CN102846503B - Refreshing, anti-dandruff, nourishing and healthful shampoo and preparation method thereof - Google Patents
Refreshing, anti-dandruff, nourishing and healthful shampoo and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a refreshing, anti-dandruff, nourishing and healthful shampoo and a preparation method thereof. The shampoo contains the following materials: sodium dodecylsulfate, sodium sarcosinate, MES, AES, CAB, 22SB, Arabia gum, tragacanth, a soapberry extract, a weeping willow branch extract, a trumpet creeper extract, a hibiscus leaf extract, a mint extract, glycerol, ethylenediaminetetraacetic acid disodium salt, Parahydroxy benzoic acid methyl easter, ethyl ester, tea seed oil, vitamin C, cationic guar gum, sodium alginate, propylene glycol, distilled water and essence. Compared with the prior art, the shampoo provided by the invention has advantages of mild property and high safety; active substances in natural plants are combined with a surfactant to inhibit dandruff, so as to achieve natural and mild anti-dandruff effect; besides, the shampoo can supplement the hair with nutrients and moisture and prevent dry scalp.
Description
Technical field
The present invention relates to a kind of shampoo paste and preparation method thereof, particularly a kind of refrigerant anti-dandruff nourishing health hair washing cream and preparation method thereof.
Background technology
The many factors such as modern society's operating pressure is large, lessons are heavy, worried many, endocrine disturbance, seasonal variations, nutrient shortage, hair dyeing, hair-waving and night owl, cause dandruff problem to present rejuvenation, generalization, scalp is the first element of human beauty, is also healthy major criterion.Having an elegant healthy hair is that every the personage that likes to be beautiful yearns for, yet youth brilliance has in the past been taken away in alopecia, also to people, brings infinite worry.People's the dandruff makes that the beauty in youth is graceful has a greatly reduced quality.The dandruff and alopecia bring people's puzzlement not only in appearance, are more the torment of heart and spirit.A full ﹑ is scurf completely on the shoulders, or the age gently with regard to bald be very big infringement to appearance really, the very big strike to self-confidence especially, also has influence on professional choosing and selects even future of ﹑ marriage.Society dog-eat-dog, away from the dandruff, is a factor of prevailing over competition away from alopecia.The dandruff is adhered to and comes off in a large number at scalp top layer, hair, this work that very little problem usually perplexing people, life and the various aspects such as social of seeming.When the dandruff occurs, usually with symptoms such as scalp inflammation and scalp itch; If do not take appropriate method to treat targetedly, this disease may be periodically, the generation of recurrent or persistence, when serious, can cause scalp hair follicles damage, forms permanent alopecia.The generation of the dandruff is general skin dirt, and namely the horny layer of epidermis constantly peels off that face produces, and is also metabolic result.The dandruff is divided into the physiological dandruff and the pathologic dandruff.
The society pathologic dandruff increases increasingly, and the major reason that the pathologic dandruff occurs is: scalp cells functional disorder.The cell of scalp also has certain metabolic processes as skin.After basal layer cell propagation, ripe toward extrapolated gradually, finally become abiotic cuticular horny layer and come off.If this process has had defect, make scalp cells maturation process incomplete.Can be to scale off.The patient that for example old people, malnutrition, acceptance are subject to chemotherapy or chronic eczema, the dandruff increases starts because of in this.
Healthy scalp ecological environment is maintained by the balance of finance, credits and materials: oils and fats, flora, metabolic balance.Skin fat secretion is unbalance right overhead, and scalp will fuel-displacedly become greasy; Unbalance when scalp flora environment, harmful bacteria grows in a large number, just there will be the phenomenon of head pruritus; And scalp horny layer tachytrophism comes off and just forms dandruff.Thus, the ecological balance of scalp is the key that we resist dandruff, how to keep good ecological balance? the most important resistance that will improve scalp.
In the 12 China's international beauty and make-up articles for washing fair, participant brainstrust is unanimously thought, natural plant kind cosmetics are the main trend that cosmetics are researched and developed both at home and abroad from now on, " Chinese herbal medicine " is the best raw material of functional cosmetics, correctly select Chinese herbal medicine to add in hair shampoo article, can well improve scalp resistance, reduce dandruff symptom.With natural plant extracts, developing new cosmetics will be up-and-coming a kind of new approaches.Chinese medicine elite is dissolved into and is washed in hair products, is the scientific and technological Development Trend of modern hair care.Utilize sophisticated technologies, the elite composition in extraction Chinese medicine, makes effective ingredient fully contact with healthy hair, brings into play better effect.For busy working clan, using and washing hair products containing the anti-dandruff nourishing of Chinese medicine elite is not only science but also easy anti-dandruff method.
Summary of the invention
The 1st technical problem to be solved by this invention is to provide a kind of new anti-dandruff health hair washing cream that contains natural component extract.
The 2nd technical problem to be solved by this invention is the preparation method of above-mentioned shampoo paste.
Technical solution problem of the present invention is: a kind of anti-dandruff health hair washing cream, contains following material and weight portion in 174g bath foam:
Described Fructus Sapindi Mukouossi extract is to prepare by the following method:
Take Fructus Sapindi Mukouossi appropriate, after pulverizing, soak 0.15-0.8h, in 90-100 ℃ of heating, decoct and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times (g/ml) of Fructus Sapindi Mukouossi weight, filters and get final product.
Described Salix babylonica L. branch extracting solution is prepared by the following method:
Take Salix babylonica L. branch appropriate, soak 0.15-0.8h, in 90-100 ℃ of heating, decoct and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times (g/ml) of Salix babylonica L. branch weight, filters and get final product.
Described Flos Campsis extracting solution is prepared by the following method:
Take Flos Campsis appropriate, soak 0.15-0.8h, in 90-100 ℃ of heating, decoct and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times (g/ml) of Flos Campsis weight, filters and get final product.
Described Herba Menthae extracting solution is prepared by the following method:
Take Herba Menthae a certain amount of, put in round-bottomed flask, and add 8-12 distilled water doubly, be positioned in electric jacket, by volatile oil extractor reflux, extract,, after 5-6 hour, be cooled to room temperature, with double gauze, filter, get filtrate stand-by.
Described Folium Hibisci extracting solution is prepared by the following method:
Take Folium Hibisci appropriate, soak 0.15-0.8h, in 90-100 ℃ of heating, decoct and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times (g/ml) of Folium Hibisci weight, filters and get final product.
Described essence is rose essence, peach flavor, flavoring pineapple essence, Fructus Citri Limoniae essence, green cucumber essence, jasmin essence, osmanthus flower fragrance.
The preparation method of described a kind of refrigerant anti-dandruff nourishing health hair washing cream, comprises the following steps:
A) take cation guar gum 0.1-4g, join in the distilled water of 50-100ml, 60-80 ℃ of heating in water bath, heats while stirring, to be mixed evenly after, standing its abundant swelling that allows, stand-by;
B) take sodium alginate 0.5-5g, be heated to 60-80 ℃, heat while stirring, after mix homogeneously, standing its abundant swelling that allows, stand-by;
C) take respectively K
124-24g, sodium sarcosinate 3-8g, CAB 3-8g, MES 3-8g, AES 3-8g, 22SB 2-8g, distilled water 30-80ml, in 60-90 ℃ of stirring and dissolving, as solution 1, stand-by;
D) take respectively Fructus Sapindi Mukouossi extracting solution 1-16g, Salix babylonica L. branch extracting solution 0.5-10g, Flos Campsis extracting solution 0.4-8g, Flos Hibisci extracting solution 0.4-8g, Herba Menthae extracting solution 1-16g, stirs, as solution 2;
E) measure Oleum Camelliae 6-17ml in mortar, then take gum arabic powder 0.8-6g, western adragant powder 0.1-5g is placed in mortar, after grinding evenly, add 2-10ml distilled water, grind rapidly in the same direction, until be that colostrum forms, then add inward 2-10ml distilled water, after grinding evenly, solution 1 is joined in mortar, continue to grind, until grind evenly, again ground emulsion is added in solution 2, form mastic 1;
F) get the cation guar gum that previous swelling is good, sodium alginate joins in mastic 1, and adds 4-18ml glycerol, stirs, and forms mastic 2;
G) take disodiumedetate 0.01-1.2g, methyl hydroxybenzoate 0.01-1mg, ethyl hydroxybenzoate 0.01-1mg, add 1-12ml propylene glycol, heating makes its dissolving, as solution 3, solution 3, the remaining distilled water of 5% vitamin C injection 3-14ml, pearling agent 0.5-3.5g are added in mastic 2, stir.
Various compositions in the present invention are as follows:
Fructus Sapindi Mukouossi fruit itself adds water just can produce natural foam, so be widely used in early days cleaning aspect, dies down afterwards because of the convenience of chemical products.In the time of in ancient times, if people's skin of family grows the dermatosiss such as fish unicorn tinea, erythema, chronic eczema, patient's household will, with the fruit of Fructus Sapindi Mukouossi, add the skin that water is crumpled patient.< < Compendium of Materia Medica > > describes: Fructus Sapindi Mukouossi hair washing can be gone wind improving eyesight, makes hair light submissive, washes one's face and can brighten speckle.Fructus Sapindi Mukouossi is the plant that in < < Compendium of Materia Medica > >, single memorial is washed one's face for having one's hair wash.Modern scientific research shows, the contained sapindoside of Fructus Sapindi Mukouossi is a kind of good natural surfactant.It has skin expansion surface blood capillary, accelerates the effect of blood flow.Can manufacture " natural nuisance-free abluent ",, beauty treatment clean for daily washing-tableware, hair washing, skin care.
Fructus Sapindi Mukouossi fruit contains natural clean rhzomorph, penetration is strong, massaging scalp during by hair washing, through root of hair, the nutritional labelings such as the aminoacid that allows root of hair absorb to be carried by Fructus Sapindi Mukouossi extraction elite and the multiple hair care factor, and then deep layer hair nutrition supplementing and moisture content, gentle nursing scalp, reaches hair care and nourishing effect.Unique Fructus Sapindi Mukouossi soap lye contains evergreen Teng, Folium Symplocoris Caudatae and vitamin C, arabinose etc. to anti-bacteria, and problem dandruff, alopecia are very powerful, for hair increases moisture content and moistens, hair is more easily arranged, and replys beautiful submissive.
Salix babylonica L. branch energy wind-dispelling heat-dissipating clearing away heat-damp and promoting diuresis rash solution pox.Modern medicine study confirmation, willow is rich in the materials such as tannin, salicylic acid and bigcatkin willow glucosides, can be used for treating disease.The traditional Chinese medical science thinks, willow (branch and leaf, root bark, fibrous root, bark, Flos Salicis Babylonicae, Semen Salicis babylonicae cum pilus) is cold in nature, has the function of heat-clearing and toxic substances removing, expelling wind and removing dampness.This sketch of < < the southern regions of the Yunnan Province says that > > says: " cure mainly the blood clotting stagnation of QI, the exterior tightened by pathogenic windcold; Children's's variola, has Aconitum carmichjaelii Debx. to fall into top, and slurry can not rise person, decoction or bathe it." < < Compendium of Materia Medica > > says: " decoction, the pox of harnessing the Yellow River, nebulousurine; Wine boils, and presses all pains swollen, removes wind, alleviating pain and detumescence." < < must join herbal > > and say: " go wind heat, except arthralgia chiefly caused by damp pathogen." Salix babylonica L. branch contains natural β-hydroxyamino acid, can allow pore keratinization thromboembolism around be easy to come off, and unobstructed follicular canal, effectively prevents that pore from blocking.Salicylic acid is plant Ramulus Salicis Babylonicae and extract of willow bark, is a kind of natural antibiotic medicine.Salicylic acid has outstanding " exfoliation, unclogging " ability, safe, and lower compared with fruit acid to the stimulation of skin.Containing mild antibiotic composition, continue to alleviate itching of scalp, rubescent.
Flos Campsis has promoting blood circulation to remove blood stasis, cooling blood, expelling wind, the effect for the treatment of skin pruritus.In the > > of < < Sheng Nong's herbal classic, formally record and reach the clouds.Its flower, stem, leaf, root all can be used as medicine.< < Kaibao Bencao > > thinks that the stem of reaching the clouds can treat rubella pruritus.Flos Campsis has again the function of cooling blood, expelling wind, is applicable to blood hot air wind producing, whole body pruritus.Flos Campsis external, can treat skin eczema, often coordinates with Rhizoma Coptidis, Alumen, Realgar, and pulverization, mixes well with vinegar, external application affected part.Flos Campsis extract joins in hair shampoo article, and scalp itch gently plays the effect of itch-stopping bactericidal, and its composition of invigorating blood circulation, nourishes scalp fully, promotes new growth, and it is close that life-time service can make hair thicken.
Folium Hibisci is cool in nature, nontoxic, has the merit of heat clearing away, dampness removing, removing heat from blood, can control scabies, the diseases such as furuncle furuncle and phyma.After Folium Hibisci is cleaned, with clear water, soak, rub out contained glue juice, be used for hair washing, the greasy dirt that deoils,, dandruff, stopping head itching, natural hair conditioner, prevent alopecia, bifurcated and the dandruff, prevention poliosis, additional issue, regulate the fat secretion of scalp, can make scalp, make hair submissive, bright, salubrious, high resilience.
Herba Menthae is pungent cool property sweating antipyretic medicine, and the anti-dandruff factor of Herba Menthae has anti-inflammation and sterilization, decomposes lipid effect, effectively improves the puzzlement of dandruff and scalp pruritus, effectively suppresses dandruff, head pruritus.External can be controlled skin pruritus, erythra and eczema etc., can nurse one's health skin unclean, that block, and it has refrigerant sensation, can shrink blood capillary, gets rid of vivotoxin, improve eczema, tinea, releive itch, inflammation and burning, soft skin, is of value to oiliness hair quality.Hair follicle, resists hair follicle aging clearly thoroughly, repairs, nourishes, protects dry hair, makes hair and scalp be full of healthy vigor, and with Herba Menthae fragrance, refreshment, makes healthy hair pleasant elegant, the brand-new experience that brings submissive easy comb.Herba Menthae also has anti-inflammatory analgetic effect, is applicable to hair antipruritic.
Seed of Camelliasinensis(L.)Ktzel oil has another name called Camellia oil, Oleum Camelliae, tea tree oil, Oleum Camelliae.Camellia oil breath delicate fragrance, local flavor is peculiar, have saying of " east olive oil ", fatty acid composition and the olive oil of finding Oleum Camelliae look like especially, linoleic content is more than 80%, Oleum Camelliae unsaturated fatty acid content is easily absorbed by the body up to 90%, can also promote the absorption of human body to trace element such as fat-soluble fiber and calcium, ferrum, zinc simultaneously.In Camellia oil, also contain in olive oil unexistent bioactive substance as camellin, Tsubaki-saponin, tea polyphenols etc.Natural tea tree oil nature is gentle, can supplement scalp skin nutrition, promotion hair growth, and sterilizing and itch-relieving, to treating, scalp is fuel-displaced, dermatitis, eczema and the dandruff have obvious effect, can nurse one's health oily skin, is very effective antibiotic anti-dandruff product.To repairing tool after skin scalp itch, dry and cracked, eczema, solarization, be significantly improved, cleaning capacity is strong, makes scalp skin keep salubrious, healthy comfortable.
Cation guar gum plays good foaming, steady bubble effect, antistatic property, and thickening power in hair shampoo article.In addition, can also improve wet comb and the dry comb property of hair, make hair keep for a long time gloss, softness, flexible, reduce the zest of detergent to skin.
Sodium alginate plays good thickening power in hair shampoo article, antistatic property, and steady bubble effect.In addition, can also improve the moisture retention of hair, make the long-term maintenance of hair submissive.Thickening agent and wetting agent common in hair shampoo article.
In this shampoo paste prescription, added a large amount of extracted form natural plant compositions.By clean scalp and hair-care and control head skin beauty water oil balance, reduce growing of antibacterial fungus on the one hand.Salicylic acid in Salix babylonica L. branch, the compositions such as Saponin in Fructus Sapindi Mukouossi be cleaning-nursing scalp and hair well, and the gentle injury skin that is difficult for of quality, activity extract in Folium Hibisci, tea tree oil is the fat secretion of scalable scalp also, makes scalp keep for a long time water oil poised state.
By anti-inflammation, reach effect anti-dandruff and alleviation head pruritus again on the other hand.In Fructus Sapindi Mukouossi, tea tree oil and Salix babylonica L. branch, all contain natural clean rhzomorph, can kill head fungus antibacterial.In Flos Campsis, Folium Hibisci, Herba Menthae, all contain antiinflammatory composition, can alleviate the bacterial scalp itch symptom of fungus.Particularly Folium Menthae extract, brings refrigerant pleasant sensation during hair washing.
In these natural extracts that add, also have a large amount of nourishing hair care ingredients and multiple important trace element, in effectively clean, anti-dandruff, also can accelerate scalp metabolism, promote new growth, make root of hair strong not easily broken, hair is shiny black submissive.
In a word, this shampoo paste can anti-bacteria fungus grow, the water oil balance of regulation and control skin of head, reaches clean anti-dandruff effect, can supplement the required nutrition of hair scalp, moisture, prevent alopecia, bifurcated and fungus grow, and can improve scalp blood circulation, enhance metabolism, make root of hair strong, healthy hair is dense submissive.
The made shampoo paste of the present invention is creamy white, and viscosity is suitable, and foam is smooth abundant, and evenly fine and smooth, stretchability is good, cool and comfortable, good stability, abnormal smells from the patient fragrance.
The specific embodiment
Below in conjunction with embodiment, the present invention will be further described.
Oleum Camelliae of the present invention, pearling agent are commercially available.
Embodiment 1
The preparation of 1.1 Fructus Sapindi Mukouossi extracts
Take Fructus Sapindi Mukouossi 200g, after pulverizing, soak 0.5h, in 90-100 ℃ of heating, decoct and extract 3 times, add 8 times of water gagings the 1st time, extract 2h, add 6 times of water gagings the 2nd time, extract 1h, add 4 times of water gagings the 3rd time, extract 0.5h, each with 3 layers of gauzes filtration, merging filtrate, it is stand-by that the volume of filtrate is concentrated into 4 times (g/ml) of Fructus Sapindi Mukouossi weight.
The preparation of 1.2 Salix babylonica L. branch extracting solution
Take Salix babylonica L. branch 100g, soak 0.5h, in 90-100 ℃ of heating, decoct and extract, extract 3 times, add 8 times of water yields the 1st time, extract 1.5h, 6 times of water yields of the 2nd use, extract 1.5h, 4 times of water yields of the 3rd use, extract 1h, with double gauze, filter at every turn, merging filtrate, the volume of filtrate is concentrated into 3 times (g/ml) of Salix babylonica L. branch weight, stand-by.
The preparation of 1.3 Flos Campsis extracting solution
Take Flos Campsis 50g, in 90-100 ℃ of heating, decoct and extract 3 times, 8 times of water yields of the 1st use, extract 1h, 6 times of water yields of the 2nd use, extract 1h, 4 times of water yields of the 3rd use, extract 0.5h, filter with double gauze at every turn, the filtrate of extracting merges, and it is stand-by that the volume of filtrate is concentrated into 3 times (g/ml) of Flos Campsis weight.
The preparation of 1.4 Folium Hibisci extracting solution
Take Folium Hibisci 60g, in 90-100 ℃ of heating, decoct and extract 3 times, 8 times of water yields of the 1st use, extract 1h, 6 times of water yields of the 2nd use, extract 1h, 4 times of water yields of the 3rd use, extract 0.5h, for extracting solution merges, double gauze filters, and it is stand-by that the volume of filtrate is concentrated into 4 times (g/ml) of Folium Hibisci weight.
The preparation of 1.5 Herba Menthae extracting solution
Take Herba Menthae 50g, put in round-bottomed flask, and add the distilled water of 9 times, be positioned in electric jacket, by volatile oil extractor reflux, extract,, after 5 hours, be cooled to room temperature, with double gauze, filter extracting solution, stand-by.
The preparation of 1.6 shampoo pastes
A) take cation guar gum 4g, join in the distilled water of 100ml, in being heated to the water-bath of 60 ℃, limit edged stirs, to be mixed evenly after, standing, allow its abundant swelling.
B) take sodium alginate 0.5g, join in the beaker that 80ml distilled water is housed, 60 ℃ of heating in water bath, limit heating edge stirs with glass plate, to be dissolved after, standing, allow its abundant swelling.
C) take respectively K12 6g, sodium sarcosinate 8g, CAB 7g, MES9g, AES 8g, 22SB 6g, distilled water 50g in beaker 1, be placed in 60 ℃ of thermostat water baths and stir 40min dissolving, after dissolving completely, be placed on water-bath, stand-by, as solution 1.
D) take respectively Fructus Sapindi Mukouossi extracting solution 9g, Salix babylonica L. branch extracting solution 10g, Flos Campsis extracting solution 8g, Flos Hibisci extracting solution 7g, Herba Menthae extracting solution 10g and be placed in beaker, and stir 5min, as solution 2.
E) measure Oleum Camelliae 10ml in mortar, then take arabic gum 3.0g, tragacanth 2.2g is placed in mortar, after grinding 10min and making it evenly, add 10ml distilled water, grind rapidly in the same direction, until hear flip-flop (being that colostrum forms), add inward again 10ml distilled water, after grinding evenly, solution 1 is joined in mortar, continue to grind 10min, until grind evenly, until grind evenly, more ground emulsion is added in solution 2, form mastic 1;
F) get previous a) and b) in the good cation guar gum of swelling, sodium alginate joins in mastic 1, and adds 15ml glycerol, with blender, stirs and makes it even, forms mastic 2.
G) take disodiumedetate 0.05g, Metagin, each 0.05g of ethyl ester, add 8ml propylene glycol, heating is dissolved it, puts into beaker after to be dissolved, as solution 3, by solution 3,5% vitamin C injection 11ml, remaining distilled water, pearling agent 0.6g joins in mastic 2, stirs 30min make it even with blender, obtains refrigerant anti-dandruff nourishing shampoo paste.
Embodiment 2
The preparation of 2.1 Fructus Sapindi Mukouossi extracts
Take Fructus Sapindi Mukouossi 100g, after pulverizing, soak 0.5h, in 90-100 heating, decoct and extract 3 times, add 9 times of water gagings the 1st time, extract 2h, add 7 times of water gagings the 2nd time, extract 1h, add 4 times of water gagings the 3rd time, extract 0.5h, each with 3 layers of gauzes filtration, merging filtrate, it is stand-by that the volume of filtrate is concentrated into 3 times (g/ml) of Fructus Sapindi Mukouossi weight.
The preparation of 2.2 Salix babylonica L. branch extracting solution
Take Salix babylonica L. branch 80g, extract 3 times, in 90-100 heating, decoct and extract 3 times, add 7 times of water yields the 1st time, extract 1.5h, 6 times of the 2nd use, extract 1.5h, the water yield, 3 times of water yields of the 3rd use, extract 1h, filter with double gauze at every turn, merging filtrate, it is stand-by that the volume of filtrate is concentrated into 4 times (g/ml) of Salix babylonica L. branch weight.
The preparation of 2.3 Flos Campsis extracting solution
Take Flos Campsis 60g, extract 3 times, in 90-100 heating, decoct and extract 3 times, 9 times of water yields of the 1st use, extract 1h, 6 times of water yields of the 2nd use, extract 1h, 4 times of water yields of the 3rd use, extract 0.5h, with double gauze, filter, the filtrate of extraction merges at every turn, and it is stand-by that the volume of filtrate is concentrated into 4 times (g/ml) of Flos Campsis weight.
The preparation of 2.4 Folium Hibisci extracting solution
Take Folium Hibisci 50g, extract 3 times, in 90-100 heating, decoct and extract 3 times, 7 times of water yields of the 1st use, extract 1h, 6 times of water yields of the 2nd use, extract 1h, 4 times of water yields of the 3rd use, extract 0.5h, for extracting solution merges, double gauze filters, and it is stand-by that the volume of filtrate is concentrated into 4 times (g/ml) of Folium Hibisci weight.
The preparation of 2.5 Herba Menthae extracting solution
Take Herba Menthae 50g, put in round-bottomed flask, and add the distilled water of 9 times, be positioned in electric jacket, by volatile oil extractor reflux, extract,, after 5.5 hours, be cooled to room temperature, with double gauze, filter extracting solution, stand-by.
The preparation of 2.6 shampoo pastes
A) take cation guar gum 2g, join in the distilled water of 100ml, in being heated to the water-bath of 70 ℃, limit edged stirs, to be mixed evenly after, standing, allow its abundant swelling.
B) take sodium alginate 2.5g, join in the beaker that 100ml distilled water is housed, 80 ℃ of heating in water bath limit heating edge stir with glass plate, to be dissolved after, standing, allow its abundant swelling.
C) take respectively K
1210g, sodium sarcosinate 6g, CAB 8g, MES 6g, AES7g, 22SB 7g, distilled water 60g, in beaker 1, are placed in 70 ℃ of thermostat water baths and stir 30min dissolving, after dissolving completely, are placed on water-bath, stand-by, as solution 1.
D) take respectively Fructus Sapindi Mukouossi extracting solution 12g, Salix babylonica L. branch extracting solution 10g, Flos Campsis extracting solution 6g, Flos Hibisci extracting solution 8g, Herba Menthae extracting solution 12g and be placed in beaker, and stir 10min, as solution 2.
E) measure Oleum Camelliae 9ml in mortar, then take arabic gum 2.5g, tragacanth 0.8g is placed in mortar, after grinding 5min and making it evenly, add 10ml distilled water, grind rapidly in the same direction, until hear flip-flop (being that colostrum forms), then add inward 10ml distilled water, after grinding evenly, solution 1 is joined in mortar, continue to grind 5min, until grind evenly, again ground emulsion is added in solution 2, form mastic 1;
F) get previous a) and b) in good cation guar gum, the sodium alginate of swelling join in mastic 1, and add 15ml glycerol, with blender, stir and make it even, form mastic 2.
G) take disodiumedetate 0.03g, methyl hydroxybenzoate 0.01g, ethyl hydroxybenzoate 0.053g, add 10ml propylene glycol, heating makes its dissolving, after to be dissolved, put into beaker, as solution 3, by solution 3,5% vitamin C injection 14ml, remaining distilled water, pearling agent 0.6g joins in mastic 2, with blender, stir 20min and make it even, obtain refrigerant anti-dandruff nourishing shampoo paste.
Embodiment 3:
The physical and chemical index of embodiment 1,2 is as follows:
3.1 character
This product is that viscosity is suitable, and foam is smooth abundant, evenly fine and smooth, the milky shampoo paste that stretchability is good.
3.2 pH value inspections
With the PH reagent paper of moistening, dip a small amount of shampoo paste, PH is 6-7.
3.3 caloric test
Shampoo paste is packaged in transparent dressing product bottle, in the refrigerator cold-storages of 4 ℃, within about one week, observes without lamination.24h in the calorstat of 55 ℃, soap lye is without the phenomenon such as layering emulsifying is spoiled.
3.4 centrifugal test
Shampoo paste is packaged in to the centrifugal 20min of 3000r/min in tool plug test tube, without lamination.
3.5 irritation tests, anaphylaxis experiment
White mice back cuts off hair, smears respectively by the shampoo paste of embodiment 1,2 preparation in cutting plucked position, and is not coated with position and compares, and result does not have zest and anaphylaxis.
Get 1 gram of embodiment and be applied in volunteer (15-65 year, 380 people) gesture and facial expression, observe after spending 30 minutes, all do not occur rubescent, dermexanthesis, foaming phenomenon.
3.6 room temperatures are placed experiment
Embodiment 1,2 made shampoo pastes are placed in to bottle for cosmetics, the standing investigation of room temperature 6 months, without lamination, unchanged with aftersensation, abnormal smells from the patient is unchanged.
3.7 anti-dandruff effects
Choose volunteer (15-65 year, 380 people), prepared shampoo paste, for volunteer's hair, is mixed and repeatedly washed by rubbing with the hands with a small amount of water, find that foam enriches, it is smooth comfortable that volunteers generally feel, feel is better.The no matter dry comb of hair should wet comb property all.After washing, the submissive as silk of hair, fluffy non-greasy, moistening effect is better, washes afterwards without scalp pruritus phenomenon, and does not need to use hair conditioner.Through the continuous use of month, hair was obviously glossy, softness, and dandruff phenomenon obviously reduces.
Embodiment 4:
This shampoo paste resultant effect is investigated
Below utilize and try out the effect of feeling to come the shampoo paste that Evaluation operation example 1,2 produces.Adopt public-opinion poll point system, the women who chooses 80 25-50 year age bracket is object on probation, is divided into arbitrarily two groups, respectively with the shampoo paste wash my hair of embodiment 1,2 preparations.Use weekly twice, be two months service time.Every result of use total points is 5 minutes: 5 are divided into best result, represents fine, very satisfied; 4 are divided into better; 3 are divided into and can accept; 3 minutes is bad below, can not accept.It is below every average.The results are shown in Table 1:
Table 1 resultant effect is investigated
| Result of use | The every average of embodiment 1 | The every average of embodiment 2 |
| Moisture retention | 4.8 | 4.9 |
| Nourishing property | 4.7 | 4.8 |
| Refrigerant property | 5 | 5 |
| Foaming characteristic | 5 | 5 |
| Soil release performance | 5 | 5 |
| Dry comb property | 4.9 | 4.9 |
| Wet comb property | 4.9 | 4.9 |
| Relieving itching and removing dandruff | 4.7 | 4.6 |
| Compliance | 4.8 | 4.9 |
In sum, this made shampoo paste foam of the present invention enriches, and has good soil release performance, moisture retention, nourishing, feels refrigerant comfortable during use, good by rear hair elasticity, has the effect of hair washing, hair care, hair care, relieving itching and removing dandruff.
Claims (2)
1. a refrigerant anti-dandruff nourishing health hair washing cream, is characterized in that: in 174g shampoo paste, contain following material:
Described Fructus Sapindi Mukouossi extract is to prepare by the following method:
Take Fructus Sapindi Mukouossi appropriate, after pulverizing, soak 0.15-0.8h, in 90-100 ℃ of heating, decoct and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times (g/ml) of Fructus Sapindi Mukouossi weight, filters and get final product;
Described Salix babylonica L. branch extracting solution is prepared by the following method:
Take Salix babylonica L. branch appropriate, soak 0.15-0.8h, in 90-100 ℃ of heating, decoct and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times (g/ml) of Salix babylonica L. branch weight, filters and get final product;
Described Flos Campsis extracting solution is prepared by the following method:
Take Flos Campsis appropriate, soak 0.15-0.8h, in 90-100 ℃ of heating, decoct and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times (g/ml) of Flos Campsis weight, filters and get final product;
Described Herba Menthae extracting solution is prepared by the following method:
Take Herba Menthae a certain amount of, and add 8-12 distilled water doubly, be positioned in electric jacket, by volatile oil extractor reflux, extract,, after 5-6 hour, be cooled to room temperature, with double gauze, filter;
Described Folium Hibisci extracting solution is prepared by the following method:
Take Folium Hibisci appropriate, soak 0.15-0.8h, in 90-100 ℃ of heating, decoct and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging the 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, filter merging filtrate at every turn, the volume of filtrate is concentrated into 3-6 times (g/ml) of Folium Hibisci weight, filters.
2. a kind of refrigerant anti-dandruff nourishing health hair washing cream according to claim 1, is characterized in that: described essence is rose essence, peach flavor, flavoring pineapple essence, Fructus Citri Limoniae essence, green cucumber essence, jasmin essence, osmanthus flower fragrance.
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| CN104013561A (en) * | 2014-05-28 | 2014-09-03 | 皖南医学院 | Supple moistening water-locking mild nourishing shampoo paste and preparation method thereof |
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| CN1370516A (en) * | 2001-02-14 | 2002-09-25 | 上海白猫有限公司 | Nourishing and amending shampoo |
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| CN104013561A (en) * | 2014-05-28 | 2014-09-03 | 皖南医学院 | Supple moistening water-locking mild nourishing shampoo paste and preparation method thereof |
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