CN103919711B - A kind of anti-ageing whitening cream of oolong tea and manufacture method thereof - Google Patents
A kind of anti-ageing whitening cream of oolong tea and manufacture method thereof Download PDFInfo
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Abstract
The open a kind of anti-ageing whitening cream of oolong tea of the present invention and manufacture method thereof; the anti-ageing whitening cream of this oolong tea comprises the anti-ageing whitening composition extracted from oolong tea, jasmine tea and multiple herbal medicine and wax gourd; with there is excellent anti-wrinkle, the biochemical component of white-skinned face function also have basic profit skin moisturizing composition etc.; wherein oolong tea, jasmine tea, Chinese medicine, wax gourd, anti-ageing whitening composition is made by oneself by ginseng, Radix Panacis Quinquefolii, sealwort, oat, Radix Codonopsis, wolfberry fruit, glossy ganoderma, Radix Glycyrrhizae, the bighead atractylodes rhizome, the bletilla striata, wax gourd, Rose, Flos Matricariae chamomillae, oolong tea etc.; Biochemical anti-ageing whitening composition is marine alga peptide, VEOil, Ascorbyl Tetraisopalmitate etc.; Basic profit skin moisturizing composition is Oleum Hippophae, Semen Maydis oil, hyaluronate sodium, marine alga rock polysaccharide, ceramide etc. these effective constituents arranged in pairs or groups through equilibrium, after scientific composition, just can obtain both safe and efficient, again the anti-ageing whitening cream product of the novel oolong tea of combination of long drives and drop shots.
Description
Technical field
The present invention relates to a kind of anti-ageing whitening cream and the manufacture method thereof that contain oolong tea composition, belong to cosmetics and skincare product technical field.
Background technology
Along with the development of society and the raising of living standard, people, after meeting the demand in material, also more and more focus on the beauty of appearance and anti-ageing whitening problem, and this is also the reason that cosmetics and skincare product industry develops rapidly in recent years. But the aging of the mankind is an irreversible progressive formation slowly, therefore anti-ageing method also should carry out delaying senility course with safe and reliable long-term maintenance process, instead of reversal procedures fast, whitening problem is also as a same reason. At present, delaying to decline and there is following problem in whitening: be 1. anxious for success, pursuing anti-ageing fast and whitening, run counter to the natural law; 2. use the chemosynthesis skin care product to skin poisonous and harmful, skin is caused very big injury.
Oolong tea is semi-fermented tea, is rich in more tea polyphenols material and catechin, because be rich in this two kinds of materials simultaneously, therefore compares with pure green tea, and oolong tea just shows the unexistent various effect of green tea, such as anti-cancer, reducing blood-fat, anti-ageing, skin whitening etc. Nineteen eighty-three, the anti-ageing test that Academy of Traditional Chinese Medicine of Fujian Province carries out shows, oolong tea is the same with VE senile-resistant efficacy. Human trial also shows, takes enough V orally in every dayCIn situation, drink oolong tea and can make the V in bloodCContent maintains higher level, and in urine, output reduces, and V in human bodyCIncreasing of content, can increase anti-ageing, the Bearberry Extract of skin undoubtedly.
Tea class, as traditional health promoting beverage, has pure natural, nontoxic, harmless feature, and many people wash one's face with tea and also obtain good skincare effect. But by numerous tea class a operation in finished product skin care product, and and other effective beauty and skin care composition have complementary advantages, synergy aspect, domestic at present also studies to obtain not system and deeply. This is the field meriting attention and deeply probing into, and is also comply with cosmetics and skincare product back to nature and megatrend safely and effectively.
Summary of the invention
The present invention is directed to current people and pursue beauty and skin care demand that is safe and effective and back to nature, the tea series products such as significant to pure natural and effect semi-fermented tea oolong tea, jasmine tea are applied in the cosmetics and skincare product of finished product type, and and other effective skin care ingredient coordinated, learn from other's strong points to offset one's weaknesses, to reach skincare effect safely and efficiently. Although it is well known that tea series products is safe and reliable, but only washing face with tea and carry out beauty and skin care, effect is also slowly. Moreover many moderns also do not have tea everyday, and washing the custom of face with surplus tea, this brings obstacle just to the extensive utilization of tea series products. Therefore a large amount of approach using tea class extract component should be found in the formulating of recipe of finished product skin care product, and consider other beauty and skin care effect raw material of balanced collocation, to reach conventional and effective, safe skincare effect.
The present invention uses the characteristic being rich in tea-polyphenol and catechin in oolong tea, by oolong tea extract and VCDerivative (i.e. Ascorbyl Tetraisopalmitate), effective extract component such as marine alga peptide, pearl extracting solution, ginseng, glossy ganoderma, oat combines, arranged in pairs or groups by equilibrium, reasonable formula, try hard to manufacture the old effect of existing removing wrinkle and resisting aging, the novel anti-ageing whitening cream product having again tender skin white-skinned face function concurrently, to meet people to skin-protection product not only safety but also efficient demand. Therefore the primary and foremost purpose of the present invention is to provide a kind of novel anti-wrinkle whitening cream product being made up of multiple anti-ageing whitening composition; Another object of the present invention is to provide the preparation method of above-mentioned oolong tea Chinese medicine extract and the preparation method of the final anti-ageing whitening cream of oolong tea.
For achieving the above object, the present invention is by the following technical solutions:
The anti-ageing whitening cream of oolong tea of the present invention, is prepared from by following component:
(1) oil phase component: described oil phase component is made up of the component of following mass parts: 16 alcohol mixture 1-1.5 parts, 16 stearyl alcohol and 16 octadecyl glucoside 2-4 parts, stearin and PEG-100 stearate 1-2 part, white oil 2-3 part, wheatgerm oil 2-3 part, Oleum Hippophae 1-2 part, iso-octyl palmitate 2-3 part, dimethyl silicone oil 2-3 part, Semen Maydis oil 1-2 part, Tegosept M 0.2-0.3 part, propylben 0.1-0.15 part, ditertbutylparacresol 0.03-0.05 part, Ascorbyl Tetraisopalmitate 2-3 part, VEOil 0.3-0.5 part, mink oil 1-1.5 part;
(2) water phase components: glycerine 5-6 part, propylene glycol 2-3 part, amino acid humectant 3-4 part, Cer NS-4 parts, Sargassum polysaccharides 2-4 part, pearl extracting solution 1-2 part, beta-glucan 0.5-1 part, hyaluronate sodium 0.1-0.2 part, marine alga peptide 3-5 part, oolong tea Chinese medicine special efficacy constituents extraction liquid 55-58 part, described oolong tea Chinese medicine special efficacy constituents extraction liquid is mainly made up of the raw material of following mass parts: oolong tea 20-30 part, ginseng, Radix Panacis Quinquefolii, glossy ganoderma, sealwort, oat, Radix Angelicae Sinensis, the Radix Astragali, wolfberry fruit, the red sage root, gynostemma pentaphylla, raspberry, Root of Kirilow Rhodiola, Radix Et Caulis Acanthopanacis Senticosi, the root of bidentate achyranthes, white spoon, Radix Glycyrrhizae, the each 5-10 part of the bletilla striata, wax gourd 15-20 part, Flos Matricariae chamomillae, Rose, G1ycyrrhiza glabra, the each 1-2 part of Globeamaranth Flower,
(3) assistant for emulsifying agent: hydroxyethylacrylate/sodium acryloyldimethyl taurate copolymers 0.5-0.8 part;
(4) sanitas: mixture 0.1-0.15 part of MIT and 3-iodo-2-propynyl butyl first ammonia acid esters;
(5) essence: Green tea essence: 0.01-0.02 part.
The preparation method of the anti-ageing whitening cream of oolong tea of the present invention, comprise the steps: the preparation of (1) oil phase component: by 16 alcohol mixtures of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, stearin and PEG-100 stearate, white oil, wheatgerm oil, Oleum Hippophae, iso-octyl palmitate, dimethyl silicone oil, Semen Maydis oil, mink oil, Tegosept M, propylben, ditertbutylparacresol adds in the stainless steel still that band stirs after taking in proportion, under the stirring of rotating speed 20-30 rev/min, heating for dissolving is complete, and at 80-85 DEG C constant temperature disinfection 20 minutes, the Ascorbyl Tetraisopalmitate of formula ratio is added before homogeneous, VEOil, stirs evenly stand-by; (2) preparation of water phase components: the glycerine of formula ratio, propylene glycol, amino acid humectant, ceramide, Sargassum polysaccharides, pearl extracting solution, beta-glucan, hyaluronate sodium, marine alga peptide, oolong tea Chinese medicine special efficacy constituents extraction liquid are taken rear first heating for dissolving in stainless steel still in proportion, it is extracted in stainless steel homogeneous still afterwards, under the stirring of 20-30 rev/min, when continuing to be heated to 80-85 DEG C, and constant temperature disinfection 20 minutes is stand-by; (3) by oil phase slowly suction aqueous phase, and scraping wall and stir, rotating speed is increased to 40-50 rev/min, stir after 2-3 minute, start high speed homogenization device homogeneous 3-5 minute under the high speed of 3000-5000 rev/min, wall rotating speed will be scraped afterwards and drop to 30-40 rev/min, and under this rotating speed, be cooled to 60 DEG C; (4) add the assistant for emulsifying agent of formula ratio, under the rotating speed of 20-30 rev/min, stir 20-30 minute, continue afterwards to cool to 40 DEG C, add the sanitas of formula ratio, essence, continuation under same rotating speed, stir 15-20 minute, get final product discharging.
Described oolong tea Chinese medicine special efficacy constituents extraction liquid prepares by the following method:
Take dry product ginseng, Radix Panacis Quinquefolii, glossy ganoderma, sealwort, oat, Radix Angelicae Sinensis, the Radix Astragali, Radix Codonopsis, wolfberry fruit, the red sage root, gynostemma pentaphylla, raspberry, Root of Kirilow Rhodiola, Radix Et Caulis Acanthopanacis Senticosi, the root of bidentate achyranthes, white spoon, Radix Glycyrrhizae, each 5-10 part of the bletilla striata, fresh wax gourd (peeling section) 15-20 part, Flos Matricariae chamomillae, Rose, G1ycyrrhiza glabra, each 1-2 part of Globeamaranth Flower add in stainless steel still, take oolong tea 20-30 part for subsequent use;
First time, when enduring processed, takes deionized water 700-800 part, ethanol 3-4 part, propylene glycol 3-4 part, first soaks before enduring system 30 minutes, then boiled with big fire, after use little fire instead and endure 1.0-1.2 hour processed, namely obtain Chinese medicine oolong tea Chinese medicine special efficacy constituents extraction liquid 1. with 600 order filter-cloth filterings afterwards;
Filter residue adds the deionized water of 500-600 mass parts and the propylene glycol of the ethanol of 1-3 mass parts and 1-3 mass parts, use little fire after big fire is boiled instead and endure 0.8-1.0 hour processed again, add oolong tea afterwards to soak 0.5-1.0 hour, afterwards with 600 order filter-cloth filterings, obtain oolong tea Chinese medicine special efficacy constituents extraction liquid 2.;
Will 1., 2. filtrate namely obtain final oolong tea Chinese medicine special efficacy constituents extraction liquid after mixing, its total amount should control add total Water half about.
The present invention is directed to current environmental pollution (such as haze etc.) serious, people's life stress is big, skin is more fragile, or experienced by unconventional aesthetic nursing, thus it is impaired to cause skin quality, cause on the contrary accelerating old and feeble and dark and gloomy reality, according to the normal growth and metabolizing of skin, adding that following oolong tea, jasmine tea, wax gourd, Chinese medicine etc. are anti-ageing and biochemical anti-ageing, the whitening composition such as whitening composition and Ascorbyl Tetraisopalmitate, make to have and promote skin growth metabolism, removing wrinkle and resisting aging is old and the anti-ageing whitening cream product of oolong tea of tender white muscle skin effect.
Oolong tea: semi-fermented tea, is rich in catechin and tea-polyphenol, under the dual function of catechin and tea-polyphenol, oolong tea has the anti-oxidant of uniqueness, senile-resistant efficacy, it is possible to eliminate the active oxygen of harm beauty treatment with health, improve allergic, also have toxin expelling, weight reducing, antitumor efficacy, and VCClass material can improve V after coordinatingCActivity.
Ginseng: " Shennong Bencaojing " is thought, and ginseng energy " tonifying the five internal organs, peace spirit, determines soul, only palpitation with fear, except perverse trend, the happy intelligence development of bright order, clothes of a specified duration are made light of one's life by commiting suicide and are prolonged life ". Modern study finds, it also has anti-oxidant, anti-ageing, antifatigue, guarantor liver, regulates the effect such as cardiovascular function, excited hemopoietic system function.
Radix Panacis Quinquefolii: the advantage with Chinese ginseng, but do not get angry. Belong to temperaturing injecting-ability ginseng.
Glossy ganoderma: " Shennong Bencaojing " is thought, glossy ganoderma energy " tonifying liver gas, peace soul ", " eat for a long time, make light of one's life by commiting suicide old, prolong life angle ". Modern study confirms, neural system, respiratory system, systema cariovasculare functional are had regulating effect by glossy ganoderma, have the functions such as immunomodulatory, scavenging free radicals, balance metabolism, directly affect human senility process.
Sealwort: taste is sweet, property is flat, can nourshing kidney moistening lung, invigorate the spleen and benefit qi, there is anti-hypoxia, antifatigue, anti-aging effects, immunologic function can be strengthened, strengthen metabolism.
Radix Angelicae Sinensis: can enrich blood and invigorate blood circulation, menstruction regulating and pain relieving, relax bowel, to rheumatic arthralgia, wound, the cold of insufficiency type is suffered from abdominal pain, and it is effective in cure that the deficiency of blood is sallow etc. The analysis research of Radix Angelicae Sinensis is shown by modern age: it contains VAVB12The plurality of active ingredients such as palmitinic acid Oleic Linoleic tetradecanoic acid Sitosterol, have enhancement blood circulation, promote cell metabolism, suppress pigmentation, and nourishing skin etc. act on.
Radix Codonopsis: immunological competence and the hemopoietic function improving human body, tonifying spleen nourishing the stomach, moistening lung is promoted the production of body fluid.
The red sage root: promoting blood flow to regulate menstruation, stasis-dispelling and pain-killing, cool blood disappears carbuncle, and clear away heart-fire relieving restlessness, nourishing blood to tranquillize the mind, and scavenging free radicals is anti-ageing.
Oat: containing compositions such as avenin, oat peptide, avenabeta glucosan, avenols. There is anti-oxidation efficacy, increase skin active, delaying skin aging, skin whitening, moisturizing, minimizing wrinkle color spot, antianaphylaxis.
Glossy Privet Fruit: reducing blood-fat and arteriosclerosis, strengthens body immune function, endocrine regulation, benefit liver and kidney tonifying, anti-ageing spot of dispelling.
Wolfberry fruit: nourishing liver and kidney, replenishing vital essence to improve eyesight, strengthens non-specific immune function, delays senility, antifatigue.
Gynostemma pentaphylla: gynostemma pentaphylla loses its name in ancient times in book on Chinese herbal medicine. Discovered in recent years, gynostemma pentaphylla has anti-ageing, antifatigue, anticancer, endocrine regulation function, can improve human body adaptability to changes and immunizing power, reduces cholesterol and transaminase, prophylaxis of tumours, suppresses ulcer, keeping tensions down, calm, analgesia.
Root of Kirilow Rhodiola: the record not having Root of Kirilow Rhodiola in ancient times in book on Chinese herbal medicine is the anti-ageing rising star just found modern age. It has help vigour, heat-clearing, removing toxic substances, hemostasis, the effect of intelligence development of allaying excitement. Root of Kirilow Rhodiola has the benefiting action of similar ginseng, energy anti-hypoxia, cold resistance, antifatigue, radioprotective, antiviral, anticancer growth, it is to increase working efficiency, delays body aging.
Raspberry: qi-restoratives continues absolutely, strong cloudy strong sun, smoothing skin, each internal organs of peace, Wen Zhongyi power, treatment strain wind are empty, the bright order of tonifying liver.
The root of bidentate achyranthes, also known as Radix Achyranthis Bidentatae. LI Shi-Zhen says it: " merit of nourishing, such as the power of ox. The acid of root of bidentate achyranthes smell is flat, cures mainly cold-dampness impotence numbness, spasm of the limbs, and goinyalgia can not be stretched and be bent and stretched, and by vim and vigour, fire of getting mildewed in warm conditions is rotten, and clothes are made light of one's life by commiting suicide always resistance to for a long time. The root of bidentate achyranthes of Boai County, is longer than benefit liver and kidney tonifying, strong waist knee and invigorating blood circulation, the effect ensuringd proper downward flow of the blood. Especially leg joint place is centrifugal dirty relatively far away for waist leg, adds Radix Achyranthis Bidentatae extract and is suitably massaged, will play good waist leg health-care effect.
The root of herbaceous peony: taste is sweet, sour, cold nature, has the effect nourished blood, it is possible to treatment shallow complexion, facial colour spot, tarnish.
Radix Glycyrrhizae: be traditional Chinese medicine, interior contained licoflavone has restraint of tyrosinase activity, suppresses the multiple action of dopachrome change enzyme and DHICA oxidase activity, can reach good whitening effect. Also having scavenging activated oxygen, anti-oxidant grade acts on. In Radix Glycyrrhizae, contained Potenlini and glycyrrhetinic acid salt, also have the effect of anti-inflammation, anti-allergic.
The bletilla striata: materials for skin whiting for removing freckle, astringing to arrest bleeding, detumescence myogenic. It is exactly good medicine of improving looks that the bletilla striata is controlled oneself, and is described as " whitening fairy maiden ", can the tetter such as Acne treatment, ringworm of the body, scar. " property of medicine opinion " cloud: " it can control sore on face, makes us flesh sliding ". Compendium of Material Medica cloud its " black, spot of dispelling of washing one's face ".
Wax gourd: also known as white melon is the bigger vegetables of head, is also the good product of U.S. face skin care, and the multiple wax gourd polysaccharide wherein contained, amino acid, VITAMIN etc. all have good moisturizing, tender skin effect.
Flos Matricariae chamomillae: anti-ageing, antifatigue, moist skin. help mediator's body immunity function, help sleep.
Rose: beauty treatment effect is remarkable, offsets removing freckle, wrinkle effect remarkable, loses weight, the Xie Yu that regulates the flow of vital energy, promoting blood circulation to remove blood stasis, improves withered skin, stimulates circulation and metabolism.
G1ycyrrhiza glabra: the title having the apple of the earth, anti-ageing, antifatigue, skin moistening and whitening.
Globeamaranth Flower: toxin-expelling and face nourishing, delays senility.
Biochemical whitening agent Ascorbyl Tetraisopalmitate: be the derivative of oil-soluble vitamine C, be easily absorbed by the skin also have good stability, be possible not only to skin whitening, also has similar SOD active, Scavenger of ROS, promotion collagen protein synthesis. The mechanism of vitamin C derivatives skin whitening is intermediate---the DOPA quinone in B150reactive Black B 150 pigment generative process mainly, plays inhibited oxidation chain, reduces the effect that melanochrome generates. But it is well known that the difficult lasting problem of the equal existence and stability of vitamin C derivatives class, with oolong tea extract, jasmine tea extract, VE oil etc. with the use of, it is possible to reach synergy and lasting whitening effect.
Marine alga peptide: the extract in the red algae in ocean, containing a large amount of algae oligosaccharides class, oligopeptide, alpha hydroxy acid, has obvious Firm, tight real level and smooth skin, effect of the aspects such as anti-sagging, crease-resistant, reparation.
Oleum Hippophae: the Oleum Hippophae extracted from the sea-buckthorn of the king of vitamins C. main active ingredient is VEAnd VC, carotene, unsaturated fatty acids and total free aminoacids etc. there is elimination interior free yl, reduce lipofuscin content and the effect such as anti-oxidant.
Although existing market is no lack of the cosmetics and skincare product adding tea extract, but not by oolong tea and Chinese herbal medicine extracting elite and VCWhitening agents etc., through equilibrium collocation, are had complementary advantages, after scientific composition, and the anti-ageing whitening cream product of the oolong tea developed.
The invention has the beneficial effects as follows: by the composition anti-oxidant, anti-ageing that is rich in oolong tea and extracts of Chinese herbal medicine, biochemical VC��The effective constituents such as marine alga peptide organically combine, the anti-ageing whitening effect of synergy can be reached, and it is safe and reliable, having no side effect. oolong tea itself has anti-ageing, anti-oxidation efficacy, but when being used alone, though safe and reliable, effect is slower, with multiple have after anti-ageing herbal medicine and biochemical preparation coordinate can increase anti-ageing effect, and the medicinal herb components with white-skinned face function and biochemical component can be made (such as VCDerivative) more stable and play better effect.
Embodiment
Embodiment 1
(1) preparation process of the present embodiment specified proportion Chinese medicine oolong tea Chinese medicine special efficacy constituents extraction liquid is as follows:
(1) dry product ginseng 5 parts, Radix Panacis Quinquefolii 10 parts, glossy ganoderma 7 parts, sealwort 5 parts, oat 7 parts, Radix Angelicae Sinensis 5 parts, the Radix Astragali 10 parts, Radix Codonopsis 5 parts, wolfberry fruit 5 parts, the red sage root 7 parts, gynostemma pentaphylla 10 parts, raspberry 7 parts, Root of Kirilow Rhodiola 5 parts, Radix Et Caulis Acanthopanacis Senticosi 7 parts, the root of bidentate achyranthes 10 parts, white 5 parts, spoon, 7 parts, Radix Glycyrrhizae, the bletilla striata 10 parts, 15 parts, fresh wax gourd (peeling section) is taken, Flos Matricariae chamomillae 1 part, Rose 2 parts, G1ycyrrhiza glabra 1 part, Globeamaranth Flower 2 parts add in stainless steel still, take 25 parts, oolong tea for subsequent use;
(2), when first time endures processed, deionized water 700 parts is taken, ethanol 3 parts, propylene glycol 3 parts, first soaks before enduring system 30 minutes, then boiled with big fire, after use instead little fire endure system 1.2 hours, namely obtain Chinese medicine oolong tea Chinese medicine special efficacy constituents extraction liquid 1. with 600 order filter-cloth filterings afterwards;
(3) in filter residue, add the deionized water of 600 mass parts and the propylene glycol of the ethanol of 2 mass parts and 2 mass parts, use little fire after big fire is boiled instead and endure system again 1.0 hours, add oolong tea afterwards and soak 1.0 hours, afterwards with 600 order filter-cloth filterings, obtain oolong tea Chinese medicine special efficacy constituents extraction liquid 2.;
(4) will 1., 2. filtrate namely obtain final oolong tea Chinese medicine special efficacy constituents extraction liquid after mixing, its total amount should control add total Water half about.
(2) the present embodiment substitutes the pure water component in the anti-ageing whitening cream of oolong tea with obtained Chinese medicine oolong tea Chinese medicine special efficacy constituents extraction liquid, and the prescription designing the anti-ageing whitening cream of oolong tea by following proportioning (mass percent) is as follows:
(1) oil phase component: described oil phase component is made up of the component of following mass parts: 16 alcohol mixtures 1 part, (match BIC Corp of France provides for 16 stearyl alcohol and 16 octadecyl glucosides, trade(brand)name: MONTANOV68) 3 parts, (match BIC Corp of France provides for stearin and PEG-100 stearate, trade(brand)name: SIMULSOL165) 2 parts, white oil 2 parts, wheatgerm oil 3 parts, Oleum Hippophae 1 part, iso-octyl palmitate 2.5 parts, dimethyl silicone oil 3 parts, Semen Maydis oil 1.5 parts, Tegosept M 0.2 part, propylben 0.1 part, ditertbutylparacresol 0.03 part, Ascorbyl Tetraisopalmitate 2 parts, VEOil 0.3 part, mink oil 1 part;
(2) water phase components: glycerine 5 parts, propylene glycol 2 parts, amino acid humectant 3 parts, Cer NS part, Sargassum polysaccharides (offer of Shanghai Lai Yu trade Co., Ltd) 4 parts, pearl extracting solution 1 part, beta-glucan 1 part, hyaluronate sodium 0.1 part, marine alga peptide 3 parts, oolong tea Chinese medicine special efficacy constituents extraction liquid 55 parts, described oolong tea Chinese medicine special efficacy constituents extraction liquid is mainly made up of the raw material of following mass parts: 20 parts, oolong tea, ginseng 5 parts, Radix Panacis Quinquefolii 7 parts, glossy ganoderma 6 parts, sealwort 5 parts, oat 10 parts, Radix Angelicae Sinensis 10 parts, the Radix Astragali 5 parts, wolfberry fruit 6 parts, the red sage root 8 parts, gynostemma pentaphylla 6 parts, raspberry 10 parts, Root of Kirilow Rhodiola 5 parts, Radix Et Caulis Acanthopanacis Senticosi 8 parts, the root of bidentate achyranthes 10 parts, 5 parts, white spoon, 10 parts, Radix Glycyrrhizae, the bletilla striata 8 parts, 15 parts, wax gourd, Flos Matricariae chamomillae 1 part, Rose 2 parts, G1ycyrrhiza glabra 1 part, Globeamaranth Flower 1.5 parts,
(3) assistant for emulsifying agent: hydroxyethylacrylate/sodium acryloyldimethyl taurate copolymers 0.5 part;
(4) sanitas: 0.1 part, the mixture (provider of Tuo Er customizations cosmetic (Shanghai) company limited product are called MicrocareMTI) of MIT and 3-iodo-2-propynyl butyl first ammonia acid esters;
(5) essence: Green tea essence: 0.01 part.
(3) preparation method of the anti-ageing whitening cream of the present embodiment oolong tea, comprises the steps:
(1) preparation of oil phase component: by 16 alcohol mixtures of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, stearin and PEG-100 stearate, white oil, wheatgerm oil, Oleum Hippophae, iso-octyl palmitate, dimethyl silicone oil, Semen Maydis oil, mink oil, Tegosept M, propylben, ditertbutylparacresol adds in the stainless steel still that band stirs after taking in proportion, under the stirring of rotating speed 20 revs/min, heating for dissolving is complete, and at 80 DEG C constant temperature disinfection 20 minutes, the Ascorbyl Tetraisopalmitate of formula ratio is added before homogeneous, VEOil, stirs evenly stand-by;
(2) preparation of water phase components: the glycerine of formula ratio, propylene glycol, amino acid humectant, ceramide, Sargassum polysaccharides, pearl extracting solution, beta-glucan, hyaluronate sodium, marine alga peptide, oolong tea Chinese medicine special efficacy constituents extraction liquid are taken rear first heating for dissolving in stainless steel still in proportion, it is extracted in stainless steel homogeneous still afterwards, under the stirring of 20 revs/min, when continuing to be heated to 82 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) by oil phase slowly suction aqueous phase, and scraping wall and stir, rotating speed is increased to 40 revs/min, stir after 2 minutes, start high speed homogenization device homogeneous 3 minutes under the high speed of 3000 revs/min, wall rotating speed will be scraped afterwards and drop to 35 revs/min, and under this rotating speed, be cooled to 60 DEG C;
(4) add the assistant for emulsifying agent of formula ratio, stir 20 minutes under the rotating speed of 20 revs/min, continue to cool to 40 DEG C afterwards, add the sanitas of formula ratio, essence, continuation stir 15 minutes under same rotating speed, get final product discharging.
Embodiment 2
(1) preparation process of the present embodiment specified proportion Chinese medicine oolong tea Chinese medicine special efficacy constituents extraction liquid is as follows:
(1) dry product ginseng 10 parts, Radix Panacis Quinquefolii 5 parts, glossy ganoderma 5 parts, sealwort 10 parts, oat 5 parts, Radix Angelicae Sinensis 7 parts, the Radix Astragali 5 parts, Radix Codonopsis 10 parts, wolfberry fruit 7 parts, the red sage root 10 parts, gynostemma pentaphylla 5 parts, raspberry 5 parts, Root of Kirilow Rhodiola 10 parts, Radix Et Caulis Acanthopanacis Senticosi 5 parts, the root of bidentate achyranthes 5 parts, white 10 parts, spoon, 5 parts, Radix Glycyrrhizae, the bletilla striata 7 parts, 18 parts, fresh wax gourd (peeling section) is taken; Flos Matricariae chamomillae 2 parts, Rose 1 part, G1ycyrrhiza glabra 2 parts, Globeamaranth Flower 1 part add in stainless steel still, take 28 parts, oolong tea for subsequent use;
(2), when first time endures processed, deionized water 750 parts is taken, ethanol 4 parts, propylene glycol 4 parts, first soaks before enduring system 30 minutes, then boiled with big fire, after use instead little fire endure system 1.1 hours, namely obtain Chinese medicine oolong tea Chinese medicine special efficacy constituents extraction liquid 1. with 600 order filter-cloth filterings afterwards;
(3) in filter residue, add the deionized water of 550 mass parts and the propylene glycol of the ethanol of 1 mass parts and 1 mass parts, use little fire after big fire is boiled instead and endure system again 0.8 hour, add oolong tea afterwards and soak 0.5 hour, afterwards with 600 order filter-cloth filterings, obtain oolong tea Chinese medicine special efficacy constituents extraction liquid 2.;
(4) will 1., 2. filtrate namely obtain final oolong tea Chinese medicine special efficacy constituents extraction liquid after mixing, its total amount should control add total Water half about.
(2) the present embodiment substitutes the pure water component in the anti-ageing whitening cream of oolong tea with obtained Chinese medicine oolong tea Chinese medicine special efficacy constituents extraction liquid, and the prescription designing the anti-ageing whitening cream of oolong tea by following proportioning (mass percent) is as follows:
(1) oil phase component: described oil phase component is made up of the component of following mass parts: 16 alcohol mixtures 1.5 parts, 16 stearyl alcohol and each 2 parts of 16 octadecyl glucosides, stearin and each 1 part of PEG-100 stearate, white oil 3 parts, wheatgerm oil 2 parts, Oleum Hippophae 1.5 parts, iso-octyl palmitate 3 parts, dimethyl silicone oil 2 parts, Semen Maydis oil 1 part, Tegosept M 0.3 part, propylben 0.15 part, ditertbutylparacresol 0.05 part, Ascorbyl Tetraisopalmitate 2.5 parts, VEOil 0.4 part, mink oil 1.5 parts.
(2) water phase components: glycerine 5.5 parts, propylene glycol 2 parts, amino acid humectant 3.5 parts, Cer NP part, Sargassum polysaccharides 3 parts, pearl extracting solution 1 part, ��--dextran 0.8 part, hyaluronate sodium 0.2 part, marine alga peptide 3 parts, oolong tea Chinese medicine special efficacy constituents extraction liquid 56.46 parts, described oolong tea Chinese medicine special efficacy constituents extraction liquid is mainly made up of the raw material of following mass parts: 25 parts, oolong tea, ginseng 8 parts, Radix Panacis Quinquefolii 5 parts, glossy ganoderma 10 parts, sealwort 7 parts, oat 5 parts, Radix Angelicae Sinensis 6 parts, the Radix Astragali 7 parts, wolfberry fruit 5 parts, the red sage root 10 parts, gynostemma pentaphylla 5 parts, raspberry 8 parts, Root of Kirilow Rhodiola 7 parts, Radix Et Caulis Acanthopanacis Senticosi 5 parts, the root of bidentate achyranthes 7 parts, 8 parts, white spoon, 5 parts, Radix Glycyrrhizae, the bletilla striata 5 parts, 18 parts, wax gourd, Flos Matricariae chamomillae 1.5 parts, Rose 1 part, G1ycyrrhiza glabra 1.5 parts, Globeamaranth Flower 1 part,
(3) assistant for emulsifying agent: hydroxyethylacrylate/sodium acryloyldimethyl taurate copolymers 0.7 part;
(4) sanitas: 0.12 part, the mixture of MIT and 3-iodo-2-propynyl butyl first ammonia acid esters;
(5) essence: Green tea essence: 0.01 part.
(3) preparation method of the anti-ageing whitening cream of the present embodiment oolong tea, comprises the steps:
(1) preparation of oil phase component: by 16 alcohol mixtures of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, stearin and PEG-100 stearate, white oil, wheatgerm oil, Oleum Hippophae, iso-octyl palmitate, dimethyl silicone oil, Semen Maydis oil, mink oil, Tegosept M, propylben, ditertbutylparacresol adds in the stainless steel still that band stirs after taking in proportion, under the stirring of rotating speed 30 revs/min, heating for dissolving is complete, and at 85 DEG C constant temperature disinfection 20 minutes, the Ascorbyl Tetraisopalmitate of formula ratio is added before homogeneous, VEOil, stirs evenly stand-by;
(2) preparation of water phase components: the glycerine of formula ratio, propylene glycol, amino acid humectant, ceramide, Sargassum polysaccharides, pearl extracting solution, beta-glucan, hyaluronate sodium, marine alga peptide, oolong tea Chinese medicine special efficacy constituents extraction liquid are taken rear first heating for dissolving in stainless steel still in proportion, it is extracted in stainless steel homogeneous still afterwards, under the stirring of 30 revs/min, when continuing to be heated to 85 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) by oil phase slowly suction aqueous phase, and scraping wall and stir, rotating speed is increased to 50 revs/min, stir after 3 minutes, start high speed homogenization device homogeneous 4 minutes under the high speed of 5000 revs/min, wall rotating speed will be scraped afterwards and drop to 40 revs/min, and under this rotating speed, be cooled to 60 DEG C;
(4) add the assistant for emulsifying agent of formula ratio, stir 20 minutes under the rotating speed of 30 revs/min, continue to cool to 40 DEG C afterwards, add the sanitas of formula ratio, essence, continuation stir 20 minutes under same rotating speed, get final product discharging.
Embodiment 3
(1) preparation process of the present embodiment specified proportion Chinese medicine oolong tea Chinese medicine special efficacy constituents extraction liquid is as follows:
(1) dry product ginseng 7 parts, Radix Panacis Quinquefolii 7 parts, glossy ganoderma 10 parts, sealwort 7 parts, oat 10 parts, Radix Angelicae Sinensis 10 parts, the Radix Astragali 7 parts, Radix Codonopsis 7 parts, wolfberry fruit 10 parts, the red sage root 5 parts, gynostemma pentaphylla 7 parts, raspberry 10 parts, Root of Kirilow Rhodiola 7 parts, Radix Et Caulis Acanthopanacis Senticosi 10 parts, the root of bidentate achyranthes 7 parts, white 7 parts, spoon, 10 parts, Radix Glycyrrhizae, the bletilla striata 5 parts, 20 parts, fresh wax gourd (peeling section) is taken, Flos Matricariae chamomillae 1 part, Rose 2 parts, G1ycyrrhiza glabra 2 parts, Globeamaranth Flower 1 part add in stainless steel still, take 30 parts, oolong tea for subsequent use;
(2), when first time endures processed, deionized water 800 parts is taken, ethanol 4 parts, propylene glycol 4 parts, first soaks before enduring system 30 minutes, then boiled with big fire, after use instead little fire endure system 1.2 hours, namely obtain Chinese medicine oolong tea Chinese medicine special efficacy constituents extraction liquid 1. with 600 order filter-cloth filterings afterwards;
(3) in filter residue, add the deionized water of 500 mass parts and the propylene glycol of the ethanol of 3 mass parts and 3 mass parts, use little fire after big fire is boiled instead and endure system again 0.8 hour, add oolong tea afterwards and soak 0.5 hour, afterwards with 600 order filter-cloth filterings, obtain oolong tea Chinese medicine special efficacy constituents extraction liquid 2.;
(4) will 1., 2. filtrate namely obtain final oolong tea Chinese medicine special efficacy constituents extraction liquid after mixing, its total amount should control add total Water half about.
(2) the present embodiment substitutes the pure water component in the anti-ageing whitening cream of oolong tea with obtained Chinese medicine oolong tea Chinese medicine special efficacy constituents extraction liquid, and the prescription designing the anti-ageing whitening cream of oolong tea by following proportioning (mass percent) is as follows:
(1) oil phase component: described oil phase component is made up of the component of following mass parts: 16 alcohol mixtures 1.2 parts, 16 stearyl alcohol and each 3 parts of 16 octadecyl glucosides, stearin and each 1.5 parts of PEG-100 stearate, white oil 2.5 parts, wheatgerm oil 2.5 parts, Oleum Hippophae 2 parts, iso-octyl palmitate 2 parts, dimethyl silicone oil 2.5 parts, Semen Maydis oil 2 parts, Tegosept M 0.3 part, propylben 0.15 part, ditertbutylparacresol 0.05 part, Ascorbyl Tetraisopalmitate 3 parts, VEOil 0.5 part, mink oil 1.2 parts;
(2) water phase components: glycerine 6 parts, propylene glycol 3 parts, amino acid humectant 4 parts, ceramide 4 parts, Sargassum polysaccharides 2 parts, pearl extracting solution 1.5 parts, beta-glucan 1 part, hyaluronate sodium 0.1 part, marine alga peptide 5 parts, oolong tea Chinese medicine special efficacy constituents extraction liquid 58 parts, described oolong tea Chinese medicine special efficacy constituents extraction liquid is mainly made up of the raw material of following mass parts: 30 parts, oolong tea, ginseng 10 parts, Radix Panacis Quinquefolii 10 parts, glossy ganoderma 5 parts, sealwort 10 parts, oat 8 parts, Radix Angelicae Sinensis 5 parts, the Radix Astragali 10 parts, wolfberry fruit 10 parts, the red sage root 5 parts, gynostemma pentaphylla 10 parts, raspberry 5 parts, Root of Kirilow Rhodiola 10 parts, Radix Et Caulis Acanthopanacis Senticosi 10 parts, the root of bidentate achyranthes 5 parts, 10 parts, white spoon, 8 parts, Radix Glycyrrhizae, the bletilla striata 10 parts, 20 parts, wax gourd, Flos Matricariae chamomillae 2 parts, Rose 1.5 parts, G1ycyrrhiza glabra 2 parts, Globeamaranth Flower 2 parts,
(3) assistant for emulsifying agent: hydroxyethylacrylate/sodium acryloyldimethyl taurate copolymers 0.8 part;
(4) sanitas: 0.15 part, the mixture of MIT and 3-iodo-2-propynyl butyl first ammonia acid esters;
(5) essence: Green tea essence: 0.02 part.
(3) preparation method of the anti-ageing whitening cream of the present embodiment oolong tea, comprises the steps:
(1) preparation of oil phase component: by 16 alcohol mixtures of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, stearin and PEG-100 stearate, white oil, wheatgerm oil, Oleum Hippophae, iso-octyl palmitate, dimethyl silicone oil, Semen Maydis oil, mink oil, Tegosept M, propylben, ditertbutylparacresol adds in the stainless steel still that band stirs after taking in proportion, under the stirring of rotating speed 30 revs/min, heating for dissolving is complete, and at 85 DEG C constant temperature disinfection 20 minutes, the Ascorbyl Tetraisopalmitate of formula ratio is added before homogeneous, VEOil, stirs evenly stand-by.
(2) preparation of water phase components: the glycerine of formula ratio, propylene glycol, amino acid humectant, ceramide, Sargassum polysaccharides, pearl extracting solution, beta-glucan, hyaluronate sodium, marine alga peptide, oolong tea, Chinese medicine special efficacy constituents extraction liquid are taken rear first heating for dissolving in stainless steel still in proportion, it is extracted in stainless steel homogeneous still afterwards, under the stirring of 30 revs/min, when continuing to be heated to 85 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) by oil phase slowly suction aqueous phase, and scraping wall and stir, rotating speed is increased to 50 revs/min, stir after 3 minutes, start high speed homogenization device homogeneous 4 minutes under the high speed of 5000 revs/min, wall rotating speed will be scraped afterwards and drop to 40 revs/min, and under this rotating speed, be cooled to 60 DEG C;
(4) add the assistant for emulsifying agent of formula ratio, stir 30 minutes under the rotating speed of 30 revs/min, continue to cool to 40 DEG C afterwards, add the sanitas of formula ratio, essence, continuation stir 15 minutes under same rotating speed, get final product discharging.
Effect example:
Detection method:
By dimethyl sulfoxide (DMSO), the sample preparation of previous embodiment becomes concentration be the concentration of mass volume ratio 1% respectively, carry out following experiment.
(1) mensuration of free radical scavenging effect:
Phenylbenzene picryl phenylhydrazine DPPH solution (solvent of this solution the is water) 2ml that extracting sample solution 2ml and concentration are 100umol/L first adds in same tool plug test tube, shake even, left at room temperature 30 minutes, take solvent as blank, measures sample absorbance under 517nm wavelength.
Inhibiting rate: k%=[1-(Ai-Aj)/AC] �� 100%
The absorbancy of Ai:2mlDPPH solution+2ml sample solution
The absorbancy of Aj:2ml sample solution+2ml solvent (i.e. dimethyl sulfoxide (DMSO))
The absorbancy of AC:2mlDPPH solution+2ml solvent (i.e. dimethyl sulfoxide (DMSO))
Experimental result:
The mensuration of free radical scavenging effect, result is as shown in table 1:
Table 1
| Inhibiting rate (%) | |
| Embodiment 1 | 90.2 8--> |
| Embodiment 2 | 90.5 |
| Embodiment 3 | 89.7 |
Above-mentioned experimental result shows, the anti-ageing whitening cream of the oolong tea of the present invention can effectively suppress the generation of free radical, and effect is remarkable.
(2) B16 cell test in mouse melanin cell is suppressed:
By B16 mouse melanin tumor cell with 1 �� 105The density of individual/ml is connected to the culture dish that diameter is 9cm, at 37 DEG C of 5%CO2When, cultivates 2 days, abandon supernatant liquor, add the sample solution 18-22ml after filtration sterilization, then cultivate 3 days, abandon supernatant liquor, PBS washs, every hole adds the trypsin solution peptic cell 3min of 0.5ml mass percent 0.2%, every ware adds 2ml maintenance medium and terminates digestion. and after piping and druming is mixed even, often kind of concentration is taken out 0.5ml and is done cell counting, and all the other cell suspensions are with the centrifugal 5min of 2500r/min, abandon supernatant liquor, adding NaoH solution in precipitation, heating makes melanochrome dissolve, and selects to survey absorbance on the enzyme-linked immunosorbent assay instrument of 490nm wavelength.
B16 cell inhibiting rate=(1-(medicine hole absorbancy+medicine porocyte density)+(control wells absorbance+control wells cell density)) �� 100%.
Experimental result:
Suppressing B16 cell test in mouse melanin cell, result is as shown in table 2:
Table 2
| Inhibiting rate (%) | |
| Embodiment 1 | 60.3 |
| Embodiment 2 | 59.3 |
| Embodiment 3 | 60.5 |
Claims (2)
1. the anti-ageing whitening cream of oolong tea, it is characterised in that be prepared from by following component:
(1) oil phase component: described oil phase component is made up of the component of following mass parts: 16 alcohol mixture 1-1.5 parts, 16 stearyl alcohol and 16 octadecyl glucoside 2-4 parts, stearin and PEG-100 stearate 1-2 part, white oil 2-3 part, wheatgerm oil 2-3 part, Oleum Hippophae 1-2 part, iso-octyl palmitate 2-3 part, dimethyl silicone oil 2-3 part, Semen Maydis oil 1-2 part, Tegosept M 0.2-0.3 part, propylben 0.1-0.15 part, ditertbutylparacresol 0.03-0.05 part, Ascorbyl Tetraisopalmitate 2-3 part, VEOil 0.3-0.5 part, mink oil 1-1.5 part;
(2) water phase components: glycerine 5-6 part, propylene glycol 2-3 part, amino acid humectant 3-4 part, Cer NS-4 parts, Sargassum polysaccharides 2-4 part, pearl extracting solution 1-2 part, beta-glucan 0.5-1 part, hyaluronate sodium 0.1-0.2 part, marine alga peptide 3-5 part, oolong tea traditional Chinese medicine ingredients extracting solution 55-58 part, described oolong tea traditional Chinese medicine ingredients extracting solution is made up of the raw material of following mass parts: oolong tea 20-30 part, ginseng, Radix Panacis Quinquefolii, glossy ganoderma, sealwort, oat, Radix Angelicae Sinensis, the Radix Astragali, Radix Codonopsis, wolfberry fruit, the red sage root, gynostemma pentaphylla, raspberry, Root of Kirilow Rhodiola, Radix Et Caulis Acanthopanacis Senticosi, the root of bidentate achyranthes, the root of herbaceous peony, Radix Glycyrrhizae, the each 5-10 part of the bletilla striata, wax gourd 15-20 part, Flos Matricariae chamomillae, Rose, G1ycyrrhiza glabra, the each 1-2 part of Globeamaranth Flower,
(3) assistant for emulsifying agent: hydroxyethylacrylate/sodium acryloyldimethyl taurate copolymers 0.5-0.8 part;
(4) sanitas: mixture 0.1-0.15 part of MIT and 3-iodo-2-propynyl butyl first ammonia acid esters;
(5) essence: Green tea essence: 0.01-0.02 part;
Described oolong tea traditional Chinese medicine ingredients extracting solution prepares by the following method:
Take dry product ginseng, Radix Panacis Quinquefolii, glossy ganoderma, sealwort, oat, Radix Angelicae Sinensis, the Radix Astragali, Radix Codonopsis, wolfberry fruit, the red sage root, gynostemma pentaphylla, raspberry, Root of Kirilow Rhodiola, Radix Et Caulis Acanthopanacis Senticosi, the root of bidentate achyranthes, the root of herbaceous peony, Radix Glycyrrhizae, each 5-10 part of the bletilla striata, wax gourd 15-20 part, Flos Matricariae chamomillae, Rose, G1ycyrrhiza glabra, each 1-2 part of Globeamaranth Flower add in stainless steel still, take oolong tea 20-30 part for subsequent use;
First time, when enduring processed, takes deionized water 700-800 part, ethanol 3-4 part, propylene glycol 3-4 part, first soaks before enduring system 30 minutes, then boiled with big fire, after use little fire instead and endure 1.0-1.2 hour processed, namely obtain Chinese medicine oolong tea traditional Chinese medicine ingredients extracting solution 1. with 600 order filter-cloth filterings afterwards;
Filter residue adds the deionized water of 500-600 mass parts and the propylene glycol of the ethanol of 1-3 mass parts and 1-3 mass parts, use little fire after big fire is boiled instead and endure 0.8-1.0 hour processed again, add oolong tea afterwards to soak 0.5-1.0 hour, afterwards with 600 order filter-cloth filterings, obtain oolong tea traditional Chinese medicine ingredients extracting solution 2.;
Will 1., 2. filtrate namely obtain final oolong tea traditional Chinese medicine ingredients extracting solution after mixing, its total amount should control add total Water half.
2. the preparation method of the anti-ageing whitening cream of oolong tea according to claim 1, it is characterized in that, comprise the steps: the preparation of (1) oil phase component: by 16 alcohol mixtures of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, stearin and PEG-100 stearate, white oil, wheatgerm oil, Oleum Hippophae, iso-octyl palmitate, dimethyl silicone oil, Semen Maydis oil, mink oil, Tegosept M, propylben, ditertbutylparacresol adds in the stainless steel still that band stirs after taking in proportion, under the stirring of rotating speed 20-30 rev/min, heating for dissolving is complete, and at 80-85 DEG C constant temperature disinfection 20 minutes, the Ascorbyl Tetraisopalmitate of formula ratio is added before homogeneous, VEOil, stirs evenly stand-by; (2) preparation of water phase components: the glycerine of formula ratio, propylene glycol, amino acid humectant, ceramide, Sargassum polysaccharides, pearl extracting solution, beta-glucan, hyaluronate sodium, marine alga peptide, oolong tea traditional Chinese medicine ingredients extracting solution are taken rear first heating for dissolving in stainless steel still in proportion, it is extracted in stainless steel homogeneous still afterwards, under the stirring of 20-30 rev/min, when continuing to be heated to 80-85 DEG C, and constant temperature disinfection 20 minutes is stand-by; (3) by oil phase slowly suction aqueous phase, and scraping wall and stir, rotating speed is increased to 40-50 rev/min, stir after 2-3 minute, start high speed homogenization device homogeneous 3-5 minute under the high speed of 3000-5000 rev/min, wall rotating speed will be scraped afterwards and drop to 30-40 rev/min, and under this rotating speed, be cooled to 60 DEG C; (4) add the assistant for emulsifying agent of formula ratio, under the rotating speed of 20-30 rev/min, stir 20-30 minute, continue afterwards to cool to 40 DEG C, add the sanitas of formula ratio, essence, continuation under same rotating speed, stir 15-20 minute, get final product discharging.
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| CN108096119A (en) * | 2018-02-05 | 2018-06-01 | 淮安智品企业管理有限公司 | A kind of pure natural whitening spot-eliminating composition |
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