CN105997793A - Mask and preparation method thereof - Google Patents
Mask and preparation method thereof Download PDFInfo
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- CN105997793A CN105997793A CN201610451632.9A CN201610451632A CN105997793A CN 105997793 A CN105997793 A CN 105997793A CN 201610451632 A CN201610451632 A CN 201610451632A CN 105997793 A CN105997793 A CN 105997793A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/981—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of mammals or bird
- A61K8/986—Milk; Derivatives thereof, e.g. butter
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention relates to the technical field of cosmetics, in particular to a mask and a preparation method thereof. The mask is prepared from, by weight, 15-50 parts of goat milk and 0.5-20 parts of lemon extracts. The preparation method of the mask includes the following steps that raw materials are preprocessed, goat milk whey essence is prepared and sterilization is conducted. Raw material components are reasonably matched, skin protecting effects of the components have a synergistic effect, no preservative is added in the raw materials, and the effect that the shelf life of goat milk reaches 60 days or longer is achieved. The mask is mild and free of irritation and harmful components. Lemons are used for removing water-insoluble casein in goat milk, no preservative is added in the whole processing process, pregnant women and people with sensitive skin can use the mask, the mask is safe and effective, and quality inspection meets national quality standards.
Description
Technical field
The present invention relates to cosmetic technical field, be specifically related to a kind of facial film and preparation method thereof.
Background technology
Facial film is a kind of cosmetics and skincare product spreading on face, and its principle is exactly to utilize to cover of short duration in face
Time, it is temporarily isolating the air in the external world, improves skin temperature, make skin pore expand, promote that sweat gland divides
Secreting and metabolism, make the oxygen content of skin increase, beneficially skin eliminating epidermis cell is metabolic
Product and the oil substances of accumulation, the moisture in facial film penetrates into the horny layer of epidermis, and skin becomes soft,
Skin light naturally is flexible.Facial film on existing market is of a great variety, and the facial film of its various functions is continuous
Occurring, but wherein most all contains synthetic material, with after skin can be made to feel various discomfort.
The especially preservative used in facial film, such as suffer from the patient of breast carcinoma during hydroxybenzoate makes women
Increasing, the preservative used in cosmetics cannot be by body metabolism simultaneously, so can be at the skin of human body
Upper accumulation.When running up to a certain amount, the aging of skin will be accelerated；On the other hand, preservative also can
Accelerate pigementation, make skin more and more obscure.Additionally preservative can cause skin abnormality hypertrophy, canceration；
Related Component generation chemical change under the irradiation of daylight, makes people produce photaesthesia, skin rubefaction, blackening,
Pain；Cause people's allergy, red, the symptom of oxygen occurs；Or cause the burn of skin.
It is applied to preservative common in facial film at present and includes phenoxyethanol, Methylisothiazolinone, benzene first
Acid formicester, ethyl hydroxybenzoate, propyl hydroxybenzoate, butyl hydroxybenzoate, iso-butyl p-hy-droxybenzoate etc., research display,
Methylparaben ester can go deep into skin, but human body cannot metabolism, can accumulation in human body.Should not
Long Term Contact.Methylparaben likely produces reaction with UVB ultraviolet on skin, and then
Increasing the risk of skin ageing, Long Term Contact can cause skin allergy, have carcinogenic risk, particularly increase
Women suffers from breast cancer and the risk of uterus carcinoma.
Simultaneously in cosmetic technical field, chemicals usually can be added, such as industrial alcohol, heavy metal,
Essence, benzoate, benzyl alcohol, simethicone, dimethylethanolamine, formaldehyde, hydroquinone, ten
Dialkyl group, mineral oil, oil, propylene glycol etc., wherein industrial alcohol may cause Systemic exposure skin
Scorching eczema and chemosensitivity；The skin irritation such as heavy metal such as aluminum, lead, hydrargyrum, arsenic, may result in A Erci
Alzheimer disease, lung disease and teratogenesis；Essence contains substantial amounts of noxious substance；Benzoate involves various
The health problem of various kinds, including carcinoma of testis, cell mutation, and other cancers；Benzyl alcohol is harmful to,
If eating, sucking or passing through skin absorption.Eyes, skin and respiratory system there is serious zest；
Simethicone is potentially carcinogenic and causes clogging of pores；Laboratory finds to cause animal tumor and gene to dash forward
Become；Dimethylethanolamine not yet has definite scientific data.Local Muscle paralysis, life-time service may be caused
Result is unknown；Formaldehyde is hidden in other compositions often, prohibits the use of in Sweden and Japan, mainly because of
Production by Bacteria acid cannot be suppressed for it, be potentially carcinogenic；Hydroquinone toxicity, zest, forbid in Europe,
Bleach can be made；Allergy and severe toxicity；Dodecyl is (such as sodium lauryl sulphate, any containing dodecane
The composition of base) it is carcinogen, it is irritating to the skin, wherein contains ammonium salt, it is possible to cause skin mutation,
Growth acne；And the skin that mineral oil covers is just as a plastics package；Interrupt the supply of skin oxygen, may
Cause the premature aging of skin；Oil expedites the emergence of acne, even xerosis cutis, respiratory tract toxin, may
Cause dizziness；Propylene glycol well-known " anti-freeze ", find at many skin nursing products.Easily
The solvent absorbed, causes contact dermatitis, skin allergy, acne and allergy.As can be seen here, for mesh
All kinds of chemical compositions in front cosmetics are relatively big to the hazardness of skin, for avoiding above-mentioned hazardness, existing
Having done substantial amounts of improvement project in technology, the most employing natural extract compositions replace chemical composition system
Standby facial film.
Wherein sheep milk is as natural component as the raw material of facial film, has the skin-protection and health-care work of looks improving and the skin nourishing
With, containing epithelial cell growth factor (EGF) (not containing in milk) in sheep milk, human body major part is thin
Born of the same parents are activated by it, drink sheep milk or wash one's face and wash one's hair epithelial cell top layer irriate, can Rapid-Repair aging,
Downright bad, the epithelial cell of abrasion, and promote that skin elasticity is formed, make skin-whitening, and recover normal raw
Reason function, prevents bacteria attack.Additionally superoxide dismutase (SOD) rich content in sheep milk, right
Human body has antiinflammatory, anti-aging effects.Therefore long-term drink or wash use, have looks improving and the skin nourishing and slow down aging it
Effect.But sheep milk is as preparing the raw material of facial film, in the case of without preservative, perishable and produce
Raw abnormal flavour, and flocky precipitate occurs, now when carrying out flush coat, stickiness is the best, is difficult to carry out flush coat
Process.In currently available technology, being added with the facial film of sheep milk, to there is the anticorrosion time short, places mutability for a long time
The shortcoming of matter, is sold to use from production, and its shelf-life has gone through half, as client needs for a long time
Go out to carry use, the most very inconvenient, it is impossible to ensure the quality of facial film.
As can be seen here, can be for deficiency of the prior art, it is provided that a kind of facial film and preparation method thereof,
Make its use natural extract composition to replace chemical composition to prepare facial film, and by add sheep milk improve
The whitening of facial film and moistness, this facial film is on the basis of being added with sheep milk simultaneously, has the anticorrosion time
Long, pro-skin sense is good, long-time placement does not produce the advantage of flocky precipitate, becomes those skilled in the art
Technical barrier urgently to be resolved hurrily.
Summary of the invention
The present invention is to solve above-mentioned technical problem, it is provided that a kind of facial film and preparation method thereof, in this facial film
Using sheep milk as raw material, and by the improvement of processing technique, it is to avoid the addition of preservative, and improve
Shelf lives.
In order to reach above-mentioned technique effect, the present invention includes techniques below scheme:
A kind of facial film, including the raw material components of following parts by weight: the sheep milk of 15～50 parts and 0.5～20 part
Citron extract.
Sheep milk in the application facial film can Rapid-Repair be aging, downright bad, the epithelial cell of abrasion, and promotes
Skin elasticity is formed, and makes skin-whitening, and recovers normal physiological function, prevents bacteria attack.Additionally sheep
In milk, superoxide dismutase (SOD) rich content, has antiinflammatory, anti-aging effects to human body.Fructus Citri Limoniae
Being the holy product of beauty treatment, the king of fruit, containing the limonene of volume, bitter principle, citric acid and vitamin in Fructus Citri Limoniae
The materials such as ABCDE, have allaying tiredness, improve muscular work ability and activating skin epidermis cell
Etc. multiple health care.Citric acid not only can prevent and eliminate pigment calmness in skin, and can be soft
Change the horny layer of skin, make skin become fair and clear glossy.In the facial film of the present invention, Fructus Citri Limoniae can be used simultaneously
In removing the most water soluble casein in the middle of sheep milk, leave the nutrition to skin beneficiating such as water miscible milk surum
Material, uses the compatibility of above-mentioned raw materials composition, makes whole processing technique all avoid the addition of preservative,
Using skinfeel more preferably, safety is higher.
Further, the raw material components of following parts by weight is also included: the macromolecule hyaluronic acid of 0.05～1 part,
The low molecule hyaluronic acid of 0.05～1 part, the amino acid humectant of 0.5～5 part, the glycerol of 1～20 part, 20～70
Distilled water, the Flos Rosae Rugosae extracting solution of 15～40 parts and the hydroxyethyl cellulose of 0.05～0.5 part of part.
The present invention passes through Proper Match above-mentioned raw materials composition, makes the facial film skin care ingredient compatibility of the application more
Rationally, skin effect is played synergism.
Further, also include that Chinese medicine extraction liquid, described Chinese medicine extraction liquid include the former of following parts by weight
Material component: the Radix Ophiopogonis of 20～50 parts, the Radix Glycyrrhizae of 1～10 part, the Radix Angelicae Dahuricae of 1～20 part, the ocean of 1～20 part are sweet
In the Herba Menthae of chrysanthemum, the Herba Portulacae of 5～25 parts, the Folium Artemisiae Argyi of 1～20 part, the Radix Codonopsis of 0.1～1 part and 0.1～1 part
One or more.
Radix Ophiopogonis can nourishing YIN and moistening the lung, reinforcing stomach reg fluid, Compendium of Materia Medica records it and has " U.S. color, happy skin "
Effect；Radix Glycyrrhizae can suppress melanin to be formed, and it has the tyrosinase inhibitory activity of brilliance, can prevent
Skin tanning, lines speckle and sunburn occur, there is whitening effect simultaneously, by Radix Ophiopogonis and light Radix Glycyrrhizae as
Monarch drug；The Radix Angelicae Dahuricae gets rid of illness the functions such as dehumidifying, evacuation of pus granulation promoting, promoting blood circulation and stopping pain；Flos Matricariae chamomillae, Herba Portulacae and Chinese mugwort
Leaf has antiallergic effect, by the Radix Angelicae Dahuricae, Flos Matricariae chamomillae, Herba Portulacae and Folium Artemisiae Argyi as ministerial drug；Radix Codonopsis benefiting qi and nourishing blood
For adjuvant drug；The pungent cool refreshment of Folium Menthae extract is for making medicine；Four medicines make a concerted effort have allaying tiredness, play YIN nourishing profit altogether
Skin, blood circulation promoting and enriching, the merit of convergence wrinkle removal.Those skilled in the art based on prior art according to cost and need
Many mentioned components are asked to screen.
Facial film of the present invention also can contain above-mentioned Chinese medicine extraction liquid, can further improve the beauty treatment of facial film of the present invention
Effect, and in the case of without preservative, the mentioned component compatibility of the present invention has antiseptic property
Good advantage.Further, also include tremella extract that parts by weight are 1～10 part, 5～40 parts
Tea tree ethereal oil, the Herba Lysimachiae foenum-graeci quintessence oil of 5～40 parts and the butanediol of 0.5～5 part.
Containing rich in protein vitamin etc. in Tremella, so tremella extract has moisturizing, anti-ageing wrinkle removing
And the effect of Firm, often apply and can also remove freckle, chloasma etc..Its main active is tremella polysaccharide,
There is graceful unique smooth skinfeel and efficient moisture-retention skin-protecting function, be therefore described as " plant hyalomitome
Acid ".
Tea tree ethereal oil has bactericidal antiphlogistic, convergence pore and the effect of anti-acne, and Herba Lysimachiae foenum-graeci quintessence oil has control oil
The effect of antiinflammatory, uses butanediol in above-mentioned each components compatibility simultaneously, adds the guarantor of facial film of the present invention
Moist, facial film is had certain bacteriostasis, extends the shelf-life of facial film of the present invention, simultaneously as molten
Agent uses, and is more suitable for above-mentioned each mating chemical composition, more comfortable during use, and safety is higher.
Effect of known facial film and the active component added have the biggest relation.The present invention passes through further
Compatibility above-mentioned raw materials composition, improves the activity of skin, while moisturizing, skin is produced white-skinned face function, its
Using effect is more excellent.
The preparation method of a kind of facial film, prepares facial film including using sheep milk and citron extract as raw material
Step.
Further, comprise the following steps:
Step one: pretreatment of raw material: take macromolecule hyaluronic acid, low molecule hyaluronic acid, amino acid humectant,
Glycerol, Flos Rosae Rugosae extracting solution and a part of distilled water are sufficiently stirred for dissolving transparent liquid；By Fructus Citri Limoniae through squeezing the juice
Process obtains citron extract；Pour into hydroxyethyl cellulose the residue distilled water boiled stirs and dissolve,
And pour in transparency liquid；
Step 2: prepare Goat milk essence: take the heated process of sheep milk, add citron extract,
Stir process makes the casein coagulation in sheep milk, through being filtrated to get Goat milk, by described Goat milk with
Transparency liquid mix homogeneously, obtains Goat milk essence；
Step 3: sterilizing: obtain facial film by after encapsulated for Goat milk essence, sterilizing.
Preparation method of the present invention is reasonable, and by above-mentioned preparation technology, it is to avoid use preservative, now
Facial film technique be the most all do anticorrosion, long-term use or improper use with various preservative can be right
Skin causes the symptom such as twinge and allergy, and the preparation method of facial film of the present invention can not use preservative
In the case of, make the fresh sheep milk facial film shelf-life reach more than 60 days.
Further, in described step 2, the temperature of the heated process of sheep milk is 90 DEG C；Described step
Three comprise the following steps: Goat milk elite liquid measure be filled in high temperature steaming sterilizing bag, use vacuum
Machine seals after draining the air in high temperature steaming sterilizing bag, puts into sealing complete high temperature steaming sterilizing bag
In high steam pot, steam 40～60min, take out after lowering the temperature and obtain facial film.
Further, being also added with Chinese medicine extract in the sheep milk after heated process, described Chinese medicine carries
The preparation method taking liquid comprises the following steps: take Radix Ophiopogonis, the Radix Angelicae Dahuricae, Radix Codonopsis, Herba Menthae, Radix Glycyrrhizae, Flos Matricariae chamomillae,
One or more in Herba Portulacae and Folium Artemisiae Argyi, boiling obtains Chinese medicine extraction liquid twice.
Further, the concrete steps of described boiling twice include: add 6～the water of 10 times for the first time
Decocting 1.5～3 hours, second time adds 6～the soak by water 1.5 of 10 times～3 hours；Merge twice decocting liquid,
Filtering, be concentrated into 0.2～2g medical material/mL, cold preservation stands 10～24 hours, filters, and add water adjustment filter
Liquid concentration is 0.2～2g medical material/mL, obtains Chinese medicine extraction liquid.
Further, the sheep milk after heated process has been also added with Tremella extract, tea tree ethereal oil, smoked
Clothing grass quintessence oil and butanediol.
Use technique scheme, including following beneficial effect: the present invention each material composition coupling is reasonable,
Make each composition skin-care effect produce in synergism, and the raw material of the application and be not added with any preservative, real
The shelf-life now allowing sheep milk facial film reaches the effect of more than 60 days.Facial film gentleness of the present invention without any stimulation,
Not having any oxious component, facial film of the present invention selects Fructus Citri Limoniae to remove the most water soluble cheese egg in the middle of sheep milk
In vain, whole processing technique all avoids the addition of preservative, and anemia of pregnant woman's sensitivity skin all can use, and safety has
Effect and quality inspection meet state quality standard.
Detailed description of the invention
Below by specific embodiment, the present invention is described in further detail.
Embodiment one: a kind of facial film, including the raw material components of following parts by weight: the sheep milk of 15 parts
With the citron extract of 20 parts.
Facial film quality testing experiment described in embodiment one:
Experimental technique:
Laboratory ambient temperature: 20～25 DEG C；The detection method of described total plate count is by " cosmetics are defended
Raw specification " (2007) inspection；The detection method that described fecal coliform falls is by " cosmetics health is advised
Model " (2007) inspection；The detection method of Pseudomonas aeruginosa presses " cosmetics health specification " (2007)
Inspection；The detection method of staphylococcus aureus is checked by " cosmetics health specification " (2007)；
Yeast and mold sum is checked by " cosmetics health specification " (2007)；Mercury content is by " changing
Cosmetic hygienic practice " (2007) inspection；Arsenic content presses " cosmetics health specification " (2007)
Inspection；Lead content is checked by " cosmetics health specification " (2007).Experimental result is shown in Table 1.
Table 1 facial film quality testing experimental data
| Inspection project | Assay |
| Colony counts | Less than 10CFU/g |
| Fecal coliform falls | Do not detect |
| Pseudomonas aeruginosa | Do not detect |
| Staphylococcus aureus | Do not detect |
| Yeast and mold sum | ＜ 10CFU/g |
| Hydrargyrum | Do not detect (＜ 0.01mg/Kg) |
| Arsenic | Do not detect (＜ 0.01mg/Kg) |
| Lead | 0.3mg/Kg |
From the data in table 1, it can be seen that the facial film of embodiment of the present invention offer is safe and effective and quality inspection meets state
Family's quality standard.
The material composition of the present invention uses citron extract and sheep milk compatibility to prepare facial film, to remove
The most water soluble casein in sheep milk, it is to avoid facial film of the present invention produces flocculent deposit when long-term placement
Thing, promotes facial film anti-corrosive properties of the present invention.When carrying out raw material screening, the present invention has carried out substantial amounts of
Screening experiment, such as, add the acid ingredients such as vinegar, remove the most water soluble casein in sheep milk,
But when its facial film obtained places more than 5 days at normal temperatures, i.e. generate flocky precipitate, and gas
Taste is pungent, and simultaneously from preservative in vinegar, Consumer's Experience is the best.Final screening obtains this
Bright optimization formula, by sheep milk and citron extract compatibility, effectively removes in sheep milk the most water soluble
Casein, taste milder, using effect is best.
Embodiment two: the preparation method of a kind of facial film, including using sheep milk and citron extract conduct
The step of facial film prepared by raw material.
Specifically may comprise steps of: Fructus Citri Limoniae obtains citron extract through process of squeezing the juice, and takes sheep milk
Heated process, adds citron extract, and stir process makes the casein coagulation in sheep milk, passes through
Filter obtains Goat milk, is mixed homogeneously with transparency liquid by described Goat milk, obtains facial film.This
The method preparing facial film described in invention is not limited to above-mentioned cited concrete grammar.
Embodiment three: a kind of facial film, including the raw material components of following parts by weight: the sheep milk of 50 parts,
The citron extract of 0.5 part, the macromolecule hyaluronic acid of 0.05 part, the low molecule hyaluronic acid of 1 part, 0.5
Part amino acid humectant, the glycerol of 20 parts, the distilled water of 20 parts, the Flos Rosae Rugosae extracting solution of 40 parts and
The hydroxyethyl cellulose of 0.05 part.
The preparation method of above-mentioned facial film, comprises the following steps:
Step one: pretreatment of raw material: take macromolecule hyaluronic acid, low molecule glass by above-mentioned parts by weight
Uric acid, amino acid humectant, glycerol, Flos Rosae Rugosae extracting solution and a part of distilled water are sufficiently stirred for dissolving
Transparent liquid；Take Fructus Citri Limoniae by above-mentioned parts by weight and obtain citron extract through process of squeezing the juice；By upper
State parts by weight to take hydroxyethyl cellulose and pour into the residue distilled water boiled stirs and dissolve, and pour into
In transparency liquid；
Step 2: prepare Goat milk essence: take the heated process of sheep milk by above-mentioned parts by weight,
Adding citron extract, stir process makes the casein coagulation in sheep milk, through being filtrated to get sheep milk breast
Clearly, described Goat milk is mixed homogeneously with transparency liquid, obtain Goat milk essence；
Step 3: sterilizing: obtain facial film by after encapsulated for Goat milk essence, sterilizing.
Facial film quality testing experiment described in embodiment three:
Experimental technique:
Laboratory ambient temperature: 20～25 DEG C；The detection method of described total plate count is by " cosmetics are defended
Raw specification " (2007) inspection；The detection method that described fecal coliform falls is by " cosmetics health is advised
Model " (2007) inspection；The detection method of Pseudomonas aeruginosa presses " cosmetics health specification " (2007)
Inspection；The detection method of staphylococcus aureus is checked by " cosmetics health specification " (2007)；
Yeast and mold sum is checked by " cosmetics health specification " (2007)；Mercury content is by " changing
Cosmetic hygienic practice " (2007) inspection；Arsenic content presses " cosmetics health specification " (2007)
Inspection；Lead content is checked by " cosmetics health specification " (2007).Experimental result is shown in Table 2.
Table 2 facial film quality testing experimental data
| Inspection project | Assay |
| Colony counts | Less than 10CFU/g |
| Fecal coliform falls | Do not detect |
| Pseudomonas aeruginosa | Do not detect |
| Staphylococcus aureus | Do not detect |
| Yeast and mold sum | ＜ 10CFU/g |
| Hydrargyrum | Do not detect (＜ 0.01mg/Kg) |
| Arsenic | Do not detect (＜ 0.01mg/Kg) |
| Lead | 0.3mg/Kg |
From the data in table 2, it can be seen that the facial film of embodiment of the present invention offer is safe and effective and quality inspection meets state
Family's quality standard.
Embodiment four: a kind of facial film, including the raw material components of following parts by weight: the sheep milk of 30 parts,
The citron extract of 5 parts, the macromolecule hyaluronic acid of 0.1 part, the low molecule hyaluronic acid of 0.8 part, 1 part
Amino acid humectant, the glycerol of 15 parts, the distilled water of 40 parts, the Flos Rosae Rugosae extracting solution of 30 parts, 0.1
The hydroxyethyl cellulose of part and the Chinese medicine extraction liquid of 30 parts.
Described Chinese medicine extraction liquid includes the raw material components of following parts by weight: the Radix Ophiopogonis extract of 20 parts,
The glabridin extract of 10 parts, the Radix Angelicae Dahuricae extracting solution of 1 part, the camomile extract of 20 parts, 5
Part Herba portulacae extract, the Folium Artemisiae Argyi extract of 20 parts, the Radix Codonopsis extracting solution of 0.1 part and 1 part thin
Lotus extract.
The preparation method of above-mentioned facial film, comprises the following steps:
Step one: pretreatment of raw material: by above-mentioned parts by weight ratio relation take macromolecule hyaluronic acid,
Low molecule hyaluronic acid, amino acid humectant, glycerol, Flos Rosae Rugosae extracting solution and a part of distilled water are abundant
The transparent liquid of stirring and dissolving；Take Fructus Citri Limoniae by above-mentioned parts by weight ratio relation to obtain through process of squeezing the juice
Citron extract；Take hydroxyethyl cellulose by above-mentioned parts by weight ratio relation and pour the residue boiled into
In distilled water, stirring is dissolved, and pours in transparency liquid；
Step 2: prepare Goat milk essence: take sheep milk warp by above-mentioned parts by weight ratio relation
90 DEG C of heat treated, add citron extract, add Chinese medicine extract simultaneously, and described Chinese medicine carries
The preparation method taking liquid comprises the following steps: by above-mentioned parts by weight ratio relation take Radix Ophiopogonis, the Radix Angelicae Dahuricae,
Radix Codonopsis, Herba Menthae, Radix Glycyrrhizae, Flos Matricariae chamomillae, Herba Portulacae and Folium Artemisiae Argyi, add the soak by water 1.5 of 6 times for the first time
Hour, second time adds the soak by water 3 hours of 10 times；Merge twice decocting liquid, filter, be concentrated into 0.2g
Medical material/mL, cold preservation stands 10 hours, filters, and the adjustment filter liquor concentration that adds water is 0.2g medical material/mL,
Obtain Chinese medicine extraction liquid；Stir process makes the casein coagulation in sheep milk, through being filtrated to get Goat milk,
Described Goat milk is mixed homogeneously with transparency liquid, obtains Goat milk essence；
Step 3: sterilizing: Goat milk elite liquid measure is filled in high temperature steaming sterilizing bag, adopts
Seal after draining the air in high temperature steaming sterilizing bag with vacuum machine, by high temperature steaming complete for sealing
Sterilizing bag is put in high steam pot, steams 40min, takes out and obtain facial film after lowering the temperature.
Embodiment five: a kind of facial film, including the raw material components of following parts by weight: the sheep milk of 30 parts,
The citron extract of 5 parts, the macromolecule hyaluronic acid of 0.8 part, the low molecule hyaluronic acid of 0.1 part, 3 parts
Amino acid humectant, the glycerol of 4 parts, the distilled water of 60 parts, the Flos Rosae Rugosae extracting solution of 20 parts, 0.3
The hydroxyethyl cellulose of part, the tremella extract of 1 part, the tea tree ethereal oil of 40 parts, the lavandula angustifolia of 5 parts
Quintessence oil, the butanediol of 5 parts, the tremella extract of 10 parts, the tea tree ethereal oil of 5 parts, 40 parts smoke
Clothing grass quintessence oil and the butanediol of 0.5 part.
The preparation method of above-mentioned facial film, comprises the following steps:
Step one: pretreatment of raw material: by above-mentioned parts by weight ratio relation take macromolecule hyaluronic acid,
Low molecule hyaluronic acid, amino acid humectant, glycerol, Flos Rosae Rugosae extracting solution and a part of distilled water are abundant
The transparent liquid of stirring and dissolving；Take Fructus Citri Limoniae by above-mentioned parts by weight ratio relation to obtain through process of squeezing the juice
Citron extract；Take hydroxyethyl cellulose by above-mentioned parts by weight ratio relation and pour the residue boiled into
In distilled water, stirring is dissolved, and pours in transparency liquid；
Step 2: prepare Goat milk essence: take sheep milk warp by above-mentioned parts by weight ratio relation
90 DEG C of heat treated, add citron extract, add the silver of above-mentioned parts by weight ratio relation simultaneously
Ear extract, tea tree ethereal oil, Herba Lysimachiae foenum-graeci quintessence oil and butanediol, stir process makes the cheese egg in sheep milk
White solidification, through being filtrated to get Goat milk, mixs homogeneously described Goat milk with transparency liquid,
Obtain Goat milk essence；
Step 3: sterilizing: Goat milk elite liquid measure is filled in high temperature steaming sterilizing bag, adopts
Seal after draining the air in high temperature steaming sterilizing bag with vacuum machine, by high temperature steaming complete for sealing
Sterilizing bag is put in high steam pot, steams 60min, takes out and obtain facial film after lowering the temperature.
Embodiment six: a kind of facial film, including the raw material components of following parts by weight: the sheep milk of 30 parts,
The citron extract of 5 parts, the macromolecule hyaluronic acid of 0.2 part, the low molecule hyaluronic acid of 0.2 part, 2 parts
Amino acid humectant, the glycerol of 5 parts, the distilled water of 30 parts, the Flos Rosae Rugosae extracting solution of 27.4 parts,
The hydroxyethyl cellulose of 0.2 part, the Chinese medicine extraction liquid of 15 parts, the Tremella of 10 parts, the Camellia sinensis essence of 5 parts
Oil, the Herba Lysimachiae foenum-graeci quintessence oil of 40 parts and the butanediol of 0.5 part.
Described Chinese medicine extraction liquid includes the raw material components of following parts by weight: Radix Ophiopogonis of 30 parts, 5 parts
Radix Glycyrrhizae, the Radix Angelicae Dahuricae of 10 parts, the Flos Matricariae chamomillae of 15 parts, the Herba Portulacae of 10 parts, the Folium Artemisiae Argyi of 5 parts and 0.5
The Radix Codonopsis of part and the Herba Menthae of 0.8 part.
The preparation method of above-mentioned facial film, comprises the following steps:
Step one: pretreatment of raw material: by above-mentioned parts by weight ratio relation take macromolecule hyaluronic acid,
Low molecule hyaluronic acid, amino acid humectant, glycerol, Flos Rosae Rugosae extracting solution and a part of distilled water are abundant
The transparent liquid of stirring and dissolving；Fructus Citri Limoniae is obtained citron extract through process of squeezing the juice；Ethoxy is fine
Dimension element is poured into stir in the residue distilled water boiled and is dissolved, and pours in transparency liquid；
Step 2: prepare Goat milk essence: take sheep milk warp by above-mentioned parts by weight ratio relation
90 DEG C of heat treated, add citron extract, add simultaneously Chinese medicine extract, Tremella extract,
Tea tree ethereal oil, Herba Lysimachiae foenum-graeci quintessence oil and butanediol, the preparation method of described Chinese medicine extraction liquid include with
Lower step: by above-mentioned parts by weight ratio relation take Radix Ophiopogonis, the Radix Angelicae Dahuricae, Radix Codonopsis, Herba Menthae, Radix Glycyrrhizae,
Flos Matricariae chamomillae, Herba Portulacae and Folium Artemisiae Argyi, add for the first time the soak by water 3 hours of 10 times, and second time adds 6 times
Soak by water 1.5 hours；Merging twice decocting liquid, filter, be concentrated into 2g medical material/mL, cold preservation stands
24 hours, filtering, the adjustment filter liquor concentration that adds water is 2g medical material/mL, obtains Chinese medicine extraction liquid；Stirring
Process the casein coagulation making in sheep milk, through being filtrated to get Goat milk, by described Goat milk with
Transparency liquid mix homogeneously, obtains Goat milk essence；
Step 3: sterilizing: Goat milk elite liquid measure is filled in high temperature steaming sterilizing bag, adopts
Seal after draining the air in high temperature steaming sterilizing bag with vacuum machine, by high temperature steaming complete for sealing
Sterilizing bag is put in high steam pot, steams 550min, takes out and obtain facial film after lowering the temperature.
Embodiment three to embodiment six using effect is tested:
Experimental technique: choose men and women totally 35 people and try out, skin type include mixed type skin,
Oiliness skin, dry skin, be randomly divided into 4 groups, often organize 10 people, smear every day once, often
Secondary 10 minutes, the most often organize the using effect of 10 people, sum up using effect contrast and experiment
It is shown in Table 3.
Table 3 embodiment three to embodiment six using effect contrast experiment
Reduce from the data in table 3, it can be seen that the embodiment of the present invention one to embodiment six is respectively provided with pore refining
Microgroove, the feature of bright color.But wherein embodiment six is most preferred embodiment, after it uses
Best results.
Embodiment seven: a kind of facial film, including the raw material components of following parts by weight: the sheep milk of 30 parts,
The citron extract of 5 parts, the macromolecule hyaluronic acid of 0.2 part, the low molecule hyaluronic acid of 0.2 part, 2 parts
Amino acid humectant, the glycerol of 5 parts, the distilled water of 30 parts, the Flos Rosae Rugosae extracting solution of 27.4 parts,
The hydroxyethyl cellulose of 0.2 part, the Chinese medicine extract of 5 parts, the Tremella of 2 parts, the tea tree ethereal oil of 8 parts,
The Herba Lysimachiae foenum-graeci quintessence oil of 12 parts and the butanediol of 2.5 parts.
Described Chinese medicine extraction liquid includes the raw material components of following parts by weight: Radix Ophiopogonis of 50 parts, 1 part
Radix Glycyrrhizae, the Radix Angelicae Dahuricae of 20 parts, the Folium Artemisiae Argyi of 1 part, the Radix Codonopsis of 1 part and the Herba Menthae of 0.1 part.
Radix Ophiopogonis can nourishing YIN and moistening the lung, reinforcing stomach reg fluid, Compendium of Materia Medica records it and has " U.S. color, happy flesh
Skin " effect；Radix Glycyrrhizae can suppress melanin to be formed, it have brilliance tyrosinase inhibitory activity,
Skin tanning can be prevented, lines speckle and sunburn occur, there is whitening effect, by Radix Ophiopogonis simultaneously
With light Radix Glycyrrhizae as monarch drug；The Radix Angelicae Dahuricae gets rid of illness the functions such as dehumidifying, evacuation of pus granulation promoting, promoting blood circulation and stopping pain；Chinese mugwort
Leaf has antiallergic effect, by the Radix Angelicae Dahuricae and Folium Artemisiae Argyi as ministerial drug；Radix Codonopsis benefiting qi and nourishing blood is adjuvant drug；Thin
The pungent cool refreshment of lotus extract is for making medicine；Four medicines make a concerted effort have allaying tiredness, play YIN nourishing skin moistening altogether, live
Blood is enriched blood, the merit of convergence wrinkle removal.
A kind of preparation method of above-mentioned facial film
Step one: pretreatment of raw material: by above-mentioned parts by weight ratio relation take macromolecule hyaluronic acid,
Low molecule hyaluronic acid, amino acid humectant, glycerol, Flos Rosae Rugosae extracting solution and a part of distilled water are abundant
The transparent liquid of stirring and dissolving；Fructus Citri Limoniae is obtained citron extract through process of squeezing the juice；Ethoxy is fine
Dimension element is poured into stir in the residue distilled water boiled and is dissolved, and pours in transparency liquid；
Step 2: prepare Goat milk essence: take sheep milk warp by above-mentioned parts by weight ratio relation
90 DEG C of heat treated, add citron extract, add simultaneously Chinese medicine extract, Tremella extract,
Tea tree ethereal oil, Herba Lysimachiae foenum-graeci quintessence oil and butanediol, the preparation method of described Chinese medicine extraction liquid include with
Lower step: by above-mentioned parts by weight ratio relation take Radix Ophiopogonis, the Radix Angelicae Dahuricae, Radix Codonopsis, Herba Menthae, Radix Glycyrrhizae and
Folium Artemisiae Argyi, adds for the first time the soak by water 2.5 hours of 8 times, and second time adds the soak by water 2 hours of 7 times；
Merging twice decocting liquid, filter, be concentrated into 1.5g medical material/mL, cold preservation stands 15 hours, filters,
The adjustment filter liquor concentration that adds water is 1.2g medical material/mL, obtains Chinese medicine extraction liquid；Stir process makes in sheep milk
Casein coagulation, through being filtrated to get Goat milk, mixes described Goat milk all with transparency liquid
Even, obtain Goat milk essence；
Step 3: sterilizing: Goat milk elite liquid measure is filled in high temperature steaming sterilizing bag, adopts
Seal after draining the air in high temperature steaming sterilizing bag with vacuum machine, by high temperature steaming complete for sealing
Sterilizing bag is put in high steam pot, steams 50min, takes out and obtain facial film after lowering the temperature.
The effect experimental of embodiment seven facial film
Experimental technique: choose men and women totally 35 people and try out, skin type include mixed type skin,
Oiliness skin, dry skin, classify according to its skin problem, is divided into 5 groups, often organizes 7 people,
Smear every day once, each 10 minutes.Trial effect is as table 4 below
The effect of table 4 trial edition invention facial film
The each material composition of the present embodiment is mutually matched and synergism.Wherein effective active component,
Anti-inflammation can be played, remove oils and fats and the effect of dirt.And, it also has well releives
And therapeutic effect, it is particularly suitable for corse sweat pore, the colour of skin is dark and gloomy, have the skin of bean scar, can promote blood
Liquid circulation, acceleration metabolism, thus play treatment skin, restorative effect.This facial film
Gentleness during use, is suitable for any skin including sensitive skin, non-stimulated.
The fungistatic effect experiment of described facial film:
Add the citron extract of various dose and sheep milk prepared facial film and carried out bacteriostatic test:
Test method: strain is inoculated in suitable culture medium, staphylococcus aureus, large intestine
Bacillus, bacillus pyocyaneus are 37 DEG C of constant temperature culture 24h, and Candida albicans is 30 DEG C of constant temperature culture 48
H, makes strain concentration at more than 108cfu/g, and then antibacterial decile is mixed into concentration is 106cfu/g
Bacteria suspension.Sample facial film is carried out comparison examination according to different citron extracts and sheep milk addition
Test.The facial film glue of uncolled shaping is selected for examination facial film.Used at the 7th, 14,21 and 28 days
Plate dilution method detects the content of microorganisms of sample respectively.
Criterion: the initial inoculum antibacterial 106cfu/g:(1 of sample) the 28th day time, in sample
Containing antibacterial ＞ 103cfu/g, this sample can not be tested by the challenge of microorganism attack；(2) the 28th days
Time, containing antibacterial at 102cfu/g～103cfu/g in sample, this sample conditional pass challenge is tested,
I.e. when in product protein or other animals and plants material compositions be not health that is the highest, that simultaneously produce
Changing commanders composite demand, when packing material is not susceptible to secondary pollution, this protective system can use, no
Then can not use；When (3) the 28th days, containing antibacterial at 10cfu/g～102cfu/g in sample, show this
The protective system of sample has stronger bactericidal effect to microorganism, is tested by challenge, and product is being given birth to
Produce, be not readily susceptible to microorganism when preserving and use and pollute；Within (4) the 15th days, rise, the antibacterial in sample
＜ 10cfu/g, at the 30th, 45,60 day, bacterial content unlike time more than the 15th day, this sample
Protective system has the bactericidal action of extra-heavy to microorganism, is tested by challenge, and product is producing, storing
It is not easy microbial contamination when hiding and use.In facial film, Bacteria Detection data are shown in Table 5.
Table 5 Bacteria Detection data
From the data in table 5, it can be seen that when described facial film include sheep milk that parts by weight are 15～50 parts and
During the citron extract of 0.5～20 part, described facial film anti-corrosive properties are cut with scissors, it is preferable that described facial film
Including the sheep milk that weight fraction is 30～45 parts, the Citric Acid Extract of 0.5～5 part, it is furthermore preferred that
When described facial film includes the Citric Acid Extract of sheep milk that parts by weight are 30 parts and 5 parts, described
Facial film antiseptic effect optimal.
Facial film described in the embodiment of the present invention three to embodiment seven all meets the facial film quality described in table 1
Test experience data, the facial film of the embodiment of the present invention three to embodiment seven is safely and effectively and quality inspection meets
State quality standard.
Known can be classified as moisture saver mask, cleawhite pack, spot-relieving face mask, tight according to facial film effect
Cause facial film, anti-wrinkle face mask, shining skin facial film, cleaning pack, compact pore facial film and local facial film；
Classify according to the dosage form of facial film and can be divided into tear-pull facial film, paste mask, cream facial film, curry face
Film and mounted facial film.Effect of facial film of the present invention and dosage form can be above-mentioned any one, and its effect can
Lay particular stress on by adjusting each component content value.
Embodiment is shown in Table 6 for sterilising conditions screening experiment in facial film preparation method of the present invention,
Carry out under the temperature of screening experiment is room temperature condition described in table 6, being 26 DEG C.
Table 6 sterilising conditions screening experiment result
From the data in table 6, it can be seen that when sterilising conditions for regulation high steam pot to 121 °, steam
When 40～60min, the facial film best results obtained, the shelf-life is the longest.And odorlessness and the change of color
Change.
The foregoing is only the preferred embodiments of the present invention, be not limited to the present invention, right
For those skilled in the art, the present invention can have various modifications and variations.All in the present invention
Spirit and principle within, any modification, equivalent substitution and improvement etc. made, should be included in
Within protection scope of the present invention.
Claims (10)
1. a facial film, it is characterised in that include the raw material components of following parts by weight: 15～50
The sheep milk of part and the citron extract of 0.5～20 part.
Facial film the most according to claim 1, it is characterised in that also include following parts by weight
Raw material components: the macromolecule hyaluronic acid of 0.05～1 part, low molecule hyaluronic acid, 0.5～5 of 0.05～1 part
The amino acid humectant of part, the glycerol of 1～20 part, the distilled water of 20～70 parts, the Flos Rosae Rugosae of 15～40 parts
Extracting solution and the hydroxyethyl cellulose of 0.05～0.5 part.
Facial film the most according to claim 2, it is characterised in that also include that parts by weight are 5～30
Part Chinese medicine extraction liquid, described Chinese medicine extraction liquid includes the raw material components of following parts by weight: 20～50
Part Radix Ophiopogonis, the Radix Glycyrrhizae of 1～10 part, the Radix Angelicae Dahuricae of 1～20 part, the Flos Matricariae chamomillae of 1～20 part, 5～25 parts
Herba Portulacae, the Folium Artemisiae Argyi of 1～20 part, the Radix Codonopsis of 0.1～1 part and 0.1～1 part Herba Menthae in one or
More than one.
Facial film the most according to claim 2, it is characterised in that also include that parts by weight are 1～10
Tremella extract, the tea tree ethereal oil of 5～40 parts, the Herba Lysimachiae foenum-graeci quintessence oil of 5～40 parts and 0.5～5 part of part
Butanediol.
5. the preparation method of the facial film described in an any one of Claims 1 to 4, it is characterised in that
The step of facial film is prepared as raw material including using sheep milk and citron extract.
The preparation method of a kind of facial film the most according to claim 5, it is characterised in that include
Following steps:
Step one: pretreatment of raw material: take macromolecule hyaluronic acid, low molecule hyaluronic acid, aminoacid guarantor
Humectant, glycerol, Flos Rosae Rugosae extracting solution and a part of distilled water are sufficiently stirred for dissolving transparent liquid；Will
Fructus Citri Limoniae obtains citron extract through process of squeezing the juice；Hydroxyethyl cellulose is poured into the residue distillation boiled
In water, stirring is dissolved, and pours in transparency liquid；
Step 2: prepare Goat milk essence: take the heated process of sheep milk, adds Fructus Citri Limoniae and extracts
Thing, stir process makes the casein coagulation in sheep milk, through being filtrated to get Goat milk, by described sheep
Milk milk surum is mixed homogeneously with transparency liquid, obtains Goat milk essence；
Step 3: sterilizing: obtain facial film by after encapsulated for Goat milk essence, sterilizing.
The preparation method of a kind of facial film the most according to claim 6, it is characterised in that described
In step 2, the temperature of the heated process of sheep milk is 90 DEG C；Described step 3 comprises the following steps:
Goat milk elite liquid measure is filled in high temperature steaming sterilizing bag, uses vacuum machine to drain high temperature and steam
Seal after boiling the air in sterilizing bag, put into high steam by sealing complete high temperature steaming sterilizing bag
In Guo, steam 40～60min, take out after lowering the temperature and obtain facial film.
The preparation method of a kind of facial film the most according to claim 6, it is characterised in that through adding
Sheep milk after heat treatment has been also added with Chinese medicine extract, the preparation method of described Chinese medicine extraction liquid
Comprise the following steps: take Radix Ophiopogonis, the Radix Angelicae Dahuricae, Radix Codonopsis, Herba Menthae, Radix Glycyrrhizae, Flos Matricariae chamomillae, Herba Portulacae and
One or more in Folium Artemisiae Argyi, boiling obtains Chinese medicine extraction liquid twice.
The preparation method of a kind of facial film the most according to claim 8, it is characterised in that described
The concrete steps that boiling is twice include: for the first time add 6～the soak by water 1.5 of 10 times～3 hours,
Second time adds 6～the soak by water 1.5 of 10 times～3 hours；Merge twice decocting liquid, filter, be concentrated into
0.2～2g medical material/mL, cold preservation stand 10～24 hours, filter, add water adjustment filter liquor concentration be 0.2～
2g medical material/mL, obtains Chinese medicine extraction liquid.
The preparation method of a kind of facial film the most according to claim 6, it is characterised in that warp
Sheep milk after heat treated has been also added with Tremella extract, tea tree ethereal oil, Herba Lysimachiae foenum-graeci quintessence oil and fourth
Glycol.
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| CN107375082A (en) * | 2017-08-08 | 2017-11-24 | 湖北瑞晟生物有限责任公司 | A kind of moisturizing anti-inflammatory facial mask liquid and preparation method thereof |
| CN107854367A (en) * | 2017-12-19 | 2018-03-30 | 广州源理生物科技有限公司 | A kind of Essence for sensitive skin reparation |
| CN116059140A (en) * | 2022-11-05 | 2023-05-05 | 安徽师范大学 | Plant source antioxidant mask and preparation method thereof |
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| CN107375082A (en) * | 2017-08-08 | 2017-11-24 | 湖北瑞晟生物有限责任公司 | A kind of moisturizing anti-inflammatory facial mask liquid and preparation method thereof |
| CN107281092A (en) * | 2017-08-15 | 2017-10-24 | 广西民族大学 | A kind of pawpaw goat milk whitening and moistening skin shower cream |
| CN107854367A (en) * | 2017-12-19 | 2018-03-30 | 广州源理生物科技有限公司 | A kind of Essence for sensitive skin reparation |
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| CN116059140A (en) * | 2022-11-05 | 2023-05-05 | 安徽师范大学 | Plant source antioxidant mask and preparation method thereof |
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Application publication date: 20161012 |