CN103565730B - A kind of scented tea body whitening crème and manufacture method thereof - Google Patents
A kind of scented tea body whitening crème and manufacture method thereof Download PDFInfo
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Abstract
The present invention discloses a kind of scented tea body whitening crème and manufacture method thereof.This scented tea body whitening crème comprises plurality of Chinese whitening composition, multiple biochemical whitening composition and by the whitening composition extracted in scented tea, green tea, protectiveness composition and basic material etc.Wherein Chinese medicine, scented tea whitening effect and protectiveness composition are formed by self-controls such as Radix Glycyrrhizae, the Pseudobulbus Bletillae (Rhizoma Bletillae), the Rhizoma Atractylodis Macrocephalae, Poria, Radix Ampelopsis, the Radix Paeoniae Alba, Flos Rosae Rugosae, Flos Moutan, Flos Mume.Biochemical whitening composition is outsourcing Ascorbyl Tetraisopalmitate and amine acid whitening agent, and basic material is 16 mixed alcohols, Jojoba oil, amino acid humectant, Sargassum rock polysaccharide, 16 stearyl alcohol and 16 octadecyl glucosides etc.These whitening compositions and anti-oxidation protection composition after balanced collocation, scientific composition, just can obtain both safe and reliable with preserving moisture and protecting skin basic ingredient, the novel scented tea body whitening crème product that effect is lasting again.
Description
Technical field
The present invention relates to a kind of body whitening crème and the manufacture method thereof that contain scented tea green tea composition, belong to cosmetics and skincare product technical field.
Background technology
Along with the development of society and the raising of living standard, people more and more pay attention to the beauty of appearance outward appearance.Due to the impact of all factors, some women that like to be beautiful can be caused, be difficult to have white-skinned skin, the appearance that water is tender.Cause the reason of this intensely dark dry hydropenia skin quality a lot, as geneogenous inherited genetic factors, subhealth state factor posteriority, disease factor, dietary factor, environmental factors etc.Especially for the women entering person in middle and old age's age bracket, the accumulation of various vivo and vitro problem, easier embody in face gloomy unglazed, the situation of shriveling hydropenia.Therefore believing in the Chinese society of " a white screening hundred is ugly ", the healthy whitening problem of women is a cosmetic problem received much attention always.But for a long time, due to whitening phychology anxious for success and eager for instant success and quick profits product design, make many whitening class skin care item move towards serious mistaken ideas, major embodiment in the following areas: (one), for the purpose of pursuing and bleaching fast, has departed from the track of self-sow rule and scientific law gradually; (2) to damage skin health for cost, to obtain temporary transient whiteness of skin; (3) whitening product that toxic and side effects is larger allows skin produce dependency more, and is absorbed in vicious cycle state.Especially the whitening class skin care item of specialized beauty parlors use, have in order to eager for instant success and quick profits object, do not stint use can cause accumulate property poisoning mercurial (i.e. heavy metal) and cause skin to rely on hormones as additive, this be moved towards infringement skin mistaken ideas.Paying the cost that skin long-term poisoning is impaired in order to skin whitening, is unworthy really.Therefore in recent years, safety whitening and skin-protecting product gradually be familiar with by farsighted women and accept, but skin-whitening is a complicated system engineering, influence factor is a lot, although some Skin whitening care cosmeticses are safe and reliable, but slow or invalid to some crowds owing to taking effect, finally cause product without market, this situation is also worthless.As can be seen here, how choose reasonable and science collocation whitening and skin-protecting raw material and additive under the major premise ensureing product safety, makes final products not only safety but also effectively, this developing direction that will be current and following whitening class skin care item.
Traditional safety whitening and skin-protecting product, some effects are slow, and what have is invalid.Or when bringing into use effectively, after life-time service, effect declines.Trace it to its cause, may there is following aspect: (one) whitening composition is more single, the person that suits the medicine to the illness uses effectively, and do not suit the medicine to the illness person, then invalid.(2) impact of other factors makes product effect decline.(3) skin produces " resistance " to after certain whitening agent of life-time service.Visible, adopt the mentality of designing of single whitening agent in traditional whitening and skin-protecting product, there is many defectives.Obviously cannot tackle complicated mechanism as " controlling all kinds of diseases and ailments with a medicine ", " melanin formation engineering " that influence factor is numerous, the effect of skin whitening is also difficult to permanent and satisfactory.
The present invention is directed to the defect of current whitening and skin-protecting product and the complexity feature of dermal melanin forming process, strive seeking breakthrough in the equilibrium collocation and Synergistic of white-skinned face function raw material.Under the prerequisite ensureing safety first, whitening in whitening composition in Chinese medicine, the whitening composition in biogenetic products, teas product and synergistic component etc. are organically combined, reach comprehensive, multipath tackles melanic product design, to reaching whitening skin and preserving moisture effect safely and effectively to greatest extent.
Summary of the invention
In numerous whitening and skin-protecting raw materials, derive from the whitening composition of plant (as Chinese herbal medicine etc.) extract, have the permanent effect of safe slow more; And the whitening composition of biochemical synthesis, then there is high, the effective fast feature of concentration; In the extract of the teas such as green tea, scented tea product, then containing multiple whitening composition and protectiveness composition.Use the whitening and skin-protecting composition in multiple source, deal with the gloomy problem of skin, then can reach and learn from other's strong points to offset one's weaknesses, the whitening skin and preserving moisture effect of Synergistic.Therefore primary and foremost purpose of the present invention be provide a kind of by multiple whitening and skin-protecting balanced composition collocation, Synergistic, effect for a long time, scented tea body whitening crème safely and effectively.Effective in controlling to what reach the intensely dark problem of numerous female skin, the effect of the lasting whitening and softening skin that secures good health.Another object of the present invention is to provide above-mentioned plant (i.e. Chinese herbal medicine), the preparation method of scented tea extract and the preparation method of final scented tea body whitening crème.
For achieving the above object, the technical solution used in the present invention is as follows:
Scented tea body whitening crème of the present invention, is prepared from by following component:
(1) oil phase component: described oil phase component is made up of the component of following mass parts: 16 mixed alcohol 1-1.5 parts, 16 stearyl alcohol and 16 octadecyl glucoside 2-4 parts, tristerin (with) PEG-100 stearate 1-3 part, iso-octyl palmitate 2-4 part, Jojoba oil 2-4 part, Semen Tritici aestivi germ oil 1-2 part, white oil 2-4 part, Camellia oil 0.5-1 part, dimethicone 2-4 part, methyl hydroxybenzoate 0.2-0.3 part, propylparaben 0.1-0.15 part, ditertbutylparacresol 0.03-0.05 part, biochemical whitening agent Ascorbyl Tetraisopalmitate 2-3 part, VE oil 0.5 part,
(2) water phase components: glycerol 5-8 part, amino acid humectant 2-3 part, Sargassum rock polysaccharide 2-4 part, amine acid whitening agent 1-2 part, green tea extractive liquor 1-2 part, Chinese medicine scented tea constituents extraction liquid 59-62 part; The raw material of described Chinese medicine scented tea constituents extraction liquid mainly following mass parts is made: Radix Glycyrrhizae 5-10 part, Rhizoma Atractylodis Macrocephalae 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 5-10 part, Radix Paeoniae Alba 5-10 part, Poria 5-10 part, Radix Ampelopsis 5-10 part, Flos Rosae Rugosae 3-5 part, Flos Moutan 3-5 part, Flos Mume 3-5 part;
(3) co-emulsifier: hydroxyethylacrylate/sodium acryloyldimethyl taurate copolymers 0.3-0.5 part;
(4) antiseptic: mixture 0.1-0.15 part of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol;
(5) essence: floral perfume 0.01-0.02 part;
The preparation method of scented tea body whitening crème of the present invention, comprises the steps:
(1) preparation of oil phase part: by 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, tristerin (with) PEG-100 stearate, iso-octyl palmitate, Jojoba oil, Semen Tritici aestivi germ oil, white oil, Camellia oil, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol, after taking in proportion, add with in the rustless steel still stirred, under the stirring of rotating speed 20-30 revs/min, heating for dissolving is complete, and at 75-80 DEG C of temperature constant temperature disinfection 20 minutes, the VE oil of formula ratio and biochemical whitening agent Ascorbyl Tetraisopalmitate is added before emulsifying, stir, stand-by,
(2) preparation of aqueous portion: by the glycerol of formula ratio, amino acid humectant, Sargassum rock polysaccharide, amine acid whitening agent, green tea extractive liquor, Chinese medicine scented tea constituents extraction liquid, after taking in proportion, first heating for dissolving in stainless steel cask, be extracted in (passing through filter screen) rustless steel homogenizing still afterwards, under the stirring of 20-30 revs/min, continue to be heated to 75--80 DEG C, and constant temperature disinfection 20 minutes, stand-by;
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 40-50 revs/min, stirs after 2-3 minutes, starts high speed homogenization device, homogenizing 3-5 minutes under the high speed of 3000-5000 revs/min, wall rotating speed will be scraped afterwards and drop to 30-40 revs/min, and be cooled to 40 DEG C under this rotating speed, add the co-emulsifier of formula ratio, antiseptic, essence, continue to stir 15-20 minutes under same rotating speed, get final product discharging.
Described Chinese medicine scented tea constituents extraction liquid prepares by the following method:
(1) take dry product Radix Glycyrrhizae 5-10 part, Rhizoma Atractylodis Macrocephalae 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 5-10 part, Radix Paeoniae Alba 5-10 part, Poria 5-10 part, Radix Ampelopsis 5-10 part, Flos Rosae Rugosae 3-5 part, Flos Moutan 3-5 part, Flos Mume 3-5 part, add in rustless steel still;
(2), when first time boils, deionized water 800-900 parts is taken, ethanol 4-6 parts, propylene glycol 4-6 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.0-1.2 hours, namely obtain Chinese medicine scented tea constituents extraction liquid 1. with 600 order filter-cloth filterings afterwards;
(3) in filtering residue, add the propylene glycol of the deionized water of 400-500 mass parts and the ethanol of 1-3 mass parts and 1-3 mass parts, use little fire after big fire is boiled instead and boil 0.8-1.0 hours again, use 600 order filter-cloth filterings afterwards, obtain Chinese medicine scented tea constituents extraction liquid 2.;
(4) will 1., 2. namely obtain final Chinese medicine scented tea constituents extraction liquid after filtrate mix homogeneously, its total amount should control about the half of adding total Water.
The present invention is directed to current environmental pollution serious, skin sub-health status, the reality that even damage situations is more, according to known melanin formation mechenism, add following green tea, scented tea extracting solution, biochemical whitening agent, Chinese medicine whitening composition, skin care moisturizing ingredient etc., make there is whitening and softening skin, improve skin quality, the body whitening crème product of preserving moisture and protecting skin effect.
Flos Rosae Rugosae: looks improving and the skin nourishing effect is remarkable, offsets removing freckle, wrinkle effect is obvious, resolving depression of regulating the flow of vital energy, promoting blood circulation to remove blood stasis, improves withered skin, blood circulation promoting and metabolism.
Flos Moutan: looks improving and the skin nourishing, functions of removing chloasma, slow down aging, the regulating liver-QI that nourishes blood, loose strongly fragrant blood stasis dispelling, can make that QI and blood is abundant, appearance is ruddy, energetic.
Flos Mume: control chloasma that endocrine regulation causes, chloasma hepaticum, skin sore be evident in efficacy, enrich blood, pathogenic fire reducing, strengthening the spleen and stomach, the meridian dredging, antiinflammatory, external makes skin become delicate ruddy.
Green tea extract: green tea is azymic tea, its characteristic determines it and more saves natural material in fresh leaf.Wherein, tea polyphenols, caffeine save more than 85% of fresh leaf, and chlorophyll saves about 50%, and vitamin loss is also less, also have lipopolysaccharide, theanine isoreactivity material.Tea polyphenols in green tea has very strong antioxidation, its oxidation resistance be synthetic antioxidant BHT, 4-6 times of BHA, being 6-7 times of vitamin E, is ascorbic 5-10 times.It is the scavenger of human free radical.Research proof 1 milligram of tea polyphenols is removed and is equivalent to 9 microgram superoxide dismutase to the usefulness of the excessive free radicals that people's human body is harmful to, and is much higher than other allied substances.Tea polyphenols has the effect blocking lipid peroxidation, scavenging capacity enzyme, and its anti-aging effects is stronger than vitamin E 18 times.Tea polyphenols is water-soluble substances, with it wash one's face can remove face greasy, convergence pore, has ultraviolet radiation in sterilization, sterilizing, resisting age of skin, minimizing daylight and computer, TV radiation to the injury of skin.Its stronger antioxidation contributes to the stable of other whitening active ingredients in formula.
The different Palmic acid acid esters of biochemical whitening agent ascorbic acid four: the derivant being fat soluble vitamin C, is easily absorbed by the skin, and also has good stability, not only can skin whitening, also has similar SOD active, Scavenger of ROS, promotes collagen protein synthesis.The mechanism of vitamin C derivatives skin whitening intermediate---the DOPA quinone mainly in vat black pigment generative process, plays inhibited oxidation chain, reduces the effect that melanin generates.But well-known, the problem that the equal existence and stability of vitamin C derivatives class is difficult lasting, with green tea extract, scented tea extract, VE wet goods with the use of, Synergistic and lasting whitening effect can be reached.
Amine acid whitening agent: i.e. hydroxyethylamino butanoic acid, its mechanism of action accelerates renewal and the metabolism of tegumentary chromatophore group, thus slow down melanin go to and productive set at epiderm skin, reach the effect of skin whitening.
Radix Glycyrrhizae: be Chinese medicine, interior contained licoflavone has restraint of tyrosinase activity, suppresses the multiple action of dopachrome interconvertible enzyme and DHICA oxidase active, can reach good whitening effect.Also has scavenging activated oxygen, the effects such as antioxidation.In Radix Glycyrrhizae, contained glycyrrhizic acid and glycyrrhetate, also have the effect of antiinflammatory, antiallergic action.
Poria: sweet in the mouth, light, property be flat, can dispelling speckles and whitening face, moist skin, can also strengthen immunologic function, blood vessel dilating." Bencao Pinhui Jingyao " is said: " Poria for end, close honey and, flush coat is treated acne vulgaris and the black bleb of puerpera, as Ovum passeris ".
The Pseudobulbus Bletillae (Rhizoma Bletillae): materials for skin whiting for removing freckle, astringing to arrest bleeding, detumescence and promoting granulation.It is exactly good medicine of improving looks that the Pseudobulbus Bletillae (Rhizoma Bletillae) is controlled oneself, and is described as " whitening fairy maiden ", can the dermatosis such as Acne treatment, tinea corporis, cicatrix." property of medicine opinion " cloud: " it can control skin ulcer on face, makes us flesh and slides ".Compendium of Material Medica cloud its " black, speckle dispelling of washing one's face ".
The Radix Paeoniae Alba: sweet in the mouth, acid, cold nature, has the effect of nourishing blood, and can treat shallow complexion, facial colour spot, tarnish.
The Rhizoma Atractylodis Macrocephalae: bitter, sweet, warm.Return spleen, stomach warp.There is air making-up and spleen enlivening, dampness diuretic, hidroschesis, antiabortive effect.Also has whitening and skin-protecting effect.The traditional Chinese medical science is thought, whether the skin of people has substantial connection with function if pleasing pool, if internal organs pathological changes, and disharmony between QI and blood, then pachylosis, the raw speckle of face.Three plain soups that Ming Dynasty's (16th century) medical literature " Elementary Medicine " records: namely the Radix Paeoniae Alba, the Rhizoma Atractylodis Macrocephalae, Poria and Radix Glycyrrhizae are made.From QI and blood regulating, the function of conditioning the five internal organs is started with, thus reaches the effect of whitening and speckle dispelling,
Radix Ampelopsis: nature and flavor: bitter sweet pungent, cool.Essentials of Matea Medica cloud: energy pathogenic fire purging, eliminating stagnation.Hardship can be let out, and pungent energy falls apart, Gan Nenghuan, cold energy heat extraction.Kill fire-toxin, eliminating stagnation gas, granulation promoting pain relieving.Control that carbuncle skin ulcer is swollen, skin ulcer, incised wound flutter damage on face.
In the market still not by multiple whitening composition, tea extract, Chinese medicine extract and the skin care moisturizing composition that wets carries out equilibrium collocation, has complementary advantages, after scientific formula, and the not only safety developed but also efficiently scented tea body whitening crème product.
The invention has the beneficial effects as follows: the whitening conditioning reason composition in biochemical whitening composition and Chinese medicine and the whitening, antioxidant content etc. in green tea scented tea are organically combined, and functionally carry out equilibrium collocation, learn from other's strong points to offset one's weaknesses, to ensure to be issued to efficient whitening and moistening skin effect in the prerequisite be perfectly safe.As everyone knows, skin-whitening problem, not only complicated mechanism, cycle are longer, and influence factor is numerous.Therefore how more scientific, rationally, enduringly given play to various whitening active thing effect; just certainly exist a balanced collocation; mutually promote and potentiation protection problem; the shelf-life of general whitening and moistening skin class cosmetics is 3 years; within so long period; how to keep and to strengthen the whitening effect of each whitening active ingredients; the method of the multiple compound protection compositions such as interpolation green tea extract of the present invention, scented tea extract, VE oil and BHT; reach the ideal effect of expection; not only whitening and moistening skin effect is remarkable; it is and effect is lasting, without any side effects.
Detailed description of the invention
Embodiment 1
(1) preparation process of special ratios Chinese medicine scented tea constituents extraction liquid is as follows:
(1) 5 parts, dry product Radix Glycyrrhizae is taken, the Rhizoma Atractylodis Macrocephalae 7.5 parts, the Pseudobulbus Bletillae (Rhizoma Bletillae) 10 parts, the Radix Paeoniae Alba 5 parts, Poria 7.5 parts, Radix Ampelopsis 10 parts, Flos Rosae Rugosae 5 parts, Flos Moutan 3 parts, Flos Mume 4 parts. add in rustless steel still;
(2), when first time boils, deionized water 800 parts is taken, ethanol 4 parts, propylene glycol 4 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.0-1.2 hours, namely obtain Chinese medicine scented tea constituents extraction liquid 1. with 600 order filter-cloth filterings afterwards.
(3) in filtering residue, add the propylene glycol of the deionized water of 500 mass parts and the ethanol of 3 mass parts and 3 mass parts, use little fire after big fire is boiled instead and boil 0.8-1.0 hours again, use 600 order filter-cloth filterings afterwards, obtain Chinese medicine scented tea constituents extraction liquid 2..
(4) will 1., 2. namely obtain final Chinese medicine ingredients extracting solution after filtrate mix homogeneously, its total amount should control about the half of adding total Water.
(2) substitute the pure water component in scented tea body whitening crème with obtained Chinese medicine scented tea constituents extraction liquid, the prescription designing scented tea body whitening crème by following proportioning (mass percent) is as follows:
A: oil phase component: 16 mixed alcohols 1 part, 16 stearyl alcohol and 16 octadecyl glucosides 2 parts, tristerin (with) PEG-100 stearate 2 parts, iso-octyl palmitate 3 parts, Jojoba oil 3 parts, Semen Tritici aestivi germ oil 1.5 parts, white oil 3 parts, Camellia oil 1 part, dimethicone 3 parts, methyl hydroxybenzoate 0.2 part, propylparaben 0.1 part, ditertbutylparacresol 0.03 part;
B:VE oil 0.5 part and biochemical whitening agent Ascorbyl Tetraisopalmitate 2 parts;
C: the preparation of aqueous portion: by glycerol 7 parts, amino acid humectant 3 parts, Sargassum rock polysaccharide 3 parts, amine acid whitening agent 2 parts, green tea extractive liquor 1.0 parts, Chinese medicine ingredients extracting solution 61.26 parts;
D: co-emulsifier: hydroxyethylacrylate/sodium acryloyldimethyl taurate copolymers 0.3 part;
E: antiseptic: 0.1 part, the mixture of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol;
F: essence: floral perfume 0.01 part;
(3) preparation process of scented tea body whitening crème is as follows:
(1) take A phase component with stainless steel cask, after taking in proportion, add with in the rustless steel still stirred, under the stirring of rotating speed 30 revs/min, heating for dissolving is complete, and at 80 DEG C of temperature constant temperature disinfection 20 minutes, add B phase component before emulsifying, stir, stand-by.
(2) to take after C phase component heating for dissolving in suction emulsifying kettle with stainless steel cask, under the stirring of 30 revs/min, continue to be heated to 80 DEG C, and constant temperature disinfection 20 minutes, stand-by.
(3) by oil phase A slowly suction aqueous phase C, and scrape wall stirring, rotating speed is increased to 50 revs/min, stir after 3 minutes, start high speed homogenization device, homogenizing 4 minutes under the high speed of 5000 revs/min, wall rotating speed will be scraped afterwards and drop to 30 revs/min, and be cooled to 40 DEG C under this rotating speed.
(4) add D, E, F phase, continue to stir under same rotating speed to get final product discharging in 15 minutes.
Embodiment 2
(1) preparation process of special ratios Chinese medicine scented tea constituents extraction liquid is as follows:
(1) 7.5 parts, dry product Radix Glycyrrhizae is taken, the Rhizoma Atractylodis Macrocephalae 10 parts, the Pseudobulbus Bletillae (Rhizoma Bletillae) 5 parts, the Radix Paeoniae Alba 7.5 parts, Poria 10 parts, Radix Ampelopsis 5 parts, Flos Rosae Rugosae 4 parts, Flos Moutan 3 parts, Flos Mume 5 parts. add in rustless steel still;
(2) first time is when boiling, and take deionized water 850 parts, ethanol 5 parts, propylene glycol 5 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.0-1.2 hours, namely obtain Chinese medicine ingredients extracting solution 1. with 600 order filter-cloth filterings afterwards.
(3) in filtering residue, add the propylene glycol of the deionized water of 450 mass parts and the ethanol of 2 mass parts and 2 mass parts, use little fire after big fire is boiled instead and boil 0.8-1.0 hours again, use 600 order filter-cloth filterings afterwards, obtain Chinese medicine ingredients extracting solution 2..
(4) will 1., 2. namely obtain final Chinese medicine scented tea constituents extraction liquid after filtrate mix homogeneously, its total amount should control about the half of adding total Water.
(2) substitute the pure water component in scented tea body whitening crème with obtained Chinese medicine scented tea constituents extraction liquid, the prescription designing scented tea body whitening crème by following proportioning (mass percent) is as follows:
A: oil phase component: 16 mixed alcohols 1.5 parts, 16 stearyl alcohol and 16 octadecyl glucosides 3 parts, tristerin (with) PEG-100 stearate 2 parts, iso-octyl palmitate 2 parts, Jojoba oil 4 parts, Semen Tritici aestivi germ oil 1 part, white oil 3.5 parts, Camellia oil 0.5 part, dimethicone 3 parts, methyl hydroxybenzoate 0.2 part, propylparaben 0.1 part, ditertbutylparacresol 0.03 part;
B:VE oil 0.5 part and biochemical whitening agent Ascorbyl Tetraisopalmitate 3 parts;
C: the preparation of aqueous portion: by glycerol 8 parts, amino acid humectant 2.5 parts, Sargassum rock polysaccharide 2 parts, amine acid whitening agent 1 part, green tea extractive liquor 2 parts, Chinese medicine scented tea constituents extraction liquid 59.66 parts;
D: co-emulsifier: hydroxyethylacrylate/sodium acryloyldimethyl taurate copolymers 0.4 part;
E: antiseptic: 0.1 part, the mixture of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol;
F: essence: floral perfume 0.01 part.
(3) preparation process of scented tea body whitening crème is as follows:
(1) take A phase component with stainless steel cask, after taking in proportion, add with in the rustless steel still stirred, under the stirring of rotating speed 25 revs/min, heating for dissolving is complete, and at 80 DEG C of temperature constant temperature disinfection 20 minutes, add B phase component before emulsifying, stir, stand-by.
(2) to take after C phase component heating for dissolving in suction emulsifying kettle with stainless steel cask, under the stirring of 25 revs/min, continue to be heated to 80 DEG C, and constant temperature disinfection 20 minutes, stand-by.
(3) by oil phase A slowly suction aqueous phase C, and scrape wall stirring, rotating speed is increased to 50 revs/min, stir after 3 minutes, start high speed homogenization device, homogenizing 5 minutes under the high speed of 4500 revs/min, wall rotating speed will be scraped afterwards and drop to 30 revs/min, and be cooled to 40 DEG C under this rotating speed.
(4) add D, E, F phase, continue to stir under same rotating speed to get final product discharging in 20 minutes.
Embodiment 3
(1) preparation process of special ratios Chinese medicine scented tea constituents extraction liquid is as follows:
(1) take 10 parts, dry product Radix Glycyrrhizae, the Rhizoma Atractylodis Macrocephalae 5 parts, the Pseudobulbus Bletillae (Rhizoma Bletillae) 7.5 parts, the Radix Paeoniae Alba 10 parts, Poria 5 parts, Radix Ampelopsis 7.5 parts, Flos Rosae Rugosae 3 parts, Flos Moutan 5 parts, Flos Mume 3 parts, add in rustless steel still;
(2) first time is when boiling, and take deionized water 900 parts, ethanol 6 parts, propylene glycol 6 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.0-1.2 hours, namely obtain Chinese medicine ingredients extracting solution 1. with 600 order filter-cloth filterings afterwards.
(3) in filtering residue, add the propylene glycol of the deionized water of 400 mass parts and the ethanol of 1 mass parts and 1 mass parts, use little fire after big fire is boiled instead and boil 0.8-1.0 hours again, use 600 order filter-cloth filterings afterwards, obtain Chinese medicine scented tea constituents extraction liquid 2..
(4) will 1., 2. namely obtain final Chinese medicine scented tea constituents extraction liquid after filtrate mix homogeneously, its total amount should control about the half of adding total Water.
(2) substitute the pure water component in scented tea body whitening crème with obtained Chinese medicine scented tea constituents extraction liquid, the prescription designing scented tea body whitening crème by following proportioning (mass percent) is as follows:
A: oil phase component: 16 mixed alcohols 1.2 parts, 16 stearyl alcohol and 16 octadecyl glucosides 2.5 parts, tristerin (with) PEG-100 stearate 2.5 parts, iso-octyl palmitate 2.5 parts, Jojoba oil 2 parts, Semen Tritici aestivi germ oil 2 parts, white oil 3.5 parts, Camellia oil 1 part, dimethicone 2 parts, methyl hydroxybenzoate 0.2 part, propylparaben 0.1 part, ditertbutylparacresol 0.03 part;
B:VE oil 0.5 part and biochemical whitening agent Ascorbyl Tetraisopalmitate 2.5 parts;
C: the preparation of aqueous portion: by glycerol 6 parts, amino acid humectant 3 parts, Sargassum rock polysaccharide 4 parts, amine acid whitening agent 1.5 parts, green tea extractive liquor 1.5 parts, Chinese medicine ingredients extracting solution 61.06 parts;
D: co-emulsifier: hydroxyethylacrylate/sodium acryloyldimethyl taurate copolymers 0.3 part;
E: antiseptic: 0.1 part, the mixture of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol;
F: essence: floral perfume 0.01 part.
(3) preparation process of scented tea body whitening crème is as follows:
(1) take A phase component with stainless steel cask, after taking in proportion, add with in the rustless steel still stirred, under the stirring of rotating speed 30 revs/min, heating for dissolving is complete, and at 80 DEG C of temperature constant temperature disinfection 20 minutes, add B phase component before emulsifying, stir, stand-by.
(2) to take after C phase component heating for dissolving in suction emulsifying kettle with stainless steel cask, under the stirring of 30 revs/min, continue to be heated to 80 DEG C, and constant temperature disinfection 20 minutes, stand-by.
(3) by oil phase A slowly suction aqueous phase C, and scrape wall stirring, rotating speed is increased to 50 revs/min, stir after 3 minutes, start high speed homogenization device, homogenizing 4 minutes under the high speed of 4800 revs/min, wall rotating speed will be scraped afterwards and drop to 30 revs/min, and be cooled to 40 DEG C under this rotating speed.
(4) add D, E, F phase, continue to stir under same rotating speed to get final product discharging in 20 minutes.
Effect example:
Detection method:
Suppress melanin genesis test in mouse melanin cell.
By B16 mouse melanin tumor cell with 1 × 10
5the density of individual/ml is connected to the culture dish that diameter is 9cm, at 37 DEG C ﹑ 5%CO
2condition under cultivate 2 days, abandon supernatant, add the sample solution 18-22ml after filtration sterilization, then cultivate 3 days, abandon supernatant, PBS washs, every hole adds the trypsin solution peptic cell 3min of 0.5ml mass percent 0.2%, every ware adds 2ml maintenance medium and stops digestion. after piping and druming mixing, often kind of concentration is taken out 0.5ml and is made cell counting. and all the other cell suspension, with the centrifugal 5min of 2500r/min, abandon supernatant, in precipitation, add NaoH solution, heating makes melanin dissolve, and selects the enzyme-linked immunosorbent assay instrument of 490nm wavelength surveys absorbance.
B16 cell suppression ratio=(1-(medicine hole absorbance+medicine porocyte density)+(control wells absorbance+control wells cell density)) × 100%.
Suppress melanin genesis test in mouse melanin cell, result is as shown in table 1
Table 1
| Suppression ratio (%) | |
| Embodiment 1 | 61．3 |
| Embodiment 2 | 62．9 |
| Embodiment 3 | 60．7 |
Above-mentioned experimental result shows, scented tea body whitening crème of the present invention can effectively generate by check melanin, and Be very effective.
Above-described embodiment is the present invention's preferably embodiment; but embodiments of the present invention are not restricted to the described embodiments; the Gai Bian ﹑ Xiu Shi ﹑ Ti Dai ﹑ Zu He ﹑ done under other any does not deviate from spirit of the present invention and principle simplifies; all should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (1)
1. a scented tea body whitening crème, is characterized in that being prepared from by following component:
(1) oil phase component: described oil phase component is made up of the component of following mass parts: 16 mixed alcohol 1-1.5 parts, 16 stearyl alcohol and 16 octadecyl glucoside 2-4 parts, tristerin/PEG-100 stearate 1-3 part, iso-octyl palmitate 2-4 part, Jojoba oil 2-4 part, Semen Tritici aestivi germ oil 1-2 part, white oil 2-4 part, Camellia oil 0.5-1 part, dimethicone 2-4 part, methyl hydroxybenzoate 0.2-0.3 part, propylparaben 0.1-0.15 part, ditertbutylparacresol 0.03-0.05 part, biochemical whitening agent Ascorbyl Tetraisopalmitate 2-3 part, VE oil 0.5 part,
(2) water phase components: glycerol 5-8 part, amino acid humectant 2-3 part, Sargassum rock polysaccharide 2-4 part, amine acid whitening agent 1-2 part, green tea extractive liquor 1-2 part, Chinese medicine scented tea constituents extraction liquid 59-62 part; The raw material of described Chinese medicine scented tea constituents extraction liquid mainly following mass parts is made: Radix Glycyrrhizae 5-10 part, Rhizoma Atractylodis Macrocephalae 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 5-10 part, Radix Paeoniae Alba 5-10 part, Poria 5-10 part, Radix Ampelopsis 5-10 part, Flos Rosae Rugosae 3-5 part, Flos Moutan 3-5 part, Flos Mume 3-5 part;
(3) co-emulsifier: hydroxyethylacrylate/sodium acryloyldimethyl taurate copolymers 0.3-0.5 part;
(4) antiseptic: mixture 0.1-0.15 part of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol;
(5) essence: floral perfume 0.01-0.02 part;
Its preparation method comprises the steps:
(1) preparation of oil phase part: by 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, tristerin/PEG-100 stearate, iso-octyl palmitate, Jojoba oil, Semen Tritici aestivi germ oil, white oil, Camellia oil, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol, after taking in proportion, add with in the rustless steel still stirred, under the stirring of rotating speed 20-30 rev/min, heating for dissolving is complete, and at 75-80 DEG C of temperature constant temperature disinfection 20 minutes, the VE oil of formula ratio and biochemical whitening agent Ascorbyl Tetraisopalmitate is added before emulsifying, stir, stand-by,
(2) preparation of aqueous portion: by the glycerol of formula ratio, amino acid humectant, Sargassum rock polysaccharide, amine acid whitening agent, green tea extractive liquor, Chinese medicine scented tea constituents extraction liquid, after taking in proportion, first heating for dissolving in stainless steel cask, be extracted in rustless steel homogenizing still by filter screen afterwards, under the stirring of 20-30 rev/min, continue to be heated to 75-80 DEG C, and constant temperature disinfection 20 minutes, stand-by;
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 40-50 rev/min, stirs after 2-3 minute, starts high speed homogenization device, homogenizing 3-5 minute under the high speed of 3000-5000 rev/min, wall rotating speed will be scraped afterwards and drop to 30-40 rev/min, and be cooled to 40 DEG C under this rotating speed, add the co-emulsifier of formula ratio, antiseptic, essence, continue to stir 15-20 minute under same rotating speed, get final product discharging;
Described Chinese medicine scented tea constituents extraction liquid prepares by the following method:
A () takes Radix Glycyrrhizae 5-10 part, Rhizoma Atractylodis Macrocephalae 5-10 part, Pseudobulbus Bletillae (Rhizoma Bletillae) 5-10 part, Radix Paeoniae Alba 5-10 part, Poria 5-10 part, Radix Ampelopsis 5-10 part, Flos Rosae Rugosae 3-5 part, Flos Moutan 3-5 part, and Flos Mume 3-5 part adds in rustless steel still;
B () first time, when boiling, takes deionized water 800-900 part, ethanol 4-6 part, propylene glycol 4-6 part, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.0-1.2 hour, namely obtain Chinese medicine scented tea constituents extraction liquid 1. with 600 order filter-cloth filterings afterwards;
In filtering residue, add the propylene glycol of the deionized water of 400-500 mass parts and the ethanol of 1-3 mass parts and 1-3 mass parts, use little fire after big fire is boiled instead and boil 0.8-1.0 hours again, use 600 order filter-cloth filterings afterwards, obtain Chinese medicine scented tea constituents extraction liquid 2.;
C () will 1., 2. namely obtain final Chinese medicine scented tea constituents extraction liquid after filtrate mix homogeneously, and its total amount should control about the half of adding total Water.
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