind of hair washing bath shampoo, be specifically related to a kind of hair washing bath shampoo of nontoxic, non-stimulated and easy flushing.
Background technology
The safety of articles for children is the problem that each head of a family is concerned about while selecting article for child the most always.For child's cleaning supplies, nontoxic, non-stimulated and easy flushing is the first-selection of most of families.Hair washing for child shower product on market is much still used fatty alcohol polyoxyethylene ether sulfate, alkanolamide, betanin and amine oxide etc. to have larger irritating surfactant to hair and skin now, in addition as containing carcinogen dioxanes in fatty alcohol polyoxyethylene ether sulfate, therefore allow for a long time child use the hair washing shower product of these preparation of raw material, can become its healthy large hidden danger of harm.
Surfactant zests such as fatty alcohol polyoxyethylene ether sulfate, alkanolamide, betanin and amine oxide that most hair washing for child shower products are used are large and defat is too strong, easily injured skin.And these surfactants the inside is containing poisonous and harmful substance, in use may sees through skin and enter and in child's body, cause health grievous injury.
The function of existing hair washing for child shower product is less, just has cleaning action.
Cause reason: the materials safety of use is not high and for the common skin problem of child, do not carry out product design.
Summary of the invention
The object of the invention is to overcome the weak point that prior art exists and a kind of hair washing bath shampoo of nontoxic, non-stimulated and easy flushing is provided, the present invention also provides the preparation method of described hair washing bath shampoo.
For achieving the above object, the technical scheme of taking: a kind of hair washing bath shampoo, described hair washing bath shampoo comprises the component of following percentage by weight: Chinese medicine extract: 1-10%, cod-liver oil: 0.1-3%, sodium isethionate: 10-30%, lanoline: 0.1-1%, glycerol: 20-50%, antiseptic: appropriate, surplus is water;
Described Chinese medicine extract comprises Folium Artemisiae Argyi extract, Cortex Dictamni extract, Flos Chrysanthemi Indici extract, Radix Scutellariae extract and Radix et Caulis Opuntiae Dillenii extract.
In hair washing bath shampoo of the present invention, the consumption 1-10% of Chinese medicine extract is preferred amount ranges, and its effect is best; In described hair washing bath shampoo, the consumption of Chinese medicine extract is lower than 1% time, and its effect can obviously reduce; In described hair washing bath shampoo, the consumption of Chinese medicine extract higher than 10% time, can increase cost greatly.
Folium Artemisiae Argyi of the present invention is perennial herb or slightly becomes suffruticose plant.All herbal medicine has the effects such as damp eliminating, cold expelling, antiinflammatory, antiallergic.
Cortex Dictamni of the present invention is the root bark of Rutaceae herbaceos perennial shaggy-fruited dittany.There is antipyretic and itching-stopping, the effect of the removing toxic substances of dispeling the wind.
Flos Chrysanthemi Indici of the present invention is Compositae herbaceos perennial.There is subduing swelling and detoxicating, dispelling wind and heat pathogens, antiviral effect.
Radix Scutellariae of the present invention is the root of Radix Scutellariae, is a kind of medical herbs, can heat clearing and damp drying, antibacterial and detoxicating.
Radix et Caulis Opuntiae Dillenii of the present invention is Cactaeous plants, has the effect of relaxing muscles and tendons and activating QI and blood in the collateral, dissipating blood stasis for subsidence of swelling, mosquito bite and healing of wound.
Sodium isethionate of the present invention, CAS NO.1562-00-1, is nontoxic non-stimulated surfactant, can send out and skin for cleaning head.
Cod-liver oil of the present invention is the fat extracting from the livers such as shark, morrhua, contains abundant nutritional labeling and can nourish hair and skin care.
Lanoline of the present invention is by smegma natural materials out, is good moistness material, can allow hair and skin keep minute water and repair because of the impaired skin histology of hydropenia.
Glycerol of the present invention, formal name used at school glycerol, has the effect of moisturizing and increase-volume, increases system stability.
As the preferred implementation of hair washing bath shampoo of the present invention, described hair washing bath shampoo comprises the component of following percentage by weight: Chinese medicine extract: 8-10%, cod-liver oil: 2-3%, sodium isethionate: 25-30%, lanoline: 0.8-1%, glycerol: 40-50%, surplus is water.
As the preferred implementation of hair washing bath shampoo of the present invention, described hair washing bath shampoo comprises the component of following percentage by weight: Chinese medicine extract: 10%, and cod-liver oil: 3%, sodium isethionate: 30%, lanoline: 1%, glycerol: 50%, surplus is water.
As the preferred implementation of hair washing bath shampoo of the present invention, described hair washing bath shampoo also comprises antiseptic.Described antiseptic plays antisepsis in hair washing bath shampoo of the present invention, described hair washing bath shampoo is deposited more of a specified duration, and the kind of described antiseptic and consumption can close kind and the consumption that cosmetics hygienic practice (2007) requires by selector.
As the preferred implementation of hair washing bath shampoo of the present invention, in described Chinese medicine extract, Folium Artemisiae Argyi extract, Cortex Dictamni extract, Flos Chrysanthemi Indici extract, Radix Scutellariae extract and Radix et Caulis Opuntiae Dillenii extract's weight ratio is Folium Artemisiae Argyi extract: Cortex Dictamni extract: Flos Chrysanthemi Indici extract: Radix Scutellariae extract: Radix et Caulis Opuntiae Dillenii extract=1:2:2:1:2.Above-mentioned damp eliminating, heat clearing away, itching-relieving efficacies composition: Folium Artemisiae Argyi extract, Cortex Dictamni extract, Flos Chrysanthemi Indici extract, Radix et Caulis Opuntiae Dillenii extract's percentage by weight is: Folium Artemisiae Argyi extract 12.5%, Cortex Dictamni extract 25%, Flos Chrysanthemi Indici extract 25%, Radix Scutellariae extract 12.5%, Radix et Caulis Opuntiae Dillenii extract 25%.As long as these damp eliminatings, heat clearing away, itching-relieving efficacies composition account for hair washing bath shampoo total composition more than 1%, just can meet Folium Artemisiae Argyi extract at percentage by weight >=0.125% of hair washing bath shampoo total composition, Cortex Dictamni extract is at percentage by weight >=0.25% of hair washing bath shampoo total composition, and Flos Chrysanthemi Indici extract is at percentage by weight >=0.25% of hair washing bath shampoo total composition; Radix Scutellariae extract is at percentage by weight >=0.125% of hair washing bath shampoo total composition; Radix et Caulis Opuntiae Dillenii extract, at percentage by weight >=0.25% of hair washing bath shampoo total composition, to guarantee the consumption of described Chinese medicine ingredients in described hair washing bath shampoo, guarantees its effect.
As the preferred implementation of hair washing bath shampoo of the present invention, described Folium Artemisiae Argyi extract obtains by dehydrated alcohol extraction; Described Cortex Dictamni extract obtains by dehydrated alcohol extraction; Described Flos Chrysanthemi Indici extract obtains by dehydrated alcohol extraction; Described Radix Scutellariae extract obtains by dehydrated alcohol extraction; Described Radix et Caulis Opuntiae Dillenii extract obtains by dehydrated alcohol extraction.
As the preferred implementation of hair washing bath shampoo of the present invention, described Folium Artemisiae Argyi, by after dehydrated alcohol extraction, is concentrated into Folium Artemisiae Argyi extract and described Folium Artemisiae Argyi identical weight; Described Cortex Dictamni, by after dehydrated alcohol extraction, is concentrated into Cortex Dictamni extract and described Cortex Dictamni identical weight; Described Flos Chrysanthemi Indici, by after dehydrated alcohol extraction, is concentrated into Flos Chrysanthemi Indici extract and described Flos Chrysanthemi Indici identical weight; Described Radix Scutellariae, by after dehydrated alcohol extraction, is concentrated into Radix Scutellariae extract and described Radix Scutellariae identical weight; Described Radix et Caulis Opuntiae Dillenii, by after dehydrated alcohol extraction, is concentrated into Radix et Caulis Opuntiae Dillenii extract and described Radix et Caulis Opuntiae Dillenii identical weight.
The present invention also provides the preparation method of hair washing bath shampoo described above, said method comprising the steps of:
(1) in agitator, add water and sodium isethionate, heat while stirring, homogenizing is to fully dissolving;
(2) temperature is down to 50 ℃ when following, adds successively Chinese medicine extract, cod-liver oil, lanoline, glycerol.
Beneficial effect of the present invention is: the present invention uses the surfactant of these damp eliminatings of Folium Artemisiae Argyi extract, Cortex Dictamni extract, Radix Scutellariae extract and Radix et Caulis Opuntiae Dillenii extract, heat clearing away, the antipruritic composite gentleness of botanical herbs composition to make hair washing bath shampoo, described hair washing bath shampoo is safer, zest and toxic and side effects are less, be difficult for causing skin allergy, inflammation, safe and reliable and simple for production, be specially adapted to skin sensitivity crowd and infant.Can help to eliminate baby's skin because antiperspirant or urine soak the anaphylaxis that causes diaper rash and eczema, also contribute to alleviate the sufferings symptom that mosquito bite and skin allergy bring simultaneously.
The specific embodiment
For the object, technical solutions and advantages of the present invention are better described, below in conjunction with specific embodiment, the invention will be further described.
Embodiment 1
A kind of embodiment of hair washing bath shampoo of the present invention, described hair washing bath shampoo comprises the component of following percentage by weight: Chinese medicine extract: 1%, cod-liver oil: 0.1%, sodium isethionate: 10%, lanoline: 0.1%, glycerol: 20%, antiseptic: appropriate, surplus is water;
Described Chinese medicine extract comprises Folium Artemisiae Argyi extract, Cortex Dictamni extract, Flos Chrysanthemi Indici extract, Radix Scutellariae extract and Radix et Caulis Opuntiae Dillenii extract, and in described Chinese medicine extract, Folium Artemisiae Argyi extract, Cortex Dictamni extract, Flos Chrysanthemi Indici extract, Radix Scutellariae extract and Radix et Caulis Opuntiae Dillenii extract's weight ratio is Folium Artemisiae Argyi extract: Cortex Dictamni extract: Flos Chrysanthemi Indici extract: Radix Scutellariae extract: Radix et Caulis Opuntiae Dillenii extract=1:2:2:1:2.
Kind and consumption that the kind of described antiseptic and consumption require for meeting cosmetics health standard (2007).
The preparation method of hair washing bath shampoo of the present invention, said method comprising the steps of:
(1) in agitator, add water and sodium isethionate, heat while stirring, homogenizing is to fully dissolving;
(2) temperature is down to 50 ℃ when following, adds successively Chinese medicine extract, cod-liver oil, lanoline, glycerol, antiseptic.
Embodiment 2
A kind of embodiment of hair washing bath shampoo of the present invention, described hair washing bath shampoo comprises the component of following percentage by weight: Chinese medicine extract: 4%, cod-liver oil: 1%, sodium isethionate: 15%, lanoline: 0.2%, glycerol: 30%, antiseptic: appropriate, surplus is water; Other qualificationss and preparation process are with embodiment 1.
Embodiment 3
A kind of embodiment of hair washing bath shampoo of the present invention, described hair washing bath shampoo comprises the component of following percentage by weight: Chinese medicine extract: 6%, cod-liver oil: 1.5%, sodium isethionate: 20%, lanoline: 0.5%, glycerol: 30%, antiseptic: appropriate, surplus is water; Other qualificationss and preparation process are with embodiment 1.
Embodiment 4
A kind of embodiment of hair washing bath shampoo of the present invention, described hair washing bath shampoo comprises the component of following percentage by weight: Chinese medicine extract: 8%, cod-liver oil: 2%, sodium isethionate: 25%, lanoline: 0.8%, glycerol: 40%, antiseptic: appropriate, surplus is water; Other qualificationss and preparation process are with embodiment 1.
Embodiment 5
A kind of embodiment of hair washing bath shampoo of the present invention, described hair washing bath shampoo comprises the component of following percentage by weight: Chinese medicine extract: 10%, cod-liver oil: 3%, sodium isethionate: 30%, lanoline: 1%, glycerol: 50%, antiseptic: appropriate, surplus is water; Other qualificationss and preparation process are with embodiment 1.
Embodiment 6
1, eye irritation test:
According to the requirement of cosmetics health standard (2007), carry out acute ocular irritation test (DAVIS).Experimental technique: select 3 healthy New Zealand rabbit that grows up, splash into this sample of 0.1ml in rabbit one branch hole conjunctival sac, another branch hole is not processed and made own control, makes a rabbit eyes closed 1s time after painting.Be painted into after tested material and do not rinse eyes in 24h.Record each leisure 1,24,48 of tested rabbit cornea, iris or conjunctiva, the reaction and the 4th of 72h, the recovery situation of 7d, carry out eye infringement grade scale scoring and the evaluation of eye stimulus intensity.
The eye irritation result of the test of table 1 hair washing bath shampoo of the present invention
Due to horn film, iris integration=0; Conjunctival congestion or chemosis integration < 2, and integration is down to 0 at < in 7 days, therefore termination test is not observed the recovery situation of 21d,, result is as shown in table 1, and stimulus intensity is classified as: embodiment 1 nonirritant; Embodiment 2 is non-stimulated, embodiment 3 nonirritants; Embodiment 4 is non-stimulated, embodiment 5 microstimulations.
2, skin irritation test
According to the requirement of cosmetics health standard (2007), carry out irritation test.Test method: select health, grow up, 4 of the white rabbit of skin zero damage, 24h before experiment, each of every rabbit back spinal column both sides cropping, can not damage epidermis, and unhairing scope left and right is respectively 3.0cm * 3.0cm.This tested material 0.5ml is applied on a side defeathering region, and area is 2.5cm * 2.5cm.Opposite side is coated with distilled water and compares.Be coated with skin every day once, before each painting, repair hair, with warm water, remove residual tested material, be coated with continuously skin 14d.
The skin irritation test result of table 2 hair washing bath shampoo of the present invention
Result is as shown in table 2, according to < < cosmetics health standard > > skin irritation strength grading, integration 0-0.5, embodiment 1,2,3,4,5 belongs to without skin irritation.
3, acute toxicity testing
According to GB15193-2003 < < foodsafety Toxicological Assessment program and method > >, adopt maximum tolerance metering experiment method, dosage is made as 10000mg/kg BW, select 20 kunming mices, male and female half and half.Animal fasting 16h before test, does not limit drinking-water.Adopt administration by gavage to give the animal 500mg/ml sample solution of concentration, gavage amount is 0.4ml/20g body weight.After gavage, observe poisoning manifestations and the death condition of animal, weigh weekly 1 time, observe 14 days.
The acute toxicity testing result of table 3 hair washing bath shampoo of the present invention
Result is as shown in table 3, and according to the acute toxicity grading criteria evaluation of food, embodiment 1,2,3,4,5 belongs to nontoxic level.
4, emollient experiment
Choose experimenter 30 people and test, men and women half and half, and the age is from 30-50 year, 38 years old mean age, and to test and within first 2 months, do not use external preparation for skin medicine, skin is without wound.Allow experimenter use respectively tap water, embodiment 1,2,3,4,5 samples, be divided into 4 days and test, only survey a sample at every turn.Before each test, experimenter is with the clean both hands of clear water, towel, and slow-witted upper 2 hour in 25 ℃, the air-conditioned room of humidity 30rh, and (each 2 of right-hand men) draws the border circular areas of diameter 2cm at random 4 positions of the back of the hand.With 1g sample, wash one's hands 3 minutes, be over after washing gently water on hand off with cotton balls and start timing.With moisture of skin instrument in test zone the 5th minute respectively, the 10th minute, the moisture value of skin in the time of the 30th minute, passed judgment on skin moistening degree according to moisture value size.(to smear hand as a control group with the common moisturizer of 1g after clear water washing).
The emollient experimental result of table 4 hair washing bath shampoo of the present invention
According to table 4 data, can find out, the sample of embodiment 1,2,3 is suitable with the clean rear moistening effect of moisturizer that uses; Along with the increase of Chinese medicine ingredients, good than with milky lotion of embodiment 4 and 5 moistening effect.
5, inflammation-resisting itch-stopping test
Adopt histamine phosphate to cause the local pruritus model of Cavia porcellus, the itching-relieving action of test sample.Choose 70 of body weight 250-400g healthy guinea pigs, be divided at random 7 groups, 10 every group, male and female half and half.Blank group (distilled water 0.1ml/100g), positive control drug antipruritic liquid medicine group (0.1ml/100g), the large, medium and small dosage group of embodiment 1-5 (0.2ml/100g, 0.1ml/100g, 0.05ml/100g).Test and within first 1 day, respectively organize the right back dorsal portion of Cavia porcellus and shave hair, and shave the corresponding laboratory sample of the outer painting in hair place 1 time at each treated animal.Test the same day, with coarse sandpaper scratch instep, shave hair place, to damage epidermis, skin is slight, and oozing of blood is to spend, area 1cm 2, part repastes laboratory sample 1 time, after last coating 10min, only starts to drip at wound surface place 0.01% histamine phosphate solution 0.05ml/.After this, every 3min, press 0.02%, 0.03%, 0.04% ... progressive concentration is only 0.05ml/ at every turn, until occur that Cavia porcellus only later licks right back foot, take and finally occur that it is itch-threshold that Cavia porcellus later licks the right back histamine phosphate total amount (ug) being given when sufficient, data respectively organized in record.
Table 5 inflammation-resisting itch-stopping result of the test
According to table 5 data, can find out, the large, medium and small dosage group of embodiment 1-5 (0.2ml/100g, 0.1ml/100g, 0.05ml/100g) and itch stopping and diminish inflammation liquid medicine group (positive control) external all can obviously improve the antipruritic threshold value of histamine phosphate to Cavia porcellus, show that embodiment 1-5 has obvious inflammation-resisting itch-stopping effect.
Last institute should be noted that; above embodiment is only in order to illustrate technical scheme of the present invention but not limiting the scope of the invention; although the present invention is explained in detail with reference to preferred embodiment; those of ordinary skill in the art is to be understood that; can modify or be equal to replacement technical scheme of the present invention, and not depart from essence and the scope of technical solution of the present invention.

Claims (8)

1. a hair washing bath shampoo, is characterized in that, described hair washing bath shampoo comprises the component of following percentage by weight: Chinese medicine extract: 1-10%, cod-liver oil: 0.1-3%, sodium isethionate: 10-30%, lanoline: 0.1-1%, glycerol: 20-50%, surplus is water;
Described Chinese medicine extract comprises Folium Artemisiae Argyi extract, Cortex Dictamni extract, Flos Chrysanthemi Indici extract, Radix Scutellariae extract and Radix et Caulis Opuntiae Dillenii extract.
2. hair washing bath shampoo according to claim 1, is characterized in that, described hair washing bath shampoo comprises the component of following percentage by weight: Chinese medicine extract: 8-10%, cod-liver oil: 2-3%, sodium isethionate: 25-30%, lanoline: 0.8-1%, glycerol: 40-50%, surplus is water.
3. hair washing bath shampoo according to claim 2, is characterized in that, described hair washing bath shampoo comprises the component of following percentage by weight: Chinese medicine extract: 10%, cod-liver oil: 3%, sodium isethionate: 30%, lanoline: 1%, glycerol: 50%, surplus is water.
4. hair washing bath shampoo according to claim 1, is characterized in that, described hair washing bath shampoo also comprises antiseptic.
5. hair washing bath shampoo according to claim 1, it is characterized in that, in described Chinese medicine extract, Folium Artemisiae Argyi extract, Cortex Dictamni extract, Flos Chrysanthemi Indici extract, Radix Scutellariae extract and Radix et Caulis Opuntiae Dillenii extract's weight ratio is Folium Artemisiae Argyi extract: Cortex Dictamni extract: Flos Chrysanthemi Indici extract: Radix Scutellariae extract: Radix et Caulis Opuntiae Dillenii extract=1:2:2:1:2.
6. hair washing bath shampoo according to claim 1, is characterized in that, described Folium Artemisiae Argyi extract obtains by dehydrated alcohol extraction; Described Cortex Dictamni extract obtains by dehydrated alcohol extraction; Described Flos Chrysanthemi Indici extract obtains by dehydrated alcohol extraction; Described Radix Scutellariae extract obtains by dehydrated alcohol extraction; Described Radix et Caulis Opuntiae Dillenii extract obtains by dehydrated alcohol extraction.
7. hair washing bath shampoo according to claim 6, is characterized in that, described Folium Artemisiae Argyi, by after dehydrated alcohol extraction, is concentrated into Folium Artemisiae Argyi extract and described Folium Artemisiae Argyi identical weight; Described Cortex Dictamni, by after dehydrated alcohol extraction, is concentrated into Cortex Dictamni extract and described Cortex Dictamni identical weight; Described Flos Chrysanthemi Indici, by after dehydrated alcohol extraction, is concentrated into Flos Chrysanthemi Indici extract and described Flos Chrysanthemi Indici identical weight; Described Radix Scutellariae, by after dehydrated alcohol extraction, is concentrated into Radix Scutellariae extract and described Radix Scutellariae identical weight; Described Radix et Caulis Opuntiae Dillenii, by after dehydrated alcohol extraction, is concentrated into Radix et Caulis Opuntiae Dillenii extract and described Radix et Caulis Opuntiae Dillenii identical weight.
8. a preparation method for hair washing bath shampoo as claimed in claim 1, is characterized in that, said method comprising the steps of:
(1) in agitator, add water and sodium isethionate, heat while stirring, homogenizing is to fully dissolving;
(2) temperature is down to 50 ℃ when following, adds successively Chinese medicine extract, cod-liver oil, lanoline, glycerol.
CN201410376357.XA 2014-07-31 2014-07-31 A kind of hair washing bath shampoo and preparation method thereof Expired - Fee Related CN104116681B (en)

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CN105943466A (en) * 2016-06-24 2016-09-21 中山爱护婴童健康科技研究有限公司 Baby hair and body shampoo
CN106236662A (en) * 2016-08-31 2016-12-21 黄沈昌 A kind of production method of Radix et Caulis Opuntiae Dillenii shampoo
CN106236658A (en) * 2016-08-31 2016-12-21 陈召林 A kind of production method of Flos Chrysanthemi Indici bath foam
CN107854415A (en) * 2017-12-29 2018-03-30 四川农业大学 A kind of Chinese gall shampoo and its preparation method and application of pet

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105662943A (en) * 2016-01-16 2016-06-15 王华清 Shampoo shower gel containing Chinese herbal medicinal ingredients
CN105943466A (en) * 2016-06-24 2016-09-21 中山爱护婴童健康科技研究有限公司 Baby hair and body shampoo
CN105943466B (en) * 2016-06-24 2019-04-02 中山爱护婴童健康科技研究有限公司 A kind of baby child's shampoo used also as bath lotion
CN106236662A (en) * 2016-08-31 2016-12-21 黄沈昌 A kind of production method of Radix et Caulis Opuntiae Dillenii shampoo
CN106236658A (en) * 2016-08-31 2016-12-21 陈召林 A kind of production method of Flos Chrysanthemi Indici bath foam
CN107854415A (en) * 2017-12-29 2018-03-30 四川农业大学 A kind of Chinese gall shampoo and its preparation method and application of pet

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