CN105853300B

CN105853300B - One kind is deoiled anti-dandruff and itching-relieving moist type shampoo paste and preparation method thereof

Info

Publication number: CN105853300B
Application number: CN201610355425.3A
Authority: CN
Inventors: 孙淑萍; 杨晶晶; 金晓灿; 华旗香; 赵天娇; 张晗; 胡小沣
Original assignee: Wannan Medical College
Current assignee: Shantou Shente Baojie Industrial Co., Ltd.
Priority date: 2016-05-26
Filing date: 2016-05-26
Publication date: 2018-09-04
Anticipated expiration: 2036-05-26
Also published as: CN105853300A

Abstract

The invention discloses a kind of anti-dandruff antipruritic moist type shampoo pastes and preparation method thereof to deoil of Chinese medicine, and the shampoo paste contains：Sodium laureth sulfate, sodium lauroyl glutamate, MES, GOC, EG, watermiscible vitamin E, amino acid surfactant, coix seed extracting solution, lemon juice extracting solution, ginger extract, peppermint extracting solution, Radix Sophorae Flavescentis extractive liquid, Miconazole aqueous solution, zinc pyrithione, climbazole, glycerine, pearling agent, ethylparaben, olive oil, camellia seed oil, cationic melon glue, carbomer gel liquid, sodium carboxymethylcellulose, sodium alginate gel liquid, distilled water, essence.The shampoo paste property of the present invention is mild, safe, and removal hair is greasy, effectively antipruritic, and inhibits the generation of dandruff, and hair nutrient can be supplemented, profit hair is nourished, improves scalp blood circulation, boosts metabolism, strong root of hair, prevents epilation, promotes kainogenesis long, keeps the submissive show of hair bright.

Description

One kind is deoiled anti-dandruff and itching-relieving moist type shampoo paste and preparation method thereof

Technical field

The present invention relates to a kind of shampoo paste, more particularly to one kind is deoiled anti-dandruff and itching-relieving moist type shampoo paste and its preparation side Method.

Background technology

How oily hair improvesEither in the still work gone to school, either man or woman, often go out The fuel-displaced phenomenon of existing hair, causes hair greasy, though just wash soon, then skin of meeting and discussing thinks that one layer of grease has covered again, this Kind feels very bad, and especially student is overstrain one's nerves when learning busy, and hair oil is very serious, washes hair second It will be greasy it is glutinous together, also in harness people pressure of going to work is big, is susceptible to the fuel-displaced serious phenomenon of hair, especially Head is connected with face, and it is greasy sometimes to will appear entire forehead, has small pox, caused by this is also skin greasing, unusual shadow Ring normal life and the mood of many people.

Fuel-displaced hair is any reasonSmegma is immediate cause, it is influenced by male sex hormone, with heredity, life The factors such as custom, environment of living have relationship.

Scalp is equally divided into oiliness, neutrality, dryness as the skin at other positions is on the face, on arm etc..When When we are children, it is not have the skin problems such as fuel-displaced scalp, acne, acne, youth can have been arrived, with male The secretion of hormone begins to " be tangled " by them at leisure.Fuel-displaced scalp is also normal physiological phenomenon, a certain amount of grease It can play a protective role, but secrete excessive just as whelk at irritating problem to skin.In fact, the sebum of scalp Glandular secretion amount be higher than facial skin, even compared with being easiest to fuel-displaced forehead, also almost it more than 2 times.

The white or the grey scales of skin that peel off that dandruff just will appear when being scalp abnormality, are caused by fungal infection, belong to skin Skin disease category.This scales of skin that peel off particle is larger, is attached on scalp surface layer or hair, combs one's hair or easily falls to shoulder when scratching On clothes.

Dandruff Producing reason is also very much：The vigorous people of metabolism is susceptible to dandruff；Overstrain one's nerves, life is not Rule will produce dandruff；Climate change eats that irritating food, excessive drinking of smoking, pressure is excessive etc. can all generate than normal The excessive dandruff ... of people

Whether hair oil is overweight or dandruff is excessive, and many puzzlements can be all brought to life.At this moment it is considered that in Medicine essence, which is dissolved into, washes in hair products, this will be the scientific and technological Development Trend of modern hair care.Using sophisticated technologies, extract in Chinese medicine Essential ingredient, so that active ingredient is come into full contact with healthy hair, go deep into hair follicle, depth oil-control reduces the generation of dandruff, preferably sends out Wave effect.For busy working clan and student race, washing hair products using the anti-dandruff nourishing of deoiling of the essence containing Chinese medicine is Not only the method for science but also simplicity.

Invention content

1st technical problem to be solved by this invention is to provide a kind of new deoiling containing natural component extract Consider antipruritic moist type shampoo paste to be worth doing.

2nd technical problem to be solved by this invention is the preparation method of above-mentioned shampoo paste.

The present invention solves technical problem：One kind is deoiled anti-dandruff and itching-relieving moist type shampoo paste and preparation method thereof, shampoo paste In include following proportionings raw material components：

The Semen Coicis extract is to be prepared by the following method：

It is appropriate to weigh coix seed, 0.15-0.8h is impregnated after crushing, heating decocts extraction 3 times, the 1st time plus 10-18 times and measures Water extracts 0.5-2h, and the 2nd time plus 8-15 times measure water, extracts 0.5-1.5h, measures water the 3rd time plus 8-10 times, extracts 0.5-1.5h, Filtration, the volume concentration of merging filtrate, filtrate are filtered to 3-6 times of g/ml of coix seed weight every time to obtain the final product.

The lemon juice extracting solution is prepared by the following method：

It is appropriate to weigh lemon, 0.15-0.8h is impregnated after incision, heating decocts extraction 3 times, the 1st time plus 8-15 times and measures water, 0.5-2h is extracted, the 2nd time plus 8-10 times measure water, extract 0.5-1.5h, measure water the 3rd time plus 8-10 times, extract 0.5-1.5h, every time Filtration, the volume concentration of merging filtrate, filtrate are filtered to 3-6 times of g/ml of lemon weight to obtain the final product.

The ginger extract is prepared by the following method：

It is appropriate to weigh ginger, thinly slices, with water refluxing extraction 3 times, measures water with 10-18 times for the first time, extracts 0.5- 2.5h, filtering measure water with 8-15 times for the second time, extract 0.5-2.5h, measure water with 6-12 times for the third time, extract 0.5-1.5h, point It does not filter, merging filtrate, the 6-10 times of g/ml for ginger weight is concentrated under reduced pressure, for use.

The peppermint extracting solution is prepared by the following method：

It is a certain amount of to weigh fresh mint, is put into round-bottomed flask, and 10-18 times of distilled water is added, is positioned over electric jacket In, it after 5-6 hour of volatile oil extractor refluxing extraction, is cooled to room temperature, filters extracting solution with double gauze, for use.

The Radix Sophorae Flavescentis extractive liquid is prepared by the following method：

It is appropriate to weigh kuh-seng, 0.15-0.8h is impregnated after crushing, heating decocts extraction 3 times, the 1st time plus 10-18 times and measures water, 0.5-2h is extracted, the 2nd time plus 10-12 times measure water, extract 0.5-1.5h, measure water the 3rd time plus 8-12 times, extract 0.5-1.5h, often The volume concentration of secondary filtration, merging filtrate, filtrate is filtered to 3-6 times of g/ml of kuh-seng weight to obtain the final product.

The essence is milk flavour, peach flavor, lily essence, cream jasmin france, osmanthus flower fragrance, flavoring rose essence.

A kind of preparation method of anti-dandruff and itching-relieving moist type shampoo paste that deoils, includes the following steps：

A) cationic melon glue 0.06-0.6g is weighed, is added in the distilled water of 50-100ml, 60-80 DEG C of heating water bath, Heat while stirring, it is to be mixed uniformly after, standing allows it to be fully swollen, and obtains cationic melon gelling glue, for use；

B) carbomer 0.05-1.5g is weighed, is added in the beaker equipped with 50-100ml distilled water, 60-80 DEG C of water-bath adds Heat heats while stirring, and standing allows it to be fully swollen, and forms carbomer gel liquid, for use；

C) sodium carboxymethylcellulose 0.08-1.5g is weighed, is added in the beaker equipped with 50-100ml distilled water, 40-50 DEG C heating water bath, heats while stirring, and standing allows it to be fully swollen, and forms sodium carboxymethylcellulose lime set, for use；

D) sodium alginate 0.06-2g is weighed, is added in the beaker equipped with 50-100ml distilled water, 60-80 DEG C of water-bath adds Heat heats while stirring, and standing allows it to be fully swollen, and forms sodium alginate gel liquid, for use；

E) Miconazole 1-15g is weighed, is added in the beaker equipped with 10-100ml distilled water, is stirred evenly with glass bar, Miconazole solution is obtained, for use；

F) sodium laureth sulfate 2-8g, sodium lauroyl glutamate 1-10g, amino acid surfactant 4- are taken respectively 12g, MES 1-15g, zinc pyrithione 2-16g, climbazole 1-10g, watermiscible vitamin E 2-10g, distilled water 10-50ml in In beaker 1, it is placed in stirring and dissolving in 60-90 DEG C of thermostat water bath, forms solution 1 after being completely dissolved, for use；

G) coix seed extracting solution 0.7-3.5ml, lemon juice extracting solution 0.5-3.2ml, ginger extract 0.5- are taken respectively 2.8ml, peppermint extracting solution 0.6-3.0ml, Radix Sophorae Flavescentis extractive liquid 0.8-3.0ml, Miconazole solution are placed in beaker 1, and are stirred equal It is even, solution 2 is formed, for use；

H) camellia seed oil 1.5-3.5g, olive oil 1.2-4.5g, simple emulsifier GOC 1-9g, emulsifier EG 1- are weighed 9g is placed in 60-90 DEG C of water-bath, as oil phase, for use；

I) 12-25ml distilled water is measured, is placed in 60-90 DEG C of water-bath, as water phase, for use；

Etc. j) when oil phases reach mutually synthermal with water phase, water phase is added in thread shape in oil phase, it is stirring while adding, until Form the fine and smooth uniform emulsion bases of milky；

K) solution 1, solution 2, cationic melon gelling glue, sodium alginate gel liquid, card wave are added into emulsion bases Nurse coagulant liquid, glycerine 2-7ml, 2% ethylparaben, 75% ethanol solution 0.5-3.5ml, essence 0.08-0.35ml and pearling agent 0.5-1.2g stirs evenly the anti-dandruff and itching-relieving moist type shampoo paste that deoils to obtain the final product with glass bar.

Various composition in the present invention is as follows：

Coix seed main component is protein, vitamin B₁、B₂, skin keratin can be made to soften, have the function of whitening, remove spot, 《Compendium of Materia Medica》Calling coix seed, " invigorating spleen and reinforcing stomach, tonifying lung heat-clearing, wind-dispelling Sheng are wet, and beauty treatment, which is stayed, to be held, macrobiosis of making light of one's life by commiting suicide." coix seed be used for head Hair has nourishing hair, prevents hair loss, and makes the smooth submissive effect of hair.

Contain more citric acid in lemon.This acid can not only promote gastric secretion, help digest, and can neutralize alkali Property, pigmentation is prevented, there is blanching effect to skin.Contain a large amount of provitamin A in lemon juice, skin absorption can be made to make Skin is moist.It is washed hair with lemon juice, the growth and development of hair can be promoted, because citric acid can neutralize the alkaline components in hair, To play the role of hair care.

The ingredients such as gingerol, zingiberene oil in ginger can make skin of head blood circulation normalization, promote scalp newly old Metabolism activates hair follicle tissue, is effectively prevented alopecia, white hair, and stimulation kainogenesis is long, and can inhibit scalp pruritus, strengthens root of hair.With Ginger directly smears head alopecia areata affected part, several days continuous, and new hair can be born at baldness.Shampoo containing ginger component, there is cleaning Scalp dispels dandruff, prevention alopecia and other effects.Especially in winter, for washing hair and coordinating scalp massage, feeling relaxed warm.

Peppermint is pungent cool property sweating antipyretic medicine, and the anti-dandruff factor of peppermint has anti-inflammation and sterilization, decomposes lipid effect, be effectively improved The puzzlement of dandruff and scalp pruritus effectively inhibits dandruff, head to itch.External application can control pruitus, fash and eczema etc., can improve not Clean, obstruction skin, has refrigerant feeling, can shrink capilary, exclude vivotoxin, improve eczema, tinea, releive itch, It inflammation and burns, soft skin is beneficial to oily hair.Can clear hair follicle, fight hair follicle aging, repair, nourish, protection Dry hair enables hair and scalp be full of healthy vigor, with peppermint fragrance, refreshes the mind, enables healthy hair pleasant elegant, bring soft Along the brand-new experience easily combed.Peppermint also has anti-inflammatory analgetic effect, and it is antipruritic to be suitable for scalp.

Kuh-seng energy heat-clearing and damp-drying drug, desinsection is antipruritic, has good mitigation to pruitus.Kuh-seng with the property of its bitter cold, The toxin for becoming silted up and being stored in scalp hair follicles can be effectively cleared up, all alopecia, disconnected the problems such as sending out caused by blocking hair follicle because of acarid, sebum Improve significantly effect, reproduces healthy scalp ecological environment, while the benefits of because of its kidney tonifying, its Hua Fa of Shen controls bone, and kidney qi is prosperous It contains, then hair is dense pitch-black glossy.

Miconazole is efficient, safety, broad-spectrum antifungal medicine, nearly all has effect to pathogenic fungus.Its mechanism is to inhibit The sterol of fungal cell membrane synthesizes, and influences permeability of cell membrane, inhibits fungi growth, leads to death.Below 4 mcg/mls Concentration can inhibit the fungi being largely clinically separated, wherein Cryptococcus neoformans, candida albicans and thick pityrosporion ovale are sensitive to this product, Blastomyces dermatitidis and histoplasma capsulatum are highly sensitive to this product, but Aspergillus is poor.In addition, Miconazole is to S. aureus L-forms and streptococcus And gram-positive cocci and anthrax-bacilus etc. also have antibacterial action.For dermatophytid infection, such as hand, foot, body, jock itch.

Zinc pyrithione (ZPT) is excellent anti-scale agent and anti-excessive fat agent, can effectively kill and generate the true of dandruff Bacterium has antipruritic, anti-dandruff, reduces alopecia and white hair is delayed to act, is efficient, safe relieving itching and removing dandruff agent.

Climbazole has broad-spectrum sterilization performance, is mainly used for the hair washing of relieving itching and removing dandruff conditioning-type, hair conditioning shampoo, it can also be used to anti- Bacterium perfumed soap, shower cream, medicated toothpaste, rinse liquid etc. top grade articles for washing in.

Camellia seed oil breath delicate fragrance, flavor is peculiar, is known as saying for " east olive oil ", find the fatty acid composition of tea oil with The special picture of olive oil, 80% or more, tea oil unsaturated fatty acid content is up to 90% and is easy to be inhaled by human body linoleic content It receives, while absorption of the human body to the trace element such as fat-soluble fiber and calcium, iron, zinc can also be promoted.Also contain olive in camellia seed oil Unexistent bioactive substance such as camellin, Tsubaki-saponin, tea polyphenols etc. in olive oil.Natural tea tree oil nature is mild, can mend Scalp skin nutrition is filled, hair growth, sterilizing and itch-relieving, dermatitis fuel-displaced to treatment scalp, eczema and dandruff is promoted to have significantly Effect can improve Oily, be very effective the anti-dandruff product of antibacterial.To being repaiied after skin itching of the scalp, dry and cracked, eczema, solarization Multiple tool is significantly improved, and cleaning capacity is strong, enables scalp skin keep salubrious, health is comfortable.

Cationic melon glue plays good foam stabilizing, antistatic and thickening power in hair shampoo article.Hair can also be improved Wet comb and dry comb property, so that hair is kept gloss, softness, flexible for a long time, reduce irritation of the detergent to skin.

Sodium alginate plays good thickening, antistatic and foam stabilizing in hair shampoo article.Further, it is also possible to improve hair Moisture retention, so that hair is kept submissive for a long time.It is thickener and moisturizer common in hair shampoo article.

Some extracted form natural plant ingredients are added in this shampoo paste prescription first.It can be by cleaning scalp and hair-care and control Skin of head water and oil balance processed reduces the growth of bacterium, fungi, prevents hair loss.Such as lemon juice, peppermint ingredient can be fine Cleaning-nursing scalp and hair, and be gentle and be not easy to injure skin；The fat secretion of scalp is adjusted in camellia seed oil, makes head Skin keeps water and oil balance state for a long time；Ginger extract can effectively prevent alopecia.

Achieve the effect that anti-dandruff and alleviation head is itched secondly by antibiosis anti-inflammatory drug.Such as zinc pyrithione, Miconazole and sweet Precious element etc. can effectively kill head fungi, bacterium, alleviate itching of the scalp symptom caused by fungi, bacterium.

In these natural extracts and bacteriostatic of addition, hair care ingredient and a variety of important micro members are nourished containing a large amount of Element, effective cleaning, it is anti-dandruff while, scalp metabolism can be accelerated, promote kainogenesis long, keep root of hair strong not easily broken, head Black bright submissive.

In short, this shampoo paste can inhibit the growth of bacterial fungus, regulate and control the water and oil balance of skin of head, it is anti-dandruff to reach cleaning Effect, nutrition needed for hair scalp, moisture can be supplemented, reduce itching of the scalp, prevent hair loss, bifurcated and fungi from growing, can Improve scalp blood circulation, boosts metabolism, keep root of hair strong, healthy hair is dense submissive.

Shampoo paste made by the present invention is creamy white, and viscosity is suitable, and foam is smooth abundant, fine and smooth uniform, stretchability Well, cool and comfortable, stability is good, fragrant.

Specific implementation mode

With reference to embodiment, the present invention will be further described.

The zinc pyrithione of the present invention, Miconazole, climbazole are commercially available.

Amino acid surfactant (GCK-12K), simple emulsifier GOC (glyceryl oleate citrate), emulsifier EG (sodium acrylate/dimethyl acrylamide sodium acyl taurine with different hexadecane, polysorbate 80) is by Beijing Cigna permanent science and trade long Co., Ltd provides.

Embodiment 1

The preparation of 1.1 Semen Coicis extracts

Coix seed 60g is weighed, 0.5h is impregnated after crushing, heating decocts 3 times, the 1st time plus 18 times amount water of extraction, extracts 2h, 2nd time plus 12 times amount water extracts 1h, and the 3rd time plus 10 times amount water extracts 0.5h, filtered every time with 3 layers of gauze, merging filtrate, filter The volume concentration of liquid to coix seed weight 3 times of g/ml, for use.

The preparation of 1.2 lemon juice extracting solutions

Lemon 50g is weighed, 0.5h is impregnated, heating decocts extraction, extracts 3 times, the 1st time plus 12 times amount water, extracts 1.5h, 2nd use, 10 times of amount water, extract 1.5h, and 8 times of amount water of the 3rd use extract 1h, filtered every time with double gauze, merging filtrate, filtered The volume concentration of liquid to lemon weight 3 times of g/ml, for use.

The preparation of 1.3 ginger extracts

Ginger 50g is weighed, is thinly sliced, with water refluxing extraction 3 times, 16 times of amount water of the 1st use extract 1h, filtering, and the 2nd Secondary 12 times of amount water, extract 1h, and 10 times of amount water of the 3rd use extract 0.5h, filter, merging filtrate, be concentrated under reduced pressure as ginger respectively 6 times of g/ml of weight, for use.

The preparation of 1.4 peppermint extracting solutions

Fresh mint 50g is weighed, is put into round-bottomed flask, and 17 times of distilled water are added, is positioned in electric jacket, with waving It after 5 hours of hair oil extractor refluxing extraction, is cooled to room temperature, filters extracting solution with double gauze, for use.

The preparation of 1.5 Radix Sophorae Flavescentis extractive liquids

Kuh-seng 60g is weighed, impregnates 0.8h after crushing, heating decocts extraction 3 times, 18 times of waters of the 1st use, extracts 1h, and the 2nd Secondary 12 times of waters extract 1h, and 10 times of waters of the 3rd use extract 0.5h, and extracting solution merging is filtered with double gauze, filtrate 3 times of g/ml of volume concentration to kuh-seng weight are for use.

The preparation of 1.6 shampoo pastes

A) cationic melon glue 0.3g is weighed, is added in the distilled water of 70ml, 60 DEG C of heating water baths are stirred in heating Mix, it is to be mixed uniformly after, standing allows it to be fully swollen, and obtains cationic melon gelling glue, for use；

B) carbomer 0.9g is weighed, is added in the beaker equipped with 80ml distilled water, 60 DEG C of heating water baths are stirred in heating It mixes, standing allows it to be fully swollen, and forms carbomer gel liquid, for use；

C) sodium carboxymethylcellulose 0.5g is weighed, is added in the beaker equipped with 80ml distilled water, 50 DEG C of heating water baths, side Side stirring is heated, standing allows it to be fully swollen, and forms sodium carboxymethylcellulose lime set, for use；

D) sodium alginate 0.3g is weighed, is added in the beaker equipped with 70ml distilled water, 60 DEG C of heating water baths, in heating Stirring, standing allow it to be fully swollen, and form sodium alginate gel liquid, for use；

E) Miconazole 2g is weighed, is added in the beaker equipped with 30ml distilled water, is stirred evenly with glass bar, obtain Miconazole Solution, for use；

F) sodium laureth sulfate 4g, sodium lauroyl glutamate 5g, amino acid surfactant 6g, MES are taken respectively 6g, zinc pyrithione 8g, climbazole 5g, watermiscible vitamin E 4g, distilled water 50ml are placed in 70 DEG C of thermostatted waters in beaker 1 Stirring and dissolving in bath forms solution 1, for use after being completely dissolved；

G) take respectively coix seed extracting solution 2ml, lemon juice extracting solution 2ml, ginger extract 2ml, peppermint extracting solution 2ml, Radix Sophorae Flavescentis extractive liquid 2ml, Miconazole solution are placed in beaker 1, and stir evenly, and form solution 2, for use；

H) camellia seed oil 2g, olive oil 2g, simple emulsifier GOC 2g, emulsifier EG1g are weighed, is placed in 80 DEG C of water-baths, As oil phase, for use；

I) 12ml distilled water is measured, is placed in 80 DEG C of water-baths, as water phase, for use；

K) solution 1, solution 2, cationic melon gelling glue, sodium alginate gel liquid, card wave are added into emulsion bases Nurse coagulant liquid, glycerine 7ml, 2% ethylparaben, 75% ethanol solution 2ml, essence 0.08ml and pearling agent 1g, are stirred with glass bar Mix the anti-dandruff and itching-relieving moist type shampoo paste that uniformly deoils to obtain the final product.

Embodiment 2

The preparation of 2.1 Semen Coicis extracts

Coix seed 100g is weighed, 0.5h is impregnated after crushing, heating decocts 3 times, the 1st time plus 15 times amount water of extraction, extracts 2h, 2nd time plus 10 times amount water extracts 1h, and the 3rd time plus 10 times amount water extracts 0.5h, filtered every time with 3 layers of gauze, merging filtrate, filter The volume concentration of liquid to coix seed weight 5 times of g/ml, for use.

The preparation of 2.2 lemon juice extracting solutions

It weighs lemon 80g, extracts 3 times, heating decocts 3 times, the 1st time plus 15 times amount water of extraction, extracts 1.5h, the 2nd time With 9 times, 1.5h is extracted, 9 times of amount water of the 3rd use extract 1h, filtered every time with double gauze, merging filtrate, the volume of filtrate is dense 5 times of g/ml of lemon weight are reduced to, for use.

The preparation of 2.3 ginger extracts

Ginger 90g is weighed, is thinly sliced, with water refluxing extraction 3 times, 14 times of amount water of the 1st use extract 1h, filtering, and the 2nd Secondary 12 times of amount water, extract 1h, and 8 times of amount water of the 3rd use extract 0.5h, filter, merging filtrate, be concentrated under reduced pressure as ginger respectively 8 times of g/ml of weight, for use.

The preparation of 2.4 peppermint extracting solutions

Fresh mint 80g is weighed, is put into round-bottomed flask, and 15 times of distilled water are added, is positioned in electric jacket, with waving It after 5.5 hours of hair oil extractor refluxing extraction, is cooled to room temperature, filters extracting solution with double gauze, for use.

The preparation of 2.5 Radix Sophorae Flavescentis extractive liquids

Kuh-seng 80g is weighed, impregnates 0.5h after crushing, heating decocts extraction 3 times, 15 times of waters of the 1st use, extracts 1h, and the 2nd Secondary 11 times of waters extract 1h, and 10 times of waters of the 3rd use extract 0.5h, and extracting solution merging is filtered with double gauze, filtrate Volume concentration to kuh-seng weight 6 times of g/ml, for use.

The preparation of 2.6 shampoo pastes

A) cationic melon glue 0.6g is weighed, is added in the distilled water of 100ml, 80 DEG C of heating water baths are stirred in heating Mix, it is to be mixed uniformly after, standing allows it to be fully swollen, and obtains cationic melon gelling glue, for use；

B) carbomer 0.5g is weighed, is added in the beaker equipped with 80ml distilled water, 70 DEG C of heating water baths are stirred in heating It mixes, standing allows it to be fully swollen, and forms carbomer gel liquid, for use；

C) sodium carboxymethylcellulose 0.7g is weighed, is added in the beaker equipped with 70ml distilled water, 50 DEG C of heating water baths, side Side stirring is heated, standing allows it to be fully swollen, and forms sodium carboxymethylcellulose lime set, for use；

D) sodium alginate 0.8g is weighed, is added in the beaker equipped with 7ml distilled water, 80 DEG C of heating water baths, in heating Stirring, standing allow it to be fully swollen, and form sodium alginate gel liquid, for use；

E) Miconazole 3g is weighed, is added in the beaker equipped with 30ml distilled water, is stirred evenly with glass bar, obtain Miconazole Solution, for use；

F) sodium laureth sulfate 4g, sodium lauroyl glutamate 5g, amino acid surfactant 5g, MES are taken respectively 5g, zinc pyrithione 8g, climbazole 3g, watermiscible vitamin E 40g, distilled water 30ml are placed in 60 DEG C of thermostatted waters in beaker 1 Stirring and dissolving in bath forms solution 1, for use after being completely dissolved；

G) take respectively coix seed extracting solution 3ml, lemon juice extracting solution 2ml, ginger extract 2ml, peppermint extracting solution 3ml, Radix Sophorae Flavescentis extractive liquid 2.0ml, Miconazole solution are placed in beaker 1, and stir evenly, and form solution 2, for use；

H) camellia seed oil 2g, olive oil 3g, simple emulsifier GOC2g, emulsifier EG 1.5g are weighed, 90 DEG C of water-baths are placed in On, as oil phase, for use；

I) 13ml distilled water is measured, is placed in 70 DEG C of water-baths, as water phase, for use；

K) solution 1, solution 2, cationic melon gelling glue, sodium alginate gel liquid, card wave are added into emulsion bases Nurse coagulant liquid, glycerine 7ml, 2% ethylparaben, 75% ethanol solution 2.0ml, essence 0.15ml and pearling agent 0.6g, use glass Stick stirs evenly the anti-dandruff and itching-relieving moist type shampoo paste that deoils to obtain the final product.

Embodiment 3

The preparation of 3.1 Semen Coicis extracts

Coix seed 80g is weighed, 0.5h is impregnated after crushing, heating decocts 3 times, the 1st time plus 16 times amount water of extraction, extracts 2h, 2nd time plus 12 times amount water extracts 1h, and the 3rd time plus 8 times amount water extracts 0.5h, filtered every time with 3 layers of gauze, merging filtrate, filter The volume concentration of liquid to coix seed weight 4 times of g/ml, for use.

The preparation of 3.2 lemon juice extracting solutions

It weighs lemon 70g, extracts 3 times, heating decocts extraction 3 times, the 1st time plus 15 times of waters, extracts 1.5h, the 2nd time With 10 times, 1.5h, water are extracted, 10 times of waters of the 3rd use are extracted 1h, filtered every time with double gauze, merging filtrate, filtrate Volume concentration to lemon weight 4 times of g/ml, for use.

The preparation of 3.3 ginger extracts

Ginger 70g is weighed, is thinly sliced, with water refluxing extraction 3 times, 14 times of amount water of the 1st use extract 2.0h, filtering, the Secondary 10 times of amount water extract 1.8h, and 8 times of amount water of the 3rd use extract 1.0h, filter respectively, merging filtrate, are concentrated under reduced pressure and are 7 times of g/ml of ginger weight, for use.

The preparation of 3.4 peppermint extracting solutions：

Fresh mint 70g is weighed, is put into round-bottomed flask, and 16 times of distilled water are added, is positioned in electric jacket, with waving It after 5.5 hours of hair oil extractor refluxing extraction, is cooled to room temperature, filters extracting solution with double gauze, for use.

The preparation of 3.5 Radix Sophorae Flavescentis extractive liquids

Kuh-seng 70g is weighed, 0.15h is impregnated after crushing, heating decocts extraction 3 times, and 15 times of amount water of the 1st use extract 1h, the 2 use, 12 times of amount water, extract 1h, and 10 times of amount water of the 3rd use extract 0.5h, extracting solution merging is filtered with double gauze, filtrate Volume concentration to kuh-seng weight 4 times of g/ml, for use.

The preparation of 3.6 shampoo pastes

B) carbomer 1.0g is weighed, is added in the beaker equipped with 100ml distilled water, 80 DEG C of heating water baths, in heating Stirring, standing allow it to be fully swollen, and form carbomer gel liquid, for use；

C) sodium carboxymethylcellulose 1.0g is weighed, is added in the beaker equipped with 100ml distilled water, 50 DEG C of heating water baths, It heats while stirring, standing allows it to be fully swollen, and forms sodium carboxymethylcellulose lime set, for use；

D) sodium alginate 1.5g is weighed, is added in the beaker equipped with 100ml distilled water, 80 DEG C of heating water baths, side heating Side is stirred, and standing allows it to be fully swollen, and forms sodium alginate gel liquid, for use；

E) Miconazole 15g is weighed, is added in the beaker equipped with 100ml distilled water, is stirred evenly with glass bar, obtain miaow health Azoles solution, for use；

F) take respectively sodium laureth sulfate 8g, sodium lauroyl glutamate 10g, amino acid surfactant 12g, MES15g, zinc pyrithione 16g, climbazole 10g, watermiscible vitamin E 10g, distilled water 50ml are placed in 80 DEG C in beaker 1 Stirring and dissolving in thermostat water bath forms solution 1, for use after being completely dissolved；

G) coix seed extracting solution 2ml, lemon juice extracting solution 3.2ml, ginger extract 2.8ml, peppermint extracting solution are taken respectively 3.0ml, Radix Sophorae Flavescentis extractive liquid 3.0ml, Miconazole solution are placed in beaker 1, and stir evenly, and form solution 2, for use；

H) camellia seed oil 3.5g, olive oil 4.5g, simple emulsifier GOC 5g, emulsifier EG 3g are weighed, 80 DEG C of water are placed in In bath, as oil phase, for use；

I) 25ml distilled water is measured, is placed in 80 DEG C of water-baths, as water phase, for use；

K) solution 1, solution 2, cationic melon gelling glue, sodium alginate gel liquid, card wave are added into emulsion bases Nurse coagulant liquid, glycerine 5ml, 2% ethylparaben, 75% ethanol solution 3ml, essence 0.35ml and pearling agent 1.2g, use glass bar Stir evenly the anti-dandruff and itching-relieving moist type shampoo paste that deoils to obtain the final product.

Embodiment 4：

The physical and chemical index of embodiment 1,2,3 is as follows：

4.1 character

This product is that viscosity is suitable, and foam is smooth abundant, fine and smooth uniform, the good milky shampoo paste of stretchability.

4.2pH value inspections

A small amount of shampoo paste, pH 6-7 are dipped with the pH test paper of wetting.

4.3 caloric test

Shampoo paste is packaged in transparence cosmetic bottle, in 4 DEG C of refrigerator cold-storage observations in one week or so without lamination.In In 55 DEG C of insulating box for 24 hours, phenomena such as soap lye is spoiled without layering emulsification.

4.4 centrifugal test

Shampoo paste is packaged in 3000r/min in tool plug test tube and centrifuges 20min, no lamination.

4.5 irritation tests, anaphylaxis experiment

Small white mouse back cuts off hair, smears the shampoo paste that is prepared by embodiment 1,2 respectively in cutting plucked position, and do not apply Position is compared, as a result without irritation and allergic reaction.

1 gram of Example is applied in volunteer (16-70 Sui, 60 people) gesture and facial expression, is observed after spending 30 minutes, is not sent out It is red, dermexanthesis, foaming phenomena.

4.6 are placed at room temperature for experiment

1,2 made shampoo paste of embodiment is placed in bottle for cosmetics, investigation 6 months is stored at room temperature, no lamination is used After feel unchanged, smell is unchanged.

4.7 anti-dandruff effects

Volunteer's (16-70 Sui, 60 people) is chosen, obtained shampoo paste is used for volunteer's hair, it is mixed with a small amount of water Merging is washed by rubbing with the hands repeatedly, it is found that foaming abundancy, volunteers generally feel smooth comfortable, feel is preferable.The no matter dry comb of hair or Wet comb property is all good.After being eluted with water, hair submissive such as silk, fluffy non-greasy, moistening effect is preferable, existing without scalp pruritus after washing As, and be not required to use hair conditioner.Through continuous use in one month, hair was obviously glossy, soft, and dandruff phenomenon obviously subtracts It is few.

Embodiment 5：

The shampoo paste resultant effect is investigated

Following on probation the effect of feeling to evaluate shampoo paste that embodiment 1,2 produces.It is scored using opinion poll Method chooses the women of 50 18-60 Sui age brackets as object is tried out, is arbitrarily divided into two groups, uses embodiment 1,2 to prepare respectively Shampoo paste wash my hair.It uses weekly twice, usage time is two months.Every using effect total score is 5 points：5 points are highest Point, indicate fine, it is very satisfied；4 points are preferable；3 points are that can receive；3 points or less are bad, cannot be received.It is each below Item average.It the results are shown in Table 1：

1 resultant effect of table is investigated

In conclusion the shampoo paste foaming abundancy that the present invention is made, has and goes oiliness well, soil release performance, wet comb property, grows Nourish one's nature, feel salubrious comfortable when use, it is good with rear hair elasticity, have deoil, take care of hair, relieving itching and removing dandruff, the effect prevented hair loss.

Claims

Anti-dandruff and itching-relieving moist type shampoo paste and preparation method thereof 1. one kind is deoiled, it is characterised in that：Match containing following in shampoo paste The raw material components of ratio：

Sodium laureth sulfate 2-8g

Sodium lauroyl glutamate 1-10g

GCK-12K 4-12g

Dodecyl Polyoxyethylene Ether sulfosuccinate disodium MES 1-15g

Simple emulsifier GOC 1-9g

Emulsifier EG 1-9g

Watermiscible vitamin E 2-10g

Coix seed extracting solution 0.7-3.5ml

Lemon extract 0.5-3.2ml

Ginger extract 0.5-2.8ml

Peppermint extracting solution 0.6-3.0ml

Radix Sophorae Flavescentis extractive liquid 0.8-3.0ml

Miconazole 1-15g

Zinc pyrithione 2-16g

Climbazole 1-10g

Glycerine 2-7ml

Pearling agent 0.5-1.2g

Olive oil 1.2-4.5g

Camellia seed oil 1.5-3.5g

Cationic melon glue 0.06-0.6g

Carbomer 0.05-1.5g

Sodium carboxymethylcellulose 0.08-1.5g

Sodium alginate 0.06-2.0g

Distilled water 232-575ml

Essence 0.08-0.35ml

2% ethylparaben, 75% ethanol solution 0.5-3.5ml.
The anti-dandruff and itching-relieving moist type shampoo paste 2. one kind according to claim 1 is deoiled, it is characterised in that：The coix seed Extracting solution is to be prepared by the following method：

It is appropriate to weigh coix seed, 0.15-0.8h is impregnated after crushing, heating decocts extraction 3 times, the 1st time plus 10-18 times and measures water, carries It takes 0.5-2h, measures water the 2nd time plus 8-15 times, extract 0.5-1.5h, measure water the 3rd time plus 8-10 times, extract 0.5-1.5h, filter every time It crosses, merging filtrate, the volume concentration of filtrate is filtered to 3-6 times of g/ml of coix seed weight to obtain the final product.
The anti-dandruff and itching-relieving moist type shampoo paste 3. one kind according to claim 1 is deoiled, it is characterised in that：The lemon carries Liquid is taken to be prepared by the following method：

It is appropriate to weigh lemon, 0.15-0.8h is impregnated after incision, heating decocts extraction 3 times, the 1st time plus 8-15 times and measures water, extracts 0.5-2h, the 2nd time plus 8-10 times measure water, extract 0.5-1.5h, measure water the 3rd time plus 8-10 times, extract 0.5-1.5h, filter every time It crosses, merging filtrate, the volume concentration of filtrate is filtered to 3-6 times of g/ml of lemon weight to obtain the final product.
The anti-dandruff and itching-relieving moist type shampoo paste 4. one kind according to claim 1 is deoiled, it is characterised in that：The ginger carries Liquid is taken to be prepared by the following method：

It is appropriate to weigh ginger, thinly slices, with water refluxing extraction 3 times, measures water with 10-18 times for the first time, extracts 0.5-2.5h, mistake Filter measures water with 8-15 times for the second time, extracts 0.5-2.5h, measures water with 6-12 times for the third time, extracts 0.5-1.5h, filters respectively, The 6-10 times of g/ml for ginger weight is concentrated under reduced pressure, for use in merging filtrate.
The anti-dandruff and itching-relieving moist type shampoo paste 5. one kind according to claim 1 is deoiled, it is characterised in that：The peppermint carries Liquid is taken to be prepared by the following method：

It is a certain amount of to weigh fresh mint, is put into round-bottomed flask, and 10-18 times of distilled water is added, is positioned in electric jacket, uses It after 5-6 hour of volatile oil extractor refluxing extraction, is cooled to room temperature, filters extracting solution with double gauze, for use.
The anti-dandruff and itching-relieving moist type shampoo paste 6. one kind according to claim 1 is deoiled, it is characterised in that：The kuh-seng carries Liquid is taken to be prepared by the following method：

It is appropriate to weigh kuh-seng, 0.15-0.8h is impregnated after crushing, heating decocts extraction 3 times, the 1st time plus 10-18 times and measures water, extracts 0.5-2h, the 2nd time plus 10-12 times measure water, extract 0.5-1.5h, measure water the 3rd time plus 8-12 times, extract 0.5-1.5h, filter every time It crosses, merging filtrate, the volume concentration of filtrate is filtered to 3-6 times of g/ml of kuh-seng weight to obtain the final product.
The anti-dandruff and itching-relieving moist type shampoo paste 7. one kind according to claim 1 is deoiled, it is characterised in that：The essence is Milk flavour, peach flavor, lily essence, cream jasmin france, osmanthus flower fragrance, flavoring rose essence.
8. a kind of preparation method of anti-dandruff and itching-relieving moist type shampoo paste that deoils according to claim 1, it is characterised in that：

a）Cationic melon glue 0.06-0.6g is weighed, is added in the distilled water of 50-100ml, 60-80 DEG C of heating water bath, side Heat side stirring, it is to be mixed uniformly after, standing allows it to be fully swollen, and obtains cationic melon gelling glue, for use；

b）Carbomer 0.05-1.5g is weighed, is added in the beaker equipped with 50-100ml distilled water, 60-80 DEG C of heating water bath, side Side stirring is heated, standing allows it to be fully swollen, and forms carbomer gel liquid, for use；

c）Sodium carboxymethylcellulose 0.08-1.5g is weighed, is added in the beaker equipped with 50-100ml distilled water, 40-50 DEG C of water Bath heating, heats while stirring, and standing allows it to be fully swollen, and forms sodium carboxymethylcellulose lime set, for use；

d）Sodium alginate 0.06-2g is weighed, is added in the beaker equipped with 50-100ml distilled water, 60-80 DEG C of heating water bath, side Side stirring is heated, standing allows it to be fully swollen, and forms sodium alginate gel liquid, for use；

e）Miconazole 1-15g is weighed, is added in the beaker equipped with 10-100ml distilled water, is stirred evenly with glass bar, obtain miaow Health azoles solution, for use；

f）Take respectively sodium laureth sulfate 2-8g, sodium lauroyl glutamate 1-10g, GCK-12K 4-12g, MES 1-15g, Zinc pyrithione 2-16g, climbazole 1-10g, watermiscible vitamin E 2-10g, distilled water 10-50ml are placed in beaker 1 Stirring and dissolving in 60-90 DEG C of thermostat water bath forms solution 1, for use after being completely dissolved；

g）Coix seed extracting solution 0.7-3.5ml, lemon extract 0.5-3.2ml, ginger extract 0.5-2.8ml, thin is taken respectively Lotus extracting solution 0.6-3.0ml, Radix Sophorae Flavescentis extractive liquid 0.8-3.0ml, Miconazole solution are placed in beaker 1, and stir evenly, and are formed Solution 2, for use；

h）Camellia seed oil 1.5-3.5g, olive oil 1.2-4.5g, simple emulsifier GOC 1-9g, emulsifier EG 1-9g are weighed, is set In in 60-90 DEG C of water-bath, as oil phase, for use；

i）12-25ml distilled water is measured, is placed in 60-90 DEG C of water-bath, as water phase, for use；

j）When equal oil phases reach mutually synthermal with water phase, water phase is added in thread shape in oil phase, it is stirring while adding, until being formed The fine and smooth uniform emulsion bases of milky；

k）It is solidifying that solution 1, solution 2, cationic melon gelling glue, sodium alginate gel liquid, carbomer are added into emulsion bases Glue, glycerine 2-7ml, 2% ethylparaben, 75% ethanol solution 0.5-3.5ml, essence 0.08-0.35ml and pearling agent 0.5- 1.2g stirs evenly the anti-dandruff and itching-relieving moist type shampoo paste that deoils to obtain the final product with glass bar.