CN106929237A - A kind of donkey-hide gelatin soap and preparation method thereof - Google Patents
A kind of donkey-hide gelatin soap and preparation method thereof Download PDFInfo
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- CN106929237A CN106929237A CN201710132087.1A CN201710132087A CN106929237A CN 106929237 A CN106929237 A CN 106929237A CN 201710132087 A CN201710132087 A CN 201710132087A CN 106929237 A CN106929237 A CN 106929237A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/38—Products in which the composition is not well defined
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/225—Polymers
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/24—Hydrocarbons
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/262—Organic compounds, e.g. vitamins containing oxygen containing carbohydrates
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/26—Organic compounds, e.g. vitamins containing oxygen
- C11D9/265—Organic compounds, e.g. vitamins containing oxygen containing glycerol
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/22—Organic compounds, e.g. vitamins
- C11D9/40—Proteins
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Abstract
A kind of donkey-hide gelatin soap and preparation method thereof, belongs to daily chemicals technical field.It is characterised in that it includes the raw material of following weight portion is made：0. 1 ~ 0.2 part of 70 ~ 90 parts of soap base, 3 ~ 8 parts of donkey-hide gelatin, 1 ~ 4 part of honey, 0.2 ~ 0.3 part of red date extract, 0.4 ~ 0.5 part of aloe extract, 0.2 ~ 0.3 part of pot marigold extract, 0.2 ~ 0.3 part of licorice, 0.2 ~ 0.3 part of ophiopogon japonicus extract, 0.01 ~ 0.05 part of shea butter, 0.1 ~ 0.2 part of saualane, 0.3 ~ 0.5 part of Sodium Hyaluronate, 0.05 ~ 0.2 part of ursin and beta glucan.A kind of donkey-hide gelatin soap of the invention has functions that preferable whitening, moisturizing, anti-aging.
Description
Technical field
The present invention relates to a kind of donkey-hide gelatin soap and preparation method thereof, belong to daily chemicals technical field.
Background technology
Donkey-hide gelatin originates in Shandong Province Gu Donga County, and good person is transparent with amber, odorless.Also known as donkey-hide gelatin.Prior art
In, donkey-hide gelatin has enriching yin of enriching blood, and moisturizes, effect of hemostasis, for blood deficiency chlorosis, dizziness palpitaition, dysphoria and insomnia, xeropulmonary cough.
Facial soap, also known as beauty soap, clean skin soap, nourishing soap, is the perfumed soap with beauty and skin care effect.Applicant is in research
It is middle to find that existing facial soap has problems with：First, effect of existing facial soap whitening, moisturizing and anti-aging is paid no attention to
Think, it is difficult to the need for meeting consumer.Secondly, in existing facial soap, the facial soap U.S. species with donkey-hide gelatin as raw material is less, and
Effect is undesirable, it is difficult to reach expected skincare effect.
The content of the invention
The technical problem to be solved in the present invention is：Overcome the deficiencies in the prior art, there is provided a kind of donkey-hide gelatin soap and its preparation side
Method, the donkey-hide gelatin soap has functions that preferable whitening, moisturizing, anti-aging.
The technical solution adopted for the present invention to solve the technical problems is：The donkey-hide gelatin soap is it is characterised in that it includes following heavy
The raw material for measuring part is made：70 ~ 90 parts of soap base, 3 ~ 8 parts of donkey-hide gelatin, 1 ~ 4 part of honey, 0.2 ~ 0.3 part of red date extract, aloe extract
0.4 ~ 0.5 part, 0.2 ~ 0.3 part of pot marigold extract, 0.2 ~ 0.3 part of licorice, 0.2 ~ 0.3 part of ophiopogon japonicus extract, breast wood
0.01 ~ 0.05 part of fruit oil, 0.1 ~ 0.2 part of saualane, 0.3 ~ 0.5 part of Sodium Hyaluronate, 0.05 ~ 0.2 part of ursin and β-Portugal gather
0. 1 ~ 0.2 part of sugar.
The donkey-hide gelatin soap, it is characterised in that：Also include 0.05 ~ 0.1 part of maniod ebish flower extract.
The donkey-hide gelatin soap, it is characterised in that：Also include 0.05 ~ 0.1 part of Flos Chrysanthemi extract, 0.05 ~ 0.1 part of extract from pine needles
With 0.05 ~ 0.1 part of Olive leaf P.E.
The donkey-hide gelatin soap, it is characterised in that：Also include 0.05 ~ 0.3 part of Tea Polyphenols.
The extraction of described red date extract, aloe extract, pot marigold extract, licorice and ophiopogon japonicus extract
Method is：It is solvent that jujube, aloe, pot marigold, Radix Glycyrrhizae, the tuber of dwarf lilyturf are used into the ethanol water of percent by volume 60 ~ 70% respectively
Immersion, through the medicinal extract that refluxing extraction, filtering, concentrated under reduced pressure, drying are obtained respectively.
Described beta glucan is the avenabeta glucosan that acquisition is extracted from oat.
The relative molecular weight of described Sodium Hyaluronate is 50,000 ~ 500,000 dalton.
Described donkey-hide gelatin is gelatin powder or donkey-hide gelatin oligopeptide powder.
Described soap base is made up of the component of following quality percentage：Stearic acid 14 ~ 17%, myristic acid 4 ~ 7%, laurate 3 ~
5%th, glycerine 14 ~ 17%, D-sorbite 16 ~ 19%, ethylenediamine tetra-acetic acid 2 ~ 4%, propane diols 10 ~ 13%, NaOH 0.5 ~ 4%,
PEG400 13 ~ 16%, water 5 ~ 11%.
The preparation method of the donkey-hide gelatin soap, it is characterised in that use following steps：
1）By weight by donkey-hide gelatin, honey, red date extract, aloe extract, pot marigold extract, licorice, the tuber of dwarf lilyturf
The mixing of extract, saualane, Sodium Hyaluronate, ursin and beta glucan, adds the ethanol water of percent by volume 10 ~ 30%,
It is standby that stirring obtains mixed liquor；
2）Soap base and shea butter are heated to 75 ~ 95 DEG C, are melted soap base and is obtained soap lye；It is 60 ~ 70 DEG C to keep soap lye temperature
To mixed liquor is added in soap lye, stir, pour into mould, cooling, the demoulding obtain final product donkey-hide gelatin soap
It is described as follows for of the invention:Preferably, the formula of the donkey-hide gelatin soap is 80 ~ 85 parts of soap base, 4 ~ 7 parts of donkey-hide gelatin, honey 2 ~ 3
Part, 0.25 ~ 0.3 part of red date extract, 0.45 ~ 0.5 part of aloe extract, 0.25 ~ 0.3 part of pot marigold extract, Radix Glycyrrhizae are extracted
0.25 ~ 0.3 part of thing, 0.25 ~ 0.3 part of ophiopogon japonicus extract, 0.01 ~ 0.05 part of shea butter, 0.15 ~ 0.2 part of saualane, hyalomitome
0. 15 ~ 0.2 part of 0.4 ~ 0.5 part of sour sodium, 0.1 ~ 0.2 part of ursin and beta glucan.
It is further preferred that the formula of the donkey-hide gelatin soap is 85 parts of soap base, 6 parts of donkey-hide gelatin, 3 parts of honey, red date extract 0.3
Part, 0.5 part of aloe extract, 0.25 part of pot marigold extract, 0.2 part of licorice, 0.3 part of ophiopogon japonicus extract, breast wood fruit
0.1 part of 0.02 ~ 0.03 part of oil, 0.2 part of saualane, 0.4 part of Sodium Hyaluronate, 0.2 part of ursin and beta glucan.
Preferably, red date extract, aloe extract, pot marigold extract, licorice, the preparation of ophiopogon japonicus extract
Method is：Jujube, aloe, pot marigold, Radix Glycyrrhizae, the tuber of dwarf lilyturf crushing that will be enucleated respectively, are separately added into percent by volume 60 ~ 70%
Ethanol water carries out immersion 1 ~ 4 hour for solvent, is heated to 80 ~ 100 DEG C of refluxing extractions 1 ~ 3 time, and filtering respectively and merges filter
Liquid, obtains jujube extract, extract solution from aloe, pot marigold extract solution, licorice extract and Radix Ophiopogonis extract, and extract solution is dense
Contracting, dry acquisition medicinal extract.Preferably, concentration is using concentrated under reduced pressure.
Soap base is commercially available handmade soap soap base, or soap base mix with NaOH for animal and plant fat, saponification, enter mould,
Demoulding gained.Soap base formula used by applicant：Stearic acid 14 ~ 17%, myristic acid 4 ~ 7%, laurate 3 ~ 5%, glycerine 14 ~
17%th, D-sorbite 16 ~ 19%, ethylenediamine tetra-acetic acid 2 ~ 4%, propane diols 10 ~ 13%, NaOH 0.5 ~ 4%, PEG400
13 ~ 16%, water 5 ~ 11%, the formula has preferable bubbling ability, and careful foam can be quickly formed after rubbing, washes and feels, and
And advantage of lower cost.
Donkey-hide gelatin is gelatin powder or donkey-hide gelatin oligopeptide powder.Gelatin powder is that donkey-hide gelatin block crushes the acquisition of 20 ~ 60 mesh sieves.Donkey-hide gelatin oligopeptide
Powder can subsequently carry out ultrafiltration, drying and other steps for donkey-hide gelatin block is size-reduced, protease hydrolyzed is obtained, and be with reference to preparation method：Patent
CN201110236322.2, patent CN201310035428.5, patent CN201110450564.1；Or, donkey-hide gelatin oligopeptide powder
Commercially available prod can directly be bought or voluntarily prepared.Oligopeptide in donkey-hide gelatin oligopeptide powder（The dalton of relative molecular weight 200 ~ 1000）Institute
It is 80 ~ 85% to account for mass percent, and donkey-hide gelatin oligopeptide powder Transdermal absorption ability is strong, has preferable moisturizing, repairs skin damage, resists
Wrinkle ability.Preferably, donkey-hide gelatin oligopeptide powder weight average molecular weight is 580 ~ 1300 dalton, and donkey-hide gelatin oligopeptide powder peptide fragment is distributed as
200 ~ 3000 dalton, wherein free amino acid be 0 ~ 5% mass percent, the dalton of relative molecular weight 200 ~ 1000 it is oligomeric
Peptide accounts for 80 ~ 85% mass percents, and the small peptide of 1001 ~ 3000 dalton accounts for 10 ~ 15% mass percents.
Honey has bowl spares, moisturizes, analgesic, and removing toxic substances, effect of sore also have functions that skin moisture-keeping.Preferably, institute
With in any proportion mixed that honey is one or more in sophorae honey, Mel Jujubae, rape nectar, chaste tree nectar, rose nectar
Compound.Most preferably Mel Jujubae, first Mel Jujubae have anti-inflammation, promotion organization regeneration, moistening lung intestines, reinforcing spleen and kidney, removing toxic substances
Liver protection, cardiac stimulant hematopoiesis, adjust blood pressure and blood sugar, regulation nerve, improve the health care of sleep, improve looks, health macrobiosis, anti-ageing salubrity it is special
Effect；Secondly Mel Jujubae gives off a strong fragrance mellow, and donkey-hide gelatin soap gas can be assigned after addition, more conducively improve consumer use it is positive
Property, Mel Jujubae is difficult to crystallize, is easily obtained again, relative inexpensiveness.
Red date extract raw material is the jujube of stoning（That is date）, vitamin, mineral matter, human body are rich in red date extract
Required 18 kinds of amino acid, red jujube polysaccharide, flavone compound and triterpene compounds have anti-aging, anticancer, enhancing immune
Power etc. is acted on.Vitamin, mineral matter and the 18 kinds of amino acid needed by human contained in red date extract can be supplemented for skin
Nutrition, wherein abundant vitamin C can promote adrenaline secretion hormone hormone to be combined with skin, both increases skin resistance
And elasticity, prevent skin heart bleeding again, and the synthesis of melanin can be reduced, promote the formation of original glue thing, make skin pure white thin
Tender, high resilience, so as to play effect of cosmetology.Red date extract can significantly improve the superoxide dismutase in body
The activity of SOD, scavenging activated oxygen and enhancing lipoid peroxidization resistant.Jujube is rich in triterpene compound and Adenosine diphosphate
Glycosides, with the function of suppressing growth of cancer cells and breeding.Red jujube polysaccharide has obvious active anticancer and promotes lymphocyte
Proliferation function, can control Skin Cell to divide and break up, and adjust growth, the anti-aging of Skin Cell.
The raw material of aloe extract is liliaceous plant aloe barbadensis Miller, polysaccharide, anthraquinone analog compound, protein, dimension
Raw element, mineral matter.The anthraquinone analog compound of aloe has makes skin contraction, softness, moisturizing, anti-inflammatory, the performance of bleaching.Also
Release hardening, angling, improvement scar effect, small wrinkle, pouch, cutis laxa can not only be prevented, moreover it is possible to keep skin wet,
It is tender and lovely, at the same time it can also treat scytitis, also there is treatment well to acne, freckle, acne and scald, knife wound, insect bite etc.
Effect.It is similarly effective to hair, hair can be made to keep moistening smooth, pre-Anti-hair loss.
Pot marigold extract is the petal extract of feverfew pot marigold, has functions that anti-aging.Also have anti-inflammatory,
Antibacterial action, it is particularly preferable to staphylococcus, streptococcus effect.
Licorice is included:Glycyrrhizin, glycyrrhizic acid, liquiritin, flavonoids of Glycyrrhiza, rear curtain are than wingceltis element, ononis spinosa
Element, Quercetin etc..The whitening function that licorice has, mainly by suppressing tyrosinase and dopachrome interconvertible enzyme
（TRP-2）Activity, hinder 5,6- dihydroxy indoles（DHl）Polymerization, the formation of melanin is prevented with this, so as to reach U.S.
The effect of pale skin.Licorice is not required to add antioxidant in formula as sun-screening agent, will not stimulate skin, stable absorption
Ability is strong.
The raw material of ophiopogon japonicus extract is the Chinese medicine tuber of dwarf lilyturf, the dried root of the liliaceous plant tuber of dwarf lilyturf.It is many in ophiopogon japonicus extract
Sugar and scavenging action of the saponins to superoxide anion and hydroxyl radical free radical are stronger, the remote super ascorbic clearance rate of comparable sodium；
Saponin(e and anthraquinones have preferable bacteriostasis simultaneously, blue to Escherichia coli, candidiasis, gram-negative bacteria, leather
Positive bacteria, bacillus subtilis have good inhibiting effect.Promotion of the ophiopogon japonicus extract to arginase activities, has research to recognize
It is, the ability of skin water holding and the active proportional relation of its arginase, therefore improves the activity of arginase to will be helpful to
The preventing and treating of Dry, furthermore ophiopogon japonicus extract wettability power under the low humidity, therefore ophiopogon japonicus extract is an outstanding guarantor
Wet additive；In dermal fibroblasts culture, the ophiopogon japonicus extract under low concentration has preferable proliferation function, and tool skin-active is made
With, superoxide anion and Qiang base Zi You Yuan eliminations are acted on reference to ophiopogon japonicus extract, can be used for the anti-ageing of cosmetics；The tuber of dwarf lilyturf extracts
Thing also plays the role of certain skin whitening.
Shea butter, soft and moist children is sliding for quality, is maximally effective natural moisture preserving product, promotes cytothesis and repairs skin moisture film
Effect, can with tender skin of releiving, promote reepithelialization, assign skin-nourishing, delay skin aging.Also, newborn wood
Fruit oil can be with the alkaline components in soap base（NaOH）Reaction, adjusts the pH value of donkey-hide gelatin soap, keeps the pH value of donkey-hide gelatin soap
Between 7 ~ 7.3.Preferably, shea butter uses refined shea butter, compared to unpurified shea butter and other animals and plants
Grease, refined shea butter contains 5 ~ 13% unsaponifiable matter, quality is soft and smooth, moisturizing skin effect is excellent, refines shea butter temperature
With it is non-stimulated and without bad smell, after addition can give user preferable use feeling.It is preferred that using German BASF life
The refined shea butter shea butter SB45 for producing, wherein unsaponifiable matter content is high（Reach 10 ~ 13%）, moisturizing skin effect
It is the most preferable.
Saualane, strengthens maintenance epidermis, is effectively formed natural diaphragm, helps the balance between skin and sebum.Saualane
It is a kind of lipid closest to human sebaceous, affinity is strong, can be combined together with the sebum film of mankind itself, in skin surface
Form one layer of natural barrier.Saualane can also suppress the peroxidating of skin lipid, can effectively infiltrate through skin, and promote skin
The propagation of basal cell, to delay skin aging, improves and eliminates chloasma and have obvious physiologic effect.Saualane can also make
Skin pore is opened, and promotes blood microcirculation, promotes the metabolism of cell, and damaged cell is repaired in help.Preferably, saualane
Using the natural saualane extracted from animal and plant fat.
Sodium Hyaluronate has preferable moisturizing, repairs the characteristic of skin.Relative point of currently preferred Sodium Hyaluronate
Son amount is 50,000 ~ 500,000（Dalton）, the Sodium Hyaluronate under the molecular weight can infiltrate through skin corium, with lasting moisturizing
The colleague of characteristic, also with filling wrinkle, the effect for making skin rejuvenate.Preferably, Sodium Hyaluronate uses West China Fu Ruidasheng
The low molecule HA of product（Molecular weight 20 ~ 400,000）.
Ursin is derived from the natural active matter of green plants, and it can rapidly permeate into skin, breeds cell is not influenceed
While concentration, can effectively suppress the activity of the tyrosinase in skin, block the formation of melanin, by itself and junket ammonia
Enzyme directly in conjunction with, accelerate the decomposition and excretion of melanin, so as to reduce Skin pigmentation, dispelling stain and freckle, and right
Melanocyte does not produce the side effects such as toxic, excitant, sensitization, while also having sterilization, anti-inflammatory, the work of anti-irritant
With.Preferably, ursin is alpha-arbutin, and alpha-arbutin has stronger whitening effect.
Beta glucan, improves resisting skin allergy ability, activates immunologic function, removes free radical, delay skin aging.It is preferred that
It is because the avenabeta glucosan extracted in oat also has antiallergy, treatment dry skin and scabies using avenabeta glucosan
Itch, repair the effect of keratoderma, be more suitable for addition in donkey-hide gelatin soap formula.Avenabeta glucosan its possess excellent anti-
Aging effect, can smooth fine wrinkles, improve skin elasticity, improve dermatoglyph degree；With unique straight-chain molecular structure,
Good Transdermal absorption performance is imparted, promotes fibroblast synthesis collagen, promote wound healing, repair impaired flesh
Skin, gives skin and smooth sense of touch is moistened such as silk.
Maniod ebish flower extract raw material is the floral parts of malvaceae plant Sunset Abelmoschus Root.Sunset abelmoschus flower sunset abelmoschus flower is extracted
Thing has stronger oxidation resistance, can improve facial complexion, and with clearing heat and detoxicating, anti-inflammatory, treat effect of furunculosis.
The preparation method of maniod ebish flower extract is：Sunset abelmoschus flower is crushed, the ethanol water for adding percent by volume 60 ~ 70% is
Solvent carries out immersion 1 ~ 4 hour, is heated to 80 ~ 100 DEG C of refluxing extractions 1 ~ 3 time, filters and merging filtrate obtains extract solution, will carry
Liquid is taken to be concentrated under reduced pressure, dry acquisition medicinal extract.Concentration can also be concentrated using normal heating, but preferably concentrated under reduced pressure, be concentrated under reduced pressure
Thickening efficiency it is high, and be prevented from the functional component in extract solution volatilization or by heat inactivation.Preferably, drying uses low temperature
Heat drying, drying temperature is 35 ~ 50 DEG C, it is to avoid high temperature inactivates functional component.
When maniod ebish flower extract is also included, the preparation method of the donkey-hide gelatin soap, using following steps：
1）By weight by donkey-hide gelatin, honey, red date extract, aloe extract, pot marigold extract, licorice, the tuber of dwarf lilyturf
The mixing of extract, saualane, Sodium Hyaluronate, ursin, beta glucan and maniod ebish flower extract, adds percent by volume 10
~ 30% ethanol water, it is standby that stirring obtains mixed liquor；
2）Soap base and shea butter are heated to 75 ~ 95 DEG C, are melted soap base and is obtained soap lye；It is 60 ~ 70 DEG C to keep soap lye temperature
To mixed liquor is added in soap lye, stir, pour into mould, cooling, the demoulding obtain final product donkey-hide gelatin soap.
Flos Chrysanthemi extract raw material is the dry capitulum of feverfew FLOS CHRYSANTHEMI ALBA from Haizhou of China；Flos Chrysanthemi extract have heat-clearing,
Anti-inflammatory, effect of calm skin；Flos Chrysanthemi extract to staphylococcus aureus, shigella dysenteriae, proteus, typhoid bacillus,
Paratyphosum Bacterium, comma bacillus, beta hemolysis streptococcus, Escherichia coli, Pseudomonas aeruginosa, Bacillus tuberculosis and influenza virus
（PR3 plants）There is inhibitory action.Extract from pine needles raw material is the pine needle of masson pine or Chinese pine；Extract from pine needles is rich in flavonoids thing
Matter, multivitamin, amino acid and mineral matter, with compared with strong anti-oxidation, anti-aging effects, extract from pine needles is added to donkey-hide gelatin soap
In have functions that regulation skin sebum secretion.Olive leaf P.E raw material is the blade of plant olive.Olive leaf P.E
Middle main component is iridoids bitterness material, and its active highest is Cleupin and hydroxytyrosol.Olive leaf P.E
With broad-spectrum antiseptic, effect that is anti-oxidant, increasing cutaneous immunisation power, Olive leaf P.E is for virus, fungi, mould and yeast
Bacterium is invaded, slight and severe bacterial infections and primary class parasitic infection, with stronger inhibitory action.Flos Chrysanthemi extract,
Extract from pine needles and Olive leaf P.E three combination have stronger anti-inflammatory, antibacterial effect, can effectively extend donkey-hide gelatin soap
Resting period；Flos Chrysanthemi extract, extract from pine needles and Olive leaf P.E, are combined with maniod ebish flower extract（In step 1
Middle addition, is made mixed liquor）, have preferable therapeutic effect for face acnes.And Flos Chrysanthemi extract, extract from pine needles and
After Olive leaf P.E compounding, the sense of washing of donkey-hide gelatin soap can be improved, strengthen the cleaning force of donkey-hide gelatin soap.Flos Chrysanthemi extract, pine needle
The preparation method of extract and Olive leaf P.E is：FLOS CHRYSANTHEMI ALBA from Haizhou of China, pine needle and olive leaf are crushed respectively, adds percent by volume
60 ~ 70% ethanol water carries out immersion 1 ~ 4 hour for solvent, is heated to 80 ~ 100 DEG C of refluxing extractions 1 ~ 3 time, filters and closes
And filtrate obtains extract solution, extract solution is concentrated under reduced pressure, acquisition medicinal extract is dried.
When Flos Chrysanthemi extract, extract from pine needles and Olive leaf P.E is also included, the preparation method of the donkey-hide gelatin soap is adopted
Use following steps：
1）By weight by donkey-hide gelatin, honey, red date extract, aloe extract, pot marigold extract, licorice, the tuber of dwarf lilyturf
Extract, saualane, Sodium Hyaluronate, ursin, beta glucan, Flos Chrysanthemi extract, extract from pine needles and olive leaf are extracted
Thing mixes, and adds the ethanol water of percent by volume 10 ~ 30%, and it is standby that stirring obtains mixed liquor；
2）Soap base and shea butter are heated to 75 ~ 95 DEG C, are melted soap base and is obtained soap lye；It is 60 ~ 70 DEG C to keep soap lye temperature
To mixed liquor is added in soap lye, stir, pour into mould, cooling, the demoulding obtain final product donkey-hide gelatin soap.
Tea Polyphenols is the general name of Polyphenols of Tea, including flavanol compound, anthocyanin class, flavonoids, flavonols
With phenolic acid class etc..Predominantly flavanols (catechin) class, catechin accounts for 60 ~ 80%.Tea Polyphenols has stronger antioxidation,
Especially ester catechin EGCG, its reproducibility is even up to 100 times of the different bad hematic acid of L-.Tea Polyphenols is except with antioxidation
Outward, also such as there is inhibitory action to staphylococcus, Escherichia coli, hay bacillus with bacteriostasis.The adsorbable food of Tea Polyphenols
In peculiar smell, therefore with certain deodorization.
When Tea Polyphenols is also included, the preparation method of the donkey-hide gelatin soap, using following steps：
1）By weight by donkey-hide gelatin, honey, red date extract, aloe extract, pot marigold extract, licorice, the tuber of dwarf lilyturf
The mixing of extract, saualane, Sodium Hyaluronate, ursin, beta glucan and Tea Polyphenols, adds the ethanol of percent by volume 10 ~ 30%
The aqueous solution, it is standby that stirring obtains mixed liquor；
2）Soap base and shea butter are heated to 75 ~ 95 DEG C, are melted soap base and is obtained soap lye；It is 60 ~ 70 DEG C to keep soap lye temperature
To mixed liquor is added in soap lye, stir, pour into mould, cooling, the demoulding obtain final product donkey-hide gelatin soap.
Preferably, 0.02 ~ 0.1 part of chamomile essential oil, 0.1 ~ 0.2 part of houttuynia extract are also included in formula.Preparation side
Chamomile essential oil and houttuynia extract, step 1 are also added with the step of method 1）Concrete operations be：By weight by Ah
Glue, honey, red date extract, aloe extract, pot marigold extract, licorice, chamomile essential oil, cordate houttuynia are extracted
The mixing of thing, saualane, Sodium Hyaluronate, ursin and beta glucan, adds ethanol water, and it is standby that stirring obtains mixed liquor.
Chamomile essential oil and houttuynia extract can effectively releive skin, improve the anti-sensitive capability of skin.Chamomile essential oil and fish raw meat
Careless extract, is combined with maniod ebish flower extract（Add in step 1, be made mixed liquor）, being capable of anti-inflammatory, antiallergic sense, increasing
The poor environment to external world and the resistance of anaphylactogen of strong skin.The preparation method of houttuynia extract is：Cordate houttuynia is crushed,
Add the ethanol water of percent by volume 60 ~ 70% for solvent carries out immersion 1 ~ 4 hour, be heated to 80 ~ 100 DEG C of refluxing extractions 1
~ 3 times, simultaneously merging filtrate obtains extract solution for filtering, and extract solution is concentrated under reduced pressure, acquisition medicinal extract is dried.
When chamomile essential oil and houttuynia extract is also included, the preparation method of the donkey-hide gelatin soap, using following steps：
1）By weight by donkey-hide gelatin, honey, red date extract, aloe extract, pot marigold extract, licorice, the tuber of dwarf lilyturf
The mixing of extract, saualane, Sodium Hyaluronate, ursin, beta glucan, chamomile essential oil and houttuynia extract, adds body
The product ethanol water of percentage 10 ~ 30%, it is standby that stirring obtains mixed liquor；
2）Soap base and shea butter are heated to 75 ~ 95 DEG C, are melted soap base and is obtained soap lye；It is 60 ~ 70 DEG C to keep soap lye temperature
To mixed liquor is added in soap lye, stir, pour into mould, cooling, the demoulding obtain final product donkey-hide gelatin soap.
In preparation method：Step 1）The middle addition ethanol water of percent by volume 10 ~ 30% its effect is that various composition is equal
Even dispersion, is easy in step 2）In quickly uniformly mix with soap lye；Step 1）Gained mixed liquor is suspension, is adding step 2）
When need to stir, be easy to various composition dispersed.Ethanol in 15 ~ 20% ethanol waters can accelerate as defoamer
Removal process 2）The bubble produced in whipping process, the quality of the ethanol water of percent by volume 10 ~ 30% for soap base quality 5 ~
10%, a small amount of ethanol is conducive to shortening the demoulding time of donkey-hide gelatin soap, and after donkey-hide gelatin soap dries the demoulding, the second of solvent 15 ~ 20%
The second alcohol and water that alcohol solution is brought into can gradually volatilize lost, there's almost no in donkey-hide gelatin soap, final gained donkey-hide gelatin soap
Moisture content is 8 ~ 12%, and the moisture content with soap base is almost equal.Step 2）It is middle that soap base and shea butter are first heated to 75 ~ 95 DEG C,
Soap base melts acquisition soap lye, and shea butter can adjust the pH value of soap lye；Soap lye is cooled again, holding soap lye temperature 60 ~
70 DEG C, the mixed liquor that soap lye has preferable mobility, addition at this temperature can be quickly dispersed in soap lye, and 60 ~ 70
DEG C ethanol not easily caused in mixed liquor quickly volatilizees so that the volatile ingredient in mixed liquor can more be stored in soap lye
In, and in soap lye can shorten demoulding time containing a small amount of ethanol.
Compared with prior art, a kind of donkey-hide gelatin soap of the invention and preparation method thereof is had an advantageous effect in that：
1st, the donkey-hide gelatin soap has preferable whitening, moisturizing, crease-resistant effect.Applicant with the addition of donkey-hide gelatin, honey, red in formula
Jujube extract, aloe extract, pot marigold extract, licorice, shea butter, saualane, Sodium Hyaluronate, ursin
And beta glucan, make donkey-hide gelatin soap that there is preferable whitening, moisturizing and anti-aging, wash rear face skin sense and moisten soft and smooth.
2nd, donkey-hide gelatin soap tool can improve appearance complexion, strengthen the resistance of skin, make facial taking on a new look.Applicant exists
Maniod ebish flower extract is with the addition of in formula can improve appearance complexion, strengthen the resistance of skin, make facial taking on a new look, also
Has preferable acne-removing.
3rd, the donkey-hide gelatin soap has preferable cleaning force and antibacterial ability, and long-term storage is difficult to go mouldy, and increased the peace for using
Quan Xing.Applicant has found that the donkey-hide gelatin soap also has effect applicant for suppressing face acnes to the addition of FLOS CHRYSANTHEMI ALBA from Haizhou of China and extracts under study for action
Thing, extract from pine needles and Olive leaf P.E have functions that preferable bactericidal antiphlogistic, anti-mildew become, anti-donkey-hide gelatin soap becomes sour, with yellow another name for Sichuan Province
Sunflower extract combination anti-acne effect is significantly improved.
Specific embodiment
Embodiment 1 ~ 11 is a kind of specific embodiment of donkey-hide gelatin soap of invention and preparation method thereof, wherein in fact
Example 1 is applied for most preferred embodiment.
The raw materials used source of embodiment 1 ~ 11 is as follows：Soap base used is constituted：Stearic acid 16%, myristic acid 6%, laurate
4%th, glycerine 15%, D-sorbite 17%, ethylenediamine tetra-acetic acid 4%, propane diols 11%, NaOH 3%, PEG400 15%
With water 9%.Honey is Mel Jujubae.Shea butter is the refined shea butter shea butter SB45 of German BASF production.
Saualane is that NOF Corp produces saualane.Ursin is that Shaanxi Sen Fu natural products Co., Ltd produces alpha-arbutin
99% mass percent.The low molecule HA that Sodium Hyaluronate is produced using West China Fu Ruida（Molecular weight 20 ~ 400,000）.Oat β-Portugal
Glycan is the mass percent of Xi'an Ze Lang bio tech ltd avenabeta glucosan 99.8%.Tea Polyphenols is the holy association's life in Shandong
The mass percent of Tea Polyphenols 99% of thing Science and Technology Ltd. production.Chamomile essential oil is the Rome of French Moellhausen productions
Chamomile essential oil（Hydrodistillation is obtained）.
Red date extract, aloe extract, pot marigold extract, licorice, ophiopogon japonicus extract, sunset abelmoschus flower are extracted
Thing, houttuynia extract, Flos Chrysanthemi extract, extract from pine needles and Olive leaf P.E are prepared using following methods：By original
Material（Jujube, aloe, pot marigold, Radix Glycyrrhizae, the tuber of dwarf lilyturf, sunset abelmoschus flower, cordate houttuynia, FLOS CHRYSANTHEMI ALBA from Haizhou of China, pine needle or olive leaf）Crush, add respectively
Enter the ethanol water of percent by volume 65% for solvent carries out immersion 2 hours, be heated to 85 ~ 90 DEG C of refluxing extractions 2 times, filtering
Merging filtrate, obtains extract solution, by extract solution it is concentrated under reduced pressure, 40 ~ 45 DEG C dry and obtain medicinal extract.
Embodiment 1
The present embodiment formula is made up of the raw material of following weight portion：
85 parts of soap base, 6 parts of donkey-hide gelatin, 3 parts of honey, 0.3 part of red date extract, 0.5 part of aloe extract, pot marigold extract 0.25
Part, 0.2 part of licorice, 0.3 part of ophiopogon japonicus extract, 0.02 ~ 0.03 part of shea butter, 0.2 part of saualane, Sodium Hyaluronate
0.1 part of 0.4 part, 0.2 part of alpha-arbutin and avenabeta glucosan.Donkey-hide gelatin used be Shandong Donga donkey-hide gelatin Co., Ltd production Ah
Blob of viscose, the mesh sieve of size-reduced mistake 40 obtains gelatin powder.When donkey-hide gelatin selects gelatin powder, gelatin powder is produced for Shandong Donga donkey-hide gelatin Co., Ltd
Donkey-hide gelatin block is beaten powder, sieving and is made.When donkey-hide gelatin is donkey-hide gelatin oligopeptide, from oligopeptide in donkey-hide gelatin oligopeptide powder（Relative molecular weight 200
The small peptide of ~ 1000 dalton）Shared mass percent is 80 ~ 85% commercially available prod.
Embodiment 2
The present embodiment is formulated with embodiment 1, and difference is that donkey-hide gelatin used is donkey-hide gelatin oligopeptide powder, oligopeptide in donkey-hide gelatin oligopeptide powder
（The dalton of relative molecular weight 200 ~ 1000）Shared mass percent is 80 ~ 85%.Donkey-hide gelatin oligopeptide powder becomes more meticulous for Zhengzhou section is auspicious
Work Co., Ltd produces donkey-hide gelatin oligopeptide powder.
Embodiment 3
The present embodiment formula is made up of the raw material of following weight portion：70 parts of soap base, 8 parts of donkey-hide gelatin, 1 part of honey, red date extract 0.3
Part, 0.4 part of aloe extract, 0.3 part of pot marigold extract, 0.2 part of licorice, 0.3 part of ophiopogon japonicus extract, shea butter
0.1 part of 0.01 part, 0.2 part of saualane, 0.3 part of Sodium Hyaluronate, 0.2 part of alpha-arbutin and avenabeta glucosan.Donkey-hide gelatin used
It is the donkey-hide gelatin block of Shandong Donga donkey-hide gelatin Co., Ltd production, the mesh sieve of size-reduced mistake 20 obtains gelatin powder.
Embodiment 4
The present embodiment is formulated with embodiment 3, and difference is that donkey-hide gelatin used is donkey-hide gelatin oligopeptide powder, oligopeptide in donkey-hide gelatin oligopeptide powder
（The small peptide of the dalton of relative molecular weight 200 ~ 1000）Shared mass percent is 80 ~ 85%.Donkey-hide gelatin oligopeptide powder is that Zhengzhou section is auspicious
Fine Chemical Co., Ltd produces donkey-hide gelatin oligopeptide powder.
Embodiment 5
The present embodiment formula is made up of the raw material of following weight portion：90 parts of soap base, 3 parts of donkey-hide gelatin, 2 parts of honey, red date extract 0.2
Part, 0.5 part of aloe extract, 0.2 part of pot marigold extract, 0.3 part of licorice, 0.2 part of ophiopogon japonicus extract, shea butter
0.2 part of 0.05 part, 0.1 part of saualane, 0.5 part of Sodium Hyaluronate, 0.05 part of alpha-arbutin and avenabeta glucosan.Donkey-hide gelatin used
It is the donkey-hide gelatin block of Shandong Donga donkey-hide gelatin Co., Ltd production, the mesh sieve of size-reduced mistake 20 obtains gelatin powder.
Embodiment 6
The present embodiment is formulated with embodiment 6, and difference is that donkey-hide gelatin used is donkey-hide gelatin oligopeptide powder, oligopeptide in donkey-hide gelatin oligopeptide powder
（The small peptide of the dalton of relative molecular weight 200 ~ 1000）Shared mass percent is 80 ~ 85%.Donkey-hide gelatin oligopeptide powder is Shanghai resistance to the present
The donkey-hide gelatin oligopeptide powder of Industrial Co., Ltd.'s production.
The preparation method of embodiment 1 ~ 6 is：
1）By weight by donkey-hide gelatin, honey, red date extract, aloe extract, pot marigold extract, licorice, the tuber of dwarf lilyturf
The mixing of extract, saualane, Sodium Hyaluronate, alpha-arbutin and avenabeta glucosan, adds the ethanol of percent by volume 15% water-soluble
Liquid, it is standby that stirring obtains mixed liquor；
2）Soap base and shea butter are heated to 80 ~ 85 DEG C, are melted soap base and is obtained soap lye；It is 65 ~ 70 DEG C to keep soap lye temperature
To mixed liquor is added in soap lye, stir, pour into mould, cooling, the demoulding obtain final product donkey-hide gelatin soap.
Embodiment 7
The present embodiment formula is made up of the raw material of following weight portion：80 parts of soap base, 5 parts of donkey-hide gelatin, 2 parts of honey, red date extract 0.2
Part, 0.4 part of aloe extract, 0.3 part of pot marigold extract, 0.2 part of licorice, 0.3 part of ophiopogon japonicus extract, shea butter
0.02 part, 0.1 part of saualane, 0.4 part of Sodium Hyaluronate, 0.2 part of alpha-arbutin, 0.1 part of avenabeta glucosan, sunset abelmoschus flower carry
Take 0.1 part of thing.Oligopeptide in donkey-hide gelatin oligopeptide powder（The small peptide of the dalton of relative molecular weight 200 ~ 1000）Shared mass percent
It is 80 ~ 85%.Donkey-hide gelatin oligopeptide powder is the donkey-hide gelatin peptide of Shanghai Nai Jin Industrial Co., Ltd.s production.
The preparation method of embodiment 7 is：
1）By weight by donkey-hide gelatin, honey, red date extract, aloe extract, pot marigold extract, licorice, the tuber of dwarf lilyturf
The mixing of extract, saualane, Sodium Hyaluronate, alpha-arbutin, avenabeta glucosan and maniod ebish flower extract, adds volume hundred
Divide 20% ethanol water of ratio, it is standby that stirring obtains mixed liquor；
2）Soap base and shea butter are heated to 80 ~ 85 DEG C, are melted soap base and is obtained soap lye；It is 65 ~ 70 DEG C to keep soap lye temperature
To mixed liquor is added in soap lye, stir, pour into mould, cooling, the demoulding obtain final product donkey-hide gelatin soap.
Embodiment 8
The present embodiment formula is made up of the raw material of following weight portion：90 parts of soap base, 7 parts of donkey-hide gelatin, 1 part of honey, red date extract 0.2
Part, 0.5 part of aloe extract, 0.2 part of pot marigold extract, 0.3 part of licorice, 0.2 part of ophiopogon japonicus extract, shea butter
0.01 part, 0.1 part of saualane, 0.4 part of Sodium Hyaluronate, 0.2 part of alpha-arbutin, 0.2 part of avenabeta glucosan, FLOS CHRYSANTHEMI ALBA from Haizhou of China extract
0.1 part of 0.05 part of thing, 0.1 part of extract from pine needles and Olive leaf P.E.Oligopeptide in donkey-hide gelatin oligopeptide powder（Relative molecular weight
The small peptide of 200 ~ 1000 dalton）Shared mass percent is 80 ~ 85%.Donkey-hide gelatin oligopeptide powder is the resistance to modern limited public affairs of industry in Shanghai
Take charge of the donkey-hide gelatin peptide of production.
The preparation method of embodiment 8 is：
1）By weight by donkey-hide gelatin, honey, red date extract, aloe extract, pot marigold extract, licorice, the tuber of dwarf lilyturf
Extract, saualane, Sodium Hyaluronate, alpha-arbutin, avenabeta glucosan, Flos Chrysanthemi extract, extract from pine needles and olive
Leaf extract mixes, and adds the ethanol water of percent by volume 15%, and it is standby that stirring obtains mixed liquor；
2）Soap base and shea butter are heated to 80 ~ 85 DEG C, are melted soap base and is obtained soap lye；It is 65 ~ 70 DEG C to keep soap lye temperature
To mixed liquor is added in soap lye, stir, pour into mould, cooling, the demoulding obtain final product donkey-hide gelatin soap.
Embodiment 9
The present embodiment formula is made up of the raw material of following weight portion：90 parts of soap base, 7 parts of donkey-hide gelatin, 1 part of honey, red date extract 0.2
Part, 0.5 part of aloe extract, 0.2 part of pot marigold extract, 0.3 part of licorice, 0.2 part of ophiopogon japonicus extract, shea butter
0.01 part, 0.1 part of saualane, 0.4 part of Sodium Hyaluronate, 0.2 part of alpha-arbutin, 0.2 part of avenabeta glucosan, Tea Polyphenols 0.05
~ 0.3 part.Oligopeptide in donkey-hide gelatin oligopeptide powder（The small peptide of the dalton of relative molecular weight 200 ~ 1000）Shared mass percent is 80
~85%.Donkey-hide gelatin oligopeptide powder is the donkey-hide gelatin oligopeptide powder of Shanghai Nai Jin Industrial Co., Ltd.s production.
The preparation method of embodiment 9 is：
1）By weight by donkey-hide gelatin, honey, red date extract, aloe extract, pot marigold extract, licorice, the tuber of dwarf lilyturf
Extract, saualane, Sodium Hyaluronate, alpha-arbutin, avenabeta glucosan, maniod ebish flower extract, Tea Polyphenols mixing, plus
Enter the ethanol water of percent by volume 20%, it is standby that stirring obtains mixed liquor；
2）Soap base and shea butter are heated to 80 ~ 85 DEG C, are melted soap base and is obtained soap lye；Soap lye temperature is kept for 60 DEG C to soap
Mixed liquor is added in liquid, is stirred, poured into mould, cooling, the demoulding obtain final product donkey-hide gelatin soap.
Embodiment 10
The present embodiment formula is made up of the raw material of following weight portion：80 parts of soap base, 5 parts of donkey-hide gelatin, 2 parts of honey, red date extract 0.2
Part, 0.4 part of aloe extract, 0.3 part of pot marigold extract, 0.2 part of licorice, 0.3 part of ophiopogon japonicus extract, shea butter
0.02 part, 0.1 part of saualane, 0.4 part of Sodium Hyaluronate, 0.2 part of alpha-arbutin, 0.1 part of avenabeta glucosan, sunset abelmoschus flower carry
Take 0.1 part of thing, 0.05 part of chamomile essential oil, 0.2 part of houttuynia extract.Oligopeptide in donkey-hide gelatin oligopeptide powder（Relative molecular weight
The small peptide of 200 ~ 1000 dalton）Shared mass percent is 80 ~ 85%.Donkey-hide gelatin oligopeptide powder is the resistance to modern limited public affairs of industry in Shanghai
Take charge of the donkey-hide gelatin oligopeptide powder of production.
The preparation method of embodiment 10 is：
1）By weight by donkey-hide gelatin, honey, red date extract, aloe extract, pot marigold extract, licorice, the tuber of dwarf lilyturf
Extract, saualane, Sodium Hyaluronate, alpha-arbutin, avenabeta glucosan, maniod ebish flower extract, chamomile essential oil, fish raw meat
Careless extract mixing, adds the ethanol water of percent by volume 20%, and it is standby that stirring obtains mixed liquor；
2）Soap base and shea butter are heated to 80 ~ 85 DEG C, are melted soap base and is obtained soap lye；Soap lye temperature is kept for 60 DEG C to soap
Mixed liquor is added in liquid, is stirred, poured into mould, cooling, the demoulding obtain final product donkey-hide gelatin soap.
Embodiment 11
The present embodiment formula is made up of the raw material of following weight portion：80 parts of soap base, 5 parts of donkey-hide gelatin, 2 parts of honey, red date extract 0.2
Part, 0.4 part of aloe extract, 0.3 part of pot marigold extract, 0.2 part of licorice, 0.3 part of ophiopogon japonicus extract, shea butter
0.02 part, 0.1 part of saualane, 0.4 part of Sodium Hyaluronate, 0.2 part of alpha-arbutin, 0.1 part of avenabeta glucosan, sunset abelmoschus flower carry
Take 0.05 part of 0.1 part of thing, 0.1 part of Flos Chrysanthemi extract, 0.05 part of extract from pine needles and Olive leaf P.E.Donkey-hide gelatin oligopeptide powder
Middle oligopeptide（The small peptide of the dalton of relative molecular weight 200 ~ 1000）Shared mass percent is 80 ~ 85%.Donkey-hide gelatin oligopeptide powder is
The donkey-hide gelatin peptide of Shanghai Nai Jin Industrial Co., Ltd.s production.
The preparation method of embodiment 11 is：
1）By weight by donkey-hide gelatin, honey, red date extract, aloe extract, pot marigold extract, licorice, the tuber of dwarf lilyturf
Extract, saualane, Sodium Hyaluronate, alpha-arbutin, avenabeta glucosan, maniod ebish flower extract, Flos Chrysanthemi extract, pine
Pin extract and Olive leaf P.E mix, and add the ethanol water of percent by volume 15 ~ 20%, and it is standby that stirring obtains mixed liquor；
2）Soap base and shea butter are heated to 80 ~ 85 DEG C, are melted soap base and is obtained soap lye；It is 65 ~ 70 DEG C to keep soap lye temperature
To mixed liquor is added in soap lye, stir, pour into mould, cooling, the demoulding obtain final product donkey-hide gelatin soap.
Clinical practice of the invention is summarized as follows：
A kind of donkey-hide gelatin soap of the invention is used for facial cleansing, and application method is：With water-soaked face, got with donkey-hide gelatin soap of the present invention
Foam, cleaning face, massage skin of face 5 ~ 10 minutes cleans face with water, washes away foam.User men and women, uses
Person's age is more than 16 years old, pregnant woman's disabling.
It is as a result as follows by being observed effect using donkey-hide gelatin soap of the invention：
Each embodiment selects every kind of illness of 1200 volunteers, each embodiment to select 300 volunteers, and the wherein colour of skin is dark
In heavy, three kinds of selected volunteers of illness of wrinkle and dry skin：Men and women respectively accounts for 50%.Minimum 18 years old most in each embodiment
It is big 60 years old, 25% is accounted within 18 ~ 30 years old, 25% is accounted within 31 ~ 40 years old, is accounted within 41 ~ 50 years old 25%, accounts for 25% within 51 ~ 60 years old；Wherein selected by whelk illness
In volunteer：Minimum 18 years old maximum 35 years old, accounts within 18 ~ 24 years old 50%, accounts within 25 ~ 30 years old 25%, accounts for 25% within 31 ~ 35 years old.Taking Pictures recording each
The face skin original state of volunteer, it is daily sooner or later each using once using donkey-hide gelatin soap face cleaning of the invention 2 months, try out
Period does not use other face cosmetics.
The symptom of primary treatment is as follows：
The colour of skin is obscure：The colour of skin jaundice, it is intensely dark；Pachylosis, pore is thick；Blee is uneven, and the colour of skin is shallow at cheek, face
T areas of portion colour of skin depth；One or more including above symptom.
Wrinkle：Skin lacks moisture, surface fat to be reduced, and face skin is lax, flexibility decrease；The lift eyebrow line of frontalis, wrinkle
The glabella line of eyebrow flesh, the crow's feet of orbicular muscle of eye, the cheek of the bicker line of musculus orbicularis oris and lip vertical line, greater zygomatic muscle and musculus quadratus labii superioris
Portion's twill；One or more including above symptom.
Dry skin：Skin of face is dried, hand is touched without moist feeling, decortication；Skin-bound is itched after washing one's face；Including with
One or more of upper symptom.
Whelk：Meaning is acne vulgaris.It is apt to occur in cheek, forehead, chin portion and nose buccal groove.
Curative effect judging standard：According to the improvement situation of symptom, it is divided into effective and invalid, effectively by volunteer, to suffer from each symptom complete
Portion is alleviated or part is alleviated, and belongs to effectively；It is invalid that symptom is suffered from without any alleviation or improvement by patient.Effect statistics is such as
Shown in table 1：
1 embodiment of table 1 is counted using a kind of effect of donkey-hide gelatin soap of the invention
2 embodiment of table 2 is counted using a kind of effect of donkey-hide gelatin soap of the invention
3 embodiment of table 3 is counted using a kind of effect of donkey-hide gelatin soap of the invention
4 embodiment of table 4 is counted using a kind of effect of donkey-hide gelatin soap of the invention
5 embodiment of table 5 is counted using a kind of effect of donkey-hide gelatin soap of the invention
6 embodiment of table 6 is counted using a kind of effect of donkey-hide gelatin soap of the invention
7 embodiment of table 7 is counted using a kind of effect of donkey-hide gelatin soap of the invention
8 embodiment of table 8 is counted using a kind of effect of donkey-hide gelatin soap of the invention
9 embodiment of table 9 is counted using a kind of effect of donkey-hide gelatin soap of the invention
10 embodiment of table 10 is counted using a kind of effect of donkey-hide gelatin soap of the invention
11 embodiment of table 11 is counted using a kind of effect of donkey-hide gelatin soap of the invention
Be can be seen that by table 1, after after donkey-hide gelatin soap of the invention with 2 months, efficient 86 ~ 94%.Embodiment 1 ~ 6 have compared with
Good whitening, moisturizing, crease-resistant effect；Embodiment 7,8,9,11 not only has whitening, moisturizing, crease-resistant effect, and to the youth
Acne has preferable curative effect.And it has been found that be added with Flos Chrysanthemi extract, extract from pine needles and Olive leaf P.E, or
Person, being added with the donkey-hide gelatin soap of Tea Polyphenols has preferable antibacterial preservative efficacy.
The above, is only presently preferred embodiments of the present invention, is not the limitation for making other forms to the present invention, is appointed
What those skilled in the art changed possibly also with the technology contents of the disclosure above or be modified as equivalent variations etc.
Effect embodiment.But it is every without departing from technical solution of the present invention content, according to technical spirit of the invention to above example institute
Any simple modification, equivalent variations and the remodeling made, still fall within the protection domain of technical solution of the present invention.
Claims (10)
1. a kind of donkey-hide gelatin soap, it is characterised in that the raw material including following weight portion is made：70 ~ 90 parts of soap base, 3 ~ 8 parts of donkey-hide gelatin, honeybee
1 ~ 4 part of honey, 0.2 ~ 0.3 part of red date extract, 0.4 ~ 0.5 part of aloe extract, 0.2 ~ 0.3 part of pot marigold extract, Radix Glycyrrhizae carry
Take 0.2 ~ 0.3 part of thing, 0.2 ~ 0.3 part of ophiopogon japonicus extract, 0.01 ~ 0.05 part of shea butter, 0.1 ~ 0.2 part of saualane, hyalomitome
0. 1 ~ 0.2 part of 0.3 ~ 0.5 part of sour sodium, 0.05 ~ 0.2 part of ursin and beta glucan.
2. a kind of donkey-hide gelatin soap according to claim 1, it is characterised in that：Also include maniod ebish flower extract 0.05 ~ 0.1
Part.
3. a kind of donkey-hide gelatin soap according to claim 1, it is characterised in that：Also include 0.05 ~ 0.1 part of Flos Chrysanthemi extract,
0.05 ~ 0.1 part of 0.05 ~ 0.1 part of extract from pine needles and Olive leaf P.E.
4. a kind of donkey-hide gelatin soap according to claim 1, it is characterised in that：Also include 0.05 ~ 0.3 part of Tea Polyphenols.
5. a kind of donkey-hide gelatin soap according to claim 1, it is characterised in that：Described red date extract, aloe extract, gold
Small cup flower extract, the extracting method of licorice and ophiopogon japonicus extract are：Respectively by jujube, aloe, pot marigold, Radix Glycyrrhizae, wheat
It is solvent soaking that winter uses the ethanol water of percent by volume 60 ~ 70%, through refluxing extraction, filtering, concentrated under reduced pressure, drying point
The medicinal extract not obtained.
6. a kind of donkey-hide gelatin soap according to claim 1, it is characterised in that：Described beta glucan is to extract to obtain from oat
The avenabeta glucosan for obtaining.
7. a kind of donkey-hide gelatin soap according to claim 1, it is characterised in that：The relative molecular weight of described Sodium Hyaluronate is
50000 ~ 500,000 dalton.
8. a kind of donkey-hide gelatin soap according to claim 1, it is characterised in that：Described donkey-hide gelatin is gelatin powder or donkey-hide gelatin oligopeptide
Powder.
9. a kind of donkey-hide gelatin soap according to claim 1, it is characterised in that：Described soap base by following quality percentage component
Composition：Stearic acid 14 ~ 17%, myristic acid 4 ~ 7%, laurate 3 ~ 5%, glycerine 14 ~ 17%, D-sorbite 16 ~ 19%, ethylenediamine
Tetraacethyl 2 ~ 4%, propane diols 10 ~ 13%, NaOH 0.5 ~ 4%, PEG400 13 ~ 16%, water 5 ~ 11%.
10. the preparation method of a kind of donkey-hide gelatin soap according to claim 1, it is characterised in that use following steps：
1）By weight by donkey-hide gelatin, honey, red date extract, aloe extract, pot marigold extract, licorice, the tuber of dwarf lilyturf
The mixing of extract, saualane, Sodium Hyaluronate, ursin and beta glucan, adds the ethanol water of percent by volume 10 ~ 30%,
It is standby that stirring obtains mixed liquor；
2）Soap base and shea butter are heated to 75 ~ 95 DEG C, are melted soap base and is obtained soap lye；It is 60 ~ 70 DEG C to keep soap lye temperature
To mixed liquor is added in soap lye, stir, pour into mould, cooling, the demoulding obtain final product donkey-hide gelatin soap.
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107557192A (en) * | 2017-10-18 | 2018-01-09 | 湖南大三湘油茶生态产业有限公司 | Tender skin soap of camellia oleifera fruit and preparation method thereof |
| CN108774601A (en) * | 2018-08-08 | 2018-11-09 | 廖家平 | Hand-guarding liquid detergent |
| CN109125611A (en) * | 2017-12-29 | 2019-01-04 | 上海晟薇生物科技有限公司 | One Plant Extracts and its preparation method and application |
| CN109777676A (en) * | 2019-03-18 | 2019-05-21 | 惠州市旭东实业有限公司 | A kind of craft facial soap |
| CN109953939A (en) * | 2019-04-25 | 2019-07-02 | 美晨集团股份有限公司 | A kind of natural moisture preserving composition and its application |
| CN114558109A (en) * | 2022-03-23 | 2022-05-31 | 武汉珈诗丽科技有限公司 | Application of donkey-hide gelatin glycopeptide in preparation of skin micro-ecological regulating preparation |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102978041A (en) * | 2012-12-10 | 2013-03-20 | 大连创达技术交易市场有限公司 | Calendula fancy soap |
| CN104069044A (en) * | 2013-04-10 | 2014-10-01 | 山东东阿阿胶股份有限公司 | Small-molecular donkey-hide gelatin facial mask, as well as preparation method and application thereof |
| CN105476911A (en) * | 2015-12-16 | 2016-04-13 | 青岛玻莱莫斯新材料技术有限公司 | Whitening cosmetics containing arbutin, tangerine powder and radix glycyrrhizae extract |
| CN105832579A (en) * | 2016-04-22 | 2016-08-10 | 南京中医药大学 | Flower wax, honey and flavone part extracted from byproduct in abelmoschus manihot pharmaceutical manufacturing process, as well as preparation method and application thereof |
| CN105886171A (en) * | 2016-04-18 | 2016-08-24 | 广西南宁皂和奇迹科技有限公司 | Transparent soap and preparation method thereof |
| CN106176276A (en) * | 2016-09-27 | 2016-12-07 | 广东丸美生物技术股份有限公司 | A kind of have defying age and the skin matrix of antiallergic effect and preparation and application thereof |
| CN106265244A (en) * | 2016-08-22 | 2017-01-04 | 袁海忠 | A kind of production method of Flos Chrysanthemi handwashing liquid |
-
2017
- 2017-03-07 CN CN201710132087.1A patent/CN106929237A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102978041A (en) * | 2012-12-10 | 2013-03-20 | 大连创达技术交易市场有限公司 | Calendula fancy soap |
| CN104069044A (en) * | 2013-04-10 | 2014-10-01 | 山东东阿阿胶股份有限公司 | Small-molecular donkey-hide gelatin facial mask, as well as preparation method and application thereof |
| CN105476911A (en) * | 2015-12-16 | 2016-04-13 | 青岛玻莱莫斯新材料技术有限公司 | Whitening cosmetics containing arbutin, tangerine powder and radix glycyrrhizae extract |
| CN105886171A (en) * | 2016-04-18 | 2016-08-24 | 广西南宁皂和奇迹科技有限公司 | Transparent soap and preparation method thereof |
| CN105832579A (en) * | 2016-04-22 | 2016-08-10 | 南京中医药大学 | Flower wax, honey and flavone part extracted from byproduct in abelmoschus manihot pharmaceutical manufacturing process, as well as preparation method and application thereof |
| CN106265244A (en) * | 2016-08-22 | 2017-01-04 | 袁海忠 | A kind of production method of Flos Chrysanthemi handwashing liquid |
| CN106176276A (en) * | 2016-09-27 | 2016-12-07 | 广东丸美生物技术股份有限公司 | A kind of have defying age and the skin matrix of antiallergic effect and preparation and application thereof |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107557192A (en) * | 2017-10-18 | 2018-01-09 | 湖南大三湘油茶生态产业有限公司 | Tender skin soap of camellia oleifera fruit and preparation method thereof |
| CN109125611A (en) * | 2017-12-29 | 2019-01-04 | 上海晟薇生物科技有限公司 | One Plant Extracts and its preparation method and application |
| CN108774601A (en) * | 2018-08-08 | 2018-11-09 | 廖家平 | Hand-guarding liquid detergent |
| CN109777676A (en) * | 2019-03-18 | 2019-05-21 | 惠州市旭东实业有限公司 | A kind of craft facial soap |
| CN109953939A (en) * | 2019-04-25 | 2019-07-02 | 美晨集团股份有限公司 | A kind of natural moisture preserving composition and its application |
| CN114558109A (en) * | 2022-03-23 | 2022-05-31 | 武汉珈诗丽科技有限公司 | Application of donkey-hide gelatin glycopeptide in preparation of skin micro-ecological regulating preparation |
| CN114558109B (en) * | 2022-03-23 | 2024-05-28 | 武汉珈诗丽科技有限公司 | Application of donkey-hide gelatin glycopeptide in preparing skin microecological preparation |
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Application publication date: 20170707 |