CN105326730B - A kind of acne-removing composition and preparation method thereof containing Chinese herbal medicine extract - Google Patents
A kind of acne-removing composition and preparation method thereof containing Chinese herbal medicine extract Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
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Abstract
The invention discloses a kind of acne-removing composition and preparation method thereof containing Chinese herbal medicine extract；It is intended to provide a kind of safety, the good acne-removing composition containing Chinese herbal medicine extract of anti-acne effect, its technical solution includes the component of following mass percents, hamamelis extract 8-12%, Fourstamen Stephania Root root extract 25-35%, Cortex Phellodendri bark extract 16-24%, Purslane extract 4-6%；Aloe leaf extract 1.5-2.5%, peony extract 4-6%, surplus is water；Belong to cosmetic technical field.
Description
Technical field
The invention discloses a kind of acne-removing compositions, specifically, be a kind of acne-removing composition containing Chinese herbal medicine extract,
The invention further relates to the preparation methods of the acne-removing composition；Belong to cosmetic technical field.
Background technique
Acne, normally referred to as dark sore, and because it is mainly in youth group, also known as whelk.Whelk is a kind of hair
Capsule sebaceous glands and its common chronic inflammation skin disease, pathogenic factor is mainly: 1, hair follicle keratinization is hyperfunction, clogging of pores；
2, endotheliosis, sebum secretion are vigorous；3, the presence of propionibacterium acnes bacterium；The pathomorphism of whelk betides skin
Most surface layer, it is different from the generation such as whitening, blackspot and wrinkle in the internal layer of skin.
The appearance of whelk causes serious influence to people's lives: 1, temporary scar: skin generates red trace
Mark appellation erythema.Whelk inflammation causes blood vessel dilatation, forms erythema fugax.Pigementation after whelk inflammation can make
Skin is obscure；2, permanent scar: whelk can leave permanent trace, and most common is exactly pothole, when inflammation degree is heavier
When injuring the collagen of more skin corium, collapsing for skin can be made and leave pothole；3, menticide: nearest research discovery
People with whelk is easier to following situation: social disconnection, the heart that lacks self-esteem do not have confidence, to people's bad taste in one's mouth, awkward hardly possible
Bear, be dejected, is angry, setback, compared with high unemployment, under these situation reciprocations, patient can be reluctant to pursue life chance, many
It is young therefore to feel oneself inferior, it is not known that how to get along with others, fear to be disliked and avoided.
The origin cause of formation of whelk mainly with hypersteatosis, pilosebaceous duct blocking, bacterium infection and inflammatory reaction
Etc. factors it is closely related.The level of androgen especially testosterone in descendant's body that adolesces increases rapidly, promotes sebaceous glands hair
It educates and generates a large amount of sebums.The dyskeratosis of pilosebaceous duct causes catheter blockage simultaneously, and dyssebacia forms angle
Matter bolt, that is, micro mist thorn.Multiple-microorganism especially propionibacterium acnes mass propagation in hair follicle, the rouge that propionibacterium acnes generate
Enzyme decomposes sebum and generates free fatty acid, while chemotactic inflammatory cell and medium, finally induces and aggravates inflammatory reaction.
For the whelk of severity, can select take drugs, the modes such as antibiotic treatment, long-term steroid.But this
It is the means that acute attack stage uses, is used for a long time and causes the bad phenomenons such as allergy, it is unfavorable to health.But the elimination of small pox
More be solve skin external factor and non-skin built in problem itself.
Summary of the invention
In view of the above-mentioned problems, the object of the present invention is to provide a kind of safety, anti-acne effect are good containing Chinese herbal medicine extract
Acne-removing composition, the invention further relates to the preparation methods of the composition.
In order to solve the above technical problems, first technical solution provided by the invention is such that
A kind of acne-removing composition containing Chinese herbal medicine extract, the component including following mass percents, hamamelis extract
8-12%, Fourstamen Stephania Root root extract 25-35%, Cortex Phellodendri bark extract 16-24%；Purslane extract 4-6%；Chinese aloe leaf mentions
Take liquid 1.5-2.5%；Peony extract 4-6%, surplus are water.
The above-mentioned acne-removing composition containing Chinese herbal medicine extract further includes extract of cinnamomum cassia bark 1- in the composition
4%.
The above-mentioned acne-removing composition containing Chinese herbal medicine extract further includes bisabolol 1-2% in the composition.
Further, the above-mentioned acne-removing composition containing Chinese herbal medicine extract, the hamamelis extract pass through following
Step is made: weighing witch hazel and is placed in flask, 8-12 times of water of witch hazel weight is added, after impregnating 0.3-1h, in 55-65 DEG C of water
Refluxing extraction 0.8-1.2h under the conditions of bath, extraction fluid, the dregs of a decoction continuously add 8-12 times of water of water, flow back and mention at 55-65 DEG C
0.8-1.2h is taken, secondary raffinate is obtained, merges extracting solution twice and filters, obtain clarified solution, be placed in 5 DEG C of standing 48h, filtering is heavy
Up to hamamelis extract after starch.
Further, the above-mentioned acne-removing composition containing Chinese herbal medicine extract, under the Fourstamen Stephania Root root extract passes through
It states step to be made: weighing Fourstamen Stephania Root root and be placed in flask, 8-12 times of 70wt% ethanol solution of Fourstamen Stephania Root root quality is added, impregnate
After 0.3-1h, refluxing extraction 0.8-1.2h, extraction fluid, the dregs of a decoction continuously add 8-12 times under 75-85 DEG C of water bath condition
70wt% ethanol solution, the refluxing extraction 0.8-1.2h at 75-85 DEG C obtain secondary raffinate, merge extracting solution twice and filter,
Clarified solution is obtained, is placed in 5 DEG C of standing 48h, up to Fourstamen Stephania Root root extract after filtering precipitate.
Further, the above-mentioned acne-removing composition containing Chinese herbal medicine extract, under the Cortex Phellodendri bark extract passes through
It states step to be made: weighing Cortex Phellodendri bark and be placed in flask, addition takes 8-12 times of 70wt% ethanol solution of Chinese corktree cortex amount, impregnates
After 0.3-1h, refluxing extraction 0.8-1.2h, extraction fluid, the dregs of a decoction continuously add 8-12 times under 75-85 DEG C of water bath condition
70wt% ethanol solution, the refluxing extraction 0.8-1.2h at 75-85 DEG C obtain secondary raffinate, merge extracting solution twice and filter,
Clarified solution is obtained, is placed in 5 DEG C of standing 48h, up to Cortex Phellodendri bark extract after filtering precipitate.
Further, the above-mentioned acne-removing composition containing Chinese herbal medicine extract, the Purslane extract pass through following
Step is made: purslane medicine materical crude slice weighed, is placed in flask, 8-12 times of 60wt% ethanol solution is added, after impregnating 0.3-0.8h,
Refluxing extraction 0.8-1.2h under 65-75 DEG C of water bath condition, extraction fluid, it is molten that the dregs of a decoction continuously add 8-12 times of 60wt% ethyl alcohol
Liquid, the refluxing extraction 0.8-1.2h at 65-75 DEG C obtain secondary raffinate, merge extracting solution twice and filter, obtain purslane and mention
Take liquid.
Further, the above-mentioned acne-removing composition containing Chinese herbal medicine extract, the aloe leaf extract pass through following
Step is made: taking fresh aloe, shreds, in the cloth bag after setting cleaning-sterilizing, squeeze out aloe juice, and with 80 mesh nylon gauzes
Filtering, obtains extract solution from aloe.
Further, the above-mentioned acne-removing composition containing Chinese herbal medicine extract, the extract of cinnamomum cassia bark are to weigh meat
Cassia bark is placed in flask, and addition takes 8-12 times of 70wt% ethanol solution of cassia quality, after impregnating 0.3-1h, in 75-85 DEG C of water
Refluxing extraction 0.8-1.2h under the conditions of bath, extraction fluid, the dregs of a decoction continuously add 8-12 times of 70wt% ethanol solution, in 75-85
Refluxing extraction 0.8-1.2h at DEG C obtains secondary raffinate, merges extracting solution twice and filters, obtains clarified solution, be placed in 5 DEG C of standings
48h, up to extract of cinnamomum cassia bark after filtering precipitate.
The above-mentioned acne-removing composition containing Chinese herbal medicine extract provided by the invention the preparation method comprises the following steps: 1) following mass ratio
Weigh each component；2) the weighed component of step 1) is uniformly mixed to obtain the final product.
Compared with prior art, technical solution provided by the invention, to said components scientific compatibility, reasonable formula can promote
Into the active material of cutin metabolism；The anti-inflammatory agents of the skins parasitism flora such as propionibacterium acnes, acarid can quickly be killed；
And moisture, nutritional ingredient are provided for skin, keeps skin equilibrium to moisten non-greasy, and repair the active material of damaged skin.
Specific embodiment
With reference to embodiment, claim of the invention is described in further detail, but do not constituted pair
Any restrictions of the invention, the modification of anyone limited times made in the claims in the present invention protection scope, still in this hair
Within bright claims.
Embodiment 1
The invention discloses a kind of acne-removing composition containing Chinese herbal medicine extract, every 100g includes following mass percents
Component, hamamelis extract 12g；Fourstamen Stephania Root root extract 35g；Cortex Phellodendri bark extract 16g；Purslane extract 6g；Aloe
Leaf extract 1.5g；Peony extract 6g, surplus are water.
Embodiment 2
The invention discloses a kind of acne-removing composition containing Chinese herbal medicine extract, every 100g includes following mass percents
Component, hamamelis extract 8g, Fourstamen Stephania Root root extract 25g, Cortex Phellodendri bark extract 24g；Purslane extract 4g；Chinese aloe leaf
Extracting solution 2.5g；Peony extract 4g, surplus are water.
Embodiment 3
The invention discloses a kind of acne-removing composition containing Chinese herbal medicine extract, every 100g includes following mass percents
Component, hamamelis extract 10g, Fourstamen Stephania Root root extract 30g, Cortex Phellodendri bark extract 20g；Purslane extract 5g；Aloe
Leaf extract 2g；Peony extract 5g, surplus are water.
Embodiment 4
The invention discloses a kind of acne-removing composition containing Chinese herbal medicine extract, every 100g includes following mass percents
Component, hamamelis extract 10g, Fourstamen Stephania Root root extract 30g, Cortex Phellodendri bark extract 20g；Purslane extract 5g；Aloe
Leaf extract 2g；Peony extract 5g, extract of cinnamomum cassia bark 3g, surplus are water.
Embodiment 5
The invention discloses a kind of acne-removing composition containing Chinese herbal medicine extract, every 100g includes following mass percents
Component, hamamelis extract 9g, Fourstamen Stephania Root root extract 28g, Cortex Phellodendri bark extract 18g；Purslane extract 5g；Chinese aloe leaf
Extracting solution 5g；Peony extract 5g, bisabolol 1.5g, extract of cinnamomum cassia bark 2g, surplus are water.
Embodiment 6
The invention discloses a kind of acne-removing composition containing Chinese herbal medicine extract, every 100g includes following mass percents
Component, hamamelis extract 10g, Fourstamen Stephania Root root extract 25g, Cortex Phellodendri bark extract 20g；Purslane extract 5g；Aloe
Leaf extract 2g；Peony extract 5g, bisabolol 2g, surplus are water.
Implement each extract described in 1 to 6 to be made by following methods respectively.
Cortex Phellodendri extract: taking 10g cork tree medicine materical crude slice, be placed in flask, and 75wt% ethanol solution 100g is added, and impregnates
After 0.5h, the refluxing extraction 1h under 80 DEG C of water bath conditions, extraction fluid, the dregs of a decoction continuously add 75wt% ethanol solution 100g,
The refluxing extraction 1h at 80 DEG C obtains secondary raffinate, merges two batches extracting solution.Cork tree extracting solution is carried out using Buchner funnel
Filtering, obtains clarified solution (Cortex Phellodendri extracting solution).By clarified solution, it is placed in 5 DEG C of standing 48h, up to cork tree after filtering precipitate
Bark extract.
Hazel extract: taking 10g witch hazel, be placed in flask, and water 100g is added, after impregnating 0.5h, in 60 DEG C of water-baths
Under the conditions of refluxing extraction 1h, extraction fluid, the dregs of a decoction continuously add water 100g, and the refluxing extraction 1h at 60 DEG C obtains secondary mention
Liquid is taken, two batches extracting solution is merged.Hazel extract is filtered using Buchner funnel, obtains clarified solution.By clarified solution, set
Up to hamamelis extract after 5 DEG C of standing 48h, filtering precipitate.
Extract solution from aloe: taking fresh aloe, chopping, in the cloth bag after setting cleaning-sterilizing, squeezes out aloe juice, and with 80
The filtering of mesh nylon gauze, obtains Aloe original juice, i.e. extract solution from aloe.
Purslane extract: taking 10g purslane medicine materical crude slice, be placed in flask, and 60wt% ethanol solution 100g is added, and impregnates
After 0.5h, the refluxing extraction 1h under 70 DEG C of water bath conditions, extraction fluid, the dregs of a decoction continuously add 60wt% ethanol solution 100g,
The refluxing extraction 1h at 70 DEG C obtains secondary raffinate, merges two batches extracting solution.Using Buchner funnel to Purslane extract into
Row filtering, obtains clarified solution (Purslane extract).
Fourstamen Stephania Root root: taking 10g Fourstamen Stephania Root root medicine materical crude slice, be placed in flask, and 70wt% ethanol solution 100g is added, and impregnates 0.5h
Afterwards, the refluxing extraction 1h under 80 DEG C of water bath conditions, extraction fluid, the dregs of a decoction continuously add 70wt% ethanol solution 100g, in 80
Refluxing extraction 1h at DEG C obtains secondary raffinate, merges two batches extracting solution.Fourstamen Stephania Root extracting solution was carried out using Buchner funnel
Filter, obtains clarified solution.By clarified solution, it is placed in 5 DEG C of standing 48h, up to Fourstamen Stephania Root root extract after filtering precipitate.
Peony extract: taking 10g Chinese herbaceous peony medicine materical crude slice, be placed in flask, and 70wt% ethanol solution 100g is added, and impregnates 0.5h
Afterwards, the refluxing extraction 1h under 80 DEG C of water bath conditions, extraction fluid, the dregs of a decoction continuously add 70wt% ethanol solution 100g, in 80
Refluxing extraction 1h at DEG C obtains secondary raffinate, merges two batches extracting solution.Chinese herbaceous peony extracting solution was carried out using Buchner funnel
Filter, obtains clarified solution.It by clarified solution, is placed in a vacuum drying oven, continues under conditions of 80 DEG C of temperature, vacuum degree -0.05MPa
Dry 48h, obtains desciccate, is crushed to get peony extract powder.
Extract of cinnamomum cassia bark: taking 10g cassia medicine materical crude slice, be placed in flask, and 70wt% ethanol solution 100g is added, and impregnates
After 0.5h, the refluxing extraction 1h under 80 DEG C of water bath conditions, extraction fluid, the dregs of a decoction continuously add 70wt% ethanol solution 100g,
The refluxing extraction 1h at 80 DEG C obtains secondary raffinate, merges two batches extracting solution.Using Buchner funnel to cassia extracting solution into
Row filtering, obtains clarified solution.By clarified solution, it is placed in 5 DEG C of standing 48h, up to extract of cinnamomum cassia bark after filtering precipitate.
Prepare the upper acne-removing composition containing Chinese herbal medicine extract in embodiment 1 to 6 the preparation method comprises the following steps: 1) by embodiment 1
Each component is weighed to any one group of mass number in 6；2) the weighed component of step 1) is uniformly mixed to obtain the final product.
For the acne-removing for verifying effect combination, a series of experiments test is carried out, 1, security test is specifically included that, examines
(potential) irritation and allergic reaction for examining composition may；2, composition restraining and sterilizing bacteria ability is investigated in both effectiveness test.
1, security test structure such as table 1.
Table 1
| Sample ID | IC50μg/ml | LD50mg/kg | Classification | Explanation |
| Acne-removing composition -1 | 241.85 | 814.1026 | Level Four | Swallow harmful (oral) |
| Acne-removing composition -2 | 242.35 | 814.1726 | Level Four | Swallow harmful (oral) |
| Acne-removing composition -3 | 241.30 | 813.0926 | Level Four | Swallow harmful (oral) |
| Acne-removing composition -4 | 240.70 | 813.1027 | Level Four | Swallow harmful (oral) |
| Acne-removing composition -5 | 241.05 | 812.1526 | Level Four | Swallow harmful (oral) |
| Acne-removing composition -6 | 240.90 | 811.0946 | Level Four | Swallow harmful (oral) |
2, efficacy test
Propionibacterium acnes (ATCC11827) plate is prepared using double-layer agar technique, plate bacteria containing amount is 104~105CFU/
Plate accurately weighs 0.5g sample, is uniformly applied on plate containing bacterium with aseptic cotton carrier, cultivates 24 under 36 ± 1 DEG C of anaerobic conditions
Hour, then observe bacterium colony growth result in plate.
Result judgement
1) have no that bacterium colony grows (showing that sample is stronger to the inhibitory effect of propionibacterium acnes, sample anti-acne effect is good)；
2) part bacterium colony growth (shows that sample has certain inhibitory effect, sample anti-acne effect to propionibacterium acnes
In)；
3) bacterium colony grows (show sample to propionibacterium acnes unrestraint effect, sample does not have anti-acne effect) completely.
Test result shows that the safety of acne-removing composition, which has, to be guaranteed, human body will not be had by being added in cosmetics
Evil consequence.
2, efficacy test structure such as table 2:
Table 2
Efficacy test is the results show that acne-removing composition is conducive to the anti-acne of cosmetics with good antibacterial and anti-inflammatory effects
Effect is realized.To exclude influence of the preservative to fungistatic effect, preservative is not added in the sample for carrying out efficacy test.
It is tested in specifically used pure acne-removing composition test sample, the acne-removing composition concentration of practical cosmetics is lower than
5%, matrix and other components are added according to this field routine techniques.
Claims (2)
1. a kind of acne-removing composition containing Chinese herbal medicine extract, which is characterized in that the component including following mass percents, gold thread
Prunus mume extract 8-12%, Fourstamen Stephania Root root extract 25-35%, Cortex Phellodendri bark extract 16-24%；Purslane extract 4-6%；
Aloe leaf extract 1.5-2.5%；Peony extract 4-6%, extract of cinnamomum cassia bark 1-4%, bisabol 1-2%, surplus are water；
The Purslane extract is made by following step: being weighed purslane medicine materical crude slice, is placed in flask, is added 8-12 times
60wt% ethanol solution, after impregnating 0.3-0.8h, the refluxing extraction 0.8-1.2h under 65-75 DEG C of water bath condition, extraction fluid,
The dregs of a decoction continuously add 8-12 times of 60wt% ethanol solution, and refluxing extraction 0.8-1.2h, obtains secondary raffinate at 65-75 DEG C,
Merge extracting solution twice to filter, obtains Purslane extract；
The hamamelis extract is made by following step: being weighed witch hazel and is placed in flask, witch hazel weight 8- is added
12 times of water, impregnate 0.3-1h after, the refluxing extraction 0.8-1.2h under 55-65 DEG C of water bath condition, extraction fluid, the dregs of a decoction continue plus
Enter 8-12 times of water of water, the refluxing extraction 0.8-1.2h at 55-65 DEG C obtains secondary raffinate, merges extracting solution twice and filters, obtains
To clarified solution, it is placed in 5 DEG C of standing 48h, up to hamamelis extract after filtering precipitate；
The Fourstamen Stephania Root root extract is made by following step: being weighed Fourstamen Stephania Root root and is placed in flask, Fourstamen Stephania Root root is added
8-12 times of 70wt% ethanol solution of quality, after impregnating 0.3-1h, the refluxing extraction 0.8-1.2h under 75-85 DEG C of water bath condition, point
From extracting solution, the dregs of a decoction continuously add 8-12 times of 70wt% ethanol solution, and refluxing extraction 0.8-1.2h, obtains two at 75-85 DEG C
Secondary extracting solution merges extracting solution twice and filters, obtains clarified solution, be placed in 5 DEG C of standings 48h, Fourstamen Stephania Root to obtain the final product after filtering precipitate
Root extract；
The Cortex Phellodendri bark extract is made by following step: being weighed Cortex Phellodendri bark and is placed in flask, addition takes Chinese corktree
8-12 times of 70wt% ethanol solution of cortex amount, after impregnating 0.3-1h, the refluxing extraction 0.8-1.2h under 75-85 DEG C of water bath condition,
Extraction fluid, the dregs of a decoction continuously add 8-12 times of 70wt% ethanol solution, and refluxing extraction 0.8-1.2h, obtains at 75-85 DEG C
Secondary raffinate merges extracting solution twice and filters, obtains clarified solution, be placed in 5 DEG C of standings 48h, Cortex Phellodendri to obtain the final product after filtering precipitate
Bark extract；
The aloe leaf extract is made by following step: fresh aloe taken, is shredded, in the cloth bag after setting cleaning-sterilizing,
Aloe juice is squeezed out, and is filtered with 80 mesh nylon gauzes, extract solution from aloe is obtained；
The extract of cinnamomum cassia bark is to weigh cassia to be placed in flask, and addition takes 8-12 times of 70wt% ethyl alcohol of cassia quality
Solution, after impregnating 0.3-1h, refluxing extraction 0.8-1.2h, extraction fluid, the dregs of a decoction are continuously added under 75-85 DEG C of water bath condition
8-12 times of 70wt% ethanol solution, the refluxing extraction 0.8-1.2h at 75-85 DEG C obtain secondary raffinate, and merging is extracted twice
Liquid filtering, obtains clarified solution, is placed in 5 DEG C of standings 48h, extract of cinnamomum cassia bark to obtain the final product after filtering precipitate.
2. the method for preparing the acne-removing composition containing Chinese herbal medicine extract described in claim 1, which is characterized in that under successively including
State step:
1) mass percent according to claim 1 weighs each component；
2) the weighed component of step 1) is uniformly mixed to obtain the final product.
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