CN113679656B - Traditional Chinese medicine extract cosmetic composition and preparation method thereof - Google Patents
Traditional Chinese medicine extract cosmetic composition and preparation method thereof Download PDFInfo
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- CN113679656B CN113679656B CN202111114321.0A CN202111114321A CN113679656B CN 113679656 B CN113679656 B CN 113679656B CN 202111114321 A CN202111114321 A CN 202111114321A CN 113679656 B CN113679656 B CN 113679656B
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Abstract
The invention discloses a traditional Chinese medicine extract cosmetic composition which comprises the following components in parts by weight: 10-50 parts of an antioxidant component, 10-50 parts of a whitening and moisturizing component, 10-100 parts of a skin conditioning component, 10-30 parts of an anti-inflammatory and bactericidal component and 10-30 parts of a soothing and anti-allergy component; the antioxidant component comprises rhizoma Ligustici Chuanxiong extractive solution, radix Angelicae sinensis extractive solution and radix Platycodi extractive solution; the whitening and moisturizing component comprises ginseng extract, atractylodes macrocephala extract, bletilla striata extract, liquorice extract and safflower extract; the skin conditioning component comprises Margarita extractive solution; the anti-inflammatory and antibacterial components comprise folium Artemisiae Argyi extract, fructus Cnidii extract, flos Chrysanthemi Indici extract and radix Sophorae Flavescentis extract; the soothing and anti-allergy component comprises radix astragali extract and herba Portulacae extract. The invention takes a plurality of traditional Chinese medicine extracting solutions as active ingredients and plant essential oil as auxiliary materials, is mild, has no chemical irritation, is easy to be absorbed by skin, can exert synergistic effect among a plurality of traditional Chinese medicine skin care components, and has multiple effects of beautifying and protecting skin.
Description
Technical Field
The invention relates to the technical field of cosmetics, and in particular relates to a traditional Chinese medicine extract cosmetic composition and a preparation method thereof.
Background
The technology of external application or natural medicine eating to achieve the purpose of beautifying is mastered in ancient China, and along with the progress of modern science and technology, the cosmetics prepared by extracting effective components from natural traditional Chinese medicines are deeply favored because of the characteristics of greenness, naturalness, safety and reliability.
Various traditional Chinese medicines with specific beautifying and skin-care effects are taken as raw materials, effective active ingredients contained in the traditional Chinese medicines are extracted to obtain various traditional Chinese medicine extracts, and the traditional Chinese medicine extracts are compounded and mixed to prepare the cosmetic with the beautifying and skin-care effects. However, if the powdery traditional Chinese medicine extract is adopted, the problems of poor compatibility with liquid raw materials, poor dispersibility, low absorption and utilization rate and the like exist. In addition, as pearls are one of the traditional Chinese medicines, active substances such as pearl protein and the like are often applied to the field of cosmetics, but the absorption effect of human skin on macromolecular pearl protein is relatively poor, so that calcium carbonate which does not have the skin care effect and is contained in pearls needs to be removed, and then the pearl protein is converted into micromolecular pearl polypeptide and amino acid to prepare pearl extracting solution.
Disclosure of Invention
Based on the problems in the prior art, the cosmetic composition with the traditional Chinese medicine extract is provided, a plurality of traditional Chinese medicine extracts are used as skin care components, plant essential oil is used as an auxiliary material, the traditional Chinese medicine extract is mild and free of chemical irritation, is easy to absorb by skin, can exert synergistic effect among a plurality of traditional Chinese medicine skin care components, and has the characteristics of multiple beautifying and skin care effects and the like.
In order to solve the technical problems, the technical scheme adopted by the invention is as follows:
a traditional Chinese medicine extract cosmetic composition comprises the following components in parts by weight: 10-50 parts of an antioxidant component, 10-50 parts of a whitening and moisturizing component, 10-100 parts of a skin conditioning component, 10-30 parts of an anti-inflammatory and bactericidal component and 10-30 parts of a soothing and anti-allergy component;
the antioxidant component comprises rhizoma Ligustici Chuanxiong extractive solution, radix Angelicae sinensis extractive solution and radix Platycodi extractive solution;
the whitening and moisturizing component comprises ginseng extract, bighead atractylodes rhizome extract, bletilla striata extract, liquorice extract and safflower extract;
the skin conditioning component comprises a pearl extract;
the anti-inflammatory and antibacterial component comprises folium Artemisiae Argyi extract, fructus Cnidii extract, flos Chrysanthemi Indici extract and radix Sophorae Flavescentis extract;
the soothing and anti-allergy component comprises radix astragali extract and herba Portulacae extract.
Preferably, the ligusticum wallichii extract, the angelica sinensis extract and the platycodon grandiflorum extract account for 10-50%, 10-50% and 10-50% of the total amount of the antioxidant components.
Preferably, the ginseng extract, the bighead atractylodes rhizome extract, the bletilla striata extract, the liquorice extract and the safflower extract account for 5% -25%, 5% -25% and 5% -25% of the total amount of the whitening and moisturizing component.
Preferably, the folium artemisiae argyi extract, the fructus cnidii extract, the wild chrysanthemum extract and the radix sophorae flavescentis extract account for 10% -30%, 10% -30% and 10% -30% of the total amount of the anti-inflammatory and bactericidal components.
Preferably, the astragalus extract and the purslane extract account for 20-80% and 20-80% of the total amount of the soothing and anti-allergy components.
Preferably, the cosmetic composition of the traditional Chinese medicine extracting solution further comprises plant essential oil, a solvent, an emulsifier, a thickening agent and a preservative.
Preferably, the plant essential oil comprises at least one of olive oil and linseed oil;
the dosage of the composition is 10 to 20 percent of the total amount of the antioxidant component, the whitening and moisturizing component, the skin conditioning component, the anti-inflammatory and bactericidal component and the soothing and anti-allergy component;
the solvent comprises pure water;
the dosage of the composition is 3-5 times of the total amount of the antioxidant component, the whitening and moisturizing component, the skin conditioning component, the anti-inflammatory and bactericidal component and the soothing and anti-allergy component;
the emulsifier comprises polysorbate-20;
the dosage of the water accounts for 1 to 2 percent of the weight of the pure water;
the thickening agent comprises at least one of xanthan gum and potassium alginate;
the dosage of the water accounts for 1-5 per mill of the weight of the pure water;
the preservative comprises phenoxyethanol.
The dosage of the water accounts for 1 to 2 percent of the weight of the pure water.
A method for preparing cosmetic composition containing Chinese medicinal extractive solution comprises the following steps:
(1) Stirring and dispersing the thickening agent in a solvent to form a viscous liquid;
(2) Adding an antioxidant component, a whitening and moisturizing component, a skin conditioning component, an anti-inflammatory and bactericidal component and a soothing and anti-allergy component into the viscous liquid, and stirring and dispersing uniformly to obtain a mixed solution;
(3) Adding plant essential oil, emulsifier and antiseptic into the above mixed solution, stirring and dispersing uniformly to obtain cosmetic composition containing Chinese medicinal extractive solution.
The cosmetic composition containing the traditional Chinese medicine extract can be used as a beautifying facial mask liquid, an essence, a cream and an emulsion.
Preferably, the skin conditioning component added in step (2) comprises a pearl extract;
the preparation method of the pearl extract comprises the following steps:
1) Pearl treatment: pulverizing Margarita to obtain Margarita powder;
the particle size of the pearl powder is 50-80 meshes;
2) Acid hydrolysis reaction: adding pure water into the pearl powder, mixing into paste, adding excessive acid solution, and performing acid reaction;
the acid solution comprises a lactic acid solution; the content of lactic acid in the lactic acid solution is 10-30%;
the mixture of the pearl powder and the lactic acid solution does not generate bubbles any more, and the acidolysis reaction can be judged to be finished;
3) And (3) carrying out enzymolysis reaction: after the acidolysis reaction is finished, filtering, collecting and washing insoluble substances, and adding an enzyme solution into the washed insoluble substances for enzymolysis reaction to obtain an enzymolysis pearl liquid;
the enzyme solution is a neutral protease solution; the content of the neutral protease in the neutral protease solution is 2-5 per mill; the dosage of the neutral protease solution is 20-30 times of the mass of the pearl powder;
the temperature of the enzymolysis reaction is 45-50 ℃, and the reaction time is 5-10h;
the insoluble substance mainly comprises pearl protein (pearl powder is mixed with acid solution, calcium carbonate in the pearl powder is dissolved by reaction with acid, and pearl protein does not react with acid solution);
4) And (3) post-treatment: and (4) carrying out enzyme deactivation and filtration treatment on the enzymolysis pearl liquid to obtain a pearl extracting solution.
The effects of the raw materials provided by the invention are as follows:
ligusticum wallichii and Chinese angelica contain rich antioxidant component-ferulic acid, which can remove free radicals in human body after being absorbed by human body, prevent the generation of brown lipid in skin cells, reduce the damage of oxide to skin cells, reduce the generation of fine lines, wrinkles, brown spots and other early and old signs, and keep the young and healthy state of skin.
The components such as saponin, flavone, polysaccharide, phenols and the like contained in the platycodon grandiflorum have good antioxidant activity, are used as antioxidants of cosmetics and skin care products, have low risk coefficient and do not cause acne.
The ginseng contains various saponins and polysaccharide components, has good permeability and good moisturizing effect, and can supplement water needed by the skin particularly in dry seasons, so that the skin becomes more brilliant and moist; can also promote cell repair and regeneration, especially remove free radicals in vivo and make skin white and smooth.
The white atractylodes rhizome has the effects of inhibiting the activity of melanocytes, inhibiting the synthesis of tyrosinase and removing free radicals, and has certain freckle removing and whitening effects; has effects in promoting skin cell metabolism, resisting aging, and can be used as humectant of cosmetics.
The bletilla striata contains rich volatile oil, pituitous substances and other components, has the effects of whitening and removing freckles, can be externally applied by being ground into powder, can eliminate marks left by acne on the face, moisten and whiten the skin, and has the effect of beautifying.
The active ingredients in Glycyrrhrizae radix include Glycyrrhrizae radix total flavone, glycyrrhizic acid and Glycyrrhiza polysaccharide etc., and Glycyrrhrizae radix total flavone can inhibit tyrosinase and dopachrome tautomerase (TRP-2) activity, and can effectively prevent melanin formation; glycyrrhizic acid and glycyrrhiza polysaccharide have certain anti-aging effect and strong moisturizing and penetrating capacity, and the moisturizing and whitening effects are obvious.
Safflower can improve the blood circulation of skin, promote skin metabolism, inhibit the generation of melanin, and accelerate color spot fading; has effects in promoting skin metabolism, caring skin, moistening skin, preventing skin aging, and enhancing pore density.
The pearl extract is used as skin conditioner and antioxidant, contains various pearl polypeptides, can make skin healthy, fine, moist, smooth and white, can restore skin elasticity to the maximum extent for aging and rough skin, can increase luster, can obviously reduce wrinkles, eliminate black spots, and has the effects of filling, healing, diminishing inflammation and promoting granulation for face sores and furuncles, whelks, wounds and the like.
Fructus Cnidii contains osthole as main active ingredient, and the osthole can inhibit activity of Trichophyton mentagrophytes and mould, and can be used for treating skin eczema; osthole has good hygroscopicity and moisture retention, and can be used as skin care product for preventing and treating dry skin; osthole has antibacterial and anti-inflammatory effects.
The folium Artemisiae Argyi contains volatile aromatic oil, mainly contains phellandrene, beta-asarone, etc., has strong killing effect on diphtheria, typhoid, tubercle bacillus, staphylococcus aureus, etc., and can be used as antiseptic and antibacterial agent of cosmetics, and also as cosmetic antiinflammatory agent.
The flos Chrysanthemi Indici contains abundant nutritional components, has anti-inflammatory and antibacterial effects, can be used for treating skin pruritus and eczema, can avoid skin dryness, and can clear away heat and toxic materials and prevent skin aging.
The active ingredient in the radix sophorae flavescentis is mainly matrine and has the effects of resisting bacteria and diminishing inflammation; has effects in promoting collagen production, promoting fibroblast proliferation, and resisting skin aging; meanwhile, the product has the efficacy of moisturizing.
Astragalus membranaceus has the functions of benefiting qi, activating blood circulation and dredging channels and collaterals, has the functions of eliminating toxins from deep to shallow in the body and finally discharging toxins completely, and also has the functions of improving capillary permeability and microcirculation, so that the astragalus membranaceus also has the effects of resisting allergy and inflammation.
Purslane contains rich amino acids with special biological activity, has a contraction effect on vascular smooth muscle, has the functions of centre and periphery, and can relieve skin and relieve itching; the herba Portulacae contains alkaloids and brass, and has anti-inflammatory effect and can be used for inhibiting skin red swelling.
The olive oil is rich in unsaturated fatty acid and various vitamins, is easy to be absorbed by skin, is fresh and natural, has no greasy feeling, contains polyphenols with antioxidant effect, and can effectively avoid the phenomena of color spots, wrinkles and the like caused by cell aging due to fat oxidation.
The alpha-linolenic acid contained in the linseed oil is a polyunsaturated fatty acid, has excellent affinity and permeability to the skin, can supplement lipid components required by the skin, repair dry skin and the level of skin fatty acid damaged by contacting with a surfactant, and maintain and enhance the normal structure and function of a skin cell membrane and interstitium; meanwhile, the linseed oil can form a breathable water retention film on the surface of the skin, so that the moisture loss of the deep layer of the skin is weakened, and the skin is kept moist, smooth and elastic.
Compared with the prior art, the invention has the following beneficial effects:
1. the skin-care cosmetic composition disclosed by the invention contains multiple functional components including an antioxidant component, a whitening and moisturizing component, a skin conditioning component, an anti-inflammatory and bactericidal component and a soothing and anti-allergic component, and various functional components are composed of traditional Chinese medicine extracting solutions, plant essential oil with a skin-care effect is added, so that the prepared cosmetic composition is uniform and stable in components, easy to absorb by skin, mild and free of chemical irritation, can exert a synergistic effect among multiple traditional Chinese medicine extracting solutions, realizes multiple skin-care effects in a whole aspect, is free of hormone, and is suitable for both males and females.
2. The skin conditioning component in the cosmetic composition is pearl extract, and the active component is micromolecular polypeptide or amino acid, so that the cosmetic composition is easy to absorb and utilize by the skin and can help to improve the sub-health state of the skin.
3. When the pearl extract is prepared, the acid solution is lactic acid solution, the acidity is relatively soft, and the activity reduction and content loss of pearl protein can not be caused while calcium carbonate in the pearl powder is dissolved.
Drawings
FIG. 1 is a flow diagram of a manufacturing process of the present invention;
FIG. 2 is a schematic view of the overall structure of the pearl enzymolysis device;
FIG. 3 is a schematic view of the inner structure of the pearl enzymolysis device;
FIG. 4 is a schematic view of the structure of the pearl enzymolysis device in the invention;
FIG. 5 is a schematic view of a pearl treatment structure of the pearl enzymolysis device;
FIG. 6 is a schematic view of the upper and lower fluted discs of the pearl enzymolysis device;
FIG. 7 is a schematic view of the inner structure of the pulverizing barrel and the grinding barrel of the pearl enzymolysis device;
FIG. 8 is a schematic diagram of the acid reaction structure of the pearl enzymolysis device in the invention;
FIG. 9 is a schematic view of an enzymolysis reaction structure of the pearl enzymolysis device in the invention;
FIG. 10 is a schematic view of the inner structure of the enzymolysis reaction chamber of the pearl enzymolysis device;
FIG. 11 is a schematic view of a heater and a heating plate of the device for enzymolysis of pearls.
In the figure: 1. a body; 2. a controller; 3. a feed inlet; 4. a funnel; 5. an upper support frame; 6. a grinding cylinder; 7. a crushing knife; 8. a lower support frame; 9. a grinding cylinder; 10. a central column; 11. an upper fluted disc; 12. a lower fluted disc; 13. processing the motor; 14. a lower disc gear; 15. an upper disc gear; 16. a draft tube; 17. a support chassis; 18. grinding the taking and placing port; 19. a storage box; 20. an acid reaction port; 21. an acid reaction bin; 22. an electrically controlled valve; 23. a flow guide pipe; 24. a washing tank; 25. a deposit taking and placing opening; 26. a filter cartridge; 27. a water inlet pipe; 28. a drain pipe; 29. a carbon dioxide content tester; 30. an enzymolysis reaction port; 31. an enzymolysis reaction bin; 32. a stirring motor; 33. a connecting rod; 34. a stirring plate; 35. a heater; 36. a heat generating plate; 37. and (6) closing the cover.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without making any creative effort based on the embodiments in the present invention, belong to the protection scope of the present invention.
Example 1
Preparation of pearl extract
1) Pearl treatment: pulverizing Margarita to obtain Margarita powder with particle size of 60 mesh;
2) Acid hydrolysis reaction: adding pure water 2-3 times of the weight of the pearl powder into the pearl powder to be blended into paste, adding excessive lactic acid solution with the lactic acid content of 15 percent, and carrying out acid reaction until no bubbles are generated;
3) And (3) carrying out enzymolysis reaction: after the acidolysis reaction is finished, filtering, collecting and washing insoluble substances, and adding an enzyme solution into the washed insoluble substances for enzymolysis reaction to obtain an enzymolysis pearl liquid;
wherein the enzyme solution is neutral protease solution with neutral protease content of 3 ‰, and the added amount of the enzyme solution is 30 times of the weight of Margarita powder;
the temperature of the enzymolysis reaction is 50 ℃, and the reaction time is 8 hours;
4) And (3) post-treatment: and (4) carrying out enzyme deactivation and filtration treatment on the enzymolysis pearl liquid to obtain a pearl extracting solution.
Example 2
A traditional Chinese medicine extract cosmetic composition comprises the following components in parts by weight: 2 parts of ligusticum wallichii extract, 4 parts of angelica sinensis extract, 4 parts of platycodon grandiflorum extract, 3 parts of ginseng extract, 2 parts of bighead atractylodes rhizome extract, 1 part of bletilla striata extract, 1 part of liquorice extract, 3 parts of safflower extract, 10 parts of pearl extract, 2 parts of folium artemisiae argyi extract, 2 parts of fructus cnidii extract, 3 parts of wild chrysanthemum extract, 3 parts of radix sophorae flavescentis extract, 2 parts of radix astragali extract, 8 parts of purslane extract, 150 parts of pure water, 5 parts of olive oil, 201.5 parts of polysorbate-201.5 parts of xanthan gum and 1.5 parts of phenoxyethanol.
The preparation method comprises the following steps:
(1) Stirring and dispersing xanthan gum in pure water to form viscous liquid;
(2) Adding rhizoma Ligustici Chuanxiong extractive solution, radix Angelicae sinensis extractive solution, radix Platycodi extractive solution, ginseng radix extractive solution, atractylodis rhizoma extractive solution, rhizoma Bletillae extractive solution, glycyrrhrizae radix extractive solution, carthami flos extractive solution, margarita extractive solution, folium Artemisiae Argyi extractive solution, fructus Cnidii extractive solution, flos Chrysanthemi Indici extractive solution, radix Sophorae Flavescentis extractive solution, radix astragali extractive solution and herba Portulacae extractive solution into the viscous liquid, stirring and dispersing uniformly to obtain mixed solution;
(3) Adding oleum Olivarum, polysorbate-20, and phenoxyethanol into the above mixture, stirring, and dispersing to obtain cosmetic composition containing Chinese medicinal extractive solution.
Example 3
A traditional Chinese medicine extract cosmetic composition comprises the following components in parts by weight: 15 parts of ligusticum wallichii extract, 15 parts of angelica sinensis extract, 20 parts of platycodon grandiflorum extract, 10 parts of ginseng extract, 10 parts of bighead atractylodes rhizome extract, 10 parts of bletilla striata extract, 10 parts of liquorice extract, 10 parts of safflower extract, 100 parts of pearl extract, 7.5 parts of folium artemisiae argyi extract, 7.5 parts of fructus cnidii extract, 7.5 parts of wild chrysanthemum flower extract, 7.5 parts of radix sophorae flavescentis extract, 15 parts of radix astragali extract, 15 parts of purslane extract, 1300 parts of pure water, 52 parts of linseed oil, polysorbate-2026 parts, 6.5 parts of potassium alginate and 26 parts of phenoxyethanol.
The preparation method comprises the following steps:
(1) Stirring and dispersing potassium alginate in pure water to form viscous liquid;
(2) Adding rhizoma Ligustici Chuanxiong extractive solution, radix Angelicae sinensis extractive solution, radix Platycodi extractive solution, ginseng radix extractive solution, atractylodis rhizoma extractive solution, rhizoma Bletillae extractive solution, glycyrrhrizae radix extractive solution, carthami flos extractive solution, margarita extractive solution, folium Artemisiae Argyi extractive solution, fructus Cnidii extractive solution, flos Chrysanthemi Indici extractive solution, radix Sophorae Flavescentis extractive solution, radix astragali extractive solution and herba Portulacae extractive solution into the viscous liquid, stirring and dispersing uniformly to obtain mixed solution;
(3) Adding oleum Lini, polysorbate-20, and phenoxyethanol into the above mixture, stirring, and dispersing to obtain cosmetic composition containing Chinese medicinal extractive solution.
Example 4
A traditional Chinese medicine extract cosmetic composition comprises the following components in parts by weight: 3 parts of ligusticum wallichii extract, 12 parts of angelica sinensis extract, 15 parts of platycodon grandiflorum extract, 1.5 parts of ginseng extract, 1.5 parts of bighead atractylodes rhizome extract, 9 parts of bletilla striata extract, 9 parts of liquorice extract, 9 parts of safflower extract, 50 parts of pearl extract, 2 parts of folium artemisiae argyi extract, 6 parts of fructus cnidii extract, 6 parts of wild chrysanthemum flower extract, 6 parts of radix sophorae flavescentis extract, 4 parts of radix astragali extract, 16 parts of purslane extract, 600 parts of pure water, 10 parts of olive oil, 12.5 parts of linseed oil, 209 parts of polysorbate-209 parts, 1.8 parts of potassium alginate and 9 parts of phenoxyethanol.
The preparation method comprises the following steps:
(1) Stirring and dispersing potassium alginate in pure water to form viscous liquid;
(2) Adding rhizoma Ligustici Chuanxiong extractive solution, radix Angelicae sinensis extractive solution, radix Platycodi extractive solution, ginseng radix extractive solution, atractylodis rhizoma extractive solution, rhizoma Bletillae extractive solution, glycyrrhrizae radix extractive solution, carthami flos extractive solution, margarita extractive solution, folium Artemisiae Argyi extractive solution, fructus Cnidii extractive solution, flos Chrysanthemi Indici extractive solution, radix Sophorae Flavescentis extractive solution, radix astragali extractive solution and herba Portulacae extractive solution into the viscous liquid, stirring and dispersing uniformly to obtain mixed solution;
(3) Adding oleum Olivarum, oleum Lini, polysorbate-20, and phenoxyethanol into the above mixture, stirring, and dispersing to obtain cosmetic composition containing Chinese medicinal extractive solution.
In examples 2 to 4, pure water was prepared by itself; the pearl extract is the pearl extract prepared in example 1; the rest raw materials are commercially available, and the rhizoma Ligustici Chuanxiong extractive solution is dark brown transparent liquid provided by Wanhong biotechnology, inc. of Guangzhou; the radix Angelicae sinensis extractive solution is light brown liquid provided by Guangzhou Crystal Biotechnology limited; the radix Platycodi extract is colorless transparent liquid provided by Wanhong biotechnology limited of Guangzhou; the ginseng extract is provided by Teng sourced biochemical engineering, inc. in Guangzhou city and is a brown transparent liquid; the Atractylodis rhizoma extractive solution is provided by Wanhong biotechnology, inc. of Guangzhou, and is yellowish liquid; the rhizoma Bletillae extractive solution is light brown transparent liquid provided by Guangzhou Sinuoke biotechnology; the Glycyrrhrizae radix extractive solution is colorless transparent liquid provided by Tonghua Yitai pharmaceutical group, inc.; the Carthami flos extract is provided by Guangzhou Sinuoke biotechnology, inc., has solid content of more than 10%, and is brown transparent liquid; the folium artemisiae argyi extract is provided by Guangzhou Peng Rui chemical technology, inc., and is a light yellow transparent liquid; the fructus Cnidii extract is provided by Guangzhou Sinuoke biotechnology limited, has solid content of more than 10%, and is brown transparent liquid; the wild chrysanthemum extracting solution is provided by Wanhong biological technology limited of Guangzhou, the solid content is more than or equal to 2.5 percent, and the wild chrysanthemum extracting solution is brown transparent liquid; the radix Sophorae Flavescentis extract is colorless transparent liquid provided by Tonghua Yitai pharmaceutical group, inc.; the radix astragali extract is light yellow transparent liquid provided by Wanhong biotechnology, inc. of Guangzhou; the herba Portulacae extractive solution is provided by Guangzhou Sinuoke biotechnology, and has solid content of more than 10% and is light yellow transparent liquid; olive oil is provided by the wanghong biotechnology limited of guangzhou, and is light yellow transparent liquid; linseed oil is provided by inner mongolia Varifa Biotechnology Co., ltd, as a pale yellow oily liquid; polysorbate-20 is provided by Haian petrochemical plant of Jiangsu province, and is amber viscous liquid; the xanthan gum is provided by Guangzhou Youbao chemical Co Ltd, and is off-white powder; the potassium alginate is provided by Shandong Ruist Biotech limited, and is white powder; phenoxyethanol is a colorless transparent liquid supplied by Youbao chemical Co., ltd., guangzhou, youbao chemical Co., ltd., U.S.A.
Comparative example 1
In comparison with example 2, in comparative example 1, olive oil was not added, and other conditions were not changed.
Comparative example 2
Compared with example 2, comparative example 2 does not add the pearl extract, and other conditions are not changed.
Example 5
The embodiment discloses a pearl enzymolysis device, and the pearl extracting solution is prepared in the device in the embodiment 1.
As shown in fig. 2-11, the pearl enzymolysis device comprises a machine body 1, a controller 2 is fixedly installed on the top surface of the machine body 1, and the controller 2 is used for controlling the operation of the device;
the pearl processing structure is used for processing pearls to obtain pearl powder, the acid reaction structure is used for processing the pearl powder to obtain insoluble substances, and the enzymolysis reaction structure is used for processing the insoluble substances to obtain pearl extracting solution.
Furthermore, the pearl processing structure comprises a crushing mechanism and a grinding mechanism, wherein the crushing mechanism is arranged on one side inside the machine body 1 and is used for crushing pearls, the grinding mechanism is arranged below the crushing mechanism, and the grinding mechanism is used for grinding the crushed pearls.
Furthermore, the crushing mechanism comprises an upper support frame 5, the upper support frame 5 is fixedly arranged on the inner side wall of the machine body 1, a crushing barrel 6 is movably arranged on the upper support frame 5, a plurality of crushing knives 7 are fixedly arranged on the inner side wall of the crushing barrel 6, and the crushing knives 7 are used for crushing pearls;
the grinding mechanism comprises a lower support frame 8, the lower support frame 8 is fixedly arranged on the inner side wall of the machine body 1, a grinding cylinder 9 is movably arranged on the lower support frame 8, a grinding layer is fixedly arranged on the inner side wall of the grinding cylinder 9, and the grinding cylinder 9 is used for grinding the crushed pearls;
the crushing cylinder 6 is provided with center post 10 with the inside of grinding cylinder 9, and the lower part of center post 10 is the cylinder, and the lower part of center post 10 is located grinding cylinder 9, and the middle part of center post 10 is the round platform body, and the middle part of center post 10 is located crushing cylinder 6, and the upper portion of center post 10 is the hemispheroid, and the upper portion of center post 10 is located the top of crushing cylinder 6, cooperates crushing cylinder 6 and grinding cylinder 9 through center post 10 in order to handle pearl.
Further, the gap between the middle part of the central column 10 and the crushing barrel 6 is smaller from top to bottom so as to ensure the crushing effect on the pearls.
Further, an upper fluted disc 11 is fixedly installed at the lower end of the outer side wall of the grinding cylinder 6, teeth are arranged on the top surface of the upper fluted disc 11, a lower fluted disc 12 is fixedly installed at the upper end of the outer side wall of the grinding cylinder 9, teeth are arranged on the top surface of the lower fluted disc 12, a processing motor 13 is fixed on the inner side wall of the machine body 1 through bolts, a lower fluted disc 14 is fixedly installed on a shaft of the processing motor 13, an upper fluted disc 15 is fixedly installed on the shaft of the processing motor 13, the lower fluted disc 14 is meshed with the lower fluted disc 12, the upper fluted disc 15 drives the upper fluted disc 11 to rotate by starting the processing motor 13, the upper fluted disc 11 drives the grinding cylinder 6 to rotate, the grinding cylinder 6 is used for grinding pearls under the action of the grinding cutter 7 and the central column 10, the ground pearls fall into a gap between the grinding cylinder 9 and the lower part of the central column 10, the lower fluted disc 14 is driven to rotate by the processing motor 13, the lower fluted disc 14 drives the lower fluted disc 12 to rotate, the grinding cylinder 9 to grind the ground pearls to form pearl powder.
Further, a supporting bottom frame 17 is fixedly installed on the inner bottom surface of the machine body 1, a guide cylinder 16 is fixedly installed at the upper end of the supporting bottom frame 17, the guide cylinder 16 is communicated with the grinding cylinder 9, the guide cylinder 16 is used for guiding the pearl powder, a grinding taking and placing opening 18 is formed in the side wall of the machine body 1, a storage box 19 is movably installed on the supporting bottom frame 17, a handle is arranged on the side wall of the storage box 19, the storage box 19 penetrates through the grinding taking and placing opening 18, the storage box 19 is taken out through the handle, and pure water is added into the storage box 19 to mix the pearl powder and the pure water to form paste.
Further, the acid reaction structure comprises an acid reaction bin 21, an electric control valve 22 is fixedly installed at the lower end of the outer side wall of the acid reaction bin 21, the electric control valve 22 is communicated with the acid reaction bin 21, a guide pipe 23 is fixedly installed at one end of the electric control valve 22, a washing box 24 is fixedly installed at one end of the guide pipe 23, the guide pipe 23 is communicated with the washing box 24, a filter box 26 is movably installed in the washing box 24, a handle is arranged on the side wall of the filter box 26, a handle is fixedly installed on the side wall of the filter box 26, the filter box 26 is used for filtering out insoluble substances, a water inlet pipe 27 is fixedly installed on the top surface of the washing box 24, the water inlet pipe 27 is communicated with the washing box 24, the water inlet pipe 27 is used for washing the insoluble substances through water, a drain pipe 28 is fixedly installed on the bottom surface of the washing box 24, the drain pipe 28 is communicated with the washing box 24, the drain pipe 28 is used for discharging washing water, a sediment taking and putting port 25 is opened on the side wall of the machine body 1, the filter box 26 penetrates through the sediment taking and putting port 25, a carbon dioxide content measuring instrument 29 is fixedly installed on the side wall of the acid reaction bin 21, the carbon dioxide measuring instrument 29 is used for detecting the carbon dioxide content in the acid reaction bin 21, excessive acid solution is added into the acid reaction bin 21 to enable the acid solution to react with the paste, insoluble substances are formed at the part which does not react with the acid solution, the upper closing cover 37 is closed, carbon dioxide generated by acid reaction is detected by a carbon dioxide content tester 29, when the content of the carbon dioxide in the acid reaction bin 21 reaches a threshold value, the acid reaction is finished, the closing cover 37 and the electric control valve 22 are opened, enough water is added into the acid reaction bin 21, so that all substances in the acid reaction bin 21 fall into the filter box 26 through the draft tube 23, the content of the filter cassette 26 is washed through the feed tube 27 to filter out insoluble substances, and the filter cassette 26 is taken out through the handle.
Further, the enzymolysis reaction structure includes enzymolysis reaction storehouse 31, the interior bottom surface bolt fastening of organism 1 has agitator motor 32, agitator motor 32 epaxial fixed mounting has connecting rod 33, connecting rod 33 runs through enzymolysis reaction storehouse 31, the upper end fixed mounting of connecting rod 33 has a plurality of stirring boards 34, stirring board 34 is located enzymolysis reaction storehouse 31's inside bottom, stirring board 34 is used for stirring in the enzymolysis reaction storehouse 31, through pouring the insoluble substance into enzymolysis reaction storehouse 31, start agitator motor 32, agitator motor 32 drives connecting rod 33 and rotates, connecting rod 33 drives stirring board 34 and rotates, in order to stir in the enzymolysis reaction storehouse 31, carry out enzymolysis reaction in enzymolysis reaction storehouse 31 through the insoluble substance in order to produce the enzymolysis liquid, at last take out the material in the enzymolysis reaction storehouse 31 is whole, filter it, the clear solution that obtains is pearl extract promptly.
Further, bottom surface fixed mounting has heater 35 in organism 1, heater 35 is used for producing the heat, the bottom surface fixed mounting in acid reaction storehouse 21 and enzymolysis reaction storehouse 31 has heating plate 36, heating plate 36 and heater 35 electric connection, heating plate 36 is used for in conducting acid reaction storehouse 21 and enzymolysis reaction storehouse 31 with the heat that produces, be provided with temperature-detecting device in acid reaction storehouse 21 and the enzymolysis reaction storehouse 31, cooperate heater 35 in order to control the temperature in acid reaction storehouse 21 and the enzymolysis reaction storehouse 31 through temperature-detecting device, a heating heat preservation that is arranged in the enzymolysis reaction process is handled and is gone out the enzyme processing with the intensification to the enzymolysis liquid.
Furthermore, a feed port 3 is formed in the top surface of the machine body 1, a funnel 4 is fixedly mounted on the top surface of the machine body 1, the funnel 4 is communicated with the feed port 3, the funnel 4 is communicated with the crushing cylinder 6, and the upper part of the central column 10 is positioned in the funnel 4;
the top surface of the machine body 1 is provided with an acid reaction port 20, the acid reaction port 20 is communicated with an acid reaction bin 21, the top surface of the machine body 1 is provided with an enzymolysis reaction port 30, the enzymolysis reaction port 30 is communicated with an enzymolysis reaction bin 31, the top surface of the machine body 1 is movably provided with a plurality of closing covers 37, the closing cover 37 on one side is opposite to the acid reaction port 20, the closing cover 37 on the other side is opposite to the enzymolysis reaction port 30, and the closing cover 37 is used for closing an opening.
When the pearl crusher is used, pearls are firstly placed into the funnel 4, the pearls fall into a gap between the middle parts of the crushing barrel 6 and the central column 10 along the gap between the upper parts of the funnel 4 and the central column 10, the processing motor 13 is started, the processing motor 13 drives the upper disc gear 15 to rotate, the upper disc gear 15 drives the upper disc gear 11 to rotate, the upper disc gear 11 drives the crushing barrel 6 to rotate, the crushing barrel 6 crushes the pearls under the action of the crushing cutter 7 and the central column 10, the crushed pearls fall into a gap between the lower parts of the grinding barrel 9 and the central column 10, the lower disc gear 14 is driven to rotate through the processing motor 13, the lower disc gear 14 drives the lower disc gear 12 to rotate, and the lower disc gear 12 drives the grinding barrel 9 to rotate so as to grind the crushed pearls to form pearl powder. The pearl powder falls into the storage box 19 through the guide flow tube 16, the storage box 19 is taken out through the handle, pure water is added into the storage box 19 to mix the pearl powder and the pure water to form paste, the cover 37 is opened, the paste is poured into the acid reaction bin 21, excessive acid solution is added into the acid reaction bin 21 to enable the acid solution to react with the paste, a part which does not react with the acid solution forms insoluble substances, the cover 37 is closed, carbon dioxide generated by acid reaction is detected by the carbon dioxide content detector 29, when the content of the carbon dioxide in the acid reaction bin 21 reaches a threshold value, the acid reaction is completed, the cover 37 and the electric control valve 22 are opened, the substances in the acid reaction bin 21 fall into the filter box 26 through the guide flow tube 23, water is added into the acid reaction bin 21 to enable all the residual substances in the acid reaction bin 21 to fall into the filter box 26 through the guide tube 23, the substances in the filter box 26 are washed through the water inlet tube 27 to filter out the insoluble substances, and the filter box 26 is taken out through the handle. Open the lid 37 that closes of opposite side again, pour the insoluble substance into enzymolysis reaction storehouse 31 in, start agitator motor 32, agitator motor 32 drives connecting rod 33 and rotates, and connecting rod 33 drives stirring board 34 and rotates to stir in the enzymolysis reaction storehouse 31, carry out the enzymolysis reaction in order to produce the enzymolysis liquid through the insoluble substance in enzymolysis reaction storehouse 31, the substance in enzymolysis reaction storehouse 31 is all taken out after the intensification goes out the enzyme, filters it, and the clear solution that obtains is pearl extract.
Furthermore, pearl is treated by a pearl treatment structure to obtain pearl powder, the pearl powder is treated by an acid reaction structure to obtain insoluble substances, and the insoluble substances are treated by an enzymolysis reaction structure to obtain pearl extract, so that the pearl is effectively extracted, and the extraction working efficiency is greatly improved by using a semi-automatic device;
furthermore, the carbon dioxide in the acid reaction bin is detected through the arrangement of the carbon dioxide content tester, the degree of acid reaction is determined by utilizing the content of the carbon dioxide, the trouble of manual confirmation is replaced, and the working efficiency of the device is effectively improved;
furthermore, through the arrangement of the heater and the heating plate, the temperature detection in the acid reaction bin and the enzymolysis reaction bin is matched, so that the temperature during reaction is effectively controlled, the reaction quality is enhanced, and the reaction is ensured to be sufficient.
Test examples
The product of the cosmetic composition of chinese herbal medicine extract prepared in examples 2 to 4 and comparative examples 1 to 2 was subjected to a performance test.
Test objects: 100 men and women each aged 35 to 45 were selected, 100 men and 100 women were each evenly and randomly divided into five groups, and a group of men and a group of women were randomly selected to form one test group, to form five test groups, i.e., 20 men and 20 women in each test group, using the product of example 2 as test group 1, using the product of example 3 as test group 2, using the product of example 4 as test group 3, using the product of comparative example 1 as test group 4, and using the product of comparative example 2 as test group 5.
The test method comprises the following steps: after cleaning the face, uniformly coating the traditional Chinese medicine extract cosmetic composition on the face, massaging the face until the composition is absorbed, using the composition once in the morning and evening, recording the skin condition once every 2 weeks, and continuously recording for 8 weeks;
the change condition of the skin is counted and analyzed, and the evaluation criteria are divided into: (1) remarkably effective: the skin color spots, darkness, red itch and white skin are removed, and the skin is white, moist and elastic; (2) effective: dry itch and red itch are relieved, and color spots and darkness become light; and (3) invalidation: no obvious change of skin;
the analytical results are shown in table 1:
TABLE 1
As can be seen from Table 1, the cosmetic composition containing the traditional Chinese medicine extract can effectively improve the sub-health state of skin, has very excellent beautifying and skin-care effects, is suitable for both males and females, and has the same level of efficacy.
In comparative example 1, since olive oil was not added, unsaturated fatty acids and various vitamins were lacked in the product, resulting in a decrease in the cosmetic skin care effect;
in comparative example 2, as no pearl extract is added, pearl polypeptide is lacked in the product, which results in the reduction of the skin care effect.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. The preparation method of the traditional Chinese medicine extract cosmetic composition is characterized in that the traditional Chinese medicine extract cosmetic composition comprises the following components in parts by weight: 10-50 parts of an antioxidant component, 10-50 parts of a whitening and moisturizing component, 10-100 parts of a skin conditioning component, 10-30 parts of an anti-inflammatory and bactericidal component and 10-30 parts of a soothing and anti-allergy component; the antioxidant component comprises rhizoma Ligustici Chuanxiong extractive solution, radix Angelicae sinensis extractive solution and radix Platycodi extractive solution; the whitening and moisturizing component consists of ginseng extract, bighead atractylodes rhizome extract, bletilla striata extract, liquorice extract and safflower extract; the skin conditioning component is pearl extract; the anti-inflammatory and bactericidal component consists of folium artemisiae argyi extract, fructus cnidii extract, wild chrysanthemum extract and radix sophorae flavescentis extract; the soothing and anti-allergy component consists of astragalus extract and purslane extract;
the preparation method comprises the following steps: (1) Stirring and dispersing the thickening agent in a solvent to form a viscous liquid; (2) Adding an antioxidant component, a whitening and moisturizing component, a skin conditioning component, an anti-inflammatory and bactericidal component and a soothing and anti-allergy component into the viscous liquid, and stirring and dispersing uniformly to obtain a mixed solution; (3) Adding plant essential oil, emulsifier and antiseptic into the above mixed solution, stirring and dispersing uniformly to obtain Chinese medicinal extractive solution cosmetic composition; the skin conditioning component added in the step (2) is pearl extract; the preparation method of the pearl extract comprises the following steps: 1) Pearl treatment: pulverizing Margarita to obtain Margarita powder; 2) Acid hydrolysis reaction: adding pure water into the pearl powder, blending into paste, adding excessive acid solution, and performing acid reaction; the acid solution is a lactic acid solution; the content of lactic acid in the lactic acid solution is 10-30%; 3) And (3) carrying out enzymolysis reaction: after the acidolysis reaction is finished, filtering, collecting and washing insoluble substances, and adding an enzyme solution into the washed insoluble substances for enzymolysis reaction to obtain an enzymolysis pearl liquid; the enzyme solution is a neutral protease solution; the content of the neutral protease in the neutral protease solution is 2-5 per mill; the dosage of the neutral protease solution is 20-30 times of the mass of the pearl powder; 4) And (3) post-treatment: performing enzyme deactivation and filtration treatment on the enzymolysis pearl liquid to obtain pearl extract;
the pearl enzymolysis device is used for preparing the pearl extracting solution and comprises a machine body (1), a controller (2) is fixedly mounted on the top surface of the machine body (1), and the controller (2) is used for controlling the operation of the device; the pearl powder treatment device further comprises a pearl treatment structure, an acid reaction structure and an enzymolysis reaction structure, wherein the pearl treatment structure is used for treating pearls to obtain pearl powder, the acid reaction structure is used for treating the pearl powder to obtain insoluble substances, and the enzymolysis reaction structure is used for treating the insoluble substances to obtain pearl extracting solution; the pearl processing structure comprises a crushing mechanism and a grinding mechanism, wherein the crushing mechanism is arranged on one side in the machine body and is used for crushing pearls, the grinding mechanism is arranged below the crushing mechanism, and the grinding mechanism is used for grinding the crushed pearls; the crushing mechanism comprises an upper support frame, the upper support frame is fixedly arranged on the inner side wall of the machine body, a crushing barrel is movably arranged on the upper support frame, a plurality of crushing knives are fixedly arranged on the inner side wall of the crushing barrel, and the crushing knives are used for crushing pearls; the grinding mechanism comprises a lower support frame, the lower support frame is fixedly arranged on the inner side wall of the machine body, a grinding cylinder is movably arranged on the lower support frame, a grinding layer is fixedly arranged on the inner side wall of the grinding cylinder, and the grinding cylinder is used for grinding the crushed pearls; the inner parts of the grinding cylinder and the grinding cylinder are provided with central columns, the lower parts of the central columns are cylinders, the lower parts of the central columns are positioned in the grinding cylinder, the middle parts of the central columns are truncated cone bodies, the middle parts of the central columns are positioned in the grinding cylinder, the upper parts of the central columns are hemispheroids, the upper parts of the central columns are positioned above the grinding cylinder, and pearls are processed by matching the grinding cylinder and the grinding cylinder through the central columns; an upper fluted disc is fixedly installed at the lower end of the outer side wall of the grinding cylinder, teeth are arranged on the top surface of the upper fluted disc, a lower fluted disc is fixedly installed at the upper end of the outer side wall of the grinding cylinder, teeth are arranged on the top surface of the lower fluted disc, a processing motor is fixed on the inner side wall of the machine body through bolts, a lower fluted disc is fixedly installed on a shaft of the processing motor, an upper fluted disc is fixedly installed on the shaft of the processing motor, the lower fluted disc is meshed with the lower fluted disc, the upper fluted disc is meshed with the upper fluted disc, the processing motor drives the upper fluted disc to rotate, the upper fluted disc drives the grinding cylinder to rotate, the grinding cylinder is used for grinding pearls under the action of a grinding knife and a central column, the ground pearls fall into a gap between the grinding cylinder and the lower part of the central column, the lower fluted disc is driven to rotate by the processing motor, the lower fluted disc drives the grinding cylinder to rotate, and the ground pearls are ground to form pearl powder; the acid reaction structure comprises an acid reaction bin, an electric control valve is fixedly mounted at the lower end of the outer side wall of the acid reaction bin, the electric control valve is communicated with the acid reaction bin, a guide pipe is fixedly mounted at one end of the electric control valve, a washing box is fixedly mounted at one end of the guide pipe, the guide pipe is communicated with the washing box, a filter box is movably mounted in the washing box, a handle is arranged on the side wall of the filter box, the handle is fixedly mounted on the side wall of the filter box, the filter box is used for filtering out insoluble substances, a water inlet pipe is fixedly mounted on the top surface of the washing box and communicated with the washing box, the water inlet pipe is used for washing the insoluble substances through water, a drain pipe is fixedly mounted on the bottom surface of the washing box and communicated with the washing box and used for draining washing water, a precipitation taking and discharging port is formed in the side wall of the machine body, the filter box penetrates through the precipitation taking and discharging port, a carbon dioxide content measuring instrument is fixedly mounted on the side wall of the acid reaction bin and used for detecting the carbon dioxide content in the acid reaction bin; the enzymolysis reaction structure includes the enzymolysis reaction storehouse, and the interior bottom surface bolt fastening of organism has agitator motor, and agitator motor's epaxial fixed mounting has the connecting rod, and the connecting rod runs through the enzymolysis reaction storehouse, and the upper end fixed mounting of connecting rod has a plurality of stirring boards, and the stirring board is located the inside bottom in enzymolysis reaction storehouse, and the stirring board is used for stirring in the enzymolysis reaction storehouse.
2. The method for preparing a cosmetic composition of Chinese herbal extracts according to claim 1, wherein the extracts of Ligusticum wallichii, angelica sinensis and Platycodon grandiflorum are 10% -50%, 10% -50% and 10% -50% of the total amount of the antioxidant component.
3. The method for preparing a cosmetic composition containing traditional Chinese medicine extract according to claim 2, wherein the ginseng extract, the white atractylodes rhizome extract, the bletilla striata extract, the licorice extract and the safflower extract account for 5% -25%, 5% -25% and 5% -25% of the total amount of the whitening and moisturizing components.
4. The method for preparing a cosmetic composition containing Chinese herbal extracts according to claim 3, wherein the folium artemisiae argyi extract, the fructus cnidii extract, the flos chrysanthemi indici extract and the radix sophorae flavescentis extract account for 10% -30%, 10% -30% and 10% -30% of the total amount of the anti-inflammatory and bactericidal components.
5. The method for preparing a cosmetic composition containing Chinese herbal medicine extract according to claim 4, wherein the astragalus extract and the purslane extract account for 20% -80% and 20% -80% of the total amount of the soothing and anti-allergy components.
6. The method for preparing a cosmetic composition of herbal extracts according to claim 5, further comprising plant essential oils, solvents, emulsifiers, thickeners and preservatives.
7. The method of claim 6, wherein the plant essential oil comprises at least one of olive oil and linseed oil;
the solvent comprises pure water;
the emulsifier comprises polysorbate-20;
the thickening agent comprises at least one of xanthan gum and potassium alginate;
the preservative comprises phenoxyethanol.
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| CN111000770A (en) * | 2019-12-25 | 2020-04-14 | 浙江长生鸟健康科技股份有限公司 | Whitening cream containing pearl peptide |
| CN113350406A (en) * | 2021-06-01 | 2021-09-07 | 山东中医药大学 | Medicinal component composition for improving gray and yellow face color and promoting white and glossy face |
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