CN108143658A - A kind of herbal mixture anti-acne emulsifiable paste and preparation method thereof - Google Patents
A kind of herbal mixture anti-acne emulsifiable paste and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
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Abstract
The present invention relates to a kind of herbal mixture anti-acne emulsifiable pastes and preparation method thereof, belong to cosmetic technical field.The present invention assists andrographolide using N sodium lauroyl sarcosines, gos deep into hair follicle depths, eliminates skin oil and fat and dirt, propionibacterium acnes flora related to other acnes is killed, recycles scutellaria that there is heat-clearing and damp-drying drug, purging intense heat and detonicating, removing pattogenic heat from the blood and toxic material from the body, the functions such as dispelling stasis of blood and stimulating the menstrual flow, carbuncle sore tumefacting virus, removing toxic substances sore, ultraviolet light can be absorbed with reference to scutelloside and Antarctic ice microalgae, scavenging activated oxygen, and the generation of melanin can be inhibited, improve anti-acne effect of ejecting poison；The present invention inhibits proliferation of fibrous tissue, promotes skin growth, and connective tissue rete vasculosum increases, and mucilage secretion increases, and fur hyperplasia accelerates, and acne skin is made quickly to heal, and achievees the purpose that treat acne；Inventive formulation product is mild, non-stimulated, and anti-acne effect is apparent, and quick, and after several weeks are used continuously, skin is restored to that sparkling clean, health is full flexible, and does not stay pockmark.
Description
Technical field
The present invention relates to a kind of herbal mixture anti-acne emulsifiable pastes and preparation method thereof, belong to cosmetic technical field.
Background technology
Acne is commonly called as whelk, is a kind of common chronic skin disease for being happened at pilosebaceous follicle, and sebaceous glands enriches
Position, such as face, shirtfront back and neck be easier to multiple and recur.It is main to be apt to occur in hebetic men and women, adult
You also have generation to image, only have different incidence and different partings in different age levels, not only greatly influence
There is large effect to daily life and social activity, and to the psychology variation in teenager's stage, result even in Asia
Health.
Acne is the chronic skin disease as caused by many factors of inside and outside, and pathogenesis is complex, it is now recognized that
Mainly with sebaceous glands excessive secretion, propionibacterium acnes proliferation, the dyskeratosis of pilosebaceous duct, environmental factor and heredity
Etc. factors it is related.Doctor trained in Western medicine is mostly symptomatic treatment for the treatment of acne, at present common anti-acne drug include antiandrogen drug,
Antibiotic, Tretinoin, benzoyl peroxide etc..Although above for oral administration and external application Western medicine has good effect to the treatment of acne
Fruit, but there is also some problems simultaneously, as that can cause centainly to damage to the skin health of patient after quick sterilization anti-acne, go out
Phenomena such as now dry skin, furfur, scorching hot, itch, erythema, coarse, pore become larger, antiandrogen drug can also bring secretion to lose
The side effect of tune, it is prudent using needing, and drug resistance easily recurs.
The effect of Chinese medicine treatment acne is affirmative, and unique effect is played in the treatment to acne, can be from a variety of
Approach reaches the curative effects such as sterilization, antibacterial, and therefore, developing a kind of external preparation with active Chinese drug component Substance treatment acne seems particularly
It is important.
Invention content
The technical problems to be solved by the invention：Easily cause a variety of adverse reactions for treatment acne application Western medicine, and
The problem of drug resistance easily recurs provides a kind of herbal mixture anti-acne emulsifiable paste and preparation method thereof.
In order to solve the above technical problems, the technical solution adopted by the present invention is：
It is formed including following weight parts raw material：2~4 parts of Andrographis Paniculatas, 8~16 parts of Chinese medical extracts, 5~10 parts of Pogostemon cablin
Essential oil, 8~16 parts of albolene, 4~8 parts of glycerine, 5~10 parts of propylene glycol, 1~2 part of allantoin, 50~100 parts of deionized waters,
10~20 parts of N- sodium lauroyl sarcosines, 2~4 parts of lauryl sodium sulfate, 0.1~0.5g preservatives.
It is that 75% ethanol solution flows back at 80~90 DEG C and carries that the Andrographis Paniculata, which is Herba Andrographitis powder by mass fraction,
It takes, extracting solution is evaporated to the paste that water content is 20~30%.
The mass ratio of the Herba Andrographitis powder and ethanol solution is 1：5~1：20.
The Chinese medical extract boils extraction filtering for Chinese medicine mixed-powder by deionized water heating, and filtrate is evaporated to aqueous
Measure the paste for 30~35%.
The Chinese medicine mixed-powder and the mass ratio of deionized water are 1：5~1：20.
The Chinese medicine mixed-powder is by 20~40 parts by weight scutellarias, 30~60 parts by weight plantain seeds, 30~60 parts by weight product
Snow grass, the ground 40 mesh sieve series of 20~40 parts by weight Antarctic ice microalgaes into.
The preservative is methyl hydroxybenzoate.
A kind of preparation method of the herbal mixture anti-acne emulsifiable paste, the specific steps are：
（1）By natural air drying after Herba Andrographitis washes clean, 40 mesh sieve is crushed, obtains Herba Andrographitis powder；
（2）Take Herba Andrographitis powder add in ethanol solution in 1~2h of refluxing extraction, filter to obtain filter residue, by filter residue repeat refluxing extraction 1~
2 times, merge extracting solution, extracting solution is evaporated to the paste that water content is 20~30%, obtains Andrographis Paniculata；
（3）Scutellaria, plantain seed, centella, Antarctic ice microalgae are taken, ground 40 mesh sieve obtains Chinese medicine mixed-powder；
（4）Chinese medicine mixed-powder is taken to add in heating in deionized water and boils 1~2h of extraction, filter cake and filtrate are filtered to obtain, by filter cake
Extraction 1~2 time, merging filtrate are repeated, then filtrate is evaporated to the paste that water content is 30~35%, obtains Chinese medical extract；
（5）Take albolene, glycerine, propylene glycol, allantoin, add in deionized water, and be heated to 90~95 DEG C of stirrings 20~
30min adds in N- sodium lauroyl sarcosines, lauryl sodium sulfate after being cooled to 85~90 DEG C, stir 20~30min, cooling
To 45~50 DEG C, Andrographis Paniculata, Chinese medical extract, Pogostemon cablin essential are added, stir 30~40min, it is cooled to 40~
Preservative is added in after 45 DEG C, stir evenly and stands 6~10h, filling discharging obtains herbal mixture anti-acne emulsifiable paste.
Compared with other methods, advantageous effects are the present invention：
（1）The present invention assists andrographolide using N- sodium lauroyl sarcosines, gos deep into hair follicle depths, eliminates skin oil and fat and dirt
Dirt kills propionibacterium acnes flora related to other acnes, scutellaria is recycled to have heat-clearing and damp-drying drug, purging intense heat and detonicating, cool blood solution
The functions such as poison, dispelling stasis of blood and stimulating the menstrual flow, carbuncle sore tumefacting virus, removing toxic substances sore can absorb ultraviolet light with reference to scutelloside and Antarctic ice microalgae, remove oxygen certainly
By base, and the generation of melanin can be inhibited, improve anti-acne effect of ejecting poison；
（2）The present invention inhibits the permeability of capillary using plantago asiatica linne polyoses, inhibits the volume of diffusate and the number of leucocyte
Amount, and also have the characteristics of certain inhibiting effect to the hyperplasia of granulation tissue, blocked with reference to Pogostemon cablin essential or inhibit TLR2's
Activation inhibits synthesis and secretion with the relevant cell factor of immune response and secondary inflammation medium, so as to avoid by a variety of
Extensive inflammation caused by bacterial component reacts, and inhibits the generation of inflammation, while inhibit collagenous fibres by asiaticosid, inhibits fine
Dimensional tissue hyperplasia promotes skin growth, local leukocytosis, and connective tissue rete vasculosum increases, and mucilage secretion increases, and fur increases
It is raw to accelerate, acne skin is made quickly to heal, achievees the purpose that treat acne；
（3）Inventive formulation product is mild, non-stimulated, and anti-acne effect is apparent, and quick, and after several weeks are used continuously, skin is extensive
It arrives that sparkling clean, health is full flexible again, and does not stay pockmark.
Specific embodiment
It by natural air drying after Herba Andrographitis washes clean, and is fitted into pulverizer and crushes, cross 40 mesh sieve, obtain Herba Andrographitis powder, take
50~100g Herba Andrographitis powder, it is the refluxing extraction 1 at 80~90 DEG C in 75% ethanol solution to add in 500~1000g mass fractions
~2h filters to obtain filter residue, and filter residue is repeated refluxing extraction 1~2 time, merges extracting solution, then extracting solution is placed in Rotary Evaporators
On be evaporated to the paste that water content is 20~30%, obtain Andrographis Paniculata, take 20~40g scutellarias, 30~60g plantain seeds, 30
~60g centellas, 20~40g Antarctic ice microalgaes are fitted into grinder and grind, and cross 40 mesh sieve, obtain Chinese medicine mixed-powder, take 80~
160g Chinese medicine mixed-powders are added in 0.8~1.6L deionized waters, and 10~15min is stirred, and heat with 300~400r/min
1~2h of extraction is boiled, filters to obtain filter cake and filtrate, filter cake is repeated into extraction 1~2 time, merging filtrate, then be transferred to Rotary Evaporators
On be evaporated to the paste that water content is 30~35%, obtain Chinese medical extract, take 8~16g albolene, 4~8g glycerine, 5~
10g propylene glycol, 1~2g allantoins add in 50~100mL deionized waters, and are heated to 90~95 DEG C, with 300~400r/
Min 20~30min of insulated and stirred add in 10~20gN- sodium lauroyl sarcosines, 2~4g dodecanes after being cooled to 85~90 DEG C
Base sodium sulphate continues 20~30min of stirring, is cooled to 45~50 DEG C, adds 2~4g Andrographis Paniculatas, 8~16g Chinese medicines
Extract, 5~10g Pogostemon cablin essentials stir 30~40min with 200~300r/min, 0.1 are added in after being cooled to 40~45 DEG C
~0.5g preservatives stir evenly and stand 6~10h, and filling discharging obtains herbal mixture anti-acne emulsifiable paste.
Example 1
It by natural air drying after Herba Andrographitis washes clean, and is fitted into pulverizer and crushes, cross 40 mesh sieve, obtain Herba Andrographitis powder, 50g is taken to wear
Heart lotus powder adds in 500g mass fractions as in 75% ethanol solution, the refluxing extraction 1h at 80 DEG C filters to obtain filter residue, by filter residue weight
Refluxing extraction 1 time again merges extracting solution, then extracting solution is placed on Rotary Evaporators to the paste for being evaporated to that water content is 20%,
Andrographis Paniculata, take 20g scutellarias, 30g plantain seeds, 30g centellas, 20g Antarctic ice microalgaes are fitted into grinder and grind, mistake
40 mesh sieve, and obtain Chinese medicine mixed-powder, take 80g Chinese medicine mixed-powders, add in 0.8L deionized waters, are stirred with 300r/min
10min, and heat and boil extraction 1h, filter cake and filtrate are filtered to obtain, filter cake is repeated into extraction 1 time, merging filtrate, then be transferred to rotation
The paste that water content is 30% is evaporated on evaporimeter, Chinese medical extract is obtained, takes 8g albolene, 4g glycerine, 5g propylene glycol,
1g allantoins add in 50mL deionized waters, and are heated to 90 DEG C, with 300r/min insulated and stirred 20min, after being cooled to 85 DEG C
10gN- sodium lauroyl sarcosines are added in, 2g lauryl sodium sulfate continues to stir 20min, is cooled to 45 DEG C, adds 2g and wear
Heart lotus extract, 8g Chinese medical extracts, 5g Pogostemon cablin essentials stir 30min with 200r/min, 0.1g are added in after being cooled to 40 DEG C
Preservative stirs evenly and stands 6h, and filling discharging obtains herbal mixture anti-acne emulsifiable paste.
Example 2
It by natural air drying after Herba Andrographitis washes clean, and is fitted into pulverizer and crushes, cross 40 mesh sieve, obtain Herba Andrographitis powder, 80g is taken to wear
Heart lotus powder adds in 800g mass fractions as in 75% ethanol solution, the refluxing extraction 1h at 85 DEG C filters to obtain filter residue, by filter residue weight
Refluxing extraction 1 time again merges extracting solution, then extracting solution is placed on Rotary Evaporators to the paste for being evaporated to that water content is 25%,
Andrographis Paniculata, take 30g scutellarias, 45g plantain seeds, 45g centellas, 30g Antarctic ice microalgaes are fitted into grinder and grind, mistake
40 mesh sieve, and obtain Chinese medicine mixed-powder, take 120g Chinese medicine mixed-powders, add in 1.2L deionized waters, are stirred with 350r/min
12min, and heat and boil extraction 1h, filter cake and filtrate are filtered to obtain, filter cake is repeated into extraction 1 time, merging filtrate, then be transferred to rotation
The paste that water content is 32% is evaporated on evaporimeter, Chinese medical extract is obtained, takes 12g albolene, 6g glycerine, 8g propylene glycol,
1g allantoins add in 80mL deionized waters, and are heated to 92 DEG C, with 350r/min insulated and stirred 25min, after being cooled to 88 DEG C
15gN- sodium lauroyl sarcosines are added in, 3g lauryl sodium sulfate continues to stir 25min, is cooled to 48 DEG C, adds 3g and wear
Heart lotus extract, 12g Chinese medical extracts, 8g Pogostemon cablin essentials stir 35min with 250r/min, are added in after being cooled to 42 DEG C
0.3g preservatives stir evenly and stand 8h, and filling discharging obtains herbal mixture anti-acne emulsifiable paste.
Example 3
It by natural air drying after Herba Andrographitis washes clean, and is fitted into pulverizer and crushes, cross 40 mesh sieve, obtain Herba Andrographitis powder, take 100g
Herba Andrographitis powder adds in 1000g mass fractions as in 75% ethanol solution, the refluxing extraction 2h at 90 DEG C filters to obtain filter residue, will filter
Slag repeats refluxing extraction 2 times, merges extracting solution, then extracting solution is placed on Rotary Evaporators to the cream for being evaporated to that water content is 30%
Shape object, obtains Andrographis Paniculata, takes 40g scutellarias, 60g plantain seeds, 60g centellas, and 40g Antarctic ice microalgaes are fitted into grinder and grind
Mill is crossed 40 mesh sieve, obtains Chinese medicine mixed-powder, take 160g Chinese medicine mixed-powders, added in 1.6L deionized waters, stirred with 400r/min
15min is mixed, and heats and boils extraction 2h, filters to obtain filter cake and filtrate, filter cake is repeated into extraction 2 times, merging filtrate, then be transferred to rotation
Turn to be evaporated to the paste that water content is 35% on evaporimeter, obtain Chinese medical extract, take 16g albolene, 8g glycerine, 10g the third two
Alcohol, 2g allantoins add in 100mL deionized waters, and are heated to 95 DEG C, with 400r/min insulated and stirred 30min, are cooled to 90
20gN- sodium lauroyl sarcosines are added in after DEG C, 4g lauryl sodium sulfate continues to stir 30min, is cooled to 50 DEG C, adds
4g Andrographis Paniculatas, 16g Chinese medical extracts, 10g Pogostemon cablin essentials stir 40min with 300r/min, add after being cooled to 45 DEG C
Enter 0.5g preservatives, stir evenly and stand 10h, filling discharging obtains herbal mixture anti-acne emulsifiable paste.
Reference examples：The herbal mixture anti-acne emulsifiable paste of Anhui company production.
The herbal mixture anti-acne emulsifiable paste of example and reference examples is detected, specific detection is as follows：
Particle size determination：Emulsifiable paste 0.1g is taken, 10ml aquae destillatas is added to dilute, ultrasonic 15min, by Nano-ZS90 type Malvern laser grains
Degree measureization is measured.
PH value measures：Emulsifiable paste 1g is weighed, 10ml is added in and newly boils in the aquae destillata let cool, sonic oscillation 15min makes its dispersion
Uniformly, its pH value is measured with PHS-2C type precision acidity meters, measured 3 times, and calculate average value.
Microorganism, which limits, to be checked：Emulsifiable paste is external preparation, therefore to carry out microbial limit detection to it.It presses《Cosmetics are micro-
Biological inspection method》It is measured.
Content assaying method：Acceptable solution is measured with high performance liquid chromatograph, does not penetrate sample and cuticula skin below sample
The content of also lotus lactone is worn in product.Experiment totally 6 groups, every group of 6 samples, each sample be divided into acceptable solution, remaining emulsifiable paste, cuticula with
Four parts of lower skin and cuticula, mesocuticle content=applied sample amount-receive liquid hold-up-residue emulsifiable paste content-angle
Skin content under matter layer, is averaged after calculating.
Specific testing result such as table 1.
1 performance characterization contrast table of table
As shown in Table 1, the herbal mixture anti-acne emulsifiable paste that prepared by the present invention has good grain size and pH value, and microorganism checking meets
Limit regulation and good transdermal effect and therapeutic effect.
Claims (8)
1. a kind of herbal mixture anti-acne emulsifiable paste, which is characterized in that formed including following weight parts raw material：
2~4 parts of Andrographis Paniculatas, 8~16 parts of Chinese medical extracts, 5~10 parts of Pogostemon cablin essentials, 8~16 parts of albolene, 4
~8 parts of glycerine, 5~10 parts of propylene glycol, 1~2 part of allantoin, 50~100 parts of deionized waters, 10~20 parts of N- Hamposyl Ls
Sodium, 2~4 parts of lauryl sodium sulfate, 0.1~0.5g preservatives.
2. a kind of herbal mixture anti-acne emulsifiable paste as described in claim 1, which is characterized in that the Andrographis Paniculata is punching
Lotus powder is 75% ethanol solution refluxing extraction at 80~90 DEG C by mass fraction, and it is 20~30% that extracting solution, which is evaporated to water content,
Paste.
3. a kind of herbal mixture anti-acne emulsifiable paste as claimed in claim 2, which is characterized in that the Herba Andrographitis powder and ethanol solution
Mass ratio be 1：5~1：20.
4. a kind of herbal mixture anti-acne emulsifiable paste as described in claim 1, which is characterized in that the Chinese medical extract is mixed for Chinese medicine
It closes powder and extraction filtering is boiled by deionized water heating, filtrate is evaporated to the paste that water content is 30~35%.
5. a kind of herbal mixture anti-acne emulsifiable paste as claimed in claim 4, which is characterized in that the Chinese medicine mixed-powder and go from
The mass ratio of sub- water is 1：5~1：20.
6. a kind of herbal mixture anti-acne emulsifiable paste as described in claim 4 or 5, which is characterized in that the Chinese medicine mixed-powder by
20~40 parts by weight scutellarias, 30~60 parts by weight plantain seeds, 30~60 parts by weight centellas, 20~40 parts by weight Antarctic ice microalgaes are ground
Honed 40 mesh sieve series into.
7. a kind of herbal mixture anti-acne emulsifiable paste as described in claim 1, which is characterized in that the preservative is Metagin
Ester.
8. a kind of preparation method of herbal mixture anti-acne emulsifiable paste as described in claim 1~7 any one, which is characterized in that
The specific steps are：
（1）By natural air drying after Herba Andrographitis washes clean, 40 mesh sieve is crushed, obtains Herba Andrographitis powder；
（2）Take Herba Andrographitis powder add in ethanol solution in 1~2h of refluxing extraction, filter to obtain filter residue, by filter residue repeat refluxing extraction 1~
2 times, merge extracting solution, extracting solution is evaporated to the paste that water content is 20~30%, obtains Andrographis Paniculata；
（3）Scutellaria, plantain seed, centella, Antarctic ice microalgae are taken, ground 40 mesh sieve obtains Chinese medicine mixed-powder；
（4）Chinese medicine mixed-powder is taken to add in heating in deionized water and boils 1~2h of extraction, filter cake and filtrate are filtered to obtain, by filter cake
Extraction 1~2 time, merging filtrate are repeated, then filtrate is evaporated to the paste that water content is 30~35%, obtains Chinese medical extract；
（5）Take albolene, glycerine, propylene glycol, allantoin, add in deionized water, and be heated to 90~95 DEG C of stirrings 20~
30min adds in N- sodium lauroyl sarcosines, lauryl sodium sulfate after being cooled to 85~90 DEG C, stir 20~30min, cooling
To 45~50 DEG C, Andrographis Paniculata, Chinese medical extract, Pogostemon cablin essential are added, stir 30~40min, it is cooled to 40~
Preservative is added in after 45 DEG C, stir evenly and stands 6~10h, filling discharging obtains herbal mixture anti-acne emulsifiable paste.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113116775A (en) * | 2021-04-07 | 2021-07-16 | 山东药品食品职业学院 | Acne-removing gel mask and preparation process thereof |
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2018
- 2018-02-10 CN CN201810137845.3A patent/CN108143658A/en active Pending
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|---|---|---|---|---|
| US5411733A (en) * | 1992-04-27 | 1995-05-02 | Hozumi; Toyoharu | Antiviral agent containing crude drug |
| CN106177222A (en) * | 2016-08-22 | 2016-12-07 | 黄琴 | For treating the medicine of acne |
| CN106389204A (en) * | 2016-10-23 | 2017-02-15 | 广东轻工职业技术学院 | Botanical drug composition with both functions of oil controlling and pox removing and application of botanical drug composition |
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| Title |
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| 王玥等: "广藿香精油抗炎祛痘功效研究", 《日用化学工业》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113116775A (en) * | 2021-04-07 | 2021-07-16 | 山东药品食品职业学院 | Acne-removing gel mask and preparation process thereof |
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