CN107137317A

CN107137317A - A kind of production method of cell activator cosmetic cream using plant extracts as main functional component

Info

Publication number: CN107137317A
Application number: CN201710396902.5A
Authority: CN
Inventors: 李青
Original assignee: Individual
Current assignee: Individual
Priority date: 2017-05-31
Filing date: 2017-05-31
Publication date: 2017-09-08

Abstract

The invention discloses a kind of production method of the cell activator cosmetic cream using plant extracts as main functional component, its production technology is as follows：1st, the making 2 of chinaroot greenbrier cream, motherwort element, the extraction 3 of leonurine, Paeoniflorin, the extraction 4 of paeoniflorin, the making 5 of Poria cocos fine powder, the preparation of matrix creams.Cream type is made spreads on body surface by manually extracting cell activator from plant, so as to suppress network amino acid enzymatic activity, block melanin generation, activate flavones, the main active substances such as saponin, trigger cell-stimulating reaction, improve the speed of cells survival metabolism, collagen is promoted to produce, and then play and brighten, nti-freckle, nourishes rough skin, delaying aging, the effects such as removing free radical, again due to the overall conditioning of its emphasis, emphasize first to nurse one's health inherence, then will shape in outer, therefore, cosmetic result is lasting, stablize and with pure natural property, with nontoxic, it is harmless, not carcinogenic the features such as.

Description

A kind of life of cell activator cosmetic cream using plant extracts as main functional component Production method

Technical field

The present invention relates to a kind of production technology of cell activator cosmetic cream, more particularly to chinaroot greenbrier, motherwort, the root of herbaceous peony, Tuckahoe extracts produce the technique of novel cell activator cosmetic cream as main component, belong to Cosmetic Manufacture technical field.

Background technology

Raising with people's living standard and the requirement more and more higher to skin care, beauty, cell activator class Cosmetics are increasingly becoming one of focus of research and development.People get used to a large amount of use and contain hexichol first during skin care, beauty Inorganic dose of ketone, dibenzoyl methane, BTA etc., its result can cause blocking pore, cause cutaneous lesions, also some products Formula is because allergic excessively using causing ultra-violet absorber, the heavy damage n cell activation function of human body.Grind Study carefully discovery, human body has cell-stimulating system in itself, cream type, which is made, by manually extracting cell activator from plant spreads on human body Body surface, so as to suppress network amino acid enzymatic activity, blocks melanin generation, activates the main active substances such as flavones, saponin, trigger cell Activating reaction, improve cells survival metabolism speed, promote collagen produce, and then play brighten, nti-freckle, nourishes rough skin, Delaying aging, the effects such as remove free radical, and due to the overall conditioning of its emphasis, emphasize first to nurse one's health inherence, then will shape it In outer, therefore, cosmetic result persistently, it is stable and with pure natural property, with it is nontoxic, harmless, not carcinogenic the features such as, therefore this A little natural cosmetic cream sensitization are low, security is good, therefore increasingly favored by people, have wide in cosmetics exploitation Application prospect.

The content of the invention

The purpose of the present invention is exactly to design one kind using chinaroot greenbrier, motherwort, the root of herbaceous peony, Poria cocos natural plants as raw material, through one After series crushing, extraction process, corresponding component is extracted, is allocated through specific formula, a kind of new high-efficiency beauty is produced and produces Product.

The first raw material chinaroot greenbrier of the invention, chinaroot greenbrier is rich in saponins, flavones etc., alkaloid, amino acid, Rhizoma Smilacis Chinensis extract tool There is very strong radical scavenging activity, can induce cellular superoxide dismutase, catalase, glutathione peroxidase Active Anti-oxidation behavior, Rhizoma Smilacis Chinensis extract make the colour of skin more it is homogeneous it is glossy, desalination senile plaque expelling, improve skin color and luster have it is special Effect.

Second of raw material motherwort of the invention, motherwort can dispel silt life newly, promoting blood circulation for regulating menstruation, rich in lot of trace such as selenium, manganese Element, can anti-oxidant, anti-aging, the beneficial face beauty functions with special-effect.

The third raw material root of herbaceous peony of the invention, the root of herbaceous peony is rich in Paeoniflorin, paeoniflorin, volatile oil, cupreol and triterpenes Deng, the root of herbaceous peony is sweet, sour, cold nature, the effect with blood-nourishing, can treat sallow complexion, facial colour spot, tarnish, so as to The effects such as with invigorating qi and benefiting blood, whitening and moistening skin.

4th kind of raw material Poria cocos of the invention, Poria cocos is rich in pachymaran, lecithin, adenine, choline, ergosterol etc., It has nutrition skin, and wrinkle is gone in whitening, eliminates effect of spot, it not only has effects that bright and clean skin, while can also be effective Delay skin aging, cosmetic result is fairly obvious.

One kind is now introduced to be extracted its active ingredient for Raw material processing by chinaroot greenbrier, motherwort, the root of herbaceous peony, Poria cocos and be equipped with specific The production technology for the novel cosmetic cream that auxiliary material makes is as follows：

1. the making of chinaroot greenbrier cream：The Roots of Smilax China L just excavated is cleaned, dry, crushed, 80 mesh sieves is crossed, takes a certain amount of chinaroot greenbrier powder End, adds 95% ethanol immersion refluxing extraction 3-5 times, and 2-4h is extracted every time, extract solution is merged, paste is concentrated under reduced pressure to give Thing, paste refrigeration is standby, and the chinaroot greenbrier cream contains saponin, flavones, alkaloid, amino acid, polyatomic phenol, organic acid and carbohydrate Deng skin care bioactive substance；

2. being crushed after a certain amount of new fresh leonurus cleaning is fully dried, 60 mesh sieves are crossed, motherwort powder is taken, is in concentration Ultrasonic-leaching in 80-95% ethanol solutions, supersonic frequency is 40kHz, and ultrasonic power 100W, extraction time is 60-90min, material Liquor ratio is 1: 20-1: 25（g/ml）, make motherwort element, the basic dissolution of leonurine material in raw material, extraction collected after filtering Liquid, leaching liquor is concentrated in vacuo recycling design, when the volume of concentrate reaches 0.2-0.3 times of stoste, by XDA-7 macropores on concentrate Resin column is adsorbed, and the rate of adsorption is 1-4BV/h, and water elution is distilled with 2BV after the completion of absorption, then normal with 95% ethanol solution Temperature elution, elution rate 2-6 BV/h collect eluent, are concentrated in vacuo, freeze-drying, obtain motherwort element, motherwort Alkali；

3. the Paeoniflorin, paeoniflorin in the root of herbaceous peony are extracted：A certain amount of dry White Peony Root is taken, the steaming of 8-20 times of quality is added Distilled water, heats 70-100min at a temperature of 60-90 DEG C, and filtrate is concentrated into original by abundant filtering and collecting filter liquid in evaporimeter 0.2-0.4 times of liquid product, 80% ethanol of 3-5 times of volume is added in concentrate, 5-10min is sufficiently stirred for, until in solution Precipitation largely formed, abandoned after filtering filtrate collect sediment, crisp solid powder is obtained after freeze-drying, as in the root of herbaceous peony Paeoniflorin, paeoniflorin；

4. the making of Poria cocos fine powder：Fresh Poria cocos is put into after clear water cleans rossing and is cut into about 15 centimeter lengths, the cm of diameter 6 Root segment, be put into beater, add the molten solution of sodium sulfite of 0.8-2.0 times of Poria cocos weight（Concentration is 200-500ppm）, And 70% edible alcohol of 1-2 times of Poria cocos weight, smash mashing 5-10min to pieces, stir, muscle is removed with 80 mesh steel wire sievings Slag, the slurry after sieving is put into sedimentation basin rapidly, is inserted slow uniform stirring in slurry with clean waddy, is sunken to impurity Bottom, is waited after its natural layering, is removed upper strata aqueous, is isolated the precipitation Poria cocos powder of lower floor, contain in container, in wet Poria cocos powder After the upper clean cotton of 3-6 layers of covering, suck dry moisture, cotton is thrown off, Poria cocos powder is separated with perching knife, then pure Poria cocos powder is existed Drying room 50-60 DEG C of pest fire drying, natural cooling 24 hours, final moisture content no more than 4-6%, using grinding for adjustable clearance Poria cocos powder after grinding machine mill-drying, crosses 200 mesh sieves, obtains Poria cocos fine powder；

5. the preparation of matrix creams：By the stearic alcohol ether of polyoxyethylene (2), C16-18 alcohol, isopropyl palmitate fat, jojoba oil, sheep Be heated to 80-100 DEG C of stirring and dissolving after hair fat mixing, be incubated as A phases it is standby, while creatine is dissolved in deionized water, plus Enter triethanolamine, glycerine, emulsifying agent AC1802 mixing, be heated to 90 DEG C be incubated as B phases it is standby, by the motherwort made Element, leonurine component, Paeoniflorin, paeoniflorin, chinaroot greenbrier cream, Poria cocos fine powder add deionized water and appropriate 95% ethanol to dissolve, Mixed under normal temperature, it is standby as C phases, when A, B two-phase temperature are roughly the same, under homogenizer state, B phases are slowly added Enter A phases, while continuing homogeneous 8-10 min with homogenizer, then in 50-80 DEG C of insulated and stirred froth breaking 2-5min of temperature, work as system When being cooled to 35-50 DEG C, C phases are added, continues to be slowly stirred, is discharged during to room temperature；

The specific formula of this product is as follows：

A phases：(w/%)：Polyoxyethylene (2) tristearin alcohol ether 2.0-5.0, jojoba oil 1.0-3.0, cosmetics C16-18 alcohol 1.0-4.0, isopropyl palmitate 2.0-6.0, lanolin 0.5-2.5, emulsifying agent 18000.1-0.5, olive oil 1.0-4.0；

B phases：（W/%)：Creatine 0.5-2.0, glycerine 5.0-12.0, triethanolamine 2-0.8, AC1802 1.0-3.0, deionized water 15.0-30.0；

C phases：（W/%)：Motherwort element, leonurine component 4.0-7.0, Paeoniflorin, paeoniflorin 3.0-5.0, chinaroot greenbrier cream 4.0- 6.0, Poria cocos powder 4.0-7.0, ethanol（95%）10.0-15.0, plus deionized water is to 100.

The main advantages of the present invention for：1. cosmetic cream main component is generally octyl salicylate, methoxycinnamate in the market Misery ester and benzophenone and its derivative, titanium dioxide, the compound such as zinc oxide.Cosmetic cream is in order to obtain more than 30 high SPF Value, additive capacity is often very big, the problem of this just causes security and cost aspect.Swashed by manually extracting cell from plant Agent living is made cream type and spreads on body surface, so as to suppress network amino acid enzymatic activity, blocks melanin generation, activation flavones, saponin etc. Main active substances, trigger cell-stimulating reaction, improve the speed of cells survival metabolism, promote collagen to produce, Jin Erqi To brightening, nti-freckle, nourishes rough skin, delaying aging, the effects such as remove free radical, and due to the overall conditioning of its emphasis, emphasize elder generation Conditioning is inherent, then will shape in outer, therefore, cosmetic result persistently, it is stable and with pure natural property, with nontoxic, nothing Harmful, not carcinogenic the features such as, these functions are that general cosmetics are unable to reach.2. the present invention is made using various plants extraction components Assembled for natural enamel, and optimize its proportioning, be allowed to reach best cosmetic result with minimum consumption.

Embodiment：

1. firm excavation 10kg Roots of Smilax China L is cleaned, dry, crushed, 80 mesh sieves are crossed, 8kg chinaroot greenbrier powder is taken, 95% is added Ethanol immersion refluxing extraction 4 times, extracts 3h, extract solution is merged, be concentrated under reduced pressure to give paste 300g, by the paste every time Refrigeration is standby, and chinaroot greenbrier cream biology containing skin cares such as saponin, flavones, alkaloid, amino acid, polyatomic phenol, organic acid and carbohydrates is living Property material；

2. being crushed after the new fresh leonurus cleanings of 4kg are fully dried, 60 mesh sieves are crossed, motherwort powder is taken, be 95% in concentration Ultrasonic-leaching in ethanol solution, supersonic frequency 40kHz, ultrasonic power 100W, extraction time are 90min, and solid-liquid ratio is 1: 23 （g/ml）, make in raw material motherwort element, the basic dissolution of leonurine material, leaching liquor is collected after filtering, leaching liquor vacuum is dense Contracting recycling design, when the volume of concentrate reaches 0.3 times of stoste, the macroporous resin columns of XDA- on concentrate 7 is adsorbed, absorption Speed is 3BV/h, and water elution is distilled with 2BV after the completion of absorption, is then eluted with 95% ethanol solution normal temperature, elution rate 3BV/ H, collects eluent, is concentrated in vacuo, freeze-drying, obtains motherwort element, leonurine component 102g；

3. taking 2kg drying White Peony Root, the distilled water of 20 times of quality is added, 90min is heated at a temperature of 85 DEG C, fully filtering After collect filtrate, filtrate is concentrated into evaporimeter to 0.3 times of stoste volume, 80% second of 5 times of volumes is added in concentrate Alcohol, is sufficiently stirred for 10min, until the precipitation in solution is largely formed, filtrate is abandoned after filtering and collects sediment, after freeze-drying To crisp solid powder 25g, as Paeoniflorin, paeoniflorin；

About 15 centimeter lengths, the root segment of the cm of diameter 6 are cut into after the clean rossing of clear water 4. the fresh Poria cocos of 6kg is put into, is put into In beater, the sodium sulfite solution of 1.5 times of Poria cocos weight is added（Concentration is 300ppm）, and 2 times of Poria cocos weight 70% Edible alcohol, smashs mashing 10min to pieces, stirs, remove muscle slag with 80 mesh steel wire sievings, the slurry after sieving is put into rapidly In sedimentation basin, slow uniform stirring in slurry is inserted with clean waddy, impurity is sunken to bottom, waits after its natural layering, Upper strata aqueous is removed, the precipitation Poria cocos powder of lower floor is isolated, contains in container, 5 layers of clean cotton are covered on wet Poria cocos powder, is inhaled After solid carbon dioxide point, cotton is thrown off, Poria cocos powder is separated with perching knife, then pure Poria cocos powder in 60 DEG C of pest fire dryings of drying room, oneself So cool down 24 hours, final moisture content may not exceed 5%, using the Poria cocos powder after the grinder mill-drying of adjustable clearance, mistake 200 mesh sieves, obtain Poria cocos fine powder 345g；

5. it is heated to after the stearic alcohol ether of polyoxyethylene (2), C16-18 alcohol, isopropyl palmitate fat, jojoba oil, lanolin are mixed 90 DEG C of stirring and dissolvings, are incubated standby as A phases, while creatine is dissolved in deionized water, add triethanolamine, glycerine, emulsification Agent AC1802 mix, be heated to 90 DEG C be incubated as B phases it is standby；By the motherwort made element, leonurine component, Chinese herbaceous peony Glucoside, paeoniflorin, chinaroot greenbrier cream, Poria cocos fine powder add deionized water and appropriate 95% ethanol to dissolve, and mix at normal temperatures, standby as C phases With；When A, B two-phase temperature are roughly the same, under homogenizer state, B phases are slowly added to A phases, at the same with homogenizer after The continuous min of homogeneous 10, then in 75 DEG C of insulated and stirred froth breaking 5min of temperature, when system is cooled to 45 DEG C, adds C phases, continues slow Slow stirring, discharges during to room temperature；

The specific formula of this product is as follows：

A phases：(w/%)：Polyoxyethylene (2) tristearin alcohol ether 4.0, jojoba oil 2.0, cosmetics C16-18 alcohol 1.5, palmitic acid Isopropyl ester 3.0, lanolin 1.0, emulsifying agent 1,800 0.5, olive oil 1.0；

B phases：（W/%)：Creatine 1.5, glycerine 8.0, triethanolamine 0.8, AC1802 3.0, deionized water 25.0；

C phases：（W/%)：Motherwort element, leonurine component 6.0, Paeoniflorin, paeoniflorin 4.0, chinaroot greenbrier cream 5.0, root of kudzu vine fine powder 5.0, ethanol（95%）15.0, plus deionized water is to 100.

The present invention is exemplarily described above, it is clear that the present invention, which is implemented, to be not subject to the restrictions described above, As long as employing the improvement of the various unsubstantialities of inventive concept and technical scheme of the present invention progress, or not improved this is sent out Bright design and technical scheme directly applies to other occasions, within protection scope of the present invention.

Claims

1. a kind of production method of cell activator cosmetic cream using plant extracts as main functional component, it is characterised in that Its step includes the making of chinaroot greenbrier cream, the extraction of motherwort element and leonurine, the extraction of Paeoniflorin and paeoniflorin, Poria cocos Making, the preparation of matrix creams of fine powder.

2. the producer of the cell activator cosmetic cream according to claim 1 using plant extracts as main functional component Method, it is characterised in that clean the Roots of Smilax China L just excavated, dry, crush, crosses 80 mesh sieves, takes a certain amount of chinaroot greenbrier powder, plus Enter 95% ethanol immersion refluxing extraction 3-5 times, 2-4h is extracted every time, extract solution is merged, paste is concentrated under reduced pressure to give, by this Paste refrigeration is standby, and the chinaroot greenbrier cream is containing skin cares such as saponin, flavones, alkaloid, amino acid, polyatomic phenol, organic acid and carbohydrates Bioactive substance.

3. the producer of the cell activator cosmetic cream according to claim 1 using plant extracts as main functional component Method, it is characterised in that crushed after a certain amount of new fresh leonurus cleaning is fully dried, cross 60 mesh sieves, take motherwort powder, The ultrasonic-leaching in concentration is 80-95% ethanol solutions, supersonic frequency is 40kHz, and ultrasonic power 100W, extraction time is 60- 90min, solid-liquid ratio is 1: 20-1: 25（g/ml）, make motherwort element, the basic dissolution of leonurine material in raw material, after filtering Leaching liquor is collected, leaching liquor is concentrated in vacuo recycling design, when the volume of concentrate reaches 0.2-0.3 times of stoste, by concentrate XDA-7 macroporous resin columns are adsorbed, and the rate of adsorption is 1-4BV/h, water elution are distilled with 2BV after the completion of absorption, then with 95% Ethanol solution normal temperature is eluted, elution rate 2-6 BV/h, collects eluent, is concentrated in vacuo, and freeze-drying obtains motherwort Element, leonurine.

4. the producer of the cell activator cosmetic cream according to claim 1 using plant extracts as main functional component Method, it is characterised in that take a certain amount of dry White Peony Root, adds the distilled water of 8-20 times of quality, at a temperature of 60-90 DEG C 70-100min is heated, filtrate is concentrated into evaporimeter 0.2-0.4 times of stoste volume by abundant filtering and collecting filter liquid, 80% ethanol of 3-5 times of volume is added in concentrate, 5-10min is sufficiently stirred for, until the precipitation in solution is largely formed, filtered After abandon filtrate collect sediment, crisp solid powder is obtained after freeze-drying, Paeoniflorin, paeoniflorin as in the root of herbaceous peony.

5. the producer of the cell activator cosmetic cream according to claim 1 using plant extracts as main functional component Method, it is characterised in that fresh Poria cocos is put into about 15 centimeter lengths, the root segment of the cm of diameter 6 are cut into after the clean rossing of clear water, It is put into beater, adds the molten solution of sodium sulfite of 0.8-2.0 times of Poria cocos weight（Concentration is 200-500ppm）, and Poria cocos 70% edible alcohol of 1-2 times of weight, smashs mashing 5-10min to pieces, stirs, muscle slag is removed with 80 mesh steel wire sievings, by sieving Slurry afterwards is put into sedimentation basin rapidly, is inserted slow uniform stirring in slurry with clean waddy, impurity is sunken to bottom, wait it After natural layering, upper strata aqueous is removed, the precipitation Poria cocos powder of lower floor is isolated, contains in container, 3-6 is covered on wet Poria cocos powder After the clean cotton of layer, suck dry moisture, cotton is thrown off, Poria cocos powder is separated with perching knife, then pure Poria cocos powder in drying room 50- 60 DEG C of pest fire dryings, natural cooling 24 hours, final moisture content grinds dry no more than 4-6% using the grinder of adjustable clearance Poria cocos powder after dry, crosses 200 mesh sieves, obtains Poria cocos fine powder.

6. the producer of the cell activator cosmetic cream according to claim 1 using plant extracts as main functional component Method, it is characterised in that mix the stearic alcohol ether of polyoxyethylene (2), C16-18 alcohol, isopropyl palmitate fat, jojoba oil, lanolin After be heated to 80-100 DEG C of stirring and dissolving, be incubated as A phases standby, while creatine is dissolved in deionized water, add three ethanol Amine, glycerine, emulsifying agent AC1802 mixing, be heated to 90 DEG C be incubated as B phases it is standby, by the motherwort made element, motherwort Alkaline constituents, Paeoniflorin, paeoniflorin, chinaroot greenbrier cream, Poria cocos fine powder add deionized water and appropriate 95% ethanol to dissolve, and mix at normal temperatures Close, it is standby as C phases, when A, B two-phase temperature are roughly the same, under homogenizer state, B phases are slowly added to A phases, together When with homogenizer continue homogeneous 8-10 min, then in 50-80 DEG C of insulated and stirred froth breaking 2-5min of temperature, when system is cooled to At 35-50 DEG C, C phases are added, continues to be slowly stirred, is discharged during to room temperature.

7. the producer of the cell activator cosmetic cream according to claim 1 using plant extracts as main functional component Method, it is characterised in that the specific formula of this product is as follows：

B phases：（W/%)：Creatine 0.5-2.0, glycerine 5.0-12.0, triethanolamine 2-0.8, AC18021.0-3.0, deionized water 15.0-30.0；