CN102846503A - Refreshing, anti-dandruff, nourishing and healthful shampoo and preparation method thereof - Google Patents
Refreshing, anti-dandruff, nourishing and healthful shampoo and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a refreshing, anti-dandruff, nourishing and healthful shampoo and a preparation method thereof. The shampoo contains the following materials: sodium dodecylsulfate, sodium sarcosinate, MES, AES, CAB, 22SB, Arabia gum, tragacanth, a soapberry extract, a weeping willow branch extract, a trumpet creeper extract, a hibiscus leaf extract, a mint extract, glycerol, ethylenediaminetetraacetic acid disodium salt, Parahydroxy benzoic acid methyl easter, ethyl ester, tea seed oil, vitamin C, cationic guar gum, sodium alginate, propylene glycol, distilled water and essence. Compared with the prior art, the shampoo provided by the invention has advantages of mild property and high safety; active substances in natural plants are combined with a surfactant to inhibit dandruff, so as to achieve natural and mild anti-dandruff effect; besides, the shampoo can supplement the hair with nutrients and moisture and prevent dry scalp.
Description
Technical field
The present invention relates to a kind of shampoo paste and preparation method thereof, particularly a kind of refrigerant anti-dandruff nourishing health hair washing cream and preparation method thereof.
Background technology
The many factors such as modern society's operating pressure is large, lessons are heavy, worried many, endocrine disturbance, seasonal variations, nutrient shortage, hair dyeing, hair-waving and night owl, cause the dandruff problem to present rejuvenation, generalization, scalp is the first element of human beauty, also is healthy major criterion.Having an elegant healthy hair is that every the personage that likes to be beautiful yearns for, yet youth brilliance has in the past been taken away in alopecia, also brings infinite worry to the people.People's the dandruff makes beautiful graceful the having a greatly reduced quality in youth.The dandruff and alopecia bring people's puzzlement not only in appearance, more are the torment of heart and spirit.A full ﹑ is scurf completely on the shoulders, or the age gently with regard to bald be very big infringement to appearance really, especially to the very big strike of self-confidence, ﹑ marriage even future are selected in the choosing that also has influence on occupation.The society dog-eat-dog away from the dandruff, is a factor of prevailing over competition away from alopecia.The dandruff is adhered to and is come off in a large number at scalp top layer, hair, this work that very little problem usually perplexing people, life and the various aspects such as social of seeming.When the dandruff occurs, usually with symptoms such as scalp inflammation and scalp itch; If do not take appropriate method to treat targetedly, this disease may be periodically, the generation of recurrent or persistence, can cause the scalp hair follicles damage when serious, forms permanent alopecia.The generation of the dandruff is general skin dirt, and namely the horny layer of epidermis peels off constantly that face produces, and also is metabolic result.The dandruff is divided into the physiological dandruff and the pathologic dandruff.
The society pathologic dandruff increases increasingly, and the major reason that the pathologic dandruff occurs is: the scalp cells functional disorder.The cell of scalp also has certain metabolic processes as skin.After basal layer cell propagation, ripe toward extrapolated gradually, become at last abiotic cuticular horny layer and come off.If this process has had defect, make the scalp cells maturation process incomplete.Namely can be to scale off.Old people, malnutrition, the acceptance patient that is subjected to chemotherapy or chronic eczema for example, the dandruff increases namely to be started because of in this.
Healthy scalp ecological environment is kept by the balance of finance, credits and materials: oils and fats, flora, metabolic balance.Haze wax fat secretion right overhead is unbalance, and scalp will fuel-displacedly become greasy; Unbalance when scalp flora environment, harmful bacteria grows in a large number, the phenomenon of head pruritus will occur; And scalp horny layer tachytrophism, coming off just forms dandruff.Thus, the ecological balance of scalp is the key that we resist dandruff, how to keep good ecological balance? the most important resistance that will improve scalp.
In the 12 China's international beauty and make-up articles for washing fair, the participant brainstrust is unanimously thought, the natural plant kind cosmetics are the main trend of cosmetics research and development both at home and abroad from now on, " Chinese herbal medicine " then is the best raw material of functional cosmetics, correctly select Chinese herbal medicine to add in the hair shampoo article, can well improve the scalp resistance, reduce dandruff symptom.Developing new cosmetics with natural plant extracts will be up-and-coming a kind of new approaches.The Chinese medicine elite being dissolved into washing in the hair products, is the Development Trend of modern hair care science and technology.Utilize sophisticated technologies, the elite composition in the extraction Chinese medicine makes effective ingredient fully contact with healthy hair, and performance is renderd a service better.For busy working clan, using the anti-dandruff nourishing that contains the Chinese medicine elite to wash hair products is not only science but also easy anti-dandruff method.
Summary of the invention
The 1st technical problem to be solved by this invention provides a kind of new anti-dandruff health hair washing cream that contains the natural component extract.
The 2nd technical problem to be solved by this invention is the preparation method of above-mentioned shampoo paste.
Technical solution problem of the present invention is: a kind of anti-dandruff health hair washing cream, contain following material and weight portion in the 174g bath foam:
Described Fructus Sapindi Mukouossi extract is to prepare by the following method:
Take by weighing Fructus Sapindi Mukouossi an amount of, soak 0.15-0.8h after pulverizing, decoct in 90-100 ℃ of heating and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging, extract 0.5-1.5h for the 2nd time, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times (g/ml) of Fructus Sapindi Mukouossi weight, filters and get final product.
Described Salix babylonica L. branch extracting solution prepares by the following method:
Take by weighing the Salix babylonica L. branch an amount of, soak 0.15-0.8h, decoct in 90-100 ℃ of heating and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging, extract 0.5-1.5h for the 2nd time, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times (g/ml) of Salix babylonica L. branch weight, filters and get final product.
Described Flos Campsis extracting solution prepares by the following method:
Take by weighing Flos Campsis an amount of, soak 0.15-0.8h, decoct in 90-100 ℃ of heating and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging, extract 0.5-1.5h for the 2nd time, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times (g/ml) of Flos Campsis weight, filters and get final product.
Described Herba Menthae extracting solution prepares by the following method:
Take by weighing Herba Menthae a certain amount of, put in the round-bottomed flask, and add 8-12 distilled water doubly, be positioned in the electric jacket, after 5-6 hour, be cooled to room temperature with the volatile oil extractor reflux, extract,, filter with double gauze, get filtrate stand-by.
Described Folium Hibisci extracting solution prepares by the following method:
Take by weighing Folium Hibisci an amount of, soak 0.15-0.8h, decoct in 90-100 ℃ of heating and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging, extract 0.5-1.5h for the 2nd time, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times (g/ml) of Folium Hibisci weight, filters and get final product.
Described essence is rose essence, peach flavor, flavoring pineapple essence, Fructus Citri Limoniae essence, green cucumber essence, jasmin essence, osmanthus flower fragrance.
The preparation method of described a kind of refrigerant anti-dandruff nourishing health hair washing cream may further comprise the steps:
A) take by weighing cation guar gum 0.1-4g, join in the distilled water of 50-100ml, 60-80 ℃ of heating in water bath heats while stirring, to be mixed evenly after, leave standstill and allow its abundant swelling, stand-by;
B) take by weighing sodium alginate 0.5-5g, be heated to 60-80 ℃, heat while stirring, behind the mix homogeneously, leave standstill and allow its abundant swelling, stand-by;
C) take by weighing respectively K
124-24g, sodium sarcosinate 3-8g, CAB 3-8g, MES 3-8g, AES 3-8g, 22SB 2-8g, distilled water 30-80ml, in 60-90 ℃ of stirring and dissolving, as solution 1, stand-by;
D) take by weighing respectively Fructus Sapindi Mukouossi extracting solution 1-16g, Salix babylonica L. branch extracting solution 0.5-10g, Flos Campsis extracting solution 0.4-8g, Flos Hibisci extracting solution 0.4-8g, Herba Menthae extracting solution 1-16g stirs, as solution 2;
E) measure Oleum Camelliae 6-17ml in mortar, take by weighing again gum arabic powder 0.8-6g, Calculus Bovis from Northwest of China natural gum over sixty years of age powder 0.1-5g and place mortar, grind evenly after, add the 2-10ml distilled water, grind rapidly in the same direction, until be that colostrum forms, add inward again the 2-10ml distilled water, after grinding evenly, solution 1 is joined in the mortar, continue to grind, until grind evenly, again ground emulsion is added in the solution 2, form mastic 1;
F) get the good cation guar gum of previous swelling, sodium alginate joins in the mastic 1, and adds 4-18ml glycerol, stirs, and forms mastic 2;
G) take by weighing disodiumedetate 0.01-1.2g, methyl hydroxybenzoate 0.01-1mg, ethyl hydroxybenzoate 0.01-1mg, adding 1-12ml propylene glycol, heating makes its dissolving, as solution 3, solution 3, the remaining distilled water of 5% vitamin C injection 3-14ml, pearling agent 0.5-3.5g are added in the mastic 2, and stirring gets final product.
Various compositions among the present invention are as follows:
The Fructus Sapindi Mukouossi fruit itself adds water just can produce natural foam, so be widely used in early days the cleaning aspect, dies down because of the convenience of chemical products afterwards.In the time of in ancient times, if people's skin of family grows the dermatosiss such as fish unicorn tinea, erythema, chronic eczema, patient's household just uses the fruit of Fructus Sapindi Mukouossi, adds water rubbing patient's skin.Compendium of Material Medica is recorded and narrated: the Fructus Sapindi Mukouossi hair washing can go wind to make eye bright, and makes the hair light submissive, washes one's face and can brighten speckle.Fructus Sapindi Mukouossi is that single memorial is used for the plant wash one's face in the Compendium of Material Medica.Modern scientific research shows, the contained sapindoside of Fructus Sapindi Mukouossi is a kind of good natural surfactant.It has skin expansion surface blood capillary, accelerates the effect of blood flow.Can make " natural nuisance-free abluent ", be used for daily washing-tableware cleaning, beauty treatment, hair washing, skin care.
The Fructus Sapindi Mukouossi fruit contains natural clean rhzomorph, penetration is strong, massaging scalp during by hair washing, through root of hair, the nutritional labelings such as the aminoacid that allows root of hair absorb to be carried by Fructus Sapindi Mukouossi extraction elite and the multiple hair care factor, and then deep layer hair nutrition supplementing and moisture content, gentle nursing scalp reaches the hair care and nourishing effect.Unique Fructus Sapindi Mukouossi soap lye contains evergreen Teng, Folium Symplocoris Caudatae and vitamin C, arabinose etc. to anti-bacteria, and problem dandruff, alopecia are very powerful, for hair increases moisture content and moist, hair is more easily arranged, and replys beautiful submissive.
The Salix babylonica L. branch can wind-dispelling heat-dissipating clearing away heat-damp and promoting diuresis rash solution pox.The modern medicine study confirmation, willow is rich in the materials such as tannin, salicylic acid and bigcatkin willow glucosides, can be used for treating disease.The traditional Chinese medical science thinks, willow (branch and leaf, root bark, fibrous root, bark, Flos Salicis Babylonicae, Semen Salicis babylonicae cum pilus) is cold in nature, and the function of heat-clearing and toxic substances removing, expelling wind and removing dampness is arranged." this sketch of the southern regions of the Yunnan Province is said " said: " cure mainly the blood clotting stagnation of QI, the exterior tightened by pathogenic windcold; Children's's variola has Aconitum carmichjaelii Debx. to fall into the top, and slurry can not rise the person, decoction or bathe it." Compendium of Material Medica says: " decoction, the pox of harnessing the Yellow River, nebulousurine; Wine boils, and presses all pains swollen, removes wind, alleviating pain and detumescence." " must join book on Chinese herbal medicine " say: " go wind heat, except arthralgia chiefly caused by damp pathogen." the Salix babylonica L. branch contains natural β-hydroxyamino acid, can allow the keratinization thromboembolism around the pore be easy to come off, and unobstructed follicular canal, prevents that effectively pore from blocking.Salicylic acid is plant Ramulus Salicis Babylonicae and extract of willow bark, is a kind of natural antibiotic medicine.Salicylic acid has outstanding " exfoliation, unclogging " ability, and is safe, and lower than fruit acid to the stimulation of skin.Contain the mild antibiotic composition, continue to alleviate itching of scalp, rubescent.
Flos Campsis has promoting blood circulation to remove blood stasis, cooling blood, expelling wind, the effect for the treatment of skin pruritus.In Shennong's Herbal, formally record and reach the clouds.Its flower, stem, leaf, root all can be used as medicine." Kaibao Bencao " thinks that the stem of reaching the clouds can treat the rubella pruritus.Flos Campsis has again the function of cooling blood, expelling wind, is applicable to the blood hot air wind producing, whole body pruritus.The Flos Campsis external can be treated skin eczema, often cooperates with Rhizoma Coptidis, Alumen, Realgar, and pulverization is mixed well with vinegar, the external application affected part.Flos Campsis extract joins in the hair shampoo article, and mild scalp itch plays the effect of itch-stopping bactericidal, and its composition of invigorating blood circulation nourishes scalp fully, promotes new growth, and it is close that life-time service can make hair thicken.
Folium Hibisci is cool in nature, and is nontoxic, and the merit of heat clearing away, dampness removing, removing heat from blood is arranged, and can control scabies, the diseases such as furuncle furuncle and phyma.After Folium Hibisci is cleaned, soak with clear water, rub out contained glue juice, be used for hair washing, the greasy dirt that deoils,, dandruff, stopping head itching, natural hair conditioner, prevent alopecia, bifurcated and the dandruff, prevention poliosis, additional issue, regulate the fat secretion of scalp, can make scalp, make hair submissive, bright, salubrious, high resilience.
Herba Menthae is hot cold sweating antipyretic medicine, and the anti-dandruff factor of Herba Menthae has anti-inflammation and sterilization, decomposes the lipid effect, effectively improves the puzzlement of dandruff and scalp pruritus, establishment dandruff, head pruritus.External can be controlled skin pruritus, erythra and eczema etc., can nurse one's health skin unclean, that block, and it has refrigerant sensation, can shrink blood capillary, gets rid of vivotoxin, improve eczema, tinea, releive itch, inflammation and burning, soft skin is of value to the oiliness hair quality.Hair follicle resists hair follicle aging clearly thoroughly, and reparation, nourishing, protection dry hair make hair and scalp be full of healthy vigor, and fragrant with Herba Menthae, refreshment makes healthy hair pleasant elegant, the brand-new experience that brings submissive easy comb.Herba Menthae also has the anti-inflammatory analgetic effect, is applicable to hair antipruritic.
Seed of Camelliasinensis(L.)Ktzel oil has another name called Camellia oil, Oleum Camelliae, tea tree oil, Oleum Camelliae.Camellia oil breath delicate fragrance, local flavor is peculiar, have saying of " east olive oil ", fatty acid composition and the olive oil of finding Oleum Camelliae look like especially, linoleic content is more than 80%, the Oleum Camelliae unsaturated fatty acid content easily is absorbed by the body up to 90%, can also promote simultaneously human body to the absorption of the trace element such as fat-soluble fiber and calcium, ferrum, zinc.Also contain in the olive oil unexistent bioactive substance such as camellin, Tsubaki-saponin, tea polyphenols etc. in the Camellia oil.The natural tea tree oil nature is gentle, can replenish the scalp skin nutrition, promotes hair growth, sterilizing and itch-relieving, and scalp is fuel-displaced to treating, dermatitis, eczema and the dandruff have obvious effect, can nurse one's health oily skin, is very effective antibiotic anti-dandruff product.Be significantly improved repairing tool after skin scalp itch, dry and cracked, eczema, the solarization, cleaning capacity is strong, makes the scalp skin keep salubrious, and is healthy comfortable.
Cation guar gum plays good foaming, steady bubble effect, antistatic property, and thickening power in hair shampoo article.In addition, can also improve the wet comb of hair and do comb property, make hair keep for a long time gloss, softness, flexible, reduce detergent to the zest of skin.
Sodium alginate plays good thickening power in hair shampoo article, antistatic property, and steady bubble effect.In addition, can also improve the moisture retention of hair, make the long-term maintenance of hair submissive.Thickening agent and wetting agent common in the hair shampoo article.
Added a large amount of extracted form natural plant compositions in this shampoo paste prescription.Reduce growing of antibacterial fungus by cleaning scalp and hair-care and control head skin beauty water oil balance on the one hand.Salicylic acid in the Salix babylonica L. branch, the compositions such as Saponin in the Fructus Sapindi Mukouossi be cleaning-nursing scalp and hair well, and the gentle injury skin that is difficult for of quality, activity extract in Folium Hibisci, the tea tree oil is the fat secretion of scalable scalp also, makes scalp keep for a long time water oil poised state.
Reach effect anti-dandruff and the alleviation head pruritus by anti-inflammation again on the other hand.All contain natural clean rhzomorph in Fructus Sapindi Mukouossi, tea tree oil and the Salix babylonica L. branch, can kill head fungus antibacterial.All contain the antiinflammatory composition in Flos Campsis, Folium Hibisci, the Herba Menthae, can alleviate the bacterial scalp itch symptom of fungus.Particularly Folium Menthae extract brings refrigerant pleasant sensation during hair washing.
In these natural extracts that add, also have a large amount of nourishing hair care ingredients and multiple important trace element, effective cleaning, anti-dandruff in, also can accelerate the scalp metabolism, promote new growth, make root of hair strong not easily broken, hair is shiny black submissive.
In a word, but growing of this shampoo paste anti-bacteria fungus, the water oil balance of regulation and control skin of head reaches the anti-dandruff effect of cleaning, can replenish the required nutrition of hair scalp, moisture, prevent alopecia, bifurcated and fungus grow, and can improve the scalp blood circulation, enhance metabolism, make root of hair strong, healthy hair is dense submissive.
The made shampoo paste of the present invention is creamy white, and viscosity is suitable, and foam is smooth abundant, and evenly fine and smooth, stretchability is good, cool and comfortable, good stability, abnormal smells from the patient fragrance.
The specific embodiment
The present invention will be further described below in conjunction with embodiment.
Oleum Camelliae of the present invention, pearling agent are commercially available.
Embodiment 1
1.1 the preparation of Fructus Sapindi Mukouossi extract
Take by weighing Fructus Sapindi Mukouossi 200g, soak 0.5h after pulverizing, decoct in 90-100 ℃ of heating and extract 3 times, add 8 times of water gagings the 1st time, extract 2h, add 6 times of water gagings the 2nd time, extract 1h, add 4 times of water gagings the 3rd time, extract 0.5h, each with 3 layers of gauzes filtration, it is stand-by that merging filtrate, the volume of filtrate are concentrated into 4 times (g/ml) of Fructus Sapindi Mukouossi weight.
1.2 the preparation of Salix babylonica L. branch extracting solution
Take by weighing Salix babylonica L. branch 100g, soak 0.5h, decoct in 90-100 ℃ of heating and extract, extract 3 times, add 8 times of water yields the 1st time, extract 1.5h, 6 times of water yields of the 2nd usefulness, extract 1.5h, 4 times of water yields of the 3rd usefulness are extracted 1h, filter with double gauze at every turn, merging filtrate, the volume of filtrate are concentrated into 3 times (g/ml) of Salix babylonica L. branch weight, and be stand-by.
1.3 the preparation of Flos Campsis extracting solution
Take by weighing Flos Campsis 50g, decoct extraction 3 times in 90-100 ℃ of heating, 8 times of water yields of the 1st usefulness are extracted 1h, 6 times of water yields of the 2nd usefulness, extract 1h, 4 times of water yields of the 3rd usefulness are extracted 0.5h, filter with double gauze at every turn, the filtrate of extracting merges, and it is stand-by that the volume of filtrate is concentrated into 3 times (g/ml) of Flos Campsis weight.
1.4 the preparation of Folium Hibisci extracting solution
Take by weighing Folium Hibisci 60g, decoct in 90-100 ℃ of heating and extract 3 times, 8 times of water yields of the 1st usefulness are extracted 1h, 6 times of water yields of the 2nd usefulness are extracted 1h, 4 times of water yields of the 3rd usefulness, extract 0.5h, extracting solution merges with double gauze and filters, and it is stand-by that the volume of filtrate is concentrated into 4 times (g/ml) of Folium Hibisci weight.
1.5 the preparation of Herba Menthae extracting solution
Take by weighing Herba Menthae 50g, put in the round-bottomed flask, and add 9 times distilled water, be positioned in the electric jacket, after 5 hours, be cooled to room temperature with the volatile oil extractor reflux, extract,, filter extracting solution with double gauze, stand-by.
1.6 the preparation of shampoo paste
A) take by weighing cation guar gum 4g, join in the distilled water of 100ml, the limit edged stirs in being heated to 60 ℃ water-bath, to be mixed evenly after, leave standstill, allow its abundant swelling.
B) take by weighing sodium alginate 0.5g, join in the beaker that the 80ml distilled water is housed, 60 ℃ of heating in water bath, the limit heating edge stirs with glass plate, after dissolving, leaves standstill, and allows its abundant swelling.
C) take by weighing respectively K12 6g, sodium sarcosinate 8g, CAB 7g, MES9g, AES 8g, 22SB 6g, distilled water 50g in beaker 1, place 60 ℃ of thermostat water baths to stir the 40min dissolving, be placed on the water-bath after the dissolving fully, stand-by, as solution 1.
D) take by weighing respectively Fructus Sapindi Mukouossi extracting solution 9g, Salix babylonica L. branch extracting solution 10g, Flos Campsis extracting solution 8g, Flos Hibisci extracting solution 7g, Herba Menthae extracting solution 10g and place beaker, and stir 5min, as solution 2.
E) measure Oleum Camelliae 10ml in mortar, take by weighing again arabic gum 3.0g, tragacanth 2.2g places mortar, after grinding 10min and making it evenly, add the 10ml distilled water, grind rapidly in the same direction, until hear flip-flop (being that colostrum forms), add inward again the 10ml distilled water, after grinding evenly, solution 1 is joined in the mortar, continue to grind 10min, until grind evenly, until grind evenly, more ground emulsion is added in the solution 2, form mastic 1;
F) get previous a) and b) in the good cation guar gum of swelling, sodium alginate joins in the mastic 1, and adds 15ml glycerol, stirs with blender to make it even, forms mastic 2.
G) take by weighing disodiumedetate 0.05g, Metagin, each 0.05g of ethyl ester, add the 8ml propylene glycol, heating makes its dissolving, puts into beaker after dissolving, as solution 3, with solution 3,5% vitamin C injection 11ml, remaining distilled water, pearling agent 0.6g joins in the mastic 2, stirs 30min with blender and makes it even, namely gets refrigerant anti-dandruff nourishing shampoo paste.
Embodiment 2
2.1 the preparation of Fructus Sapindi Mukouossi extract
Take by weighing Fructus Sapindi Mukouossi 100g, soak 0.5h after pulverizing, decoct in the 90-100 heating and extract 3 times, add 9 times of water gagings the 1st time, extract 2h, add 7 times of water gagings the 2nd time, extract 1h, add 4 times of water gagings the 3rd time, extract 0.5h, each with 3 layers of gauzes filtration, it is stand-by that merging filtrate, the volume of filtrate are concentrated into 3 times (g/ml) of Fructus Sapindi Mukouossi weight.
2.2 the preparation of Salix babylonica L. branch extracting solution
Take by weighing Salix babylonica L. branch 80g, extract 3 times, decoct in the 90-100 heating and extract 3 times, add 7 times of water yields the 1st time, extract 1.5h, 6 times of the 2nd usefulness are extracted 1.5h, the water yield, 3 times of water yields of the 3rd usefulness are extracted 1h, filter with double gauze at every turn, it is stand-by that merging filtrate, the volume of filtrate are concentrated into 4 times (g/ml) of Salix babylonica L. branch weight.
2.3 the preparation of Flos Campsis extracting solution
Take by weighing Flos Campsis 60g, extract 3 times, decoct in the 90-100 heating and extract 9 times of water yields of the 1st usefulness 3 times, extract 1h, 6 times of water yields of the 2nd usefulness are extracted 1h, 4 times of water yields of the 3rd usefulness, extract 0.5h, filter with double gauze, the filtrate of extraction merges at every turn, and it is stand-by that the volume of filtrate is concentrated into 4 times (g/ml) of Flos Campsis weight.
2.4 the preparation of Folium Hibisci extracting solution
Take by weighing Folium Hibisci 50g, extract 3 times, decoct extraction 3 times in the 90-100 heating, 7 times of water yields of the 1st usefulness are extracted 1h, 6 times of water yields of the 2nd usefulness, extract 1h, 4 times of water yields of the 3rd usefulness are extracted 0.5h, extracting solution merges with double gauze and filters, and it is stand-by that the volume of filtrate is concentrated into 4 times (g/ml) of Folium Hibisci weight.
2.5 the preparation of Herba Menthae extracting solution
Take by weighing Herba Menthae 50g, put in the round-bottomed flask, and add 9 times distilled water, be positioned in the electric jacket, after 5.5 hours, be cooled to room temperature with the volatile oil extractor reflux, extract,, filter extracting solution with double gauze, stand-by.
2.6 the preparation of shampoo paste
A) take by weighing cation guar gum 2g, join in the distilled water of 100ml, the limit edged stirs in being heated to 70 ℃ water-bath, to be mixed evenly after, leave standstill, allow its abundant swelling.
B) take by weighing sodium alginate 2.5g, join in the beaker that the 100ml distilled water is housed, 80 ℃ of heating in water bath limit heating edge stir with glass plate, after dissolving, leave standstill, and allow its abundant swelling.
C) take by weighing respectively K
1210g, sodium sarcosinate 6g, CAB 8g, MES 6g, AES7g, 22SB 7g, distilled water 60g place 70 ℃ of thermostat water baths to stir the 30min dissolving in beaker 1, are placed on the water-bath after the dissolving fully, and be stand-by, as solution 1.
D) take by weighing respectively Fructus Sapindi Mukouossi extracting solution 12g, Salix babylonica L. branch extracting solution 10g, Flos Campsis extracting solution 6g, Flos Hibisci extracting solution 8g, Herba Menthae extracting solution 12g and place beaker, and stir 10min, as solution 2.
E) measure Oleum Camelliae 9ml in mortar, take by weighing again arabic gum 2.5g, tragacanth 0.8g places mortar, after grinding 5min and making it evenly, add the 10ml distilled water, grind rapidly in the same direction, until hear flip-flop (being that colostrum forms), add inward again the 10ml distilled water, after grinding evenly, solution 1 is joined in the mortar, continue to grind 5min, until grind evenly, again ground emulsion is added in the solution 2, form mastic 1;
F) get previous a) and b) in good cation guar gum, the sodium alginate of swelling join in the mastic 1, and add 15ml glycerol, stir with blender and make it even, form mastic 2.
G) take by weighing disodiumedetate 0.03g, methyl hydroxybenzoate 0.01g, ethyl hydroxybenzoate 0.053g, add the 10ml propylene glycol, heating makes its dissolving, after dissolving, put into beaker, as solution 3, with solution 3,5% vitamin C injection 14ml, remaining distilled water, pearling agent 0.6g joins in the mastic 2, stir 20min with blender and make it even, namely get refrigerant anti-dandruff nourishing shampoo paste.
Embodiment 3:
Embodiment 1,2 physical and chemical index are as follows:
3.1 character
This product is that viscosity is suitable, and foam is smooth abundant, and is evenly fine and smooth, the milky shampoo paste that stretchability is good.
3.2 pH value inspection
PH reagent paper with moistening dips a small amount of shampoo paste, and PH is 6-7.
3.3 caloric test
Shampoo paste is packaged in the transparent dressing product bottle, observes without lamination about one week in 4 ℃ refrigerator cold-storages.24h in 55 ℃ calorstat, soap lye is without the phenomenon such as layering emulsifying is spoiled.
3.4 centrifugal test
Shampoo paste is packaged in the centrifugal 20min of 3000r/min in the tool plug test tube, without lamination.
3.5 irritation test, anaphylaxis experiment
The white mice back cuts off hair, smears respectively shampoo pastes by embodiment 1,2 preparations in cutting plucked position, and is not coated with the position and compares, and the result does not have zest and anaphylaxis.
Get embodiment 1 gram and be applied on volunteer (15-65 year, the 380 people) gesture and facial expression, observe after spending 30 minutes, all do not occur rubescent, dermexanthesis, foaming phenomenon.
3.6 room temperature is placed experiment
Embodiment 1,2 made shampoo pastes are placed bottle for cosmetics, and room temperature leaves standstill investigates 6 months, and without lamination, unchanged with aftersensation, abnormal smells from the patient is unchanged.
3.7 anti-dandruff effect
Choose volunteer (15-65 year, 380 people), prepared shampoo paste is used for volunteer's hair, mix and repeatedly wash by rubbing with the hands with a small amount of water, find that foam is abundant, volunteers generally feels to slide suitable comfortable, and feel is better.No matter hair does comb should be wet comb property all.After washing, the submissive as silk of hair, fluffy non-greasy, moistening effect is better, washes afterwards without the scalp pruritus phenomenon, and need not use hair conditioner.Through one month continuous use, hair was obviously glossy, softness, and dandruff phenomenon obviously reduces.
Embodiment 4:
This shampoo paste resultant effect is investigated
Below utilize and try out the effect of feeling to come the shampoo paste that Evaluation operation example 1,2 produces.Adopt the public-opinion poll point system, the women who chooses 80 25-50 year age bracket is object on probation, is divided into arbitrarily two groups, respectively with the shampoo paste wash my hairs of embodiment 1,2 preparations.Use weekly twice, be two months service time.Every result of use total points is 5 minutes: 5 are divided into best result, represent fine, very satisfied; 4 are divided into better; 3 are divided into and can accept; Be bad below 3 minutes, can not accept.It below is every average.The results are shown in Table 1:
Table 1 resultant effect is investigated
| Result of use | Embodiment 1 every average | Embodiment 2 every averages |
| Moisture retention | 4.8 | 4.9 |
| Nourishing property | 4.7 | 4.8 |
| Refrigerant property | 5 | 5 |
| Foaming characteristic | 5 | 5 |
| Soil release characteristics | 5 | 5 |
| Do comb property | 4.9 | 4.9 |
| Wet comb property | 4.9 | 4.9 |
| Relieving itching and removing dandruff | 4.7 | 4.6 |
| Compliance | 4.8 | 4.9 |
In sum, this made shampoo paste foam of the present invention enriches, and good soil release characteristics, moisture retention, nourishing are arranged, and feels refrigerant comfortable during use, and is good with rear hair elasticity, and the effect of hair washing, hair care, hair care, relieving itching and removing dandruff is arranged.
Claims (8)
1. refrigerant anti-dandruff nourishing health hair washing cream is characterized in that: contain following material and weight portion in the 174g bath foam:
2. a kind of refrigerant anti-dandruff nourishing health hair washing cream according to claim 1, it is characterized in that: described Fructus Sapindi Mukouossi extract is to prepare by the following method:
Take by weighing Fructus Sapindi Mukouossi an amount of, soak 0.15-0.8h after pulverizing, decoct in 90-100 ℃ of heating and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging, extract 0.5-1.5h for the 2nd time, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times (g/ml) of Fructus Sapindi Mukouossi weight, filters and get final product.
3. a kind of refrigerant anti-dandruff nourishing health hair washing cream according to claim 1, it is characterized in that: described Salix babylonica L. branch extracting solution prepares by the following method:
Take by weighing the Salix babylonica L. branch an amount of, soak 0.15-0.8h, decoct in 90-100 ℃ of heating and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging, extract 0.5-1.5h for the 2nd time, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times (g/ml) of Salix babylonica L. branch weight, filters and get final product.
4. a kind of refrigerant anti-dandruff nourishing health hair washing cream according to claim 1, it is characterized in that: described Flos Campsis extracting solution prepares by the following method:
Take by weighing Flos Campsis an amount of, soak 0.15-0.8h, decoct in 90-100 ℃ of heating and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging, extract 0.5-1.5h for the 2nd time, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times (g/ml) of Flos Campsis weight, filters and get final product.
5. a kind of refrigerant anti-dandruff nourishing health hair washing cream according to claim 1, it is characterized in that: described Herba Menthae extracting solution prepares by the following method:
Take by weighing Herba Menthae a certain amount of, and add 8-12 distilled water doubly, be positioned in the electric jacket, after 5-6 hour, be cooled to room temperature with the volatile oil extractor reflux, extract,, filter with double gauze, get final product.
6. a kind of refrigerant anti-dandruff nourishing health hair washing cream according to claim 1, it is characterized in that: described Folium Hibisci extracting solution prepares by the following method:
Take by weighing Folium Hibisci an amount of, soak 0.15-0.8h, decoct in 90-100 ℃ of heating and extract 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging, extract 0.5-1.5h for the 2nd time, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume of filtrate is concentrated into 3-6 times (g/ml) of Folium Hibisci weight, filters to get final product.
7. a kind of refrigerant anti-dandruff nourishing health hair washing cream according to claim 1, it is characterized in that: described essence is rose essence, peach flavor, flavoring pineapple essence, Fructus Citri Limoniae essence, green cucumber essence, jasmin essence, osmanthus flower fragrance.
8. the preparation method of a kind of refrigerant anti-dandruff nourishing health hair washing cream claimed in claim 1 is characterized in that:
A) take by weighing cation guar gum 0.1-4g, join in the distilled water of 50-100ml, 60-80 ℃ of heating in water bath heats while stirring, to be mixed evenly after, leave standstill and allow its abundant swelling, stand-by;
B) take by weighing sodium alginate 0.5-5g, be heated to 60-80 ℃, heat while stirring, behind the mix homogeneously, leave standstill and allow its abundant swelling, stand-by;
C) take by weighing respectively K
124-24g, sodium sarcosinate 3-8g, CAB 3-8g, MES 3-8g, AES 3-8g, 22SB 2-8g, distilled water 30-80ml, in 60-90 ℃ of stirring and dissolving, as solution 1, stand-by;
D) take by weighing respectively Fructus Sapindi Mukouossi extracting solution 1-16g, Salix babylonica L. branch extracting solution 0.5-10g, Flos Campsis extracting solution 0.4-8g, Flos Hibisci extracting solution 0.4-8g, Herba Menthae extracting solution 1-16g, stir, as solution 2;
E) measure Oleum Camelliae 6-17ml in mortar, take by weighing again gum arabic powder 0.8-6g, Calculus Bovis from Northwest of China natural gum over sixty years of age powder 0.1-5g and place mortar, grind evenly after, add the 2-10ml distilled water, grind rapidly in the same direction, until be that colostrum forms, add inward again the 2-10ml distilled water, after grinding evenly, solution 1 is joined in the mortar, continue to grind, until grind evenly, again ground emulsion is added in the solution 2, form mastic 1;
F) get the good cation guar gum of previous swelling, sodium alginate joins in the mastic 1, and adds 4-18ml glycerol, stirs, and forms mastic 2;
G) take by weighing disodiumedetate 0.01-1.2g, methyl hydroxybenzoate 0.01-1mg, ethyl hydroxybenzoate 0.01-1mg, adding 1-12ml propylene glycol, heating makes its dissolving, as solution 3, solution 3, the remaining distilled water of 5% vitamin C injection 3-14ml, pearling agent 0.5-3.5g are added in the mastic 2, and stirring gets final product.
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| CN103479539A (en) * | 2013-08-16 | 2014-01-01 | 广州环亚化妆品科技有限公司 | Shampoo containing natural saponin and natural thickener |
| CN104146931A (en) * | 2014-08-29 | 2014-11-19 | 皖南医学院 | Natural nourishment and maintenance type hair conditioner and preparation method thereof |
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| CN102247309A (en) * | 2010-05-21 | 2011-11-23 | 吴苏 | Shampoo with a mint tea fragrance, and preparation method thereof |
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| CN103479539A (en) * | 2013-08-16 | 2014-01-01 | 广州环亚化妆品科技有限公司 | Shampoo containing natural saponin and natural thickener |
| CN103479539B (en) * | 2013-08-16 | 2016-01-27 | 广州环亚化妆品科技有限公司 | A kind of shampoo containing saponin and natural thickener |
| CN104146931A (en) * | 2014-08-29 | 2014-11-19 | 皖南医学院 | Natural nourishment and maintenance type hair conditioner and preparation method thereof |
| CN106999391A (en) * | 2014-12-15 | 2017-08-01 | 大塚制药株式会社 | Cleaning products |
| CN104434698A (en) * | 2014-12-16 | 2015-03-25 | 皖南医学院 | Anti-static and anti-radiation shampoo paste and preparation method thereof |
| CN104434698B (en) * | 2014-12-16 | 2018-02-09 | 皖南医学院 | A kind of antistatic, radiation proof hair cream and preparation method thereof |
| CN104721124A (en) * | 2015-04-13 | 2015-06-24 | 王国华 | Hibiscus shampoo |
| CN105662970A (en) * | 2016-03-04 | 2016-06-15 | 皖南医学院 | Emulsion capable of nourishing hair roots and removing oil and dandruff and preparation method thereof |
| CN105662970B (en) * | 2016-03-04 | 2018-08-21 | 皖南医学院 | A kind of nourishing root of hair deoils anti-dandruff lotion and preparation method thereof |
| CN107308057A (en) * | 2017-07-24 | 2017-11-03 | 皖南医学院 | A kind of submissive nourishing hair and nontoxic soft hair cream and preparation method thereof |
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| CN109380851A (en) * | 2018-12-15 | 2019-02-26 | 邝春燕 | A kind of medical hair-washing hat suit of Chinese medicine |
| CN112656724A (en) * | 2020-12-29 | 2021-04-16 | 娇时日化（杭州）股份有限公司 | Shampoo and preparation method thereof |
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