CN105106099A - Acne-removing bamboo charcoal mask containing plant compound preservative - Google Patents
Acne-removing bamboo charcoal mask containing plant compound preservative Download PDFInfo
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
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- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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Abstract
The invention discloses an acne-removing bamboo charcoal mask containing a plant compound preservative. The mask comprises components in parts by weight as follows: 15-25 parts of nano modified bamboo charcoal powder, 20-35 parts of an acne-removing active ingredient, 5-10 parts of tea juice, 1-3 parts of EDTA-2Na, 0.1-0.5 parts of the plant compound preservative and 30-60 parts of deionized water, wherein the plant compound preservative comprises components in parts by weight as follows: 1-20 parts of a plant root extract, 1-20 parts of a plant flower extract, 10-30 parts of a plant leaf extract and 1-10 parts of a plant bark extract. The acne-removing bamboo charcoal mask containing the plant compound preservative can reduce oil secretion and absorb skin oil, has good effects of removing acne, removing scars and promoting skin repair, and is obvious in effect; meanwhile, the added plant compound preservative can effectively inhibit growth of microorganisms such as bacteria, fungi and the like in skin-care products, can prolong service lives of the skin care products and has the advantages that the preservative is non-toxic, non-irritating, capable of avoiding skin allergies and the like.
Description
Technical field
The present invention relates to household chemicals field, particularly a kind of anti-acne bamboo charcoal mask with plant Compositional antiseptic agent.
Background technology
For acne skin that is neutral and oiliness, the secretion of its skin oil and fat is vigorous, easily causes oils and fats to pile up at forehead, wing of nose place, and many corse sweat pore, and skin is thick firmly rough.The oils and fats of too much secretion easily causes the blocking of pore, the growing of blackhead and small pox, and at present, a lot of anti-acne (acne of dispelling) product uses hormone, antibiotic, retinoic acid, the compositions such as fruit acid, zest is large, and easily cause skin to the drug resistance of Propiobacterium, safety is constantly under suspicion.Such as, often be used as acne, itch-stopping bactericidal, the cuticular salicylic acid of softening skin just can not consumption more than 0.5%, and uses rear xerosis cutis, can produce tight sense, and in existing natural composition product for resolving poxes, often just single selection natural extract carrys out anti-inflammation and sterilization, does not solve problem for the antibacterial of caused acne, so the speed that takes effect is not often very fast.Little to skin irritation, gentle, effective product for resolving poxes, has become the primary selection of nowadays acne skin fast, particularly along with people's living standard improves constantly, also more and more higher to requirement that is healthy and environmental protection.And the bamboo charcoal mask of anti-acne effect receives the concern of consumer, but its effect is relatively limited, and the cycle is longer, does not reach desirable control oil anti-acne effect to comparatively serious acne (small pox) at all.And what current most of anti-acne skin care item company used is all chemosynthesis antiseptic, and chemosynthesis antiseptic all exists zest is large, toxicity is large defect, safety aspect is not very satisfactory.
Summary of the invention
The invention provides a kind of anti-acne bamboo charcoal mask with plant Compositional antiseptic agent, it can reduce fat secretion, absorb skin oil and fat, and has good anti-acne, scar eliminating and promote skin repair effect, successful; Meanwhile, the plant Compositional antiseptic agent added effectively can suppress the microbial growth such as antibacterial, fungus in skin care item, extends skin care item useful lifes, and have nontoxic, non-stimulated, without advantages such as skin allergy.
The present invention is achieved in that a kind of anti-acne bamboo charcoal mask with plant Compositional antiseptic agent, is made up of the following each component with weight portion: 15 ~ 25 parts, nano modified bamboo charcoal powder, anti-acne active component 20 ~ 35 parts, 5 ~ 10 parts, tea juice, EDTA-2Na1 ~ 3 part, plant Compositional antiseptic agent 0.1 ~ 0.5 part, deionized water 30 ~ 60 parts, wherein, described anti-acne active component is made up of the following each component with weight portion: 5 ~ 10 parts, oil suction powder, fresh aloe juice 75 ~ 85 parts, Lac regis apis extract 3 ~ 8 parts, Radix Salviae Miltiorrhizae extract 2 ~ 10 parts, Radix Glycyrrhizae extract 1 ~ 5 part, sugared Thallus Laminariae (Thallus Eckloniae) extract 1 ~ 5 part, flower of Fructus Mali pumilae extract 1 ~ 5 part, allantoin 1 ~ 5 part, described plant Compositional antiseptic agent is made up of the following each component with weight portion: plant roots extract 1 ~ 20 part, Plant flawer extracts 1 ~ 20 part, leaves of plants extract 10 ~ 30 parts and plant peel extract 1 ~ 10 part, described plant roots extract is by Radix Scutellariae 1 ~ 5 part, Radix Sophorae Flavescentis 0.1 ~ 1 part, 0.1 ~ 1 part, moss, Herba Houttuyniae 1 ~ 5 part and Radix Paeoniae 1 ~ 5 part of mixed extraction obtain, described Plant flawer extracts is by Flos Inulae 5 ~ 10 parts, Flos Hibisci Mutabilis 1 ~ 10 part and Flos Lonicerae 1 ~ 10 part of mixed extraction obtain, described leaves of plants extract is by 1 ~ 10 part, Folium Nelumbinis, Folium Ginkgo 5 ~ 10 parts, leaf of Herba Rosmarini Officinalis 2 ~ 5 parts, 1 ~ 5 part, Folium olive and Folium Perillae 5 ~ 10 parts of mixed extraction obtain, described plant peel extract is obtained by pomelo peel 5 ~ 10 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 1 ~ 5 part of mixed extraction.
Peony Root contains peoniflorin, benzoic acid isoreactivity composition, and peoniflorin has blood vessel dilating, comparatively broad-spectrum antiseptic and antiinflammation, and benzoic acid has antibacterial, antioxidative effect, and can also have certain therapeutical effect to mottle by blood circulation promoting and blood stasis dispelling, has white-skinned face function; In scutellariae,radix, main active has baicalin and baicalin, and wherein baicalin and baicalin etc. have stronger inhibitory action to pathogen such as staphylococcus aureus, Staphylococcus albus, bacillus subtilis, escherichia coli; Radix Sophorae Flavescentis contains number of chemical composition and has biological activity widely, based on antibacterial, arrhythmia, it all has significant inhibitory action to dysentery bacterium, gold-coloured staphylococci, dimension Hakuri Salmonella, also has inhibitory action in various degree to ten various skin funguses such as a beautiful gem color trichophytons; The effective ingredient decanoylacetaldehyde etc. of Herba Houttuyniae has bacteriostasis, and houttuynine sodium bisulfite, to micrococcus catarrhalis, staphylococcus aureus, hemophilus influenza, streptococcus pneumoniae and Hemolytic streptococcus etc., has obvious inhibitory action; To escherichia coli, dysentery bacterium, bacillus pyocyaneus, Bacillus proteus, diphtheria corynebacterium and mycobacteria, there is certain inhibitory action; To Bacillus typhi and leptospira, also there is stronger inhibitory action; Flos Inulae has antibacterial, antiinflammation, particularly better to staphylococcus, streptococcus effect; Containing the Flavonoid substances such as the organic acid such as chlorogenic acid, isochlorogenic acid and luteolin, luteolin-7-O-α-D glucoside, luteolin-7-O-β-D galactoside, quercetin-3-O-β-D glucoside in Flos Lonicerae, these active substances have very strong anti-inflammation effect and antioxidation; Containing phenols and tannin isoreactivity composition in leaf of Herba Rosmarini Officinalis, there is broad-spectrum antibacterial effect; Flos Hibisci Mutabilis, except having antibacterial effect, also has white-skinned face function; Containing alkaloids such as nuciferine, N-nornuciferine, the nor-nuciferine of O-, reticulines in Folium Nelumbinis, they have strong antimitotic effect, thus have stronger bacteriostasis; Containing flavone, lactone and ginkgoic acid in Folium Ginkgo, wherein ginkgoic acid is 6-alkyl or the salicylic derivant of 6-thiazolinyl, multiple fungus and bacterium can be suppressed, better to the inhibition of the anaerobe such as Streptococcus mutans, also there is the activity suppressing hyaluronidase and tryrosinase simultaneously, have effect of skin whitening, meanwhile, Folium Ginkgo also has good anti-oxidation efficacy; Folium olive, except having antibacterial effect, also has very strong free radical resisting effect; Containing physiologically active ingredients such as alkaloids, flavonoid, terpenoid in pomelo peel, wherein, flavone compound has the effects such as antioxidation, antiallergic, anti-inflammation, slow down aging.Pomelo peel has obvious inhibition to E.coli and yeast; The main active of Cortex cinnamomi japonici (Ramulus Cinnamomi) has cinnamic aldehyde, and it is antifungal active substance, mainly by destroying fungal cell wall, making medicine infiltrate in fungal cell, destroys organelle and play bacteriostasis.
The present invention has following beneficial effect: bamboo charcoal face pack of the present invention realizes continuing control oil and acne-removing, fat secretion can be reduced, absorb skin oil and fat, and there is good anti-acne, scar eliminating and promote skin repair effect, the abilities such as anti-acne effect are higher than commercially available prod; Screen the pure natural plants such as the root of various plants, flower, leaf and skin, and extract its active component and make natural, green plant Compositional antiseptic agent, this antiseptic effectively can suppress the microbial growth such as middle antibacterial, fungus in skin care item, antiseptic effect is close to chemical preservative, but the defect that the zest overcoming chemical preservative is large, toxicity is large, nontoxic to human-body safety, also there is the advantages such as antioxidation, whitening and antiinflammatory.And scientific formulation of the present invention, dosage is applicable to, cheap, and curative effect is rapidly, significantly.
Detailed description of the invention
Below in conjunction with embodiment, the present invention will be described in detail, and embodiment is only the preferred embodiment of the present invention, is not limitation of the invention.
Plant roots extract is obtained by following methods: finishing collecting Radix Scutellariae, Radix Sophorae Flavescentis, moss, Herba Houttuyniae and Radix Paeoniae are positioned in pulverizer cylinder body, add the ethanol mixing that concentration is 64%, liquid material mass ratio is 25:1, soak 3h, historrhexis is carried out 4 times with the rotating speed of 10000r/min, each 8 minutes, then leave standstill 3 hours, obtain mixed liquor; Then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; With membrane filtration, obtain preliminary filtrate; Concentrate with reverse osmosis membrane at normal temperatures, obtain the first concentrated solution of solid contents 15%; Get the vacuum concentration that half first concentrated solution carries out at 35 DEG C, obtain the second concentrated solution of solid content 35%; By dry after the first remaining concentrated solution and the mixing of the second concentrated solution, to obtain final product.
Plant flawer extracts is obtained by following methods: finishing collecting Flos Hibisci Mutabilis, Flos Inulae and Flos Lonicerae are positioned in pulverizer cylinder body, add the ethanol mixing that concentration is 52%, liquid material mass ratio is 12:1, soak 3h, historrhexis is carried out 2 times with the rotating speed of 5000r/min, each 5 minutes, then leave standstill 3 hours, obtain mixed liquor; Then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; With membrane filtration, obtain preliminary filtrate; Concentrate with reverse osmosis membrane at normal temperatures, obtain the first concentrated solution of solid contents 5%; Get the vacuum concentration that half first concentrated solution carries out at 35 DEG C, obtain the second concentrated solution of solid content 15%; By dry after the first remaining concentrated solution and the mixing of the second concentrated solution, to obtain final product.
Leaves of plants extract is obtained by following methods: finishing collecting Folium Nelumbinis, Folium Ginkgo, leaf of Herba Rosmarini Officinalis, Folium olive and Folium Perillae are positioned in pulverizer cylinder body, add the ethanol mixing that concentration is 58%, liquid material mass ratio is 20:1, soak 3h, historrhexis is carried out 3 times with the rotating speed of 8000r/min, each 8 minutes, then leave standstill 3 hours, obtain mixed liquor; Then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; With membrane filtration, obtain preliminary filtrate; Concentrate with reverse osmosis membrane at normal temperatures, obtain the first concentrated solution of solid contents 15%; Get the vacuum concentration that half first concentrated solution carries out at 35 DEG C, obtain the second concentrated solution of solid content 28%; By dry after the first remaining concentrated solution and the mixing of the second concentrated solution, to obtain final product.
Plant peel extract is obtained by following methods: finishing collecting pomelo peel and Cortex cinnamomi japonici (Ramulus Cinnamomi) are positioned in pulverizer cylinder body, add the ethanol mixing that concentration is 55%, liquid material mass ratio is 10:1, soak 3h, historrhexis is carried out 3 times with the rotating speed of 5000r/min, each 8 minutes, then leave standstill 3 hours, obtain mixed liquor; Then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; With membrane filtration, obtain preliminary filtrate; Concentrate with reverse osmosis membrane at normal temperatures, obtain the first concentrated solution of solid contents 8%; Get the vacuum concentration that half first concentrated solution carries out at 35 DEG C, obtain the second concentrated solution of solid content 20%; By dry after the first remaining concentrated solution and the mixing of the second concentrated solution, to obtain final product.
Fresh aloe juice is obtained by following methods: select organic Aloe Barbadensis Miller fresh leaf (fresh leaf of U.S.'s Curacao, trophophase more than 2 years, pollution-free disease-free) as raw material, after cleaning, sterilizing, remove end to end, trimming peeling, grind process, one-step method process that the Aloe gel after grinding is taked " stabilisation and sterilizing ", then be cooled to less than 40 DEG C rapidly with liquid nitrogen, then be aseptically separated by gravy, obtain the fresh juice of organic aloe.Wherein stabilisation sterilization treatment refers to by adding 0.23% citric acid and 0.085%EDTA-2Na in the Aloe gel after grinding respectively as acidulant, chelating agen, by heat treatment (85 DEG C), passivation is carried out to the enzyme in Aloe gel, to realize Aloe gel stabilisation sterilization treatment.In addition, in processing procedure, any enzyme should not be added.
It is a kind of ω-hydroxy acid be present in nature Lac regis apis that Lac regis apis extract contains 10-hydroxydecanoic acid, decanedioic acid, decanediol and 10-HDA, 10-HDA, and the Lac regis apis extract in the present invention is the AcnacidolBG purchased from ISP company.
Radix Salviae Miltiorrhizae extract is obtained by following methods: get salvia piece, adds 10 times of water gagings of Radix Salviae Miltiorrhizae dry weight, under reduced pressure, 75 DEG C of extractions 3 times of seething with excitement, each 2.5h, merge extractive liquid, filter, less than 60 DEG C concentrating under reduced pressure, are concentrated into the clear paste that relative density is 1.2, clear paste is 190 DEG C in spray dryer inlet temperature, and outlet temperature is 80 DEG C, under moisture less than 8% condition, carry out spraying dry, the granule that spraying dry obtains is pulverized, and crosses 80 mesh sieves, obtains Radix Salviae Miltiorrhizae extract.Radix Salviae Miltiorrhizae extract has the functions such as promoting blood flow to regulate menstruation, promoting tissue regeneration by removing blood stasis, tranquillizing and allaying excitement, removing heat from blood eliminating carbuncle, reducing swelling and alleviating pain.In Radix Salviae Miltiorrhizae, active component TANSHINONES has antibacterial action, extremely sensitive to Propiobacterium, and be a kind of estrogen-like product of mitigation, play anti-androgen effect, also there is the antiinflammatory action of similar hydrocortisone simultaneously, strong to gram-positive bacteria antibacterial action, obviously can reduce propionibacterium acnes counting, and can suppress acute and react with subacute inflammation, there is antiinflammatory action.Still have gentle estrogenic activity and anti-in acid andrusol effect, anti-androgenic effect and the effect of anti-sebum glandular secretion definite.Gonadal hormone especially androgen has close relationship with the generation of acne, development, persistent state.TANSHINONES avoids application estrin treatment acne usually, and the shortcoming of interference patient body intracellular metabolite, improves the clinical symptoms of acne from many aspects. and subject range is wider.In addition, the blood circulation promoting and blood stasis dispelling function that TANSHINONES has still raised path between farm fields improves the blood circulation of face, promotes the metabolism of affected skin.
Radix Glycyrrhizae extract is obtained by following methods: according to 1:5 weight ratio, drops into ethanol and carries out extracting, filtering, obtain extracting solution in Radix Glycyrrhizae; Extracting solution is concentrated, makes the concentration ratio of extracting solution simmer down to 30 Brix degree; Add distilled water according to the ratio of 1:2 in extracting solution after above-mentioned concentrating, the extracting solution after concentrated is washed; Extracting solution after washing carries out concentrating under reduced pressure again; Extracting solution after concentrated is carried out drying, obtains Radix Glycyrrhizae extract.Radix Glycyrrhizae has the anti-aging effect of whitening antiinflammatory.
Sugar Thallus Laminariae (Thallus Eckloniae) extract is brown algae extract; Preferably purchased from Féraud stamen gold and/or the Féraud stamen gold BG of MarineBiotech, France, can also be that the product being HG657 from the product designation of Ennagram, France company obtains.Sugar Thallus Laminariae (Thallus Eckloniae) extract can regulation of skin fat secretion well, significantly improves sebum overflow, suppresses the inflammation that lipolytic enzyme causes, rebuild skin physiology balance.
Flower of Fructus Mali pumilae extract is obtained by following methods: finishing collecting apple flower is positioned in pulverizer cylinder body, adds the ethanol mixing that concentration is 65%, carries out historrhexis 3 times, each 10 minutes, then leave standstill 3 hours, obtain mixed liquor with the rotating speed of 5000r/min; With membrane filtration, obtain feed liquid; Feed liquid is positioned in distillator and distills, obtain concentrate; Concentrate is placed in oil water separator and is separated, obtain flower of Fructus Mali pumilae extract.
Described oil suction powder is the mixture of starch ocentyl succinic aluminum, acrylic copolymer, magnesium carbonate composition, and wherein the part by weight of starch ocentyl succinic aluminum, acrylic copolymer, magnesium carbonate is 3:2:1.This oil suction powder is the modified starch of a oil absorption, and oil absorption is outstanding, energy deep layer cleaning skin, the oils and fats piled up in sucking-off pore and dirt.
Green tea tender shoots and green tea stalk that weight ratio is 2:5 is included in described tea juice.Described tea juice is obtained by following methods: first green tea tender shoots and green tea stalk are cleaned, pulverize, by weight ratio mixing green tea tender shoots and the green tea stalk of 2:5, add in deionized water and fully soak 5 hours, then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; Tentatively filtered by the secondary filter film of coarse filtration liquid containing polypropylene fibre membrane cartridge, the fine particle in removing coarse filtration liquid, obtains preliminary filtrate; Preliminary filtrate is carried out ultra-filtration filters, then ultrafiltration permeate reverse osmosis membrane (20 ~ 40 DEG C) is concentrated, obtain the first concentrated solution of solid contents 10%; The half of getting the first concentrated solution carries out vacuum concentration (40 ~ 45 DEG C), obtains the second concentrated solution that solid contents is 35%; The first remaining concentrated solution and the second concentrated solution are mixed to get tea juice.
Embodiment 1
A kind of anti-acne bamboo charcoal mask with plant Compositional antiseptic agent obtains by the following method:
By following portions by weight, plant roots extract, Plant flawer extracts, leaves of plants extract and plant peel extract Homogeneous phase mixing are obtained plant Compositional antiseptic agent.Described plant Compositional antiseptic agent is made up of the following each component with weight portion: plant roots extract 5 parts, Plant flawer extracts 15 parts, leaves of plants extract 15 parts and plant peel extract 10 parts, described plant roots extract is obtained by Radix Scutellariae 1 part, Radix Sophorae Flavescentis 0.1 part, 1 part, moss, Herba Houttuyniae 3 parts and Radix Paeoniae 5 parts of mixed extraction, described Plant flawer extracts is obtained by Flos Inulae 5 parts, Flos Hibisci Mutabilis 10 parts and Flos Lonicerae 1 part of mixed extraction, and described leaves of plants extract is obtained by 1 part, Folium Nelumbinis, Folium Ginkgo 10 parts, 1 part, Folium olive, Folium Perillae 10 parts and leaf of Herba Rosmarini Officinalis 5 parts of mixed extraction; Described plant peel extract is obtained by pomelo peel 5 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 5 parts of mixed extraction.
10 parts, oil suction powder, fresh aloe juice 75 parts, Lac regis apis extract 8 parts, Radix Salviae Miltiorrhizae extract 10 parts, Radix Glycyrrhizae extract 5 parts, sugared Thallus Laminariae (Thallus Eckloniae) extract 1 part, flower of Fructus Mali pumilae extract 1 part, allantoin 5 parts of mix homogeneously are obtained anti-acne active component; Microwave vacuum process is carried out again by after 18 parts, nano modified bamboo charcoal powder, anti-acne active component 32 parts, 8 parts, tea juice, plant Compositional antiseptic agent 0.2 part, EDTA-2Na2 part, deionized water 40 parts mixing, then pour in facial film mould, cooling, prepares bamboo charcoal face pack finished product.
Embodiment 2
A kind of anti-acne bamboo charcoal mask with plant Compositional antiseptic agent obtains by the following method:
By following portions by weight, plant roots extract, Plant flawer extracts, leaves of plants extract and plant peel extract Homogeneous phase mixing are obtained plant Compositional antiseptic agent.Described plant Compositional antiseptic agent is made up of the following each component with weight portion: plant roots extract 18 parts, Plant flawer extracts 10 parts, leaves of plants extract 10 parts and plant peel extract 6 parts, described plant roots extract is obtained by Radix Scutellariae 3 parts, Radix Sophorae Flavescentis 0.6 part, 0.1 part, moss, Herba Houttuyniae 5 parts and Radix Paeoniae 1 part of mixed extraction, described Plant flawer extracts is obtained by Flos Inulae 8 parts, Flos Hibisci Mutabilis 5 parts and Flos Lonicerae 10 parts of mixed extraction, and described leaves of plants extract is obtained by 7 parts, Folium Nelumbinis, Folium Ginkgo 8 parts, 5 parts, Folium olive, Folium Perillae 8 parts and leaf of Herba Rosmarini Officinalis 4 parts of mixed extraction; Described plant peel extract is obtained by pomelo peel 8 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 3 parts of mixed extraction.
8 parts, oil suction powder, fresh aloe juice 82 parts, Lac regis apis extract 5 parts, Radix Salviae Miltiorrhizae extract 8 parts, Radix Glycyrrhizae extract 3 parts, sugared Thallus Laminariae (Thallus Eckloniae) extract 2 parts, flower of Fructus Mali pumilae extract 1 part, allantoin 3 parts of mix homogeneously are obtained anti-acne active component; Microwave vacuum process is carried out again by after 18 parts, nano modified bamboo charcoal powder, anti-acne active component 32 parts, 8 parts, tea juice, plant Compositional antiseptic agent 0.3 part, EDTA-2Na2 part, deionized water 40 parts mixing, then pour in facial film mould, cooling, prepares bamboo charcoal face pack finished product.
Embodiment 3
A kind of anti-acne bamboo charcoal mask with plant Compositional antiseptic agent obtains by the following method:
By following portions by weight, plant roots extract, Plant flawer extracts, leaves of plants extract and plant peel extract Homogeneous phase mixing are obtained plant Compositional antiseptic agent.Described plant Compositional antiseptic agent is made up of the following each component with weight portion: plant roots extract 12 parts, Plant flawer extracts 6 parts, leaves of plants extract 25 parts and plant peel extract 2 parts, described plant roots extract is obtained by Radix Scutellariae 5 parts, Radix Sophorae Flavescentis 1 part, 0.5 part, moss, Herba Houttuyniae 1 part and Radix Paeoniae 2 parts of mixed extraction, described Plant flawer extracts is obtained by Flos Inulae 10 parts, Flos Hibisci Mutabilis 1 part and Flos Lonicerae 5 parts of mixed extraction, and described leaves of plants extract is obtained by 10 parts, Folium Nelumbinis, Folium Ginkgo 5 parts, 2 parts, Folium olive, Folium Perillae 5 parts and leaf of Herba Rosmarini Officinalis 2 parts of mixed extraction; Described plant peel extract is obtained by pomelo peel 10 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 1 part of mixed extraction.
6 parts, oil suction powder, fresh aloe juice 78 parts, Lac regis apis extract 7 parts, Radix Salviae Miltiorrhizae extract 4 parts, Radix Glycyrrhizae extract 5 parts, sugared Thallus Laminariae (Thallus Eckloniae) extract 1 part, flower of Fructus Mali pumilae extract 5 parts, allantoin 1 part of mix homogeneously are obtained anti-acne active component; Microwave vacuum process is carried out again by after 18 parts, nano modified bamboo charcoal powder, anti-acne active component 32 parts, 8 parts, tea juice, plant Compositional antiseptic agent 0.1 part, EDTA-2Na2 part, deionized water 40 parts mixing, then pour in facial film mould, cooling, prepares bamboo charcoal face pack finished product.
Embodiment 4
A kind of anti-acne bamboo charcoal mask with plant Compositional antiseptic agent obtains by the following method:
By following portions by weight, plant roots extract, Plant flawer extracts, leaves of plants extract and plant peel extract Homogeneous phase mixing are obtained plant Compositional antiseptic agent.Described plant Compositional antiseptic agent is made up of the following each component with weight portion: plant roots extract 18 parts, Plant flawer extracts 9 parts, leaves of plants extract 12 parts and plant peel extract 5 parts, described plant roots extract is obtained by Radix Scutellariae 2 parts, Radix Sophorae Flavescentis 0.5 part, 0.2 part, moss, Herba Houttuyniae 2 parts and Radix Paeoniae 4 parts of mixed extraction, described Plant flawer extracts is obtained by Flos Inulae 7 parts, Flos Hibisci Mutabilis 2 parts and Flos Lonicerae 5 parts of mixed extraction, and described leaves of plants extract is obtained by 8 parts, Folium Nelumbinis, Folium Ginkgo 5 parts, 2 parts, Folium olive, Folium Perillae 5 parts and leaf of Herba Rosmarini Officinalis 3 parts of mixed extraction; Described plant peel extract is obtained by pomelo peel 6 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 4 parts of mixed extraction.
5 parts, oil suction powder, fresh aloe juice 85 parts, Lac regis apis extract 3 parts, Radix Salviae Miltiorrhizae extract 2 parts, Radix Glycyrrhizae extract 1 part, sugared Thallus Laminariae (Thallus Eckloniae) extract 5 parts, flower of Fructus Mali pumilae extract 1 part, allantoin 5 parts of mix homogeneously are obtained anti-acne active component; Microwave vacuum process is carried out again by after 18 parts, nano modified bamboo charcoal powder, anti-acne active component 32 parts, 8 parts, tea juice, plant Compositional antiseptic agent 0.5 part, EDTA-2Na2 part, deionized water 40 parts mixing, then pour in facial film mould, cooling, prepares bamboo charcoal face pack finished product.
Comparative example 1
A kind of anti-acne bamboo charcoal mask with plant Compositional antiseptic agent obtains by the following method:
By following portions by weight, plant roots extract, Plant flawer extracts, leaves of plants extract and plant peel extract Homogeneous phase mixing are obtained plant Compositional antiseptic agent.Described plant Compositional antiseptic agent is made up of the following each component with weight portion: plant roots extract 12 parts, leaves of plants extract 25 parts, described plant roots extract is obtained by Radix Scutellariae 5 parts, Radix Sophorae Flavescentis 1 part, 0.5 part, moss, Herba Houttuyniae 1 part and Radix Paeoniae 2 parts of mixed extraction, and described leaves of plants extract is obtained by 10 parts, Folium Nelumbinis, Folium Ginkgo 5 parts, 2 parts, Folium olive, Folium Perillae 5 parts and leaf of Herba Rosmarini Officinalis 2 parts of mixed extraction.
Fresh aloe juice 85 parts, Lac regis apis extract 3 parts, Radix Salviae Miltiorrhizae extract 2 parts, Radix Glycyrrhizae extract 1 part, sugared Thallus Laminariae (Thallus Eckloniae) extract 5 parts, flower of Fructus Mali pumilae extract 1 part, allantoin 5 parts of mix homogeneously are obtained anti-acne active component; Microwave vacuum process is carried out again by after 18 parts, nano modified bamboo charcoal powder, anti-acne active component 32 parts, 8 parts, tea juice, plant Compositional antiseptic agent 0.2 part, EDTA-2Na2 part, deionized water 40 parts mixing, then pour in facial film mould, cooling, prepares bamboo charcoal face pack finished product.
Comparative example 2
A kind of anti-acne bamboo charcoal mask with plant Compositional antiseptic agent obtains by the following method:
By following portions by weight, plant roots extract, Plant flawer extracts, leaves of plants extract and plant peel extract Homogeneous phase mixing are obtained plant Compositional antiseptic agent.Described plant Compositional antiseptic agent is made up of the following each component with weight portion: described plant Compositional antiseptic agent is made up of the following each component with weight portion: Plant flawer extracts 15 parts and plant peel extract 10 parts, described Plant flawer extracts is obtained by Flos Inulae 5 parts, Flos Hibisci Mutabilis 10 parts and Flos Lonicerae 1 part of mixed extraction, and described plant peel extract is obtained by pomelo peel 5 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 5 parts of mixed extraction.
8 parts, oil suction powder, fresh aloe juice 85 parts, Lac regis apis extract 3 parts, Radix Salviae Miltiorrhizae extract 2 parts, Radix Glycyrrhizae extract 1 part, allantoin 5 parts of mix homogeneously are obtained anti-acne active component; Microwave vacuum process is carried out again by after 18 parts, nano modified bamboo charcoal powder, anti-acne active component 32 parts, 8 parts, tea juice, plant Compositional antiseptic agent 0.2 part, EDTA-2Na2 part, deionized water 40 parts mixing, then pour in facial film mould, cooling, prepares bamboo charcoal face pack finished product.
Comparative example 3
A kind of anti-acne bamboo charcoal mask with plant Compositional antiseptic agent obtains by the following method:
By following portions by weight, plant roots extract, Plant flawer extracts, leaves of plants extract and plant peel extract Homogeneous phase mixing are obtained plant Compositional antiseptic agent.Described plant Compositional antiseptic agent is made up of the following each component with weight portion: plant roots extract 18 parts and Plant flawer extracts 9 parts, described plant roots extract is obtained by Radix Scutellariae 2 parts, Radix Sophorae Flavescentis 0.5 part, 0.2 part, moss, Herba Houttuyniae 2 parts and Radix Paeoniae 4 parts of mixed extraction, and described Plant flawer extracts is obtained by Flos Inulae 7 parts, Flos Hibisci Mutabilis 2 parts and Flos Lonicerae 5 parts of mixed extraction.
Fresh aloe juice 85 parts, Radix Salviae Miltiorrhizae extract 2 parts, Radix Glycyrrhizae extract 1 part of mix homogeneously are obtained anti-acne active component; Microwave vacuum process is carried out again by after 18 parts, nano modified bamboo charcoal powder, anti-acne active component 32 parts, 8 parts, tea juice, plant Compositional antiseptic agent 0.2 part, EDTA-2Na2 part, deionized water 40 parts mixing, then pour in facial film mould, cooling, prepares bamboo charcoal face pack finished product.
It should be noted that the preparation method of the various embodiments described above and comparative example product is not limited to this, as long as bamboo charcoal face pack finished product can be made into according to described proportioning.
This bamboo charcoal face pack efficacy test:
1. tester's data: select all places of forehead, Face and cheek, mouth or cervical region to have comedo patient 160 example, each 80 examples of men and women, 16 ~ 40 years old age.Be divided into eight groups at random: embodiment 1,20 examples, each 10 examples of men and women, 26 years old age; Embodiment 2,20 examples, each 10 examples of men and women, 27 years old age; Embodiment 3,20 examples, each 10 examples of men and women, 26.5 years old age; Embodiment 4,20 examples, each 10 examples of men and women, 28 years old age; Comparative example 1,20 examples, each 10 examples of men and women, 26 years old age; Comparative example 2,20 examples, each 10 examples of men and women, 28.5 years old age; Comparative example 3,20 examples, each 10 examples of men and women, 28 years old age; Commercially available prod, 20 examples, each 10 examples of men and women, 27.3 years old age.
2. method of testing and effect standard
(1) with reference to " new Chinese medicine guideline of clinical investigations ", Evaluation of Synthetic Effect of Holistic calculates curative effect rate with the total mark of skin lesion degree, skin lesion distribution, symptom, sign.Skin lesion counting * 100% before curative effect=(before treatment the rear skin lesion counting of skin lesion counting-treatment)/treatment.Cure: skin lesion disappears more than 90%, only has a little pigmentation; Effective: skin lesion disappears 60% ~ 90%, and symptom alleviates; Effective: skin lesion disappears 20% ~ 60%, symptom is improved; Invalid: skin lesion disappears <20%, and clinical symptoms is not improved.Total effective rate=cure rate+obvious effective rate+effective percentage.Test result is in table 1.
(2) fat secretion reduction test: detect respectively with oils and fats measuring instrument and use before product and use product after 24 hours, skin surface fat content, the reduction of calculating skin surface fat content, average, test evaluation the results are shown in Table 1.
(3) lasting fat secretion reduction: use product 1 week continuously, with oils and fats measuring instrument detection of skin surface fat content, product of stopping using, after 28 days, then detection of skin surface fat content, calculate the lasting fat secretion reduction of skin, average, test evaluation the results are shown in Table 1.
(4) cure the time of acne: use product, see to look into and cure the time used, average, test evaluation the results are shown in Table 1.
The efficacy test result of table 1 embodiment of the present invention 1 ~ 4 and comparative example 1 ~ 3
Stability test: evaluate stability in each temperature observations stability over 1 month, concrete outcome is in table 2.
Stability under the different temperatures of table 2 embodiment of the present invention 1 ~ 4 and comparative example 1 ~ 3
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Comparative example 1 | Comparative example 2 | Comparative example 3 | |
| Room temperature | Stable | Stable | Stable | Stable | Stable | Stable | Stable |
| 4℃ | Stable | Stable | Stable | Stable | Stable | Stable | Stable |
| 37℃ | Stable | Stable | Stable | Stable | Stable | Stable | Stable |
| 45℃ | Stable | Stable | Stable | Stable | Stable | Stable | Stable |
| Circulation | Stable | Stable | Stable | Stable | Stable | Stable | Stable |
Zest is tested: a certain amount of different tested material is put into speckle examination device, spread on the Medial upper arm of experimenter's (selecting 20 ~ 40 years old N/R healthy men and women of skin as study subject), continue 48 hours; Zest is confirmed according to erythema degree and to the enquirement of experimenter.
Detailed method is as follows:
Smearing method: closedpatchtest(Medial upper arm);
Applying amount: 20ul ~ 30ul/chamber;
Smear number of times and time limit: stick 24 hours, observe 24 hours after sticking test.
Observing response: observe according to the term (terminology) of CTFA criterion after patch test 30 points and 24 hours, result is as follows:
The dermoreaction of embodiment 1 to 4 and comparative example 1 to 3 is small erythema, and adopt mixing methyl parahydroxybenzoate 0.2 part, nipasol 0.1 part and imidazolidinyl urea 0.1 part of dermoreaction as antiseptic to be that strong erythema is to edema, illustrate that this plant Compositional antiseptic agent is almost non-stimulated to skin, but methyl hydroxybenzoate, nipasol, stimulation confirmed as by the antiseptic of imidazolidinyl urea composition.
Microorganism level detects: undertaken canned by the skin care item dark brown vial that embodiment 1 to 4 and comparative example 1 to 3 obtain respectively, open wide bottle cap, under being placed in the environment of ambient temperature 40 DEG C, relative humidity 85%, continuous observation is also tested, and concrete outcome sees the following form 3; Test item, detection method and examination criteria carry out according to QB/T2872-2007.
The microorganism detection result of each embodiment of table 3 and comparative example
| Observe phenomena | |
| Embodiment 1 | No abnormality seen after 60 days, pure in smell |
| Embodiment 2 | No abnormality seen after 60 days, pure in smell |
| Embodiment 3 | No abnormality seen after 60 days, pure in smell |
| Embodiment 4 | No abnormality seen after 60 days, pure in smell |
| Comparative example 1 | After 45 days, occur mildew, microorganism exceeds standard, and distributes unhappy abnormal smells from the patient |
| Comparative example 2 | After 45 days, occur mildew, microorganism exceeds standard, and distributes unhappy abnormal smells from the patient |
| Comparative example 3 | After 45 days, occur mildew, microorganism exceeds standard, and distributes unhappy abnormal smells from the patient |
| Chemical preservative | No abnormality seen after 60 days, pure in smell |
| Do not add antiseptic | After 5 days, occur mildew, microorganism exceeds standard, and distributes unhappy abnormal smells from the patient |
The above embodiment only have expressed embodiments of the present invention; it describes comparatively concrete and detailed; but therefore can not be interpreted as the restriction to the scope of the claims of the present invention; in every case the technical scheme adopting the form of equivalent replacement or equivalent transformation to obtain, all should drop within protection scope of the present invention.
Claims (9)
1. there is an anti-acne bamboo charcoal mask for plant Compositional antiseptic agent, be made up of the following each component with weight portion: 15 ~ 25 parts, nano modified bamboo charcoal powder, anti-acne active component 20 ~ 35 parts, 5 ~ 10 parts, tea juice, EDTA-2Na1 ~ 3 part, plant Compositional antiseptic agent 0.1 ~ 0.5 part, deionized water 30 ~ 60 parts, wherein, described anti-acne active component is made up of the following each component with weight portion: 5 ~ 10 parts, oil suction powder, fresh aloe juice 75 ~ 85 parts, Lac regis apis extract 3 ~ 8 parts, Radix Salviae Miltiorrhizae extract 2 ~ 10 parts, Radix Glycyrrhizae extract 1 ~ 5 part, sugared Thallus Laminariae (Thallus Eckloniae) extract 1 ~ 5 part, flower of Fructus Mali pumilae extract 1 ~ 5 part, allantoin 1 ~ 5 part, described plant Compositional antiseptic agent is made up of the following each component with weight portion: plant roots extract 1 ~ 20 part, Plant flawer extracts 1 ~ 20 part, leaves of plants extract 10 ~ 30 parts and plant peel extract 1 ~ 10 part, described plant roots extract is by Radix Scutellariae 1 ~ 5 part, Radix Sophorae Flavescentis 0.1 ~ 1 part, 0.1 ~ 1 part, moss, Herba Houttuyniae 1 ~ 5 part and Radix Paeoniae 1 ~ 5 part of mixed extraction obtain, described Plant flawer extracts is by Flos Inulae 5 ~ 10 parts, Flos Hibisci Mutabilis 1 ~ 10 part and Flos Lonicerae 1 ~ 10 part of mixed extraction obtain, described leaves of plants extract is by 1 ~ 10 part, Folium Nelumbinis, Folium Ginkgo 5 ~ 10 parts, leaf of Herba Rosmarini Officinalis 2 ~ 5 parts, 1 ~ 5 part, Folium olive and Folium Perillae 5 ~ 10 parts of mixed extraction obtain, described plant peel extract is obtained by pomelo peel 5 ~ 10 parts, Cortex cinnamomi japonici (Ramulus Cinnamomi) 1 ~ 5 part of mixed extraction.
2. the anti-acne bamboo charcoal mask with plant Compositional antiseptic agent according to claim 1, it is characterized in that: described plant roots extract is obtained by following methods: finishing collecting Radix Scutellariae, Radix Sophorae Flavescentis, moss, Herba Houttuyniae and Radix Paeoniae are positioned in pulverizer cylinder body, add the ethanol mixing that concentration is 64%, liquid material mass ratio is 25:1, soak 3h, carry out historrhexis 4 times with the rotating speed of 10000r/min, each 8 minutes, then leave standstill 3 hours, obtain mixed liquor; Then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; With membrane filtration, obtain preliminary filtrate; Concentrate with reverse osmosis membrane at normal temperatures, obtain the first concentrated solution of solid contents 15%; Get the vacuum concentration that half first concentrated solution carries out at 35 DEG C, obtain the second concentrated solution of solid content 35%; By dry after the first remaining concentrated solution and the mixing of the second concentrated solution, to obtain final product;
Described Plant flawer extracts is obtained by following methods: finishing collecting Flos Hibisci Mutabilis, Flos Inulae and Flos Lonicerae are positioned in pulverizer cylinder body, add the ethanol mixing that concentration is 52%, liquid material mass ratio is 12:1, soak 3h, historrhexis is carried out 2 times with the rotating speed of 5000r/min, each 5 minutes, then leave standstill 3 hours, obtain mixed liquor; Then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; With membrane filtration, obtain preliminary filtrate; Concentrate with reverse osmosis membrane at normal temperatures, obtain the first concentrated solution of solid contents 5%; Get the vacuum concentration that half first concentrated solution carries out at 35 DEG C, obtain the second concentrated solution of solid content 15%; By dry after the first remaining concentrated solution and the mixing of the second concentrated solution, to obtain final product;
Described leaves of plants extract is obtained by following methods: finishing collecting Folium Nelumbinis, Folium Ginkgo, leaf of Herba Rosmarini Officinalis, Folium olive and Folium Perillae are positioned in pulverizer cylinder body, add the ethanol mixing that concentration is 58%, liquid material mass ratio is 20:1, soak 3h, historrhexis is carried out 3 times with the rotating speed of 8000r/min, each 8 minutes, then leave standstill 3 hours, obtain mixed liquor; Then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; With membrane filtration, obtain preliminary filtrate; Concentrate with reverse osmosis membrane at normal temperatures, obtain the first concentrated solution of solid contents 15%; Get the vacuum concentration that half first concentrated solution carries out at 35 DEG C, obtain the second concentrated solution of solid content 28%; By dry after the first remaining concentrated solution and the mixing of the second concentrated solution, to obtain final product;
Described plant peel extract is obtained by following methods: finishing collecting pomelo peel and Cortex cinnamomi japonici (Ramulus Cinnamomi) are positioned in pulverizer cylinder body, add the ethanol mixing that concentration is 55%, liquid material mass ratio is 10:1, soak 3h, historrhexis is carried out 3 times with the rotating speed of 5000r/min, each 8 minutes, then leave standstill 3 hours, obtain mixed liquor; Then pour in countercurrent extraction machine and extract, obtain coarse filtration liquid; With membrane filtration, obtain preliminary filtrate; Concentrate with reverse osmosis membrane at normal temperatures, obtain the first concentrated solution of solid contents 8%; Get the vacuum concentration that half first concentrated solution carries out at 35 DEG C, obtain the second concentrated solution of solid content 20%; By dry after the first remaining concentrated solution and the mixing of the second concentrated solution, to obtain final product.
3. the anti-acne bamboo charcoal mask with plant Compositional antiseptic agent according to claim 1, it is characterized in that: described fresh aloe juice is obtained by following methods: select organic Aloe Barbadensis Miller fresh leaf as raw material, after cleaning, sterilizing, remove end to end, trimming peeling, grind process, one-step method process that Aloe gel after grinding is taked " stabilisation and sterilizing ", be cooled to less than 40 DEG C rapidly with liquid nitrogen again, be then aseptically separated by gravy, obtain the fresh juice of organic aloe; Wherein stabilisation sterilization treatment refers to that interpolation 0.23% citric acid and 0.085%EDTA-2Na are respectively as acidulant, chelating agen, carry out passivation by heat treatment to the enzyme in Aloe gel, to realize Aloe gel stabilisation sterilization treatment.
4. the anti-acne bamboo charcoal mask with plant Compositional antiseptic agent according to claim 1, is characterized in that: described Lac regis apis extract is the AcnacidolBG purchased from ISP company.
5. the anti-acne bamboo charcoal mask with plant Compositional antiseptic agent according to claim 1, it is characterized in that: described Radix Salviae Miltiorrhizae extract is obtained by following methods: get salvia piece, add 10 times of water gagings of Radix Salviae Miltiorrhizae dry weight, under reduced pressure, 75 DEG C of extractions 3 times of seething with excitement, each 2.5h, merge extractive liquid, filter, less than 60 DEG C concentrating under reduced pressure, be concentrated into the clear paste that relative density is 1.2, clear paste is 190 DEG C in spray dryer inlet temperature, outlet temperature is 80 DEG C, under moisture less than 8% condition, carry out spraying dry, the granule that spraying dry obtains is pulverized, cross 80 mesh sieves, obtain Radix Salviae Miltiorrhizae extract.
6. the anti-acne bamboo charcoal mask with plant Compositional antiseptic agent according to claim 1, is characterized in that: described Radix Glycyrrhizae extract is obtained by following methods: according to 1:5 weight ratio, drops into ethanol and carries out extracting, filtering, obtain extracting solution in Radix Glycyrrhizae; Extracting solution is concentrated, makes the concentration ratio of extracting solution simmer down to 30 Brix degree; Add distilled water according to the ratio of 1:2 in extracting solution after above-mentioned concentrating, the extracting solution after concentrated is washed; Extracting solution after washing carries out concentrating under reduced pressure again; Extracting solution after concentrated is carried out drying, obtains Radix Glycyrrhizae extract.
7. the anti-acne bamboo charcoal mask with plant Compositional antiseptic agent according to claim 1, it is characterized in that: described sugared Thallus Laminariae (Thallus Eckloniae) extract is purchased from MarineBiotech, France Féraud stamen gold and/or Féraud stamen gold BG or from the product designation of Ennagram, France company be HG657 product obtain.
8. the anti-acne bamboo charcoal mask with plant Compositional antiseptic agent according to claim 1, it is characterized in that: described flower of Fructus Mali pumilae extract is obtained by following methods: finishing collecting apple flower is positioned in pulverizer cylinder body, add the ethanol mixing that concentration is 65%, historrhexis is carried out 3 times with the rotating speed of 5000r/min, each 10 minutes, then leave standstill 3 hours, obtain mixed liquor; With membrane filtration 3 times, obtain feed liquid; Feed liquid is positioned in distillator and distills, obtain concentrate; Concentrate is placed in oil water separator and is separated, obtain flower of Fructus Mali pumilae extract.
9. the anti-acne bamboo charcoal mask with plant Compositional antiseptic agent according to claim 1, it is characterized in that: described oil suction powder is the mixture of starch ocentyl succinic aluminum, acrylic copolymer, magnesium carbonate composition, and wherein the part by weight of starch ocentyl succinic aluminum, acrylic copolymer, magnesium carbonate is 3:2:1.
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| CN106619438A (en) * | 2016-11-17 | 2017-05-10 | 东莞波顿香料有限公司 | Plant-derived antibacterial agent and liquid soap and toothpaste with plant-derived antibacterial agent |
| CN107802565A (en) * | 2017-12-21 | 2018-03-16 | 李冬梅 | A kind of composite vegetables extractive and its application in cosmetics preservative |
| CN105326730B (en) * | 2015-12-16 | 2018-12-25 | 广州市中通生化制品有限公司 | A kind of acne-removing composition and preparation method thereof containing Chinese herbal medicine extract |
| CN109125133A (en) * | 2018-10-24 | 2019-01-04 | 西安惟颐生物科技有限公司 | Female chest maintains compound essential oil |
| CN110115695A (en) * | 2019-04-16 | 2019-08-13 | 欧智弘 | A kind of gel applying film containing carbon material |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109125133A (en) * | 2018-10-24 | 2019-01-04 | 西安惟颐生物科技有限公司 | Female chest maintains compound essential oil |
| CN110115695A (en) * | 2019-04-16 | 2019-08-13 | 欧智弘 | A kind of gel applying film containing carbon material |
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