CN105769725A - Rosemary moisturizing water and making method thereof - Google Patents
Rosemary moisturizing water and making method thereof Download PDFInfo
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Abstract
The invention provides rosemary moisturizing water which is prepared from, by mass, 0.3-0.9% of rosemary water-soluble extract, 0.05-0.15% of rosemary essential oil, 5-10% of ethyl alcohol, 5-10% of glycerinum, 0.05-0.12% of hyaluronic acid, 8-15% of a hydrolyzed pearl solution and the balance purified water.The produced rosemary moisturizing water has fragrance peculiar to rosemary and has the special functions of being resistant to corrosion, resisting to oxidization and delaying aging, the moisturizing function is more obvious through compounding of the glycerinum and the hyaluronic acid, and a more complete moisturizing effect is achieved; the hydrolyzed pearl solution contains multiple types of amino acid and microelements, and the beautifying effect on the skin is better.The rosemary moisturizing water has charming fragrance of rosemary and an obvious moisturizing effect, has multiple functions of whitening and resisting to aging at the same time and is suitable for skin dryness caring and whitening.
Description
Technical field
The invention belongs to cosmetics and production technology field thereof, be specifically related to a kind of rosemary moisture retention water and making thereof
Method.
Background technology
Natural moisture preserving system in human body skin is mainly made up of water, lipid, NMF (NMF).Existing
At widely used moisture-keeping cosmetics in order to simulate the natural moisture preserving system being made up of in human body skin oil, water, NMF
System, effect be to delay loss of moist, increase dermoepidermal moisture penetration, temporarily provide for skin protection,
Reduce damage, promote repair process.Moisturizer be mainly composed of water, NMF and grease.
Glycerine has another name called glycerine, is a kind of colourless, thick liquid that odorless, taste are sweet, has the strongest hygroscopicity,
Pure glycerine can absorb the moisture of 40%, can form thin film so putting on the skin on skin, have isolation air and
Prevent the effect that moisture evaporates, moreover it is possible to absorb the moisture in air.Glycerine is that in cosmetics, consumption is maximum,
Common NMF, safety, cheap.
Hyaluronic acid (HA) has another name called sodium hyaluronate, has special water retention, and its hyalomitome molecule can carry 500
Moisture more than times, is the material that in the nature having now been found that, moisture retention is best, is referred to as the most natural
NMF.HA is a kind of multi-functional matrix, is distributed widely in partes corporis humani position.Wherein skin also contains greatly
The hyaluronic acid of amount, it can improve skin-nourishing metabolism, makes that skin is tender, smooth, go wrinkle, increase bullet
Property, prevent aging, be again good skin penetration enhancer while moisturizing.HA can also promote that epidermis is thin
The propagation of born of the same parents and differentiation, scavenging activated oxygen, can prevent and repair skin injury.Hyaluronic acid aqueous solution has
There is the highest viscosity, aqueous phase thickening can be made；Lotion uniform and smooth after emulsifying with oil phase, has stable emulsion
Effect.HA is the natural moisture preserving composition that the cosmetics of super quality are best, and its compatibility is good, almost can add and take office
In what cosmetics, being widely used in the cosmetics such as cream, emulsion, moisture retention water, general addition is
0.05 0.5%.
NMF conventional in cosmetics has glycerine, propane diols, polyethylene glycol, pyrrolidone sodium carboxylate, collagen
Albumen etc., test shows, compared with these NMFs, the moisture retention of HA is affected less by ambient humidity.
HA hygroscopic capacity under low relative humidity (such as 30%) is higher, and hygroscopic capacity under high relative humidity (such as 70%)
Relatively low.The character of this uniqueness, positive adaptation skin is under Various Seasonal, varying environment humidity, to cosmetics
The requirement of moisture-keeping function.HA can be used alone as NMF, it is also possible to other NMFs with the use of.
Pearl is a kind of ancient organic gemstone, produces in pearl shellfish and pearl oyster shellfish mollusk body, due to
Endocrine effect and the mineral bead calciferous that generates, be to be formed by the most small aragonite crystals set
's.Important biomolecule active material in biochemical reaction process, energy in contained by pearl, chemical composition is human body
Promote human metabolism, regulation physiological function, thus play treatment and the health care of pearl.Modern medicine
Reason research proves that pearl has anti-aging, resisting stress, anti-oxidant, eyeshield, antiulcer, spoke antitumor, anti-
Penetrate, establishing-Yang, the effect such as antibacterial and hemostasis, the immunologic function of human body can also be strengthened simultaneously and promote wound healing
Deng effect.Clinic be widely used in treatment eye illness, canker, osteoporosis, burn, scald, soft group
Knit defect, uterine hemorrhage, cervix erosion etc..Along with growth in the living standard, the more and more application of pearl
In health care and beautification product.Chitosan-alginate microcapsules, amino acid contained by pearl, that various trace elements can strengthen skin is new
Old metabolism, promotion reepithelialization, the pearl powder massaging skin that fineness is enough has good conduit to pore
Effect.It is tender fair and clear that reasonable employment pearl powder can protect skin, moistens smooth, prevents unique merit of skin senescence
Effect.
Pearl is the grit parcel that will be dropped into by sea cowry or the freshwater mussel organic matter oneself secreted.
Wherein, calcium carbonate, leucine, glycine methionine, alanine, glutamic acid, aspartic acid and some
Trace element lead, copper, magnesium, zinc, manganese, sodium, selenium etc..It is introduced, amino acid is that health grows it
Required, in the trace element that pearl contains: selenium has anti-aging effects；Zinc is the constituent of multiple enzyme, ginseng
Machine-processed with internal degree of exempting from and metabolic, directly affect human physiological activity.According to modern medical analysis, precious
After integument absorption of human body, the vigor of human enzymes, the acid-base value of regulation blood can be promoted, make the life of cell
Life power strengthens, thus delays the aging of cell, makes wrinkle of skin reduce, plays the mesh promoted longevity and improve looks
's.
Pearl powder can be clearing heat and detoxicating, cleaning skin, controls oil point, may additionally facilitate damaged tissues regeneration and recovers.
But owing to pearl powder containing substantial amounts of calcium component, it is unfavorable for the human body absorption to active ingredient.Pass through acidolysis
The hydrolyzed pearl solution of pearl powder gained has eliminated substantial amounts of calcium carbonate, remain amino acid in pearl and
Various trace elements, can preferably should have in cosmetics.
Rosemary, is a kind of time-honored spice berry originating in Mediterranean, and 1981 by section of China
Institute is firstly introduced China and cultivates successfully, and the ground such as present Henan, Yunnan, Hunan, Sichuan, Guizhou has
Plantation.Extracting the powdered substance obtained from rosemary plant, main component has anti-oxidation function
Phenol, acid, flavones ingredient；Rosemary Oil is then a kind of fluid oil being made up of more than 30 kinds of volatile ingredients
Shape thing.Rosmarinus officinalis extract has efficient, nontoxic antioxidant effect, can be widely applied to food, function
In food, spices and the industry such as flavouring and daily-use chemical industry.
Main component Rosmarinic acid in rosemary water-soluble extractive is that a kind of natural multiple physiology that has is lived
The soluble phenolic compounds of property, has extremely strong many biologically actives, such as: anti-oxidant, antibacterial,
Anti-inflammatory, suppression hiv integrase, suppression hyaluronidase isoreactivity.As natural, rosemary
Acid has the extremely strong activity removing interior free yl, protects cell tissue, the generation of prevention numerous disease,
The protection cardiovascular and cerebrovascular circulatory system, the anticancer and physiological action such as delay senility.
Rosemary extracts and Rosemary Oil has limitless purposes at cosmetic field.Rosemary in the world
Existing multinomial cosmetics patent, Rosmarinus officinalis extract is widely used in skin care item, shampoo, perfume (or spice) by people already
In water etc..Rosmarinus officinalis extract has convergence, can Rosemary Extract.Human free radical and suppression can also be removed
The degraded of basic protein such that it is able to keep elasticity and the gloss of skin.Because it has reparation, strongly moisturizing
Function and easy absorbed advantage, it is also possible to improve the problem such as dry skin, coarse, decortication.Rosmarinic acid
The activity of hyaluronidase can be suppressed, keep hyaluronic acid to exist for a long time at epidermal cell, hence help to
The microorganism and the toxicant that stop invasion spread in epidermis.Rosmarinus officinalis extract is excellent in cosmetics adding
Add agent.It can play in the cosmetics color spot, anti-oxidant, increase skin elasticity, delay senility etc. and to make
With.
Summary of the invention
Obvious in order to make a kind of moistening effect, have the moisture retention water of whitening and anti-aging effect concurrently, the present invention provides
A kind of rosemary moisture retention water and preparation method thereof.
The technical solution used in the present invention is:
A kind of rosemary moisture retention water, its constituent includes rosemary water-soluble extractive, Rosemary Oil, second
Alcohol, glycerine, hyaluronic acid, hydrolyzed pearl solution and purified water, the addition of each composition divides by mass percentage
Not Wei rosemary water-soluble extractive 0.3-0.9%, Rosemary Oil 0.05-0.15%, ethanol 5-10%, glycerine
5-10%, hyaluronic acid 0.05-0.12%, hydrolyzed pearl solution 8-15%, remaining is purified water.
Described ethanol is absolute ethyl alcohol or edible ethanol.
Described rosemary water-soluble extractive is prepared by following method: the fresh leaf of rosemary, through naturally drying, is used
Purified water refluxing extraction, extract is concentrated, ethyl acetate extracts, cross AB-8 resin column, reclaims eluent
Ethanol is extremely without ethanol taste, then concentrated extracting solution obtains concentrate, and concentrate is spray-dried i.e. obtains rosemary
Water-soluble extractive.
In described rosemary water-soluble extractive, the content of Rosmarinic acid is 35-45%.
Described Rosemary Oil is prepared by following method: the fresh leaf of rosemary or cured leaf through steam distillation,
Obtaining Rosemary Oil and the mixed solution of water, through extraction equipment, the water removing lower floor i.e. obtains Rosemary Oil.
During the preparation of described hyaluronic acid, the first hyaluronic acid of preparation 1%, then it is diluted to desired concn.
Described hydrolyzed pearl solution is prepared by following method: crushing pearl, crosses 100 mesh sieves, and gained pearl powder is used
Phosphoric acid solution refluxing extraction, extract filters, obtains hydrolyzed pearl solution.
The preparation method of described a kind of rosemary moisture retention water, by above-mentioned rosemary water-soluble extractive, glycerine,
Hyaluronic acid and hydrolyzed pearl solution join in ethanol, stirring and dissolving, add purified water and mix, so
Rear addition Rosemary Oil, pasteurization after being sufficiently stirred for dissolving, the most filling for finished product.
The temperature of described described pasteurization is 80-95 DEG C, and the time is 4-6min.
The rosemary moisture retention water that the preparation method of described a kind of rosemary moisture retention water obtains.
The invention has the beneficial effects as follows: the rosemary moisture retention water that the present invention produces has the distinctive fragrance of rosemary,
Improve the multiple efficacies such as skin moisture-keeping situation, moisturizing whitening, Rosmarinic acid and rosemary in Rosmarinus officinalis extract
Essential oil is natural antioxidant, has the special role of moisturizing, anticorrosion, whitening, delaying senility；Glycerine
It is combined moisture-keeping function with hyaluronic acid to become apparent from, reaches more fully moistening effect；In hydrolyzed pearl solution
The several amino acids contained and trace element, amino acid is the basic element of tissue synthetic protein, ammonia
Base acid is directly entered human body, is more beneficial for the metabolic adsorption of human body, and trace element has anti-aging and whitening etc.
Multiple efficacies, to the cosmetic result of skin more preferably；Ethanol has antisepsis, and accelerates active ingredient absorption
Effect, glycerine and hyaluronic acid are excellent NMF, and moistening effect is fine, and product of the present invention has
Significantly moistening effect, has the multiple effects such as whitening and anti-aging concurrently, is suitable for dry skin nursing and whitening.
Detailed description of the invention
A kind of rosemary moisture retention water, its constituent includes rosemary water-soluble extractive, Rosemary Oil, second
Alcohol, glycerine, hyaluronic acid, hydrolyzed pearl solution and purified water, the addition of each composition divides by mass percentage
Not Wei rosemary water-soluble extractive 0.3-0.9%, Rosemary Oil 0.05-0.15%, ethanol 5-10%, glycerine
5-10%, hyaluronic acid 0.05-0.12%, hydrolyzed pearl solution 8-15%, remaining is purified water.
Described ethanol is absolute ethyl alcohol or edible ethanol.
During preparation hyaluronic acid, the first hyaluronic acid of preparation 1%, then it is diluted to desired concn.
Described rosemary water-soluble extractive is prepared by following method: the fresh leaf of rosemary, through naturally drying, is used
Purified water refluxing extraction, extract is concentrated, ethyl acetate extracts, cross AB-8 resin column, reclaims eluent
Ethanol is extremely without ethanol taste, then concentrated extracting solution obtains concentrate, and concentrate is spray-dried i.e. obtains rosemary
Water-soluble extractive.In rosemary water-soluble extractive, the content of Rosmarinic acid is 35-45%.
The fresh leaf of rosemary, through naturally drying, with purified water according to solid-liquid ratio 1:20, divides through circumfluence distillation 30-50
Clock, extracts concentrate, and the proportion of concentrate is 1.15-1.20, and concentrate and ethyl acetate are according to the ratio of 1:2
Extract 2 times, each 30 minutes, when extract i.e. upper strata ethyl acetate solution reduced pressure concentration is recycled to original volume
1/10 time, add the purified water concentration and recovery of 1 times of volume to without ethyl acetate taste, concentrate is with 10%
Hydrochloric acid solution regulation pH value is 3.0, upper AB-8 resin column, then with ethanol elution, reclaims eluent i.e.
The ethanol solution that wash-out is collected is extremely without ethanol taste, then with the content of Rosmarinic acid in HPLC detection concentrate is
35-45%, finally obtains rosemary water-soluble extractive by concentrate by spray drying.
Described Rosemary Oil is prepared by following method: the fresh leaf of rosemary or cured leaf through steam distillation,
Obtain Rosemary Oil and the mixed solution of water, through extraction equipment, remove the water of lower floor and obtain Rosemary Oil.
Described hydrolyzed pearl solution is prepared by following method: crushing pearl, crosses 100 mesh sieves, and gained pearl powder is used
Phosphoric acid solution refluxing extraction, extract filters, obtains hydrolyzed pearl solution.
After gained pearl powder mixes according to solid-liquid ratio 1:9-1:11 with the sulfuric acid solution of 3.5-4.0%, refluxing extraction 8-10
Hour, filter, obtain hydrolyzed pearl solution.
The preparation method of a kind of above-mentioned rosemary moisture retention water, by above-mentioned rosemary water-soluble extractive, glycerine, thoroughly
The acid of bright matter and hydrolyzed pearl solution join in ethanol, and stirring and dissolving adds purified water and mixes, then
Add Rosemary Oil, pasteurization after being sufficiently stirred for dissolving, the most filling for finished product.Described Pasteur disappears
The temperature of poison is 80-95 DEG C, and the time is 4-6min.
The rosemary moisture retention water that the preparation method of described a kind of rosemary moisture retention water obtains.
Embodiment 1
A kind of rosemary moisture retention water, its constituent includes rosemary water-soluble extractive, Rosemary Oil, second
Alcohol, glycerine, hyaluronic acid, hydrolyzed pearl solution and purified water, the addition of each composition divides by mass percentage
Not Wei rosemary water-soluble extractive 0.5%, Rosemary Oil 0.1%, ethanol 5%, glycerine 10%, transparent
Matter acid 0.1%, hydrolyzed pearl solution 10%, remaining is purified water.Described ethanol is absolute ethyl alcohol or edible ethanol.
The hyaluronic acid solution that hyaluronic acid contents is 1% the most first prepared by described hyaluronic acid, then adds
The amount of hyaluronic acid solution be 10%.
The fresh leaf of rosemary, through naturally drying, with purified water according to solid-liquid ratio 1:20 circumfluence distillation 30 minutes, carries
Taking concentrate, the densimeter detected value of concentrate is 1.18, and concentrate extracts according to the ratio of 1:2 with ethyl acetate
Take 2 times, each 30 minutes, when extract i.e. upper strata ethyl acetate solution reduced pressure concentration is recycled to original volume
When 1/10, add the purified water concentration and recovery of 1 times of volume to without ethyl acetate taste, concentrate with 10% salt
Acid solution regulation pH value is 3.0, upper AB-8 resin column, according to 3 times of column volume loadings, and flow velocity 1.5BV/h,
Clean by 5BV purified water after end of the sample, then with 3BV, the ethanol elution of 40%, flow velocity 1.5BV/h,
Eluent i.e. elutes the ethanol solution of collection and reclaims ethanol extremely without ethanol taste, by HPLC detection concentrate
The content of Rosmarinic acid is 36.88%, i.e. obtains rosemary water-soluble extractive after concentrate is spray-dried.
Described Rosemary Oil preparation method is as follows: rosemary cured leaf, through steam distillation, obtains rosemary
Essential oil and the mixed solution of water, through extraction equipment, remove the water of lower floor and obtain Rosemary Oil.
Described hydrolyzed pearl solution is prepared by following method: crushing pearl, crosses 100 mesh sieves, is 3.8% with concentration
Phosphoric acid solution according to solid-liquid ratio 1:10 mix, refluxing extraction 10h, extract filter, obtain pearl hydrolysis
Liquid；
The preparation method of a kind of rosemary moisture retention water, by above-mentioned rosemary water-soluble extractive, glycerine, hyalomitome
Acid and hydrolyzed pearl solution join in ethanol, and stirring and dissolving adds purified water and mixes, is subsequently adding
Rosemary Oil, pasteurization after being sufficiently stirred for dissolving, the most filling for finished product.Described pasteurization
Temperature is 82 DEG C, and the time is 6min.
Embodiment 2
A kind of rosemary moisture retention water, its constituent includes rosemary water-soluble extractive, Rosemary Oil, second
Alcohol, glycerine, hyaluronic acid, hydrolyzed pearl solution and purified water, the addition of each composition by volume percentage divides
Not Wei rosemary water-soluble extractive 0.39%, Rosemary Oil 0.15%, ethanol 10%, glycerine 5%, thoroughly
Bright matter acid solution 0.05%, hydrolyzed pearl solution 10%, remaining is purified water.Described ethanol is absolute ethyl alcohol or food
Use ethanol.The hyaluronic acid solution that hyaluronic acid contents is 1% the most first prepared by described hyaluronic acid,
The amount of the hyaluronic acid solution then added is 5%.
Described rosemary water-soluble extractive is prepared by following method: the fresh leaf of rosemary, through naturally drying, is used
Purified water refluxing extraction, extract is concentrated, ethyl acetate extracts, cross AB-8 resin column, reclaims eluent
Ethanol is extremely without ethanol taste, then concentrated extracting solution obtains concentrate, and concentrate is spray-dried i.e. obtains rosemary
Water-soluble extractive.
The fresh leaf of rosemary, through naturally drying, with purified water according to solid-liquid ratio 1:20 circumfluence distillation 30 minutes, carries
Taking concentrate, the densimeter detected value of concentrate is 1.18, and concentrate extracts according to the ratio of 1:2 with ethyl acetate
Take 2 times, each 30 minutes, when extract i.e. upper strata ethyl acetate solution reduced pressure concentration is recycled to original volume
When 1/10, add the purified water concentration and recovery of 1 times of volume to without ethyl acetate taste, concentrate with 10% salt
Acid solution regulation pH value is 3.0, upper AB-8 resin column, according to 3 times of column volume loadings, and flow velocity 1.5BV/h,
Clean by 5BV purified water after end of the sample, then with 3BV, the ethanol elution of 40%, flow velocity 1.5BV/h,
Reclaim eluent and i.e. elute the ethanol solution of collection to without ethanol taste, changed by fan in HPLC detection concentrate
The content of fragrant acid is 36.88%, i.e. obtains rosemary water-soluble extractive after concentrate is spray-dried.
Described Rosemary Oil preparation method is as follows: rosemary cured leaf, through steam distillation, obtains rosemary
Essential oil and the mixed solution of water, through extraction equipment, remove the water of lower floor and obtain Rosemary Oil.
Described hydrolyzed pearl solution is prepared by following method: crushing pearl, crosses 100 mesh sieves, is 3.8% with concentration
Phosphoric acid solution according to solid-liquid ratio 1:10 mix, refluxing extraction 10h, extract filter, obtain pearl hydrolysis
Liquid；
The preparation method of a kind of rosemary moisture retention water, by above-mentioned rosemary water-soluble extractive, glycerine, hyalomitome
Acid solution and hydrolyzed pearl solution join in ethanol, stirring and dissolving, add purified water and mix, then
Add Rosemary Oil, pasteurization after being sufficiently stirred for dissolving, the most filling for finished product.Described Pasteur disappears
The temperature of poison is 95 DEG C, and the time is 5min.
Table 1 is the part combination of each composition of the present invention
In remaining embodiment, suitable according to shown in above-mentioned of rosemary water-soluble extractive and Rosemary Oil
Sequence circulate, ethanol according to 5,6,7,8,9,10 sequential loop, glycerine is 5, and hyaluronic acid is 0.05,
Hydrolyzed pearl solution is 8, and remaining is purified water；In above-mentioned rosemary water-soluble extractive, Rosemary Oil and second
Alcohol circulation on the basis of, glycerine according to 5,6,7,8,9,10 sequential loop, hyaluronic acid is 0.05,
Hydrolyzed pearl solution is 8, and remaining is purified water；In above-mentioned rosemary water-soluble extractive, Rosemary Oil, second
On the basis of alcohol and glycerine circulation, hyaluronic acid according to 0.05,0.06,0.07,0.08,0.09,0.10,
0.11, the sequential loop of 0.12, hydrolyzed pearl solution is 8, and remaining is purified water；Water-soluble at above-mentioned rosemary
Property extract, Rosemary Oil, ethanol, glycerine and hyaluronic acid circulation on the basis of, hydrolyzed pearl solution is pressed
According to the sequential loop of 8,9,10,11,12,13,14,15, remaining is purified water.
Claims (10)
1. a rosemary moisture retention water, it is characterized in that: its constituent includes rosemary water-soluble extractive, Rosemary Oil, ethanol, glycerine, hyaluronic acid, hydrolyzed pearl solution and purified water, the addition of each composition is respectively rosemary water-soluble extractive 0.3-0.9% by mass percentage, Rosemary Oil 0.05-0.15%, ethanol 5-10%, glycerine 5-10%, hyaluronic acid 0.05-0.12%, hydrolyzed pearl solution 8-15%, remaining is purified water.
A kind of rosemary moisture retention water the most according to claim 1, it is characterised in that: described ethanol is absolute ethyl alcohol or edible ethanol.
A kind of rosemary moisture retention water the most according to claim 1, it is characterized in that: described rosemary water-soluble extractive is prepared by following method: the fresh leaf of rosemary is through naturally drying, use purified water refluxing extraction, extract is concentrated, ethyl acetate extracts, cross AB-8 resin column, reclaim eluant ethanol to without ethanol taste, concentrated extracting solution obtains concentrate again, and concentrate is spray-dried i.e. obtains rosemary water-soluble extractive.
A kind of rosemary moisture retention water the most according to claim 3, it is characterised in that: in described rosemary water-soluble extractive, the content of Rosmarinic acid is 35-45%.
A kind of rosemary moisture retention water the most according to claim 1, it is characterized in that: described Rosemary Oil is prepared by following method: the fresh leaf of rosemary or cured leaf are through steam distillation, obtain Rosemary Oil and the mixed solution of water, through extraction equipment, the water removing lower floor i.e. obtains Rosemary Oil.
A kind of rosemary moisture retention water the most according to claim 1, it is characterised in that: during the preparation of described hyaluronic acid, the first hyaluronic acid of preparation 1%, then it is diluted to desired concn.
A kind of rosemary moisture retention water the most according to claim 1, it is characterised in that: described hydrolyzed pearl solution is prepared by following method: crushing pearl, crosses 100 mesh sieves, gained pearl powder phosphoric acid solution refluxing extraction, and extract filters, obtains hydrolyzed pearl solution.
8. the preparation method of an a kind of rosemary moisture retention water as claimed in claim 1, it is characterized in that: above-mentioned rosemary water-soluble extractive, glycerine, hyaluronic acid and hydrolyzed pearl solution are joined in ethanol, stirring and dissolving, add purified water to mix, it is subsequently adding Rosemary Oil, pasteurization after being sufficiently stirred for dissolving, the most filling for finished product.
The preparation method of a kind of rosemary moisture retention water the most according to claim 8, it is characterised in that: the temperature of described described pasteurization is 80-95 DEG C, and the time is 4-6min.
The rosemary moisture retention water that the preparation method of a kind of rosemary moisture retention water the most according to claim 8 obtains.
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| CN201610116989.1A CN105769725A (en) | 2016-03-02 | 2016-03-02 | Rosemary moisturizing water and making method thereof |
| PCT/CN2016/105849 WO2017148180A1 (en) | 2016-03-02 | 2016-11-15 | Rosemary moisturizing solution and manufacturing method therefor |
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| CN201610116989.1A CN105769725A (en) | 2016-03-02 | 2016-03-02 | Rosemary moisturizing water and making method thereof |
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| WO2017148180A1 (en) | 2017-09-08 |
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