Summary of the invention
For above-mentioned the deficiencies in the prior art, the invention provides a kind of antistatic, radioprotective hair cream and preparation method thereof, overcome hair to be tanned severely, can not get hair care, breakage, fracture, bifurcated, a withered and yellow difficult problem occur, and there is antibacterial, anti-dandruff, anticreep, antistatic, radiation-resistant effect.
For achieving the above object, the invention provides a kind of antistatic, radioprotective hair cream, state in shampoo paste and contain following material and content thereof:
As further improvement, also containing golden yellow Jojoba oil 1-5g, Herba Ecliptae extracting solution 1-3ml in described hair cream.This hair cream can not only hair conditioning further, also has the effect of black hair.
Here can add essence according to different demands, described essence is one or more in green cucumber essence, rose essence, osmanthus flower fragrance, peach flavor, Fructus Citri Limoniae essence, flavoring pineapple essence, jasmin essence.
Described antistatic, radioprotective hair cream preparation method, comprise the steps:
Step one: take 0.1-1g ice crystal forming agent AVC, be dissolved in the water of 30-100ml, stir, leaves standstill 2-3h, treats its naturally swelling dissolving, obtain gel A;
Step 2: take cation guar gum 1-2g, is dissolved in the water of 30-100ml, stirs, and continues to be stirred to dissolving in 70-90 DEG C of water-bath, cools 30min under room temperature, obtains conditioner B;
Step 3: take Semen Tritici aestivi germ oil 2-10g, shea butter 1-5g, Oleum Cocois 1-5g, stearic acid 0.1-1g, liquid crystal type be placed in beaker from thickener/emulsifier Lipomulse LUXE 2-3g, water-bath 70-90 DEG C of heating is oil phase;
Step 4: take distilled water 10-25g, water-bath 70-90 DEG C of heating is aqueous phase;
Aqueous phase, when aqueous phase, oil phase reach identical temperature, is that thread shape adds in oil phase by step 5: wait oil phase clear, and limit edged stirs, and forms emulsion bases C;
Step 6: take distilled water 10-30g, add polyoxyethylenated alcohol sodium sulfate 1-5g, Dutch sodium lactate 2-10g, cocamidopropyl betaine CAB 1-5g, alkyl polyglucoside APG 1-5g, sodium lauroyl sarcosine LS301-5g, water solublity Ve 0.1-1g, trehalose 1-2g, polyquaternary ammonium salt 1-5g, biological polyoses glue FUCOGEL 1.5P 1-5g, sodium lauryl sulphate 0.1-3g, sodium chloride 0.1-3g, stirring and dissolving, obtains solution D;
Step 7: add Fructus Sapindi Mukouossi extracting solution 1-5g, Herba Menthae extracting solution 1-5g in emulsion bases C, be uniformly mixed, then add gel A, conditioner B, solution D, be uniformly mixed;
Step 8: take disodiumedetate 0.01-0.05g, ethyl hydroxybenzoate or sorbic acid 0.1-0.3g, add distilled water 5-18ml, heating makes it dissolve, add in step 7 system, add essence 0.05-0.3ml again, with 20% citric acid solution 0.1-3ml, adjust ph is after 6.5-7.5, stirs 10-15min, mix homogeneously, obtains antistatic, radioprotective hair cream.
Described soapberry extract is prepared by the following method: get the Fructus Sapindi Mukouossi peelling off kernel, soaks 0.15-1h, is heated to 90-100 DEG C, decoct extraction 3 times, add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging 2nd time, extract 0.5-1.5h, add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, each filtration, merging filtrate, the volume concentration of filtrate, to 3-6 times of g/ml of Fructus Sapindi Mukouossi weight, filters and get final product.
Described Herba Menthae extracting solution is prepared by the following method: get Herba Menthae and soak 0.5-1h, reflux, extract, 3 times, adds 10-15 times of water gaging the 1st time, extract 0.5-2h, add 8-12 times of water gaging the 2nd time, extract 0.5-1.5h, add 6-10 times of water gaging 3rd time, extract 0.5-1.5h, filter at every turn, merging filtrate, the volume concentration of filtrate, to 4-7 times of g/ml of Herba Menthae weight, adds liquid weight 1%-5% active carbon, and 60-100 DEG C of heating in water bath stirs, sucking filtration, gets filtrate.
The golden yellow Jojoba oil having 1-5 weight portion is also added in described step step 3.
The Herba Ecliptae extracting solution having 1-5 weight portion is also added in described step 7.Described Herba Ecliptae extracting solution is prepared by the following method: get Herba Ecliptae, reflux, extract, 2 times, add the 10-18 times of water yield 1st time, extract 0.5-1.5h, by the 10-12 times of water yield, extract 0.5-1.5h the 2nd time, each use 3 layers of gauze filter, merging filtrate, heating is concentrated into 2-10 times of g/ml of Herba Ecliptae weight, filters and get final product.
Various compositions in the present invention are as follows:
Fructus Sapindi Mukouossi is also named fruit of washing one's hands.Containing triterpene saponin such as sapindosides in its peel.Record in Compendium of Material Medica: Fructus Sapindi Mukouossi fruit contains natural clean rhzomorph.That Chinese traditional natural is washed and protect precious fruit since ancient times.It has body of not hurting sb.'s feelings, not the characteristic of polluted source.Fructus Sapindi Mukouossi also has effect that is antibacterial, anti-dandruff, anticreep.
Herba Ecliptae has nourishing the liver and kidney, crow palpus teeth consolidating, effect of cooling blood for hemostasis.Smash juice painting eyebrow to send out, can promote hair growth, for oral administration have black hair, hair color effect." the southern regions of the Yunnan Province book on Chinese herbal medicine " carries, Herba Ecliptae " teeth consolidating, black hair wash nine kinds of hemorrhoid ".Compendium of Material Medica is pointed out, Herba Ecliptae " black beard and hair, kidney tonifying is cloudy ".Herba Ecliptae controls early whitening of beard and hair, eyebrow moustache comes off.
Herba Menthae contains the materials such as volatile oil, peppermint essence and tannin, and contributing to smoothing indignation, the negative emotions such as dejected, is allaying tiredness, relieving stress, dispassionate soul tonic.Herba Menthae has refrigerant sensation, can be antibacterial, antibacterial, antipruritic.
Semen Tritici aestivi germ oil is rich in various nutrition; easily be absorbed by the body; there is suppression free radical; antioxidation, delay body aging, Cell protection film, promote skin metabolism; improve body immunity, strengthen anti-cancer, anticancer and blood circulation promoting effect; also have moisturizing, skin is moistened, improve looks, retain youth, make women's skin become soft and moist and the effects such as high resilience.Extremely helpful to moist dry hair quality, maintenance scalp, be applicable to various skin quality, have certain effect to chronic eczema, eczema, also there is sun-screening function, can be used for health, hair sun-proof.
Golden yellow Jojoba oil has good permeability, and the oils and fats of molecules align and people is very similar, is that stability is high, the special good base oil of ductility, coarse hair quality can be improved, the optimum selection of Hair grooming oil, can prevent hair tan severely, soft hair, contribute to hair pitch-black, prevention bifurcated.Another characteristic of Jojoba oil is its hydrophilic, and skin being had to the function regulating moisture, is the natural keep-fit composition of a kind of very perfect skin protection and hair care.
Cation guar gum can provide excellent conditioning performance to hair products, has good foaming, steady bubble, antistatic property, reduces dry, the wet comb resistance of hair, improves the wet comb of hair and dry comb property, make hair keep gloss, softness for a long time, high resilience.It can be adsorbed in a mao bar, forms monomolecular adsorbed film, makes hair soft, be rich in gloss and elasticity, and stops generation electrostatic, and combing is very convenient, is a kind of desirable conditioner producing transparent daily chemical products.
Trehalose has excellence, the moisture-retaining capacity of safety and the characteristic of biomacromolecule activity.Hair, under the environment such as high temperature, high and cold, dry, high wind, intensive ultraviolet radiation, very easily dries out, and breakage, fracture, bifurcated, withered and yellow occurs.Trehalose can form the special protecting film of one deck in this case on hair top layer; keep the original nutrition of scalp and moisture; protection hair fiber and hair scale sheet exempt from the injury of dehydration; healthy hair is helped to keep natural structure; therefore it is a kind of wetting agent efficiently, and provides the protective effect of the potential injury of not climate.Trehalose also has the function of being gone out by external heat radiation, thus protection hair is unlikely impaired.Trehalose can suppress the generation of the volatile aldehyde caused due to Fatty acid degradation, can suppress the abnormal flavour caused therefrom.Trehalose has good radioprotective, antistatic effect.
Beneficial effect: the hair cream made by the present invention has effect, salubrious, comfortable, fragrant of good radioprotective, antistatic, hair care hair care, also has the effect of antibacterial bacteriostatic simultaneously, also has effect that is anti-dandruff, antipruritic, anticreep.Cation guar gum has good foaming surely bubble effect, antistatic property, improves the wet comb of hair and dry comb property, makes hair keep gloss, softness for a long time, high resilience.In prescription, composition complements each other, this shampoo paste is made to have good moistening effect, hair can be nourished comprehensively, repair damaged hair, supplement hair follicle desired nutritional, promote hair follicle cell metabolism, hair is nursed one's health from inside to outside comprehensively, hair one is made to comb on earth, smooth soft bright as silk, high resilience.
Detailed description of the invention
Below in conjunction with embodiment, the present invention will be further described.
Golden yellow Jojoba oil of the present invention, Semen Tritici aestivi germ oil, Oleum Cocois are commercially available.
Embodiment 1
The present embodiment antistatic, radioprotective hair cream obtain as follows:
Step one: take 0.5g ice crystal forming agent AVC, be dissolved in the water of 100ml, stir, leaves standstill 2h, treats its naturally swelling dissolving, obtain gel A;
Step 2: take cation guar gum 2g, is dissolved in the water of 100ml, stirs, and continues to be stirred to dissolving in 80 DEG C of water-baths, cools 30min under room temperature, obtains conditioner B;
Step 3: take Semen Tritici aestivi germ oil 2g, shea butter 1.5g, Oleum Cocois 1g, stearic acid 0.5g, liquid crystal type be placed in beaker from thickener/emulsifier Lipomulse LUXE 2g, water-bath 80 DEG C heating is oil phase;
Step 4: take distilled water 15g, water-bath 85 DEG C heating is aqueous phase;
Aqueous phase, when aqueous phase, oil phase reach identical temperature, is that thread shape adds in oil phase by step 5: wait oil phase clear, and limit edged stirs, and forms emulsion bases C;
Step 6: take distilled water 10g, add polyoxyethylenated alcohol sodium sulfate 3g, Dutch sodium lactate 3g, cocamidopropyl betaine CAB 2g, alkyl polyglucoside APG 3g, sodium lauroyl sarcosine LS30 2g, water solublity Ve 0.8g, trehalose 1.5g, polyquaternary ammonium salt 2g, biological polyoses glue FUCOGEL 1.5P 1.5gg, sodium lauryl sulphate 0.3g, sodium chloride 0.5g, stirring and dissolving, obtains solution D;
Step 7: add Fructus Sapindi Mukouossi extracting solution 2g, Herba Menthae extracting solution 1.5g in emulsion bases C, be uniformly mixed, then add gel A, conditioner B, solution D, be uniformly mixed;
Step 8: take disodiumedetate 0.02g, ethyl hydroxybenzoate or sorbic acid 0.1g, add distilled water 8ml, heating makes it dissolve, add in step 7 system, add essence 0.05ml again, with 20% citric acid solution 1ml, adjust ph is after 6.8, stirs 10-15min, mix homogeneously, obtains antistatic, radioprotective hair cream.Here can add essence according to different demands, described essence is one or more in green cucumber essence, rose essence, osmanthus flower fragrance, peach flavor, Fructus Citri Limoniae essence, flavoring pineapple essence, jasmin essence.
The wherein preparation of soapberry extract: Fructus Sapindi Mukouossi peels off kernel, takes 40g, then soaks 1h, be heated to 100 DEG C, decoct extraction 3 times, add 9 times of water gagings the 1st time, extract 1.5h, add 9 times of water gagings the 2nd time, extract 1h, add 7 times of water gagings 3rd time, extract 1h, filter, merging filtrate at every turn, the volume concentration of filtrate, to 4 times (g/ml) of Fructus Sapindi Mukouossi weight, filters and get final product.
The wherein preparation of Herba Menthae extracting solution: take Herba Menthae 30g, soaks 1h, reflux, extract, 3 times, add 15 times of water gagings 1st time, extract 1.5h, add 12 times of water gagings the 2nd time, extract 1h, add 9 times of water gagings the 3rd time, extract 1h, each filtration, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Herba Menthae weight, add liquid weight 3% active carbon, 80 DEG C of heating in water bath stir, sucking filtration.
Embodiment 2
The present embodiment and embodiment 1 difference are also to add the golden yellow Jojoba oil having 1.5g in described step step 3, also add the Herba Ecliptae extracting solution having 2g in described step 7.Described Herba Ecliptae extracting solution is prepared by the following method: take Herba Ecliptae 30g, extract 2 times, add 15 times of water yields 1st time, extract 1h, the 2nd use 10 times of water yields, extract 1h, each use 3 layers of gauze filter, merging filtrate, heating is concentrated into 5 times (g/ml) of Herba Ecliptae weight, filters and get final product.
Embodiment 3
The present embodiment antistatic, radioprotective hair cream obtain as follows:
Step one: take 0.8 ice crystal forming agent AVC, be dissolved in 80ml water, stir, standing 2h treats its naturally swelling dissolving;
Step 2: take cation guar gum 1g, is dissolved in 80ml water, stirs, and continues to be stirred to dissolving, cools 30min under room temperature, obtain conditioner B with 80 DEG C of water;
Step 3: take Semen Tritici aestivi germ oil 4g, shea butter 3g, Oleum Cocois 3g, golden yellow Jojoba oil 1.5g, stearic acid 0.5g, liquid crystal type be placed in beaker from thickener/emulsifier Lipomulse LUXE 3g, water-bath 80 DEG C heating is oil phase;
Step 4: take distilled water 20g, water-bath 80 DEG C heating is aqueous phase;
Aqueous phase, when aqueous phase, oil phase reach identical temperature, is that thread shape adds in oil phase by step 5: wait oil phase clear, and limit edged stirs, and forms emulsion bases C;
Step 6: take distilled water 15g, add polyoxyethylenated alcohol sodium sulfate 2g, Dutch sodium lactate 4g, cocamidopropyl betaine CAB 3g, alkyl polyglucoside APG 2g, sodium lauroyl sarcosine LS30 3g, water solublity Ve 0.5g, trehalose 1g, polyquaternary ammonium salt 3g, biological polyoses glue FUCOGEL 1.5P 3g, sodium lauryl sulphate 0.8g, sodium chloride 0.5g, stirring and dissolving, obtains solution D;
Step 7: add Fructus Sapindi Mukouossi extracting solution 3g, Herba Ecliptae extracting solution 3g, Herba Menthae extracting solution 3g in emulsion bases C, be uniformly mixed, then add gel A, conditioner B, solution D, be uniformly mixed;
Step 8: take disodiumedetate 0.04g, ethyl hydroxybenzoate or sorbic acid 0.3g, add distilled water 15ml, heating makes it dissolve, add g) in system, add essence 0.09ml again, with 20% citric acid solution 0.7ml, adjust ph is after 7, stirs 15min, mix homogeneously, obtains antistatic, radioprotective hair cream.Here can add essence according to different demands, described essence is one or more in green cucumber essence, rose essence, osmanthus flower fragrance, peach flavor, Fructus Citri Limoniae essence, flavoring pineapple essence, jasmin essence.
The wherein preparation of soapberry extract: Fructus Sapindi Mukouossi peels off kernel, takes 40g, then soaks 1h, be heated to 100 DEG C, decoct extraction 3 times, add 9 times of water gagings the 1st time, extract 1.5h, add 9 times of water gagings the 2nd time, extract 1h, add 7 times of water gagings 3rd time, extract 1h, filter, merging filtrate at every turn, the volume concentration of filtrate, to 4 times (g/ml) of Fructus Sapindi Mukouossi weight, filters and get final product.
The wherein preparation of Herba Ecliptae extracting solution: take Herba Ecliptae 50g, extracts 2 times, adds 15 times of water yields the 1st time, extracts 1h, 2nd use, 12 times of water yields, extract 1h, filter with 3 layers of gauze at every turn, merging filtrate, heating is concentrated into 5 times (g/ml) of Herba Ecliptae weight, filters and get final product.
The wherein preparation of Herba Menthae extracting solution: take Herba Menthae 30g, soaks 1h, reflux, extract, 3 times, add 15 times of water gagings 1st time, extract 1.5h, add 12 times of water gagings the 2nd time, extract 1h, add 9 times of water gagings the 3rd time, extract 1h, each filtration, merging filtrate, the volume concentration of filtrate is to 6 times (g/ml) of Herba Menthae weight, add liquid weight 3% active carbon, 80 DEG C of heating in water bath stir, sucking filtration.
Physical and chemical index and the result of embodiment 1,2,3 are as follows:
Character: each embodiment is viscosity and is suitable for, foaming abundancy, cool and comfortable, good stability, fragrant, fine and smooth uniform milky hair cream.
Get each embodiment gained hair cream, measure with pH meter, recording pH value is between 6.0-7.0.
Each hair cream is packaged in transparence cosmetic bottle, within one month, observes without lamination in the refrigerator cold-storage of 4 DEG C.24h in the calorstat of 55 DEG C, hair cream is without layering, the phenomenon such as spoiled.
Each hair cream is packaged in 3000r/min in tool plug test tube, centrifugal 20min, without lamination.
By embodiment 1,2,3 made hair creams are placed in bottle for cosmetics, room temperature leaves standstill investigation 6 months, without lamination, with after feel unchanged, abnormal smells from the patient is unchanged.
Irritation test, anaphylaxis are tested
White mice back cuts off hair, smearing the hair cream prepared by embodiment 1,2,3 respectively in cutting plucked position, rubbing foam, then clean with clear water with a small amount of water, and is not coated with position and compares, and result does not have zest and anaphylaxis.
Volunteer's (15-65 year, 150 people) wash hair with hair cream prepared by embodiment 1,2,3, observing after spending 30 minutes, all there is not rubescent, dermexanthesis, foaming phenomena in scalp, there is not dry and astringent, uninteresting phenomenon in hair yet, and in use find that this hair cream is homogeneous, easily go out foam, foam is fine and smooth, easily clean, fragrant, washes rear sensation hair submissive, glossy, high resilience.
Hair cream resultant effect is investigated
Below utilize to try out and feel the effect carrying out the hair cream that Evaluation operation example 1,2,3 produces.Adopt public-opinion poll point system, choose 150 25-65 year age bracket people as object on probation, be divided into arbitrarily three groups, clean hair with the hair cream of embodiment 1,2,3 preparation respectively.Wash hair weekly twice, service time is two months.Every result of use total score is 5 points: 5 be divided into best result, represents better, very satisfaction; 4 are divided into very well; 3 are divided into and can accept; Less than 3 points is bad, can not accept.Be below every average, the results are shown in Table 1:
Table 1 resultant effect is investigated
In sum, this hair cream exquisiteness is soft and smooth, and have alimentary, moisture retention and antistatic effect very well, during use, sensation is very clearly comfortable, easy to clean, and foam exquisiteness is stable.Embodiment 2 is the present invention's more preferably embodiment.
To embodiment 2,3 black hair measure of merit
Choose 100 25-40 year age bracket hair have the people of sallow situation as object on probation, be divided into arbitrarily two groups, before test, first do contrast use by taking pictures and cutting a small amount of hair separately.Then hair is cleaned with hair cream prepared by embodiment 2,3 respectively.Wash hair 3 times weekly, service time is 3 months, and period takes a morsel hair paired observation every other month separately.After off-test, by observing, record experimental result can find out that the sallow situation of the hair of two groups of people all makes moderate progress, and along with the lengthening of service time, pitch-black phenomenon is more obvious.Experiment can find out that this hair cream has the effect of good pitch-black hair thus, and life-time service hair is pitch-black shinny, elegant submissive.
The present invention is not limited to above-described embodiment; do not departing under the present invention's spirit and real situation thereof; those of ordinary skill in the art can make various corresponding change and distortion according to the present invention; these are tackled amendment that the present invention carries out mutually or equivalently to replace, and it all should be encompassed in the middle of the scope of claim of the present invention protection.