CN104490678B - A kind of rosemary hydrosol toner and preparation method thereof - Google Patents
A kind of rosemary hydrosol toner and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a kind of rosemary hydrosol toner and preparation method thereof, include the material composition of following mass fraction：Chinese gooseberry seed extract solution 1% 5%, sponge gourd water 0.5% 2.0%, Sodium Hyaluronate 3% 5%, caprylic acid 0.1% 0.5%, sodium alginate 0.7% 1.2%, squalene 1% 2%, propane diols 0.2% 1.0%, ivy extract solution 1.5% 2.5%, methyl benzoate 2.0% 3.5%, rosemary hydrosol complements to 100%.Its preparation method comprises the following steps：Rosemary hydrosol is prepared, Chinese gooseberry seed extract solution is prepared, prepares ivy extract solution, prepares sponge gourd water, batch mixing, sterilization, filling step.The present invention uses rosemary hydrosol as primary raw material, is equipped with the plant components such as ivy extract solution, sponge gourd water, Chinese gooseberry seed extract solution and is prepared, and has the multi-efficiencies such as water conservation, moisturizing, whitening, firm skin；Meanwhile whole fabrication process condition is very gentle, maintain that the active component in plant material is not destroyed and lose, and the toner skincare effect of preparation is good completely.
Description
Technical field
The present invention relates to a kind of toner, and in particular to a kind of rosemary hydrosol toner and preparation method thereof.
Background technology
Cosmetics are the articles for daily use for cleaning and beautifying the positions such as human body skin, face, hair or tooth and use；
At present, cosmetics have been deep into daily life, turn into modern society's each ages crowd indispensable day
Normal running stores, it is even more particularly important particularly with the female group liked to be beautiful, cosmetics.Cosmetics by purposes can be divided into cleaning class,
Nurse the cosmetics such as class, nutrition class, beauty modification class, specific use class.Toner belongs to nursing class cosmetics, is a kind of transparent
The cosmetics of liquid, the surface of skin is applied to, with the purpose for reaching cleaning skin, keeping skin health, it is in basic skin care
In play a part of to take over from the past and set a new course for the future.With the continuous improvement that people are required cosmetics, toner is pressed its effect demand, developed
Multiple kinds such as moisture retention water, toner, astringent lotion, smoothing toner are formed, and processing raw material for toner is also become increasingly abundant, especially
It is that the cosmetics prepared using natural, safe, green plant extracts as raw material are just enjoying consumer to pursue.Currently, with plant
Thing extract is raw material, and toner of the exploitation with multi-efficiency is following trend；But when researching and developing toner, plant
The effect of thing extract plays effect still needs to be investigated, and after the high strength physical chemical action of such as high temperature, high pressure etc., plants
Thing active component is more easily damaged, and its efficacy effect will also be lost；And use synthesis chemical raw material when, its security be not easy by
People receive.
Chinese patent (publication number 102293723A) discloses a kind of preparation method of konjaku moisturizing astringent, including following
Step：Prepare konjac sol, mix stirring, filtering and sterilization.The preparation method of the konjaku moisturizing astringent, only by simple
Physical operations, without substantial amounts of equipment investment；Preparation technology is simple, cost is low；Product rich in ceramide element, vitamin,
Mineral matter and water, during use can rapid osmotic, supplement skin energy, beauty and health care effect is good, has no toxic side effect, and is a kind of moisturizing
Good, the pure natural moisturizing astringent of effect.But the konjaku toner only has better effects in terms of moisturizing, and other are sought
Foster skin care effect is still indefinite.
Chinese patent (publication number 101966135A) discloses a kind of toner containing nanometer moisturizing composition, comprising：Table
Face activating agent 0.1-20%, preferably 0.5-10%；Polyalcohol 0.1-30%, preferably 1-20%；Emollient 0.1-20%, preferably
0.2%-15%；NMF 0.1-30%, preferably 0.5-20%；Preservative 0.001-3%, preferably 0.005-2.5%；It is other to add
Add agent 0.01-15%, preferably 0.05-10%；Water 50-98%, preferably 65-95%；The particle diameter of the emollient of above-mentioned toner is equal
For less than 200nm；The toner both can overcome the disadvantages that generalization adornment water can not effective moisturizing deficiency, and can realize common milky lotion,
Skin cream can not rapid moisturizing the shortcomings that, and, skin sense salubrious the features such as simple with preparation technology, can be that user simplifies shield
Skin step.Although the toner has moisturizing and the double effectses of moisturizing, the additive of a variety of chemical syntheses is used, health
Had a greatly reduced quality with security.
Chinese patent (publication number 102415974A) discloses a kind of toner containing rose water and preparation method thereof.The change
Rose water in adornment water is made using rose and water distillation, and the weight that water is added in rose is the 8 of rose weight
~10 times, distillation speed is the 10~20% of total Water for distillate per hour, to final distillate and rose weight used
Stop distillation when equal, produce rose water, natural glycerin, allantoin and compound amino acid are with the addition of simultaneously in this kind of toner
Etc. a variety of natural components, make the whitenings of this kind of cosmetics, moisturizing, skin softening and desalinate color spot effect it is more obvious, this and the change
Spirituosity, preservative etc. may not cause the material of sensitivity to skin in adornment water, and it is simple and tasteful to remain the sweet of natural rose, delicate fragrance
Odor characteristic, provide a kind of new way for the utilization of rose.Although this contain toner of rose water using plant into
Point rose water, but the effect of be extremely difficult to described whitening, moisturizing, skin softening using only rose water, its still need addition compared with
More additives are coordinated, to reach a variety of skin effects.
The content of the invention
In order to solve the above technical problems, the present invention is intended to provide a kind of prepared using various plants extract as raw material, tool
There are moisturizing, water conservation, nourish rosemary hydrosol toners of multi-efficiency such as firm skin and preparation method thereof.
The present invention is achieved through the following technical solutions.
A kind of rosemary hydrosol toner, include the material composition of following mass fraction：Chinese gooseberry seed extract solution 1%-
5%, sponge gourd water 0.5%-2.0%, Sodium Hyaluronate 3%-5%, caprylic acid 0.1%-0.5%, sodium alginate 0.7%-
1.2%, squalene 1%-2%, propane diols 0.2%-1.0%, ivy extract solution 1.5%-2.5%, methyl benzoate
2.0%-3.5%, rosemary hydrosol complement to 100%.
Preferably, the rosemary hydrosol toner includes the material composition of following mass fraction：Chinese gooseberry seed extract solution
1%, sponge gourd water 2.0%, Sodium Hyaluronate 3%, caprylic acid 0.5%, sodium alginate 0.7%, squalene 2%, propane diols
0.2%, ivy extract solution 1.5%, methyl benzoate 3.5%, rosemary hydrosol complements to 100%.
Preferably, the rosemary hydrosol toner includes the material composition of following mass fraction：Chinese gooseberry seed extract solution
5%, sponge gourd water 0.5%, Sodium Hyaluronate 5%, caprylic acid 0.1%, sodium alginate 1.2%, squalene 1%, propane diols
1.0%, ivy extracts thing liquid 2.5%, methyl benzoate 2.0%, and rosemary hydrosol complements to 100%.
Preferably, the rosemary hydrosol toner includes the material composition of following mass fraction：Chinese gooseberry seed extract solution
3%, sponge gourd water 1.5%, Sodium Hyaluronate 3.5%, caprylic acid 0.3%, sodium alginate 1.0%, squalene 1.2%, propane diols
0.6%, ivy extract solution 1.7%, methyl benzoate 3.0%, rosemary hydrosol complements to 100%.
The method for preparing above-mentioned rosemary hydrosol toner, comprises the following steps：
(1) preparation of rosemary hydrosol：It is 1 by floral leaf mass ratio to take rosemary to spend with rosemary leave:After 2-5 is well mixed
Crush, be afterwards 1 by feed liquid mass ratio by the rosemary floral leaf chip of crushing:1.2-2.0 adds deionized water, ultrasonication
15-30min, after vapo(u)rizing temperature be less than 65 DEG C under conditions of be evaporated in vacuo, collect distillate, cool down and produce rosemary
Hydrosol；
(2) preparation of Chinese gooseberry seed extract solution：Chinese gooseberry seed is crushed to 40-50 mesh, with feed liquid mass ratio 1:2-4 is added
Deionized water, ice-water bath concussion carry out refrigerated centrifuge after extracting 3-10h, take the supernatant after centrifugation to cross microfiltration membrane and are taken off
Color cleans, and collects filtrate, produces Chinese gooseberry seed extract solution；
(3) preparation of ivy extract solution：Ivy is crushed to 20-40 mesh, by feed liquid mass ratio 1:4-10 additions are gone
Ionized water, ice-water bath concussion carry out refrigerated centrifuge after extracting 3-5h, take the supernatant after centrifugation to cross microfiltration membrane and are decolourized
Removal of impurities, filtrate is collected, produces ivy extract solution；
(4) preparation of sponge gourd water：Luffa vine in growth course is cut at 5-10cm from the ground, luffa vine insertion is connect
Receive in bottle, seal bottleneck with preservative film, place 24-48h, take out receiving bottle, the liquid in receiving bottle is filtered, filtrate is sponge gourd
Water；
(5) batch mixing：By Sodium Hyaluronate, caprylic acid, sodium alginate, squalene, propane diols, methyl benzoate and preparation
Chinese gooseberry seed extract solution, sponge gourd water, ivy extract solution, rosemary hydrosol are put into stainless steel together, carry out vacuum low speed
Stirring, it is 15-50 DEG C to control whipping temp, stirs 1-4h, obtains mixed liquor；
(6) sterilize, be filling：The degerming rear progress of mixed liquor progress filtering with microporous membrane is filling, produce product of the present invention.
Rosemary hydrosol is rich in fan repeatedly essential oil and the natural strong anti-oxidation composition of rosemary phenols, tannin, protein, plant sugar
Etc. water-soluble components, aged skin cells can be activated, promotes skin blood circulation, improve skin oil and fat secretion balance, keep skin
Skin water is tender to compact, and has therapeutic effect to acne, dermatitis, eczema and oedema.The main active of ivy extract solution is gleditsia sinensis
Glycosides, it is present in each position of ivy, and it has good effect to inflammation and pain of alleviation, and with convergence and shrinks blood
The effect of pipe, microcirculation, convergence, calm and conditioning sebum secretion can be promoted.Sponge gourd water contain abundant plant polyose, mucus,
The NMF such as vitamin and mineral matter, the normal moisture content of cuticula can be maintained, slow down dehydration with extending aquation,
The necessary moisture of skin can be supplemented, keeps skin water tender, fine and smooth；And containing the B family vitamin for preventing skin aging in sponge gourd water
With the composition such as the vitamin C of skin whitening, skin can be protected, eliminate patch, make skin pure white, delicate.Chinese gooseberry seed extract solution
Rich in flavones, polyphenol and trace elements of selenium, it can effectively suppress the deposition of skin senescence and pigment, can skin whitening.
The present invention uses rosemary hydrosol as primary raw material, is equipped with ivy extract solution, sponge gourd water, Chinese gooseberry seed extract solution
It is prepared etc. natural activity plant component, there is the multi-efficiencies such as water conservation, moisturizing, whitening, firm skin.Meanwhile entirely add
Work technique is carried out under conditions of very gently；Wherein, rosemary hydrosol is distilled using cryogenic vacuum；Ivy extract solution, Mi
Monkey peach seed extract solution is combined using ice-water bath concussion extraction, refrigerated centrifuge and membrane filtration；Mixing process is using vacuum and low temperature, low
Speed stirring, can prevent bubble；The active component that the mutual cooperation of above-mentioned operation maintains in plant material completely is not broken
Bad and loss, still has a stronger bioactivity, and the toner skincare effect of preparation is good.
The main component such as table 1 of product rosemary hydrosol toner of the present invention.
The main component of the rosemary hydrosol toner of table 1
| Project | Content | Project | Content |
| Moisture | 81.5%-97.0% | Protein | 0.11-0.72% |
| General flavone | 0.11-0.27% | Sodium Hyaluronate | 3%-5% |
| Vitamin C | 0.012-0.24% | Caprylic acid | 0.1%-0.5% |
| Vitamin B | 0.01-0.024‰ | Sodium alginate | 0.7%-1.2% |
| Plant polyphenol | 0.15-0.48‰ | Squalene | 1%-2% |
| Saponin | 0.011-0.014‰ | Propane diols | 0.2%-1.0% |
| Polysaccharide | 0.21-0.69% | Methyl benzoate | 1.5%-2.5% |
Water conservation, whitening, the firm skin effect test of product rosemary hydrosol toner of the present invention：
(1) cosmetic water sample is prepared：Rosemary hydrosol toner is prepared by the inventive method, on probation.
(2) subject：Choose cheek dry skin, it is coarse, have obvious patch, tested volunteer can be completed on request,
31 people altogether, the wherein people of male 11, the people of women 20, average age 31 ± 8 years old.
(3) trial method：Every other day, with after warm water cleaning cheek before sleeping at night, this product toner is taken to be applied to the centre of the palm,
Cheek about 5min is gently patted afterwards, to promote the absorption of toner active ingredient；It is tested in the toner stage of the present invention on probation
Person is without using other cosmetics.
(4) judgment criteria：After two months, subject carries out self-appraisal to sample on probation to trying out front and rear effect, be divided into it is satisfied,
It is unsatisfied with two grades.
(5) result on trial is shown in Table 2
The water conservation of the product rosemary hydrosol toner of the present invention of table 2, whitening, firm skin effect
| Subject | Sex | Age | Water-saving effect | Whitening effect | Firm skin effect | Whole structure |
| 1 (Chen) | Man | 32 | It is satisfied | It is satisfied | It is satisfied | It is satisfied |
| 2 (Lee) | Female | 22 | It is dissatisfied | It is satisfied | It is satisfied | It is satisfied |
| 3 (Mas) | Female | 26 | It is satisfied | It is satisfied | It is satisfied | It is satisfied |
| 4 (cars) | Man | 23 | It is satisfied | It is dissatisfied | It is satisfied | It is satisfied |
| 5 (Wus) | Female | 24 | It is satisfied | It is satisfied | It is dissatisfied | It is satisfied |
| 6 (Yans) | Man | 30 | It is dissatisfied | It is dissatisfied | It is satisfied | It is dissatisfied |
| 7 (Wus) | Female | 34 | It is satisfied | It is satisfied | It is satisfied | It is satisfied |
| 8 (Tang) | Female | 33 | It is satisfied | It is satisfied | It is satisfied | It is satisfied |
| 9 (thanking so-and-so) | Female | 21 | It is satisfied | It is dissatisfied | It is satisfied | It is satisfied |
| 10 (weeks certain) | Female | 22 | It is dissatisfied | It is dissatisfied | It is satisfied | It is dissatisfied |
| 11 (dragons so-and-so) | Man | 25 | It is satisfied | It is satisfied | It is dissatisfied | It is satisfied |
| 12 (Shandongs so-and-so) | Female | 29 | It is dissatisfied | It is dissatisfied | It is satisfied | It is dissatisfied |
| 13 (Bians) | Female | 37 | It is satisfied | It is dissatisfied | It is satisfied | It is satisfied |
| 14 (shens so-and-so) | Female | 24 | It is satisfied | It is satisfied | It is satisfied | It is satisfied |
| 15 (Zhangs) | Female | 35 | It is dissatisfied | It is dissatisfied | It is satisfied | It is dissatisfied |
| 16 (gold certain) | Female | 32 | It is dissatisfied | It is satisfied | It is satisfied | It is satisfied |
| 17 (what certain) | Female | 25 | It is satisfied | It is dissatisfied | It is dissatisfied | It is dissatisfied |
| 18 (Chens) | Man | 45 | It is dissatisfied | It is dissatisfied | It is satisfied | It is dissatisfied |
| 19 (Chens) | Female | 21 | It is satisfied | It is dissatisfied | It is satisfied | It is satisfied |
| 20 (fourths so-and-so) | Man | 33 | It is satisfied | It is satisfied | It is satisfied | It is satisfied |
| 21 (Mr. Wangs) | Female | 35 | It is satisfied | It is satisfied | It is satisfied | It is satisfied |
| 22 (Xiaos) | Female | 25 | It is satisfied | It is satisfied | It is dissatisfied | It is satisfied |
| 23 (Bians so-and-so) | Man | 26 | It is satisfied | It is dissatisfied | It is satisfied | It is satisfied |
| 24 (what so-and-so) | Man | 48 | It is dissatisfied | It is satisfied | It is satisfied | It is satisfied |
| 25 (Chens) | Man | 47 | It is satisfied | It is satisfied | It is satisfied | It is satisfied |
| 26 (Luos) | Female | 23 | It is satisfied | It is satisfied | It is dissatisfied | It is satisfied |
| 27 (Lee) | Female | 46 | It is dissatisfied | It is dissatisfied | It is satisfied | It is dissatisfied |
| 28 (Lee) | Man | 35 | It is satisfied | It is satisfied | It is satisfied | It is satisfied |
| 29 (Mr. Lis) | Female | 33 | It is satisfied | It is satisfied | It is dissatisfied | It is satisfied |
| 30 (Zhangs) | Female | 27 | It is dissatisfied | It is satisfied | It is satisfied | It is satisfied |
| 31 (Wus) | Man | 36 | It is satisfied | It is satisfied | It is satisfied | It is satisfied |
As seen from the above table, after 31 subjects use toner of the present invention, the number to Water-saving effect satisfaction is 22 people, full
Meaning rate is 71%；Number to whitening effect satisfaction is 19 people, satisfaction rate 61%；Number to firm skin good results is
25 people, satisfaction rate 81%；Number to water conservation, whitening, the satisfaction of firm skin whole structure is 24 people, satisfaction rate 77%；
From the foregoing, it will be observed that product of the present invention has the multi-efficiencies such as preferable water conservation, whitening, firm skin.
Embodiment
Explanation is further explained to the present invention with reference to specific embodiment, but the invention is not restricted to following examples.
Embodiment 1
A kind of rosemary hydrosol toner, include the material composition of following mass fraction：Chinese gooseberry seed extract solution 1%-
5%, sponge gourd water 0.5%-2.0%, Sodium Hyaluronate 3%-5%, caprylic acid 0.1%-0.5%, sodium alginate 0.7%-
1.2%, squalene 1%-2%, propane diols 0.2%-1.0%, ivy extract solution 1.5%-2.5%, methyl benzoate
2.0%-3.5%, rosemary hydrosol complement to 100%.
The preparation method of above-mentioned rosemary hydrosol toner comprises the following steps：
(1) prepared by rosemary hydrosol：It is 1 by floral leaf mass ratio to take rosemary to spend with rosemary leave:Powder after 2-5 is well mixed
It is broken, it is afterwards 1 by feed liquid mass ratio by the rosemary floral leaf chip of crushing:1.2-2.0 adds deionized water, ultrasonication
15-30min, after vapo(u)rizing temperature be less than 65 DEG C under conditions of be evaporated in vacuo, collect distillate, cool down and produce rosemary
Hydrosol；
(2) preparation of Chinese gooseberry seed extract solution：Chinese gooseberry seed is crushed to 40-50 mesh, with feed liquid mass ratio 1:2-4 is added
Deionized water, ice-water bath concussion carry out refrigerated centrifuge after extracting 3-10h, take the supernatant after centrifugation to cross microfiltration membrane and are taken off
Color cleans, and collects filtrate, produces Chinese gooseberry seed extract solution；
(3) preparation of ivy extract solution：Ivy is crushed to 20-40 mesh, by feed liquid mass ratio 1:4-10 additions are gone
Ionized water, ice-water bath concussion carry out refrigerated centrifuge after extracting 3-5h, take the supernatant after centrifugation to cross microfiltration membrane and are decolourized
Removal of impurities, filtrate is collected, produces ivy extract solution；
(4) preparation of sponge gourd water：Luffa vine in growth course is cut at 5-10cm from the ground, luffa vine insertion is connect
Receive in bottle, seal bottleneck with preservative film, place 24-48h, take out receiving bottle, the liquid in receiving bottle is filtered, filtrate is sponge gourd
Water；
(5) batch mixing：By Sodium Hyaluronate, caprylic acid, sodium alginate, squalene, propane diols, methyl benzoate and preparation
Chinese gooseberry seed extract solution, sponge gourd water, ivy extract solution, rosemary hydrosol are put into stainless steel together, carry out vacuum low speed
Stirring, it is 15-50 DEG C to control whipping temp, stirs 1-4h, obtains mixed liquor；
(6) sterilize, be filling：The degerming rear progress of mixed liquor progress filtering with microporous membrane is filling, produce product of the present invention.
Embodiment 2
A kind of rosemary hydrosol toner, include the material composition of following mass fraction：Chinese gooseberry seed extract solution 1%, silk
Melon water 2.0%, Sodium Hyaluronate 3%, caprylic acid 0.5%, sodium alginate 0.7%, squalene 2%, propane diols 0.2%, Chang Chun
Rattan extract solution 1.5%, methyl benzoate 3.5%, rosemary hydrosol complement to 100%.
Preparation method is the same as embodiment 1.
Embodiment 3
A kind of rosemary hydrosol toner, include the material composition of following mass fraction：Chinese gooseberry seed extract solution 5%, silk
Melon water 0.5%, Sodium Hyaluronate 5%, caprylic acid 0.1%, sodium alginate 1.2%, squalene 1%, propane diols 1.0%, Chang Chun
Boisiana extract liquid 2.5%, methyl benzoate 2.0%, rosemary hydrosol complement to 100%.
Preparation method is the same as embodiment 1.
Embodiment 4
A kind of rosemary hydrosol toner, include the material composition of following mass fraction：Chinese gooseberry seed extract solution 3%, silk
Melon water 1.5%, Sodium Hyaluronate 3.5%, caprylic acid 0.3%, sodium alginate 1.0%, squalene 1.2%, propane diols 0.6%,
Ivy extract solution 1.7%, methyl benzoate 3.0%, rosemary hydrosol complement to 100%.
Preparation method is the same as embodiment 1.
Embodiment 5
A kind of rosemary hydrosol toner, include the material composition of following mass fraction：Chinese gooseberry seed extract solution 1%-
5%, sponge gourd water 0.5%-2.0%, Sodium Hyaluronate 3%-5%, caprylic acid 0.1%-0.5%, sodium alginate 0.7%-
1.2%, squalene 1%-2%, propane diols 0.2%-1.0%, ivy extract solution 1.5%-2.5%, methyl benzoate
2.0%-3.5%, rosemary hydrosol complement to 100%.
The preparation method of above-mentioned rosemary hydrosol toner comprises the following steps：
(1) prepared by rosemary hydrosol：It is 1 by floral leaf mass ratio to take rosemary to spend with rosemary leave:2 well mixed rear powder
It is broken, it is afterwards 1 by feed liquid mass ratio by the rosemary floral leaf chip of crushing:1.2 addition deionized waters, ultrasonication 15min,
After vapo(u)rizing temperature be less than 65 DEG C under conditions of be evaporated in vacuo, collect distillate, cool down and produce rosemary hydrosol；
(2) preparation of Chinese gooseberry seed extract solution：Chinese gooseberry seed is crushed to 40-50 mesh, with feed liquid mass ratio 1:2 additions are gone
Ionized water, refrigerated centrifuge is carried out after ice-water bath concussion extraction 3h, takes the supernatant after centrifugation to cross microfiltration membrane and carry out decolouring and removes
It is miscellaneous, filtrate is collected, produces Chinese gooseberry seed extract solution；
(3) preparation of ivy extract solution：Ivy is crushed to 20 mesh, by feed liquid mass ratio 1:4 addition deionized waters,
Refrigerated centrifuge is carried out after ice-water bath concussion extraction 5h, takes the supernatant after centrifugation to cross microfiltration membrane and carries out decolouring removal of impurities, collect
Filtrate, produce ivy extract solution；
(4) preparation of sponge gourd water：Luffa vine in growth course is cut at 5-10cm from the ground, luffa vine insertion is connect
Receive in bottle, seal bottleneck with preservative film, place 24h, take out receiving bottle, the liquid in receiving bottle is filtered, filtrate is sponge gourd water；
(5) batch mixing：By Sodium Hyaluronate, caprylic acid, sodium alginate, squalene, propane diols, methyl benzoate and preparation
Chinese gooseberry seed extract solution, sponge gourd water, ivy extract solution, rosemary hydrosol are put into stainless steel together, carry out vacuum low speed
Stirring, it is 15 DEG C to control whipping temp, stirs 4h, obtains mixed liquor；
(6) sterilize, be filling：The degerming rear progress of mixed liquor progress filtering with microporous membrane is filling, produce product of the present invention.
Embodiment 6
A kind of rosemary hydrosol toner, include the material composition of following mass fraction：Chinese gooseberry seed extract solution 1%-
5%, sponge gourd water 0.5%-2.0%, Sodium Hyaluronate 3%-5%, caprylic acid 0.1%-0.5%, sodium alginate 0.7%-
1.2%, squalene 1%-2%, propane diols 0.2%-1.0%, ivy extract solution 1.5%-2.5%, methyl benzoate
2.0%-3.5%, rosemary hydrosol complement to 100%.
The preparation method of above-mentioned rosemary hydrosol toner comprises the following steps：
(1) prepared by rosemary hydrosol：It is 1 by floral leaf mass ratio to take rosemary to spend with rosemary leave:5 well mixed rear powder
It is broken, it is afterwards 1 by feed liquid mass ratio by the rosemary floral leaf chip of crushing:2.0 addition deionized waters, ultrasonication 30min,
After vapo(u)rizing temperature be less than 65 DEG C under conditions of be evaporated in vacuo, collect distillate, cool down and produce rosemary hydrosol；
(2) preparation of Chinese gooseberry seed extract solution：Chinese gooseberry seed is crushed to 40-50 mesh, with feed liquid mass ratio 1:4 additions are gone
Ionized water, refrigerated centrifuge is carried out after ice-water bath concussion extraction 10h, takes the supernatant after centrifugation to cross microfiltration membrane and carry out decolouring and removes
It is miscellaneous, filtrate is collected, produces Chinese gooseberry seed extract solution；
(3) preparation of ivy extract solution：Ivy is crushed to 20-40 mesh, by feed liquid mass ratio 1:10 addition go from
Sub- water, ice-water bath concussion carry out refrigerated centrifuge after extracting 5h, take the supernatant after centrifugation to cross microfiltration membrane and carry out decolouring removal of impurities,
Filtrate is collected, produces ivy extract solution；
(4) preparation of sponge gourd water：Luffa vine in growth course is cut at 5-10cm from the ground, luffa vine insertion is connect
Receive in bottle, seal bottleneck with preservative film, place 48h, take out receiving bottle, the liquid in receiving bottle is filtered, filtrate is sponge gourd water；
(5) batch mixing：By Sodium Hyaluronate, caprylic acid, sodium alginate, squalene, propane diols, methyl benzoate and preparation
Chinese gooseberry seed extract solution, sponge gourd water, ivy extract solution, rosemary hydrosol are put into stainless steel together, carry out vacuum low speed
Stirring, it is 50 DEG C to control whipping temp, stirs 1h, obtains mixed liquor；
(6) sterilize, be filling：The degerming rear progress of mixed liquor progress filtering with microporous membrane is filling, produce product of the present invention.
Embodiment 7
A kind of rosemary hydrosol toner, include the material composition of following mass fraction：Chinese gooseberry seed extract solution 1%-
5%, sponge gourd water 0.5%-2.0%, Sodium Hyaluronate 3%-5%, caprylic acid 0.1%-0.5%, sodium alginate 0.7%-
1.2%, squalene 1%-2%, propane diols 0.2%-1.0%, ivy extract solution 1.5%-2.5%, methyl benzoate
2.0%-3.5%, rosemary hydrosol complement to 100%.
The preparation method of above-mentioned rosemary hydrosol toner comprises the following steps：
(1) prepared by rosemary hydrosol：It is 1 by floral leaf mass ratio to take rosemary to spend with rosemary leave:3.5 well mixed rear powder
It is broken, it is afterwards 1 by feed liquid mass ratio by the rosemary floral leaf chip of crushing:1.6 addition deionized waters, ultrasonication 25min,
After vapo(u)rizing temperature be less than 65 DEG C under conditions of be evaporated in vacuo, collect distillate, cool down and produce rosemary hydrosol；
(2) preparation of Chinese gooseberry seed extract solution：Chinese gooseberry seed is crushed to 40-50 mesh, with feed liquid mass ratio 1:3 additions are gone
Ionized water, refrigerated centrifuge is carried out after ice-water bath concussion extraction 7h, takes the supernatant after centrifugation to cross microfiltration membrane and carry out decolouring and removes
It is miscellaneous, filtrate is collected, produces Chinese gooseberry seed extract solution；
(3) preparation of ivy extract solution：Ivy is crushed to 20-40 mesh, by feed liquid mass ratio 1:7 addition deionizations
Water, ice-water bath concussion carry out refrigerated centrifuge after extracting 4h, take the supernatant after centrifugation to cross microfiltration membrane and carry out decolouring removal of impurities, receive
Collect filtrate, produce ivy extract solution；
(4) preparation of sponge gourd water：Luffa vine in growth course is cut at 5-10cm from the ground, luffa vine insertion is connect
Receive in bottle, seal bottleneck with preservative film, place 32h, take out receiving bottle, the liquid in receiving bottle is filtered, filtrate is sponge gourd water；
(5) batch mixing：By Sodium Hyaluronate, caprylic acid, sodium alginate, squalene, propane diols, methyl benzoate and preparation
Chinese gooseberry seed extract solution, sponge gourd water, ivy extract solution, rosemary hydrosol are put into stainless steel together, carry out vacuum low speed
Stirring, it is 35 DEG C to control whipping temp, stirs 2.5h, obtains mixed liquor；
(6) sterilize, be filling：The degerming rear progress of mixed liquor progress filtering with microporous membrane is filling, produce product of the present invention.
Claims (4)
1. a kind of rosemary hydrosol toner, it is characterised in that include the material composition of following mass fraction：Chinese gooseberry seed extracts
Liquid 1%-5%, sponge gourd water 0.5%-2.0%, Sodium Hyaluronate 3%-5%, caprylic acid 0.1%-0.5%, sodium alginate
0.7%-1.2%, squalene 1%-2%, propane diols 0.2%-1.0%, ivy extract solution 1.5%-2.5%, benzoic acid first
Ester 2.0%-3.5%, rosemary hydrosol complement to 100%；
The preparation method of above-mentioned rosemary hydrosol toner comprises the following steps：
(1) prepared by rosemary hydrosol：It is 1 by floral leaf mass ratio to take rosemary to spend with rosemary leave:3.5 it is well mixed after crush,
It is afterwards 1 by feed liquid mass ratio by the rosemary floral leaf chip of crushing:1.6 deionized water is added, ultrasonication 25min, it
It is evaporated in vacuo under conditions of vapo(u)rizing temperature is less than 65 DEG C, collects distillate, cool down and produce rosemary hydrosol；
(2) preparation of Chinese gooseberry seed extract solution：Chinese gooseberry seed is crushed to 40-50 mesh, with feed liquid mass ratio 1:3 addition deionizations
Water, ice-water bath concussion carry out refrigerated centrifuge after extracting 7h, take the supernatant after centrifugation to cross microfiltration membrane and carry out decolouring removal of impurities, receive
Collect filtrate, produce Chinese gooseberry seed extract solution；
(3) preparation of ivy extract solution：Ivy is crushed to 20-40 mesh, by feed liquid mass ratio 1:7 addition deionized waters,
Refrigerated centrifuge is carried out after ice-water bath concussion extraction 4h, takes the supernatant after centrifugation to cross microfiltration membrane and carries out decolouring removal of impurities, collect
Filtrate, produce ivy extract solution；
(4) preparation of sponge gourd water：Luffa vine in growth course is cut at 5-10cm from the ground, luffa vine is inserted into receiving bottle
In, bottleneck is sealed with preservative film, places 32h, takes out receiving bottle, the liquid in receiving bottle is filtered, filtrate is sponge gourd water；
(5) batch mixing：By Sodium Hyaluronate, caprylic acid, sodium alginate, squalene, propane diols, methyl benzoate and the macaque prepared
Peach seed extract solution, sponge gourd water, ivy extract solution, rosemary hydrosol are put into stainless steel together, carry out vacuum stirring at low speed,
It is 35 DEG C to control whipping temp, stirs 2.5h, obtains mixed liquor；
(6) sterilize, be filling：It is filling that mixed liquor is subjected to the degerming rear progress of filtering with microporous membrane.
2. a kind of rosemary hydrosol toner as claimed in claim 1, it is characterised in that include the material of following mass fraction
Composition：Chinese gooseberry seed extract solution 1%, sponge gourd water 2.0%, Sodium Hyaluronate 3%, caprylic acid 0.5%, sodium alginate 0.7%, angle
MF59 2%, propane diols 0.2%, ivy extract solution 1.5%, methyl benzoate 3.5%, rosemary hydrosol complement to 100%.
3. a kind of rosemary hydrosol toner as claimed in claim 1, it is characterised in that include the material of following mass fraction
Composition：Chinese gooseberry seed extract solution 5%, sponge gourd water 0.5%, Sodium Hyaluronate 5%, caprylic acid 0.1%, sodium alginate 1.2%, angle
MF59 1%, propane diols 1.0%, ivy extraction thing liquid 2.5%, methyl benzoate 2.0%, rosemary hydrosol complement to
100%.
4. a kind of rosemary hydrosol toner as claimed in claim 1, it is characterised in that include the material of following mass fraction
Composition：Chinese gooseberry seed extract solution 3%, sponge gourd water 1.5%, Sodium Hyaluronate 3.5%, caprylic acid 0.3%, sodium alginate 1.0%,
Squalene 1.2%, propane diols 0.6%, ivy extract solution 1.7%, methyl benzoate 3.0%, rosemary hydrosol complement to
100%.
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| CN104856905A (en) * | 2015-05-30 | 2015-08-26 | 防城港市防城区那梭香料厂 | Hydrolat containing cymbopogon citratus |
| CN105055236A (en) * | 2015-08-13 | 2015-11-18 | 刘汉科 | Rosemary hydrosol lotion and preparation method thereof |
| CN105769725A (en) * | 2016-03-02 | 2016-07-20 | 禹州市天源生物科技有限公司 | Rosemary moisturizing water and making method thereof |
| CN105662971A (en) * | 2016-03-04 | 2016-06-15 | 佛山市聚成生化技术研发有限公司 | Chinese herbal medicine composition and application thereof |
| CN106236657A (en) * | 2016-08-30 | 2016-12-21 | 湖南省雅迭香科技有限公司 | Herba Rosmarini Officinalis pure natural cosmetic water |
| CN106511142A (en) * | 2017-01-18 | 2017-03-22 | 广西南宁博智生物科技有限公司 | Centella asiatica floral water and preparation method and application thereof |
| CN109966204A (en) * | 2019-04-02 | 2019-07-05 | 北京旋光普利生物医药科技开发有限公司 | A kind of preparation of hydrosol oligopeptides polypeptide toner |
| CN110693791A (en) * | 2019-11-29 | 2020-01-17 | 北京旋光普利生物医药科技开发有限公司 | Preparation of pure dew yeast essence toner (toning lotion) |
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| FR2788435B1 (en) * | 1999-01-15 | 2002-08-02 | Oreal | USE OF AN EXTRACT OF A PLANT OF THE GENUS ROSMARINUS IN COMPOSITIONS FOR TREATING SKIN SIGNS OF AGING |
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| JP2002047143A (en) * | 2000-07-31 | 2002-02-12 | Reiko Tokuchi | Rosemary-distilled water and method for manufacturing the same |
| CN101569602A (en) * | 2009-06-11 | 2009-11-04 | 合肥红峥果业科技有限公司 | Method for preparing towel gourd water and towel gourd water prepared thereby |
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