CN102805722A - Whitening essence lotion containing natural extracts and preparation method thereof - Google Patents
Whitening essence lotion containing natural extracts and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a whitening essence lotion containing natural extracts and a preparation method thereof. The whitening essence lotion comprises self-emulsifying glycerin monostearate, stearic acid, camellia seed oil, wheat-germ oil, medical vaseline, synthetic squalane, triethanolamine, L-serine, distilled water, glycerol, tremella extract, bletilla striata extract, motherwort extract, lily extract, towel gourd extract, sorbitol, sodium hyaluronate, vitamin C, ethylenediamine tetraacetic acid disodium, carbomer 940, methylparaben/sorbic acid, citric acid and essence. Compared with the prior art, the whitening essence lotion is milky, appropriate in thickness, light, moist, exquisite, uniform, brightly white, fine in spreadability, and fragrant, and can supplement nutrients and moisture needed by the skin, adjust immunity of the skin, enhance skin resistance to external stimulation, improve blood circulation of the skin, promote metabolism and make the skin white, fully elastic and soft.
Description
Technical field
The present invention relates to a kind of elite emulsion, particularly a kind of tender Virgin's milk liquid that is rich in the natural component extract and preparation method thereof.
Background technology
Liking to be beautiful is people's nature; Development along with society; The women is also increasing about the demand of skin care item and makeup; But factors such as the skin aging that variations in temperature caused, metabolism that work that grows with each passing day and life stress, environmental pollution, season, conversion brought slow down all can cause the skin water loss, make skin coarsely, dim make, form dried stricture of vagina mute, cause many skin problems.With advancing age, many middle-aged womens grow the big mottle of Semen Glycines on face.Then finger is big, and quantity is on the increase.Mottle is that a kind of bothersome capacitive skin pigment that hinders is sick, and the lighter's yellowish complexion is itched like soil, skin.Weight person's skin produces the irregular speckle of yellowish-brown or pitchy, and mottle has brought misery not only for the patient mentally, causes heavy thought pressure, and influence orthobiosis, work, youth of both sexes that have even the chance that loses love and get married because of mottle.How to prevent the aging of skin, the glamour that retains youth is the topic that people extremely are concerned about.
Nowadays various products are too plenty for the eye to take it all on the market; Also more and more plentifuler and substantial; People more and more hanker after toward the own cosmetics of piling up on the face seemingly, make great efforts to let oneself can keep out that environmental pollution changes, the influence of factors such as work life stress, self skin aging, constantly U.S.A again.
Yet according to investigations, many producers, businessman are under the ordering about of interests, and in order to let product can play best effect, the chemosynthesis material that is harmful to skin is added in beginning in cosmetics, skin care item.In fact, some easily available natural Chinese medicines, fruit and vegerable composition, most composition that also is rich in skin nutrition has the effect of improving skin matter, even edible, safe in utilization relieved.
Under the promotion of the trend that goes back to nature, natural cosmetics becomes a kind of trend and fashion, is the main trend of domestic and international from now on cosmetics research and development.Chinese herbal medicine beauty treatment really is an aboundresources, use extensively, convenient and simple, very wide of its development prospect has great demand to auxotype and the drug effect type elite emulsion that contains the natural plant active component on the market.
Summary of the invention
The 1st technical problem to be solved by this invention provides a kind of new tender white elite emulsion that contains the natural component extract.
The 2nd technical problem to be solved by this invention is the method for preparing of above-mentioned elite emulsion.
Technical solution problem of the present invention is: a kind of tender Virgin's milk liquid, contain following material and weight portion in per 100 gram emulsions:
Described Pseudobulbus Bletillae (Rhizoma Bletillae) extract is through following method preparation:
It is an amount of to take by weighing the Pseudobulbus Bletillae (Rhizoma Bletillae), soaks 0.15-1h, is heated to 90-100 ℃, decocts and extracts 3 times; Add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging, extract 0.5-1.5h for the 2nd time; Add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, the each filtration; Merging filtrate, the volume of filtrating are concentrated into 3-6 times (g/ml) of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filter promptly to get.
Described tremella extract prepares through following method:
It is an amount of to take by weighing Tremella, extracts 2 times, adds the 8-12 times of water yield the 1st time, extracts 0.5-1.5h, extracts 0.5-1.5h h with the 3-5 times of water yield the 2nd time, filter with 3 layers of gauze at every turn, and merging filtrate, heating is concentrated into 2-10 times (g/ml) of Tremella weight, gets final product.
Described Bulbus Lilii extracting solution prepares through following method:
It is an amount of to take by weighing Bulbus Lilii, soaks 0.5-1h, is heated to 90-100 ℃, decocts and extracts 3 times, adds 10-15 times of water gaging the 1st time; Extract 0.5-2h, add 8-12 times of water gaging the 2nd time, extract 0.5-1.5h, add 6-10 times of water gaging the 3rd time; Extract 0.5-1.5h, the each filtration, merging filtrate, the volume of filtrating are concentrated into 4-7 times (g/ml) of Pseudobulbus Bletillae (Rhizoma Bletillae) weight; Add liquid weight 1%-5% active carbon, 80-100 ℃ of heating in water bath stirs, and sucking filtration gets final product.
Described Herba Leonuri extract prepares through following method:
It is an amount of to take by weighing Herba Leonuri, soaks 0.15-1.5h, is heated to 90-100 ℃, decocts and extracts 3 times; Add 6-15 times of water gaging the 1st time, extract 0.5-1.5h, add 4-10 times of water gaging, extract 0.5-1.5h for the 2nd time; Add 4-8 times of water gaging the 3rd time, extract 1h, filter merging filtrate at every turn with 3 layers of gauze; Heating is concentrated into 2-10 times (g/ml) of Herba Leonuri weight, filters with double gauze, gets final product.
Described Fructus Luffae extract prepares through following method:
Fresh Fructus Luffae peeling is thinly sliced, and weighs, and soaks 0.15-1.5h, is heated to 90-100 ℃; Decoct to extract 3 times, add 6-15 times of water gaging the 1st time, extract 0.25-1.5h, add 5-14 times of water gaging the 2nd time; Extract 0.25-1.5h, add 4-12 times of water gaging, extract 0.25-1h, for the 3rd time at every turn with 3 layers of gauzes filtration; Merging filtrate, heating are concentrated into 2-5 times (g/ml) of Herba Leonuri weight, filter with double gauze, get final product.
Described essence is rose essence, green cucumber essence, Bulbus Lilii essence, honey peach essence, osmanthus flower fragrance, flavoring pineapple essence, Fructus Citri Limoniae essence.
Described a kind of method for preparing that is rich in the tender Virgin's milk liquid of natural component extract may further comprise the steps
A) take by weighing the 0.1-10g Acritamer 940, be dissolved in the 150-350ml water, stir; Leave standstill and treated its natural swelling dissolving in 2-3 hour, be warming up to 80-90 ℃, be incubated 10-30 minute; Swelling fully after, drip 0.05-1ml5%-15% (weight) triethanolamine when being neutralized to PH and being 5-7, get final product;
B) take by weighing glyceryl monostearate 1-8g, stearic acid 1-5g, camellia seed oil 2-10g, Semen Tritici aestivi germ oil 2-10g, vaseline 2-15g, squalane 0.2-5g, be warming up to 80-90 ℃, heating and melting obtains oil phase;
C) take by weighing L-serine 0.010-0.100g and place beaker, add the 50-80g distilled water, be warming up to 80-90 ℃, obtain water;
D) treat the complete fusion of oil phase, water poured in the oil phase that the limit edged stirs 10-15min to same direction, to being even milky white liquid shape, promptly gets substrate, and substrate is chilled to room temperature;
E) treat substrate put cold after, add glycerol 1-10g, tremella extract 0.5-5g, Herba Leonuri extracting solution 0.5-5g, Bulbus Lilii extracting solution 0.5-5g, Rhizoma Bletillae extraction solution 0.5-5g, Fructus Luffae extracting solution 0.5-5g, sorbitol 0.1-1g, hyaluronate sodium 0.01-0.20g;
F) emulsion of e step gained is added swelling completely in the thickening agent Acritamer 940 gel, adds vitamin C 0.1-1g, uses citric acid 0.1-0.5g regulate pH value as 5-7 after, stirring 10-15min, mix homogeneously;
G) take by weighing disodiumedetate 0.001-0.007g, methyl hydroxybenzoate or sorbic acid 0.1-0.3g add 2-12ml 1, the 2-propylene glycol, and heating makes its dissolving, puts into f step institute antigalactic after waiting to dissolve, and mix homogeneously gets final product.
Various compositions among the present invention are following:
Tremella also is Tremella, Tremella, and the laudatory title of " hat in the bacterium " is arranged.Tremella is sage's article of beauty treatment; Compendium of Material Medica from China's Han dynasty Shennong's Herbal to the outstanding physician's Li Shizhen (1518-1593 A.D.) of the Ming Dynasty; And " grand ceremony of Chinese pharmacy diction " all done record to the Tremella medicinal efficacy modern age, and the successive dynasties, the noble of imperial family regarded Tremella as " article of life lengthening ", " good medicine of looks improving and the skin nourishing " especially.On the books in Chinese medicine and pharmacy ancient book " Tai Ping Classic favour side " lining, Tremella just is used to do balneation during the Tang Dynasty, has effect moist, smooth skin.Tremella is rich in the natural characteristic colloid, adds its nourishing yin effect, can skin moistening, and dispel face's chloasma, freckle, the effect of beauty treatment, skin care, life lengthening is arranged.
Tremella is a kind of famous and precious tonic that benefiting action is arranged.Modern medicine study confirms that Tremella contains rich nutrient contents, comprises plurality of inorganic salt and B such as protein, carbohydrate, fat, crude fibre, carotene, ferrum, calcium, phosphorus
1, B
2With multivitamin such as C, there are 7 kinds to be essential amino acid in wherein contained 18 seed amino acids.The pharmacology effective ingredient of Tremella is a tremella polysaccharide: mainly contain compositions such as acidic polysaccharose, neutral heteropolysaccharide., acidic oligomer sugar.Tremella polysaccharide has obvious antioxidation, and has the effect of enhances human body cellular immunization and humoral immunization, can also resist tumor patient because of the immunologic function that chemicotherapy causes reduces, and suppresses the growth of tumor cell.Contain a large amount of tremella polysaccharides in the Tremella; Its main active is α-mannan, enrich the mucopolysaccharide body of compositions such as glucose, trehalose, polyacid pentose and mannitol; Structure and hyaluronic acid are very similar, and the power of preserving moisture is splendid, are described as " phyto-hyaluronic acid ".Therefore the tremella polysaccharide body is littler than the molecule of hyaluronic acid, is coated in that to absorb seepage velocity on the skin faster, also is not easy the viscose glue sense to occur, is the more natural vegetalitas high-quality composition of preserving moisture, and is the cause of Tremella facial beautification and skin rejuvenation function.Contain a large amount of hydroxyls, carboxyl isopolarity group in the polysaccharide molecule, it is unique and persistent along sliding skin sense and extremely strong lock water, moisture-keeping efficacy that it is had.Simultaneously, the Tremella mannan has good enhancing skin immunization and anti-oxidation efficacy, to improving cell viability remarkable result is arranged.Normal drink dried tremella soup can also be whitened, skin care, speckle dispelling, beauty treatment.
Herba Leonuri is the herb of labiate Herba Leonuri, have invigorate blood circulation, the effect of blood stasis dispelling.The beautification function of Herba Linderniae Crustaceae mainly is the function of promoting blood circulation to disperse blood clots that has through Herba Leonuri itself, promotes facial blood circulation, faces upward the system fungi growth, reaches that speckle dispelling is crease-resistant, the effect of beauty and skin care.It contains trace element such as multiple nutritional components such as protein, carbohydrate, selenium and manganese, but antioxidation, anti-aging, resisting fatigue and anticancer hypertrophy.Leonurine clean, deoil, preserve moisture blood circulation promoting and blood stasis dispelling, tissue regeneration promoting, detumescence, toxin expelling, enhancing skin barrier defence capability wherein, antioxidation is anti-aging; The laurelline cleaning is deoiled and is preserved moisture, and shrinks sebaceous gland, control oil, pore refining; The stachydrine cleaning is deoiled and is preserved moisture, and microcirculation improvement has bacteriostasis to dermatophytes, shrinks sebaceous gland, control oil, pore refining.Therefore, skin care, anti-ageing, anti-old, desalination mottle effect are arranged.With the Herba Leonuri beauty treatment, with a long history in China, the Herba Leonuri chopping is dried in " the angle teenage girl side " in the Yuan Dynasty " Imperial drug institution side ", grinds to be superfine powder, and medication powder massage is sooner or later washed one's face every day.Have the wrinkle-chasing stricture of vagina, move back the effect of brown patch, the skin that makes us commonly used is bright and clean, can treat diseases such as freckle, chloasma.People from Chaoyang creatively added Herba Leonuri in " the Lu Ling side of whitening " of " imperial palace case ", bring out the best in each other with Chinese crude drugs such as Aloe, Poria, the Rhizoma Atractylodis Macrocephalae in the original formulation, improved the effect of freckle removing and whitening.Herba Leonuri is used for external application, can exfoliation, improve speckle, acne problem, and short cell regeneration, it is bright and clean moist to let skin keep.Herba Leonuri is rich in vitamin A, and is also very effective for the maintenance of eyes.
Bulbus Lilii contains nutrients such as aminoacid, vitamin B, vitamin C in starch, protein, fat, calcium, phosphorus, ferrum, pantothenic acid, carotene, lymphatic temperament, solubility total sugar, reducing sugar, sucrose, pectin, the crude fibre, 8, and is useful to skin cell metabolism, can remove intravital harmful substance simultaneously; Slow down aging has the merit of good nutritious tonifying, and can looks improving and the skin nourishing; The bright skin of moisturizing, Glycerin prevents, repairs microgroove; Crease-resistant preserving youthful looks, the black light speckle of dispelling, be whiten, moisturizing, antidotal good medicine; Have good enhancing skin immunization and anti-oxidation efficacy, minimizing melanin deposition, alleviation skin allergy symptom are had remarkable result.The trace element that Bulbus Lilii is contained helps cell excitement, the ability resisting fatigue, and moist skin makes the skin delicacy smooth.To removing oxygen-derived free radicals significant effect is arranged.Especially to various heatings recover the back hold wan and sallow, long-term psychasthenia, insomnia and dreamful sleep and climacteric women recover appearance gloss has better action.Life-time service can make skin-whitening moisten, and is of pink and healthy-looking, rosy lips and pretty white teeth, and skin is delicate.
To be that Cucurbitaceae is annual climb up by holding on to herbaceous plant to Fructus Luffae.The Fructus Luffae aqueous is sweet, gentleness, the facial sebum secretion of scalable, to skin of face have clearly, restrain, calmness, equilibrated function.Fructus Luffae is delicate bright sliding, nutritious.Fructus Luffae water contains vitamin, protein, carbohydrate, ascorbic acid, carbohydrate, plant mucilage, xylane, mineral, thiamine, riboflavin, nicotinic acid, especially the content rich of phosphorus, calcium, ferrum.These materials all have health-care effect to skin, can keep the normal water content of horny layer, and dehydration and prolongation hydration slow down; Can replenish the necessary moisture of skin, keep skin water tender, fine and smooth, and contain a large amount of nature moisturizing factor; The not glutinous greasy composition of preserving moisture can effectively be releived and tightened exsiccant skin; Make face skin keep moistening, high resilience, the colour of skin is beautiful, ruddy, clean, pale.As medical material, Fructus Luffae water can enhance metabolism, and soft aging cutin is removed the deep layer dirt, suppresses melanocyte and generates, and can effectively improve coarse skin wrinkly, and it is tender bright and clean to make skin reply the children, and it is soft and moist glossy to make the skin qualitative change get.Have in the Compendium of Material Medica of China: Fructus Luffae liquid has the meridian dredging, and promoting the circulation of blood feeling pulse merit is in order to the greasy record of big de-sludging of washing one's face.
The Pseudobulbus Bletillae (Rhizoma Bletillae) is an astringing to arrest bleeding Chinese medicine simply.Its rich in starch, glucose, Pseudobulbus Bletillae polysaccharose (Pseudobulbus Bletillae (Rhizoma Bletillae) glue), volatile oil, phlegmatic temperament etc., external is embrocated, and can eliminate the vestige that acne on the face stays, and the beauty treatment speckle removing makes skin smooth seamless.The Pseudobulbus Bletillae (Rhizoma Bletillae) is exactly the good medicine of improving looks from ancient times, and " property of medicine opinion " cloud its " control skin ulcer on the face, make skin smooth ", Compendium of Material Medica cloud its " it is black to wash one's face, speckle dispelling " are described as " fairy maiden whitens ".The Pseudobulbus Bletillae (Rhizoma Bletillae) has the effect of tangible promotion keratinocyte, and Pseudobulbus Bletillae (Rhizoma Bletillae) glue is participated in the reparation and the metabolic process of damaged tissues or cell directly.Pseudobulbus Bletillae (Rhizoma Bletillae) glue is added in antifreeze, anticracking cosmetics, the anti-aging and nutritive cosmetics, can replenish skin nutrition, eliminate excessive free radical in the body; Can improve local blood circulation; Promote the epithelial cell reparation, can stop blooding, hold back skin ulcer and skin moistening, to treating and preventing that the skin chilblain from having obvious effect with breaking; The skin-nourishing situation be can improve and wrinkle, delaying skin aging prevented.
Hyaluronate sodium has another name called hyaluronic acid sodium, hyaluronic acid sodium, is a kind of acid mucopolysaccharide.Hyaluronic acid is from buphthalmos, cockscomb, people's special materials such as umbilical cord, to extract, and also has from some antibacterial such as actinomycetes recently and extracts.Hyaluronate sodium itself is one of formation of human body skin, is the widest a kind of acidic mucopolysaccharide that distributes in the human body, is present in the substrate of connective tissue, has the good moisture preserving effect.Contain a large amount of carboxyls and hydroxyl in the hyaluronan molecule; In aqueous solution, form intramolecularly and intermolecular hydrogen bond; This makes it have powerful water retention; Can combine self water more than 400 times, be the best material of finding at present of occurring in nature moisture retention, is called as ideal nature moisturizing factor.The water-soluble fluid power of 2% pure hyaluronic acid keeps 98% moisture securely.
Squalane is that the Squalene hydrogenation reaction that obtains in the stricture of vagina shark liver oil of deep-sea makes, and main component is myristic acid, butyrum nucistae, Squalene, squalane etc.For establishing the image to the responsible health of environment for human survival, cosmetic industry can not use natural squalane again, generally utilizes Vegetable oil lipoprotein to synthesize squalane.Synthetic squalane has the cosmetic properties of natural squalane, and pure plant origin and natural squalane character are very approaching; But considerably cheaper, has crease-resistant effect at non-oxidizability and excellent heat stability, has velvety feel; With skin lipid structural similarity, moderate polar oil, good absorbing can strengthen skin elasticity; Give the soft and smooth sense of skin nature, and a kind of affinity is arranged between skin, thereby become protective barrier one.Synthetic squalane is prone to absorb, the moistness of height, moisture retention, lubricity, with the back skin smooth, moisten non-greasy, percutaneous permeability better and in quickening to fill a prescription other active component in skin, permeate; Can also form the anti-moisture content of protecting film at epiderm skin runs off; But not cutaneous eupnea, and good natural sun-prevention function.With other cosmetic ingredients splendid compatibility is arranged, skin is had affinity preferably, do not stimulate, sensitization not; Free from extraneous odour; As safe as a house, but the also growth of mould fungus inhibition is selected its ideal that becomes numerous skin care products and personal hygiene article; The strong recommendation is used for child care products, gives product fabulous feel.
Semen Tritici aestivi germ oil is to be a kind of grain germ oil that raw material is produced with the Fructus Tritici aestivi, is ideal beauty treatment base oil, is described as eatable cosmetics; It is human natural nutrition treasure-house; Can strengthen the connective tissue of skin, keep skin elasticity, be suitable for ripe with old and feeble skin most.It has concentrated the nutrition elite of Semen Tritici aestivi; 8 seed amino acids of rich in vitamin E, B, protein, calcium, ferrum, magnesium, zinc, potassium, phosphorus, copper, linoleic acid, linolenic acid, needed by human, the lysine and the multiple physiologically active component of shortage in the particularly general corn, the needed by human unsaturated fatty acid content is up to more than 80%; Only linoleic content just accounts for more than 55%; Help to keep skin delicate, skin care is the hat of vegetable oil with increasing skin elasticity, particularly content of vitamin E; The vitamin treasure-house that is called as skin have the title of " king of vitamin E ", " liquid golden ".Vitamin E α, β, γ, δ possess for four types entirely; Physiologically active usefulness is 30 times of synthesising complex E; Being famous natural powerful antioxidant, is human antidotal antioxidants that really are applied to few in number, is prone to be absorbed by the body; Prevent the generation of lipid oxide in vivo; Have the inhibition free radical, antioxidation, delay body aging, protection cell membrane, promote skin metabolism, improve body immunity, strengthen anti-cancer, anticancer and blood circulation promoting effect; Prevent mottle, black speck and pigmentation in addition, preserve moisture, dispel wrinkle, make skin moist, improve looks, retain youth, make women's skin to become soft and moist and effects such as high resilience.Especially effective to moistening drying and the aged skin of circumference of eyes.To drying, hydropenia, aging, the wrinkle skin is extremely helpful, is fit to various skin matter, and chronic eczema, eczema are had certain effect, also has sun-proof function, it is sun-proof to can be used for health.Semen Tritici aestivi germ oil also can reduce cicatrix injured or that operation is caused, can also reduce the left vestige of long on the face comedo.
Camellia seed oil has another name called Oleum Camelliae, Camellia oil; Derive from the mature seed of plant of theaceae oil tea or lobule oil tea, also claim " intelligence developmental oil ", " health doctor ", " blood vessel street cleaner ", " puerperal period is precious ", " beauty's oil ", " parent-offspring's oil ", " NAOHUANGJIN ", " Weight reducing oil ", " long life oil ", " east olive oil " etc.Containing the linoleic acid that abundant vitamin A, D, E, K, camellin, tea polyphenols and other antioxidant, oleic acid relative amount account for 76%-85%, 7%-8% in the Oleum Camelliae almost is that content is the highest in all vegetable oil commonly used, very easily is absorbed by the body.Oleum Camelliae is the highest edible oil of finding at present of unsaturated fatty acid content, and up to more than 90%, wherein oleic acid and linoleic ratio are very rationally.Linoleic acid, linolenic acid, oleic acid are claimed " beauty treatment acid " again.Unsaturated fatty acid is in liberal supply, and people's skin can be delicate moist, and hair is pitch-black shinny; Otherwise, the pachylosis that will become, alopecia.Squalene in the Oleum Camelliae has good oxygen enrichment ability, but anti-hypoxia and resisting fatigue improve body immunity; Tea polyphenols has very strong antioxidation; Zinc is described as " flower of life ", and the content of zinc is 10 times of soybean oil in the Oleum Camelliae, can promote the growth promoter and the tissue regeneration of body.Therefore it can protect skin, especially can prevent skin injury and aging, makes skin have gloss.Camellia seed oil is the end oil of high-grade women, baby skin protection article, the base oil of senior quintessence oil, is put on skin and just can be absorbed by the body rapidly.Monounsaturated fatty acid content is The more the better, can eliminate free radical.Oleum Camelliae meets the human body needs most, is a kind of oil the most affine with human body.Oleum Camelliae can be preserved moisture, moistened, blacking hair and nourishing face, be used for hair care; Can prevent hairs break and alopecia; Rub one's body with a towel after the bath, strengthen skin elasticity, remove striae gravidarum, anti-canthus wrinkle; Can prevent and treat old people's skin pruritus in winter, also can control burn, scald, chap, uvioresistant injury, accelerating wound healing, prevention radical damage, antioxidation etc.
Glycerol formal name used at school glycerin belongs to polyalcohols, is the most universal the most common composition of preserving moisture in the cosmetics, have preserve moisture, the effect of Glycerin.Can make horny layer keep hydration status.It more can rise to the water holding capacity of candy aldehydic acid best and perfection with after hyaluronic acid combines.The moisturizing effect is very good, with back skin water profit, softness, touches very comfortable.People in winter glycerol commonly used is put on the skin in hands and face etc. and is exposed to airborne skin surface, plays the frosted effect of skin that prevents.Good to cutaneous safety, be difficult for causing allergy.
Numerous compositions in this Emulsion prescription have the elimination free radical; Thereby antioxidation influences melanin, and the generation of lipofuscin and various speckles postpones the effect of skin aging; Like trace element-selenium, manganese, the monounsaturated fatty acid that Tremella mannose, Herba Leonuri etc. contain, vitamin A, C, E.Pseudobulbus Bletillae (Rhizoma Bletillae) glue can be participated in the reparation and the metabolic process of damaged tissues or cell, promotes the epithelial cell reparation, the skin ulcer that disappears speckle dispelling.
Want to have the good skin matter bright, that water is tender, full, preserving moisture is indispensable basic maintenance merit forever.Only guarantee that the skin water content is sufficient, water retaining function sound, just can not let dim heavy, coarse, microgroove and problem such as lax let your ugly, the ageing of skin change.The present invention preserves moisture through blood circulation promoting regulates qi, lock water again and protects skin and guarantee skin-nourishing; Make the colour of skin smooth, ruddy; Like not glutinous greasy nature moisturizing factor such as hyaluronate sodium, a-mannan, plant mucilage, mineral, polysaccharide, organic acid, can effectively releive and tighten exsiccant skin, soft old useless cutin; In effective skin moistening, skin protection, increase the effect of preserving moisture, nourishing.
The made emulsion viscosity of the present invention suits, slim and graceful water profit, and evenly fine and smooth, bright pale, stretchability is good, abnormal smells from the patient fragrance.Can eliminate the effect of oxygen-derived free radicals, suppress the generation of mottle, anti aging effect; Can replenish nutrition, the moisture that skin needs, regulate skin immune function controlling, strengthen skin and resist environmental stimuli; Improve cutaneous circulation, enhance metabolism, make skin be full of elasticity, softness.
The specific embodiment
Below in conjunction with embodiment the present invention is done further description.
Camellia seed oil of the present invention, Semen Tritici aestivi germ oil are commercially available.
Embodiment 1
1.1 the preparation of Pseudobulbus Bletillae (Rhizoma Bletillae) extract:
It is an amount of to take by weighing Pseudobulbus Bletillae (Rhizoma Bletillae) 40g, soaks 0.5h, is heated to 100 ℃, decocts and extracts 3 times, adds 8 times of water gagings the 1st time; Extract 1h, add 6 times of water gagings the 2nd time, extract 1h, add 5 times of water gagings, extract 0.5h for the 3rd time; The each filtration, merging filtrate, the volume of filtrating is concentrated into 500ml, filters promptly to get.
1.2 the preparation of tremella extract:
Take by weighing Tremella 22.3g, extract 2 times, add 10 times of water yields the 1st time, extract 1h, 4 times of water yields of the 2nd usefulness are extracted 1h, filter with 3 layers of gauze at every turn, and merging filtrate heats and is concentrated into 200ml, and is for use.
1.3 the preparation of Bulbus Lilii extracting solution:
Take by weighing Bulbus Lilii 20g, soak 0.5h, be heated to 100 ℃, decoct and extract 3 times, add 15 times of water gagings the 1st time; Extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time; Extract 1h, the each filtration, merging filtrate, the volume of filtrating are concentrated into 5 times (g/ml) of Pseudobulbus Bletillae (Rhizoma Bletillae) weight; Add amount of liquid 1%-5% active carbon, 80 ℃ of heating in water bath stir, and sucking filtration is subsequent use.
1.4 the preparation of Herba Leonuri extract:
Take by weighing Herba Leonuri blade of grass 20.5g, soak 1h, be heated to 100 ℃, decoct and extract 3 times; Add 10 times of water gagings the 1st time, extract 1h, add 8 times of water gagings, extract 1h for the 2nd time; Add 5 times of water gagings the 3rd time, extract 1h, filter merging filtrate at every turn with 3 layers of gauze; Heating is concentrated into the 250ml of Herba Leonuri weight, filters with double gauze, and is subsequent use.
1.5 the preparation of Fructus Luffae extract:
Fresh Fructus Luffae peeling is thinly sliced and is weighed, and soaks 1h, is heated to 100 ℃; Decoct to extract 3 times, add 10 times of water gagings the 1st time, extract 0.5h, add 8 times of water gagings the 2nd time; Extract 0.5h, add 6 times of water gagings, extract 0.5h, for the 3rd time at every turn with 3 layers of gauzes filtration; Merging filtrate, heating is concentrated into 2 times (g/ml) of Herba Leonuri weight, filters with double gauze, and is for use.
1.6 the preparation of 100g emulsion
A) take by weighing Acritamer 940 0.8g, be dissolved in the 200ml water, be stirred to rapidly evenly, if any caking; With the Glass rod crushing, leave standstill on one side, treat its natural swelling dissolving 2.5h; Connect beaker and put into 80 ℃ of water proof heating of water-bath, after the 25min swelling is complete, drip the 10% triethanolamine neutralization of 0.5ml; The limit edged stirs, and surveys pH value, when PH=6, is clear gel.
B) take by weighing glyceryl monostearate 3g, stearic acid 3g, camellia seed oil 5g, Semen Tritici aestivi germ oil 5g, vaseline 5g, squalane 0.8g and place evaporating dish on water-bath, to keep 85 ℃ of heating in water bath fusions of temperature, as oil phase.
C) take by weighing L-serine 0.055g and place beaker, add the 60g distilled water, be placed in the water-bath (keeping 85 ℃ of bath temperatures) limit heating edge and stir, quicken its dissolving, as water with glass plate.
D) the complete fusion of oil phase in the ware to be evaporated is poured the water in the beaker of equality of temperature in the evaporating dish in the oil phase, and the limit edged stirs 10min to same direction, and is liquid to being creamy white, and promptly gets substrate.From water-bath, take out and be chilled to room temperature.
E) treat substrate put cold after, add glycerol 4g, tremella extract 1g, Herba Leonuri extracting solution 1g, Bulbus Lilii extracting solution 1g, Rhizoma Bletillae extraction solution 1g, Fructus Luffae extracting solution 1g, sorbitol 1.5g, hyaluronate sodium 0.1g.
F) emulsion of e step gained is added swelling completely in the Acritamer 940 gel, add vitamin C 0.1g, after using citric acid to regulate pH value to be 6, stir 10min, mix homogeneously;
G) take by weighing disodiumedetate 0.003g, methyl hydroxybenzoate 0.1g adds 2ml 1, the 2-propylene glycol, and heating makes its dissolving, puts into f step institute antigalactic after waiting to dissolve, and mix homogeneously gets final product.
Embodiment 2
2.1 the preparation of Pseudobulbus Bletillae (Rhizoma Bletillae) extract:
It is an amount of to take by weighing Pseudobulbus Bletillae (Rhizoma Bletillae) 50g, soaks 0.5h, is heated to 100 ℃, decocts and extracts 3 times, adds 10 times of water gagings the 1st time; Extract 1.5h, add 6 times of water gagings the 2nd time, extract 1h, add 6 times of water gagings, extract 0.5h for the 3rd time; The each filtration, merging filtrate, the volume of filtrating is concentrated into 500ml, filters promptly to get.
2.2 the preparation of tremella extract:
Take by weighing Tremella 22.3g, extract 2 times, add 10 times of water yields the 1st time, extract 1h, 4 times of water yields of the 2nd usefulness are extracted 1h, filter with 3 layers of gauze at every turn, and merging filtrate heats and is concentrated into 200ml, and is for use.
2.3 the preparation of Bulbus Lilii extracting solution:
Take by weighing Bulbus Lilii 20g, soak 0.5h, be heated to 100 ℃, decoct and extract 3 times, add 15 times of water gagings the 1st time; Extract 1h, add 10 times of water gagings the 2nd time, extract 1h, add 8 times of water gagings the 3rd time; Extract 1h, the each filtration, merging filtrate, the volume of filtrating are concentrated into 5 times (g/ml) of Pseudobulbus Bletillae (Rhizoma Bletillae) weight; Add amount of liquid 4% active carbon, 90 ℃ of heating in water bath stir, and sucking filtration is subsequent use.
2.4 the preparation of Herba Leonuri extract:
Take by weighing Herba Leonuri blade of grass 20.5g, soak 1h, be heated to 100 ℃, decoct and extract 3 times; Add 10 times of water gagings the 1st time, extract 1h, add 8 times of water gagings, extract 1h for the 2nd time; Add 5 times of water gagings the 3rd time, extract 1h, filter merging filtrate at every turn with 3 layers of gauze; Heating is concentrated into the 250ml of Herba Leonuri weight, filters with double gauze, and is subsequent use.
2.5 the preparation of Fructus Luffae extract:
Fresh Fructus Luffae peeling is thinly sliced and is weighed, and soaks 1h, is heated to 95 ℃; Decoct to extract 3 times, add 10 times of water gagings the 1st time, extract 0.8h, add 8 times of water gagings the 2nd time; Extract 0.8h, add 6 times of water gagings, extract 0.5h, for the 3rd time at every turn with 3 layers of gauzes filtration; Merging filtrate, heating is concentrated into 3 times (g/ml) of Herba Leonuri weight, filters with double gauze, and is for use.
2.6 the preparation of 100g emulsion
A) take by weighing the 0.9g Acritamer 940, be dissolved in the 200ml water, be stirred to rapidly evenly,,, leave standstill on one side, treat that its natural swelling dissolves 3h with the Glass rod crushing if any caking.Or promote the dissolving of its swelling, and connect beaker and put into 80 ℃ of water proof heating of water-bath, after the 25min swelling is complete, drip the 10% triethanolamine neutralization of 0.5ml, the limit edged stirs, and surveys pH value, when PH=7, is clear gel.
B) take by weighing from glyceryl monostearate 2.2g, stearic acid 1.4g, camellia seed oil 5g Semen Tritici aestivi germ oil 5g, vaseline 5g, squalane 0.8g and place evaporating dish on water-bath, to keep 85 ℃ of heating in water bath fusions of temperature, as oil phase.
C) take by weighing L-serine 0.055g and place beaker, add the 60g distilled water, be placed in the water-bath (keeping 85 ℃ of bath temperatures) limit heating edge and stir, quicken its dissolving, as water with glass plate.
D) the complete fusion of oil phase in the ware to be evaporated is poured the water in the beaker of equality of temperature in the evaporating dish in the oil phase, and the limit edged stirs 10min to same direction, and is liquid to being creamy white, and promptly gets substrate.From water-bath, take out and be chilled to room temperature.
E) treat substrate put cold after, add glycerol 3g, Tremella is carried 1g, Herba Leonuri extracting solution 1g, Bulbus Lilii extracting solution 1g, Rhizoma Bletillae extraction solution 1g, Fructus Luffae extracting solution 1g, sorbitol 1g, hyaluronate sodium 0.1g.
F) emulsion of e step gained is added swelling completely in the Acritamer 940 gel, add vitamin C 1g, after using citric acid to regulate pH value to be 6, stir 15min, mix homogeneously;
G) take by weighing disodiumedetate 0.006g, sorbic acid 0.3g adds 1 of 12ml, the 2-propylene glycol, and heating makes its dissolving, puts into f step institute antigalactic after waiting to dissolve, and mix homogeneously gets final product.
Embodiment 3:
The physical and chemical index of embodiment 1,2 is following:
3.1 character
This emulsion is creamy white, and denseness is suitable, slim and graceful water profit, and evenly fine and smooth, light is pale, and stretchability is good, abnormal smells from the patient is fragrant.
3.2PH value inspection
These article of getting, fixed with the PH instrumentation, recording pH value is between the 5-6.
3.3 caloric test
Emulsion is packaged in the transparent dressing article bottle, observed no lamination in one month in 4 ℃ refrigerator cold-storages.24h in 55 ℃ calorstat, emulsion does not have phenomenons such as layering emulsifying is spoiled.
3.4 centrifugal test
Emulsion is packaged in the centrifugal 20min of 3000r/min in the tool plug test tube, no lamination.
3.5 room temperature is placed experiment
Embodiment 1,2 made emulsions are placed bottle for cosmetics, and room temperature leaves standstill investigates 6 months, and no lamination is used the aftersensation no change, the abnormal smells from the patient no change.
3.6 irritation test, anaphylaxis experiment
The white mice back cuts off hair, and the emulsion of smearing respectively by embodiment 1,2 preparations compares in cutting plucked position and not being coated with the position, and the result does not have zest and anaphylaxis.
Get embodiment 1 gram and be applied on volunteer (15-65 year, the 250 people) gesture and facial expression, observe after spending 30 minutes, all do not occur rubescent, dermexanthesis, foaming phenomenon.
3.7 suppress the experiment of tryrosinase vigor in the mouse melanin cell
Emulsion by embodiment 1,2 preparations is got 1g respectively, difference adding distil water 40ml, diluted for use.With B
16Melanocyte is inoculated in 96 orifice plates, every hole 100 μ l, put in the incubator cultivate educate 24h after, add the emulsion diluent.Behind the drug effect 3d, discard the liquid that disappears, with pH 6.8 poly butylene succinates (PBS) flushing twice, every hole adds the PBS that 90 μ l contain 1% (volume fraction) TritonX-100.Ultrasonication in the ice bath, every hole add the L-DOPA (L-dopa) of 10 μ l 10mmol/L, hatch 60min for 37 ℃, the colorimetric in the 475nm place, and each hole absorbance is surveyed in the blank well zeroing.
Suppression ratio %=(1-drug group mean light absorbency value ÷ matched group mean light absorbency value) * 100%
3.8 suppress melanin compound experiment in the mouse melanin cell
Emulsion by embodiment 1,2 preparations is got 1g respectively, difference adding distil water 40ml, diluted for use.Will be from the B of mice
16Melanoma cells is with 1x10
5The density of individual/ml is inoculated in culture dish, at 37 ℃, 5%CO
2Condition under cultivate 2d.Abandon supernatant, add the emulsion diluent, behind the drug effect 3d, abandon supernatant, the PBS washing, every hole adds 0.5ml trypsin digestion cell 3min, and every hole adds 2m1 and keeps liquid termination digestion.Behind the piping and druming mixing, every kind of concentration is taken out 0.5ml and is done the cell counting.All the other cell suspension are abandoned supernatant with the centrifugal 5min of 2500r/min, in deposition, add NaOH solution, and heating makes the melanin dissolving, select the 490nm wavelength on enzyme-linked immunosorbent assay instrument, to survey absorbance.
Melanin synthesizes suppression ratio %=[1-(medicine hole absorbance ÷ medicine porocyte density) ÷ (control wells absorbance ÷ control wells cell density)] * 100%
3.7-3.8 experimental result is seen table 1:
Table 1 experimental result
| Embodiment 1 suppression ratio (%) | Embodiment 2 suppression ratio (%) | |
| The restraint of tyrosinase vigor | 58.9 | 59.1 |
| It is synthetic to suppress melanin | 65.7 | 68.5 |
Experiment shows that this emulsion has the restraint of tyrosinase vigor, suppresses melanic synthetic, explains that also this emulsion has whitening function.
Embodiment 4:
The whitening effect experiment
Estimate the whitening effect of embodiment 1,2 through experiment on probation.The emulsion and the commercially available whitening emulsion that utilize embodiment 1,2 to produce compare experiment.Choose 120 of 25-45 year women, utilize ultraviolet radiation device to cause the deposition of dermal melanin.Be divided into three groups to them arbitrarily.Every day, each twice usefulness emulsion was put arm on the skin sooner or later, and embodiment uses the emulsion of pressing embodiment 1 preparation for 1 group, and embodiment uses the emulsion of pressing embodiment 2 preparations for 2 groups, and matched group is smeared the commercially available tender Virgin's milk liquid of preserving moisture, and uses continuously two months.The improvement evaluation on the arm of the detecting by an unaided eye tender white effect of preserving moisture.This result sees table 2:
The tender white experimental result of table 2
| Effectively (people) | A little effectively (people) | Invalid (people) | Total effective rate (%) | |
| Embodiment 1 | 32 | 5 | 3 | 92.4 |
| Embodiment 2 | 34 | 4 | 2 | 95.0 |
| Matched group | 23 | 10 | 7 | 82.5 |
Embodiment 5:
This emulsion resultant effect is investigated
Below utilize the effect of feeling to estimate the emulsion that embodiment 1,2 produces on probation.Adopt the public-opinion poll point system, the women who chooses 80 20-50 year age bracket is object on probation, is divided into two groups arbitrarily, and the emulsion for preparing with embodiment 1,2 is respectively put arm on the skin.Use twice every day, two months service time.Each item result of use total points is 5 minutes: five are divided into best result, represent fine, very satisfied; 4 are divided into better; 3 are divided into and can accept; Be bad below 3 minutes, can not accept.It below is each item average.The result sees 3 tables:
Table 3 resultant effect is investigated
| Result of use | Embodiment 1 each item average | Embodiment 2 each item averages |
| Moisture retention | 4.8 | 4.9 |
| Nourishing property | 4.8 | 4.8 |
| Whitening property | 4.6 | 4.5 |
In sum, this made emulsion of the present invention have good moistly preserve moisture, skin care, the effect of whitening, flexible, pale with back skin.
Claims (8)
1. tender white elite emulsion that contains the natural component extract is characterized in that: contain following material and weight portion in the 100g emulsion:
2. a kind of tender Virgin's milk liquid that contains the natural component extract according to claim 1 is characterized in that: described Pseudobulbus Bletillae (Rhizoma Bletillae) extract is through following method preparation:
It is an amount of to take by weighing the Pseudobulbus Bletillae (Rhizoma Bletillae), soaks 0.15-1h, is heated to 90-100 ℃, decocts and extracts 3 times; Add 6-12 times of water gaging the 1st time, extract 0.5-2h, add 4-10 times of water gaging, extract 0.5-1.5h for the 2nd time; Add 3-8 times of water gaging the 3rd time, extract 0.5-1.5h, the each filtration; Merging filtrate, the volume of filtrating are concentrated into 3-6 times (g/ml) of Pseudobulbus Bletillae (Rhizoma Bletillae) weight, filter promptly to get.
3. a kind of tender Virgin's milk liquid that contains the natural component extract according to claim 1, it is characterized in that: described tremella extract prepares through following method:
It is an amount of to take by weighing Tremella, extracts 2 times, adds the 8-12 times of water yield the 1st time, extracts 0.5-1.5h, extracts 0.5-1.5h h with the 3-5 times of water yield the 2nd time, filter with 3 layers of gauze at every turn, and merging filtrate, heating is concentrated into 2-10 times (g/ml) of Tremella weight, gets final product.
4. a kind of tender Virgin's milk liquid that contains the natural component extract according to claim 1, it is characterized in that: described Bulbus Lilii extracting solution prepares through following method:
It is an amount of to take by weighing Bulbus Lilii, soaks 0.5-1h, is heated to 90-100 ℃, decocts and extracts 3 times, adds 10-15 times of water gaging the 1st time; Extract 0.5-2h, add 8-12 times of water gaging the 2nd time, extract 0.5-1.5h, add 6-10 times of water gaging the 3rd time; Extract 0.5-1.5h, the each filtration, merging filtrate, the volume of filtrating are concentrated into 4-7 times (g/ml) of Pseudobulbus Bletillae (Rhizoma Bletillae) weight; Add liquid weight 1%-5% active carbon, 80-100 ℃ of heating in water bath stirs, and sucking filtration gets final product.
5. a kind of tender Virgin's milk liquid that contains the natural component extract according to claim 1, it is characterized in that: described Herba Leonuri extract prepares through following method:
It is an amount of to take by weighing Herba Leonuri, soaks 0.15-1.5h, is heated to 90-100 ℃, decocts and extracts 3 times; Add 6-15 times of water gaging the 1st time, extract 0.5-1.5h, add 4-10 times of water gaging, extract 0.5-1.5h for the 2nd time; Add 4-8 times of water gaging the 3rd time, extract 1h, filter merging filtrate at every turn with 3 layers of gauze; Heating is concentrated into 2-10 times (g/ml) of Herba Leonuri weight, filters with double gauze, gets final product.
6. a kind of tender Virgin's milk liquid that contains the natural component extract according to claim 1, it is characterized in that: described Fructus Luffae extract prepares through following method:
Fresh Fructus Luffae peeling is thinly sliced, and weighs, and soaks 0.15-1.5h, is heated to 90-100 ℃; Decoct to extract 3 times, add 6-15 times of water gaging the 1st time, extract 0.25-1.5h, add 5-14 times of water gaging the 2nd time; Extract 0.25-1.5h, add 4-12 times of water gaging, extract 0.25-1h, for the 3rd time at every turn with 3 layers of gauzes filtration; Merging filtrate, heating are concentrated into 2-5 times (g/ml) of Herba Leonuri weight, filter with double gauze, get final product.
7. a kind of tender Virgin's milk liquid that contains the natural component extract according to claim 1, it is characterized in that: described essence is rose essence, green cucumber essence, Bulbus Lilii essence, honey peach essence, osmanthus flower fragrance, flavoring pineapple essence, Fructus Citri Limoniae essence.
8. the described a kind of method for preparing that contains the tender Virgin's milk liquid of natural component extract of claim 1 is characterized in that:
A) take by weighing the 0.1-10g Acritamer 940, be dissolved in the 150-350ml water, stir; Leave standstill and treated its natural swelling dissolving in 2-3 hour; Be heated to 80-90 ℃, be incubated 10-30 minute, after swelling is complete; When 5%-15% (weight concentration) triethanolamine that drips 0.05-1ml is neutralized to PH and is 5-7, get final product;
B) take by weighing glyceryl monostearate 1-8g, stearic acid 1-5g, camellia seed oil 2-10g, Semen Tritici aestivi germ oil 2-10g, vaseline 2-15g, squalane 0.2-5g, be warming up to 80-90 ℃, make its complete fusion, obtain oil phase;
C) take by weighing L-serine 0.010-0.100g and place beaker, add the 50-80g distilled water, be warming up to 80-90 ℃, make its dissolving, obtain water;
D) treat the complete fusion of oil phase, water poured in the oil phase that the limit edged stirs 10-15min to same direction, to being even milky white liquid shape, promptly gets substrate, is chilled to room temperature;
E) treat substrate put cold after, add glycerol 1-10g, tremella extract 0.5-5g, Herba Leonuri extracting solution 0.5-5g, Bulbus Lilii extracting solution 0.5-5g, Rhizoma Bletillae extraction solution 0.5-5g, Fructus Luffae extracting solution 0.5-5g, sorbitol 0.1-1g, hyaluronate sodium 0.01-0.20g;
F) emulsion of e step gained is added swelling completely in the Acritamer 940 gel, adds vitamin C 0.1-1g, uses citric acid regulate pH value as 5-7 after, stirring 10-15min, mix homogeneously;
G) take by weighing disodiumedetate 0.001-0.007g g, methyl hydroxybenzoate or sorbic acid 0.1-0.3g add 2-12ml 1, the 2-propylene glycol, and heating makes its dissolving, puts into f step institute antigalactic after waiting to dissolve, and mix homogeneously gets final product.
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