CN103690434B - Pu' er tea anti-aging cream and preparation method thereof - Google Patents
Pu' er tea anti-aging cream and preparation method thereof Download PDFInfo
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- CN103690434B CN103690434B CN201310697281.6A CN201310697281A CN103690434B CN 103690434 B CN103690434 B CN 103690434B CN 201310697281 A CN201310697281 A CN 201310697281A CN 103690434 B CN103690434 B CN 103690434B
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- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses a Pu ' er tea anti-aging cream and a preparation method thereof, the Pu ' er tea anti-aging cream comprises a plurality of Chinese herbal medicine anti-aging components, antioxidant and anti-aging components extracted from Pu ' er tea and scented tea, biochemical anti-aging components, basic skin moistening components and the like, wherein the effective antioxidant and anti-aging components of the Chinese herbal medicine, the scented tea and the Pu ' er tea are self-made by ginseng, lucid ganoderma, acanthopanax, rhodiola rosea, gynostemma pentaphylla, Pu ' er tea, chrysanthemum morifolium, forgetfulness me-not, peony and the like; biochemical anti-aging component VEOil and collagen; the basic skin-moistening and moisture-preserving components comprise jojoba oil, amino acid humectant, tea seed oil, etc.; the anti-oxidation and anti-aging components and the basic skin-moistening and moisturizing components are matched in a balanced manner and are reasonably formulated, so that the Pu' er tea anti-aging cream product which is safe and effective and combines long-term effect and short-term effect can be obtained.
Description
Technical field
The present invention relates to a kind of anti-aging cream and the manufacture method thereof that contain Folium camelliae assamicae composition, belong to cosmetics and skincare product technical field.
Background technology
Along with the development of society and the raising of living standard, the concern of people to appearance defying age problem is more and more stronger.Especially the vast women that likes to be beautiful, because the youth is of short duration, spends easy mistake, therefore while aspect of material is rich in gradually, just energy can be concentrated on the defying age aspect of appearance more and more early, is everlasting to reaching the youth, agerasia ideal effect.Due to the impact of all factors, some women that like to be beautiful can be caused, are difficult to reach the effect of desirable slow down aging.Here many reasons is had, as environmental factors, dietary habit, living habit, operating pressure and emotional problem etc.But only from this aspect of anti-aging product of current anti-aging skin care product especially specialized beauty parlors, also some mistaken ideas and defect is had, be mainly manifested in following aspect: (one) blindly compels to ask quick-acting quick effective results, even to see the wrinkle removing anti-aging effects got instant result, this just makes portioned product in recipe design, deviate from the track of nature and science, and biases toward the realization of wrinkle removing false appearance.(2) some eager for instant success and quick profits beauty parlors covet quick-acting effects of product, cause in some anti-aging products and add some not yet at the cocksure raw material of secure context.This just may cause the healthy potential problem of skin.(3) portioned product is often for the purpose of short-term is effective, therefore consider less in permanent safety and effect, this just may enter the vicious circle of " always using; continuously effective; once stop using; effect is poorer ", although use anti-aging skin care product year in year out, lacks the true effect of long-acting, safe, stable delay skin aging.As can be seen here, develop, persistent authentic and valid to skin and safe and reliable anti-aging product, walk out the product design mistaken ideas of chasing new raw material, new folk prescription, new special effect simply, veritably for the maintenance of skin provides permanent help reliably, it is the developing direction of current and later defying age series products.
The present invention is directed to the defect of current defying age class skin care item, and the self-sow metabolic rule of human skin, the product thinking complied with the nature with back to nature, tries hard to from natural materials and popular conventional security classes raw material, optimize that applicable people commonly use, have the optimum feed stock of permanent effect.As everyone knows, in diet, after the pure natural epoch that people experienced by several thousand, enter without restraint the epoch of " improvement ", the abuse of chemical fertilizer, pesticide, hormone, medicine and various additive, many people the are tasted varieties of hardship of " excessively improve ", have again the strong desire returning peace and quiet free of contamination naturalness now, as a same reason, beauty and skin care industry development so for many years, also by naturalness enter the state of " excessively improve ", side effect is apparent.Some event examples especially of disfeaturing, therefore back to nature, comply with the self-sow rule of human body, effectively combined by nature, be only the road of the long-term stability of cosmetics and skincare product with improvement.Anti-aging product is all the more so, because human senility is nature and an irreversible process, therefore the rule of excessive improvement defying age likely makes the self-sow rule of human body be destroyed, also can bring to a certain extent and accelerate old and feeble side effect, so the method for ideal defying age should be under the prerequisite complying with human body natural's growth and naturally-aged rule, seek safe and effective, the method delayed of long-term stability, excessive quick growth (as used various somatomedin in a large number) can not be pursued, excessive growth inhibited can not be pursued again (as various creotoxin, the abuse etc. of class creotoxin), appropriate pure natural composition and biochemical effective ingredient is selected to carry out the aging of moderately delaying skin, thus reach safe and effective, the anti-aging effects of long-term stability.
Summary of the invention
Primary and foremost purpose of the present invention is to provide a kind of by multiple antisenility skin care balanced composition collocation, Synergistic, effect is permanent, and can the anti-aging skin cream product of life-time service, to meeting the safety of numerous women to skin anti-aging skin care item, effectively pursue, reach and can use, can use be grown again, existing short run effect, more have the product design of long-term effect to conceive.Another object of the present invention is to provide above-mentioned plant (i.e. Chinese herbal medicine), the preparation method of teas (i.e. Folium camelliae assamicae etc.) extract and the preparation method of final Folium camelliae assamicae anti-aging cream.
To achieve these goals, the technical solution used in the present invention is as follows:
Folium camelliae assamicae anti-aging cream of the present invention, is prepared from by following component:
(1) oil phase component: described oil phase component is made up of the component of following mass parts: 16 mixed alcohol 1-1.5 parts, 16 stearyl alcohol and 16 octadecyl glucosides 2-4 parts, tristerin and PEG-100 stearate 1-3 parts, Oleum Camelliae 1-1.5 parts, Jojoba oil 2-4 parts, Semen Tritici aestivi germ oil 2-4 parts, Oleum Vitis viniferae 0.1-1.0 parts, V
eoil 0.2-0.5 part, white oil 2-4 parts, iso-octyl palmitate 2-4 parts, Oleum Hippophae 0.5-1.0 parts, dimethicone 2-4 parts, methyl hydroxybenzoate 0.2-0.3 part, propylparaben 0.1-0.15 part, ditertbutylparacresol 0.03-0.05 part.
(2) water phase components: glycerol 6--8 part, propylene glycol 2-3 parts, amino acid humectant 3-4 parts, the different poly-polysaccharide 0.05-0.08 part of Tremella, green tea extract 1-2 parts, collagen protein 1-2 parts, pure water 3-6 parts, Chinese medicine PUERHUACHA constituents extraction liquid 53-57 part; The raw material of described Chinese medicine Pu'er magistery extracting solution mainly following mass parts is made: Folium camelliae assamicae 20-40 parts, Radix Ginseng, Ganoderma, Radix Et Caulis Acanthopanacis Senticosi, Radix Rhodiolae, Herb Gynostemmae Pentaphylli, Radix Angelicae Sinensis, the Radix Astragali, each 10-15 parts of Radix Notoginseng, foreign glycosides chrysanthemum, Myosotis sylvatica, Flos Moutan, each 2-4 parts of Dianthus carryophyllus.
(3) antiseptic: 0.1-0.15 part, the mixture of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol.
(4) essence: rice essence 0.01-0.02 part.
The preparation method of Folium camelliae assamicae anti-aging cream of the present invention, comprises the steps:
(1) preparation of oil phase part: by 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, tristerin and PEG-100 stearate, Oleum Camelliae, Jojoba oil, Semen Tritici aestivi germ oil, Oleum Vitis viniferae, V
eoil, white oil, iso-octyl palmitate, Oleum Hippophae, dimethicone, methyl hydroxybenzoate, propylparaben, after ditertbutylparacresol takes in proportion, adds in the rustless steel still of band stirring, under the stirring of rotating speed 20-30 revs/min, heating for dissolving is complete, and constant temperature disinfection 20 minutes is stand-by at 80-85 DEG C.
(2) preparation of aqueous portion: by the glycerol of formula ratio, propylene glycol, amino acid humectant, the different poly-polysaccharide of Tremella, green tea extract, Chinese medicine PUERHUACHA constituents extraction liquid, after taking in proportion, first heating for dissolving in rustless steel still, be extracted in rustless steel homogenizing still afterwards, under the stirring of 20-30 revs/min, continue to be heated to 80--85 DEG C, and constant temperature disinfection 20 minutes, stand-by.
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 40-50 revs/min, stir after 2-3 minutes, start high speed homogenization device, homogenizing 3-5 minutes under the high speed of 3000-5000 revs/min, wall rotating speed will be scraped afterwards and drop to 30-40 revs/min, and 50 DEG C are cooled under this rotating speed, add collagen protein solvent in advance, homogenizing 2-4 minutes, then continue to be cooled to 40 DEG C, add the antiseptic of formula ratio, essence, continue to stir 15-20 minutes under same rotating speed, get final product discharging.
Described Chinese medicine PUERHUACHA constituents extraction liquid prepares by the following method:
(1) take dry product Radix Ginseng, Ganoderma, Radix Et Caulis Acanthopanacis Senticosi, Radix Rhodiolae, Herb Gynostemmae Pentaphylli, Radix Angelicae Sinensis, the Radix Astragali, each 10-15 parts of Radix Notoginseng, foreign glycosides chrysanthemum, Myosotis sylvatica, Flos Moutan, each 2-4 parts of Dianthus carryophyllus, add in rustless steel still; Take Folium camelliae assamicae 20-40 parts for subsequent use.
(2) when first time boils, take deionized water 700-800 parts, ethanol 4-6 parts, propylene glycol 4-6 parts, 30 minutes are first soaked before boiling, then use big fire boiled, after use little fire instead and boil 1.0-1.2 hours, namely obtain Chinese medicine Folium camelliae assamicae scented tea magistery extracting solution 1. with 600 order filter-cloth filterings afterwards.
(3) in filtering residue, add the propylene glycol of the deionized water of 500-600 mass parts and the ethanol of 1-3 mass parts and 1-3 mass parts, use little fire after big fire is boiled instead and boil 0.8-1.0 hours again, add Folium camelliae assamicae afterwards to soak 0.5-1.0 hours, use 600 order filter-cloth filterings afterwards, obtain Chinese medicine Folium camelliae assamicae scented tea magistery extracting solution 2..
(4) will 1., 2. namely obtain final Chinese medicine Folium camelliae assamicae scented tea magistery extracting solution after filtrate mix homogeneously, its total amount should control about the half of adding total Water.
The present invention is directed to current environmental pollution serious, people's life stress is large, skin subhealth state person is more, and easily impaired in beauty and skin care, it is anti-that you cause very fast old and feeble reality, according to the normal growth and metabolizing of skin, add following Folium camelliae assamicae, green tea, scented tea Chinese medicine aging ingredient and biochemical aging ingredient, make to have and promote skin growth metabolism, delay skin aging, the Folium camelliae assamicae anti-aging cream product of skin care moisture-keeping efficacy.
In numerous wrinkle removing antisenility skin care raw materials, derive from the aging ingredient of plant (as teas, Chinese herbal medicine etc.) extract, there is safe and effective and long-acting feature, especially from the Folium camelliae assamicae in Yunnan, not only pure natural, pollution-free, be also rich in multiple aging ingredient, can life-time service and being free from side effects, and Chinese herbal medicine is as Radix Ginseng, Ganoderma, Radix Notoginseng, the Radix Astragali etc., defying age non-defective unit since ancient times especially.Some biochemical components, as vitamin E, collagen protein etc., then have the feature that concentration is high, effect is strong, and side effect are very little, or there is no side effect.If use the antisenility skin care composition in multiple source to deal with the old and feeble problem of skin, can reach both safety, again effectively, existing short run effect, has again the perfect condition of long-term effect.
Folium camelliae assamicae: Folium camelliae assamicae is Elevation, contained catechin total amount is higher than other local tea variety, contained by enrich polyphenol and can play good antioxidation, anti-aging effects, lipids contents can also be reduced simultaneously, make vasodilation, thus accelerate blood circulation, solve the obscure and various irritating speckle of the colour of skin because QI and blood does not freely cause.Modern scientific research shows: containing reaching tens kinds of antioxidation phenols in yunnan puer tea, as (-)-nutgall catechin (GC, 1), EC (GC, 2), (+)-catechin (C, 3), ampelopsin, gallic acid, Rhizoma Kaempferiae acid, kaempferol-3-0-β-D-Glucose glycoside (7), kaempferol-3-0-rutinoside, Quercetin, Quercetin-3-0-β-D glycoside and 2, 5 one resorcylic acids, DPPH free radical scavenging activity test result shows, compound 2, 3, activity and the positive reference substance ascorbic acid of 5 are close, wherein contained simple catechin and simple phenolic compound all have higher antioxidant activity, the antioxidation of visible Folium camelliae assamicae, senile-resistant efficacy has material base, add in skin protection cosmetics and can play good anti-aging effects.
Radix Ginseng: Shennong's Herbal is thought, and Radix Ginseng energy " determine soul, spasmolytic is throbbed with fear for tonifying five ZANG-organs, peace spirit, except pathogen, and the happy Fructus Alpiniae Oxyphyllae of improving eyesight, clothes are made light of one's life by commiting suicide and are prolonged life for a long time ".Modern study finds, it also has antioxidation, defying age, resisting fatigue, protects the liver, regulates the effect such as cardiovascular function, excited hemopoietic system function.
Radix Notoginseng: Qing Dynasty well-known doctor ZHAO Xue-Min he supplementary Amplifications of the Compendium of Materia Medica in say: " ginseng qi-tonifying the first, Radix Notoginseng enriches blood the first, taste with and merit also etc. ", claim Radix Notoginseng to be " the most precious person of Chinese medicine ".Modern study finds, the chemical composition of Radix Notoginseng, pharmacological action and clinical practice and Radix Ginseng have similarity, and its ginsenoside content exceedes Radix Ginseng.The expansible blood vessel of Radix Notoginseng, reduces vascular resistance, increases cardiac output, decreased heart rate, reduces the permeability of myocardial oxygen consumption and blood capillary, in preventing and treating cardiovascular disease, has obvious advantage than Radix Ginseng.
Ganoderma: Shennong's Herbal is thought, Ganoderma energy " tonifying liver gas, peace soul ", " eat for a long time, make light of one's life by commiting suicide old, prolong life angle ".Modern study confirms, Ganoderma has regulating action to nervous system, respiratory system, systema cariovasculare functional, has the functions such as immunomodulating, scavenging free radicals, balance metabolism, directly affects human senility process.
Radix Acanthopanacis Senticosi: Compendium of Material Medica is referred to as " for a long time clothes make light of one's life by commiting suicide resistance to old ", " Ning get Yi slender acanthopanax, need not the full car of gold and jade ".Modern study finds, Radix Acanthopanacis Senticosi has defying age, resisting fatigue (its antifatigue effect more also than ginsenoside strong), strong effect, can also nervous system regulation, hormonal system, systema cariovasculare functional, and has anti-inflammation and certain antitumaous effect.
Radix Rhodiolae: the record not having Radix Rhodiolae in ancient times in book on Chinese herbal medicine is the defying age rising star just found modern age.It has tonification vigour, heat clearing away, removing toxic substances, hemostasis, effect of the mind calming and mentality promoting.Radix Rhodiolae has the benefiting action of similar Radix Ginseng, and energy anti-hypoxia, cold resistance, resisting fatigue, radioprotective, antiviral, anticancer growth, increase work efficiency, delay body aging.
Herb Gynostemmae Pentaphylli: Herb Gynostemmae Pentaphylli loses its name in book on Chinese herbal medicine in ancient times.Discovered in recent years, Herb Gynostemmae Pentaphylli has defying age, resisting fatigue, anticancer, endocrine regulation function, can improve human body adaptability to changes and immunity, reduces cholesterol and transaminase, prophylaxis of tumours, suppresses ulcer, keeping tensions down, calm, analgesia
The Radix Astragali: the traditional Chinese medical science is thought " the spleen being the foundation of acquired constitution ".Think the Radix Astragali " beneficial vigour and mend three burnt ", be " all medicines of QI invigorating ".Modern study finds, the Radix Astragali can not only coronary artery dilator, improves blood supply of cardiac muscle, improves immunologic function, and can delaying cell aging.
Radix Angelicae Sinensis: can enrich blood and invigorate blood circulation, menstruction regulating and pain relieving, loosening bowel to relieve constipation, to rheumatic arthralgia, traumatic injury, asthenia cold abdominalgia, blood deficiency and yellow complexion etc. are effective in cure.Modern age, the analysis and research to Radix Angelicae Sinensis showed: it contains V
a﹑ V
b12the plurality of active ingredients such as ﹑ Zong Lv Suan ﹑ You Suan ﹑ Ya You Suan ﹑ Rou Dou Kou Suan – sitosterol, have enhancement blood circulation, promote cell metabolism, suppress pigmentation, the effects such as nourishing the human Body skin.
Flos Matricariae chamomillae: have defying age, resisting fatigue, moist skin, help mediator's body immunity function, the effect helped for sleep.
Myosotis sylvatica: can skin whitening, delaying cell aging, accelerates metabolic effect especially remarkable, more can liver heat removing and eyesight improving, and enriching yin and nourishing kidney, improve immunity.Also certain eliminating effect is had to freckle, acne.
Flos Moutan: looks improving and the skin nourishing, removing chloasma, slow down aging, the regulating liver-QI that nourishes blood, loose strongly fragrant blood stasis dispelling, Chang Yinke makes that QI and blood is abundant, appearance is ruddy, energetic, reduce blood pressure, alleviate dysmenorrhea, basin blood situation.Invigorating blood circulation with blood, is Women's health-care good merchantable brand.
Dianthus carryophyllus: speckle dispelling wrinkle removal, has and improve blood circulation, enhances metabolism, gets rid of vivotoxin, regulates effect of female incretion.
In the market still not by Folium camelliae assamicae, scented tea and multiple medicinal herb components equilibrium collocation, after comprehensive effective component extracting, then coordinate with the effective moisturizing aging ingredient of biochemistry, have complementary advantages, after scientific formula, the not only safety but also efficient Folium camelliae assamicae anti-aging cream product that develop.
The invention has the beneficial effects as follows: the aging ingredient in the nearly Chinese herbal medicine such as antioxidation, aging ingredient and traditional Radix Ginseng, Ganoderma, Radix Angelicae Sinensis, the Radix Astragali, Radix Notoginseng and newfound Radix Rhodiolae, Herb Gynostemmae Pentaphylli of tens kinds in Folium camelliae assamicae, scented tea is effectively combined, and with modern times biochemistry, antioxidation, aging ingredient is balanced arranges in pairs or groups, learn from other's strong points to offset one's weaknesses.The novel puer tea anti-aging cream developed thus just has the features such as potentiation complementation, safety and effectivity, long-acting quick-acting perfect adaptations.Effectively can meet people to the effect demand of anti-aging skin care product aspect and demand for security, reach safe and effective, long-acting Expected Results, can life-time service, without any side effects.
Detailed description of the invention:
Embodiment 1
The preparation process of special ratios Chinese medicine Folium camelliae assamicae, scented tea magistery extracting solution is as follows:
(1) dry product Radix Ginseng 10 parts, Ganoderma 13 parts, Radix Et Caulis Acanthopanacis Senticosi 15 parts, Radix Rhodiolae 10 parts, Herb Gynostemmae Pentaphylli 13 parts, Radix Angelicae Sinensis 15 parts, the Radix Astragali 10 parts, Radix Notoginseng 15 parts is taken. foreign glycosides chrysanthemum 2 parts, Myosotis sylvatica 4 parts, Flos Moutan 3 parts, Dianthus carryophyllus 3 parts. add in rustless steel still; Take Folium camelliae assamicae 30 parts for subsequent use.
(2), when first time boils, deionized water 700 parts is taken, ethanol ethanol 4 parts, propylene glycol 5 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.2 hours, namely obtain Chinese medicine Folium camelliae assamicae scented tea magistery extracting solution 1. with 600 order filter-cloth filterings afterwards.
(3) in filtering residue, add the propylene glycol of the deionized water of 600 parts and the ethanol of 3 parts and 2 parts, use little fire after big fire is boiled instead and boil 1.0 hours again, add Folium camelliae assamicae afterwards and soak 0.5 hour, use 600 order filter-cloth filterings afterwards, obtain Chinese medicine Folium camelliae assamicae scented tea magistery extracting solution 2..
(4) will 1., 2. namely obtain final Chinese medicine Folium camelliae assamicae scented tea magistery extracting solution after filtrate mix homogeneously, its total amount should control about the half of adding total Water.
Substitute the pure water component in Folium camelliae assamicae, scented tea anti-aging cream with obtained Chinese medicine Folium camelliae assamicae, scented tea magistery extracting solution, by following proportioning (mass percent) design Folium camelliae assamicae, scented tea anti-aging cream prescription as follows:
(1) oil phase component: described oil phase component is made up of the component of following mass parts: 16 mixed alcohols 1 part, 16 stearyl alcohol and 16 octadecyl glucosides 3 parts, tristerin and PEG-100 stearate 2 parts, Oleum Camelliae 1 part, Jojoba oil 4 parts, Semen Tritici aestivi germ oil 3 parts, Oleum Vitis viniferae 0.3 part, white oil 3 parts, iso-octyl palmitate 4 parts, Oleum Hippophae 0.8 part, V
eoil 0.2 part, dimethicone 3 parts, methyl hydroxybenzoate 0.2 part, propylparaben 0.1 part, ditertbutylparacresol 0.03 part.
(2) water phase components: glycerol 6 parts, propylene glycol 3 parts, amino acid humectant 4 parts, the different poly-polysaccharide 0.06 part of Tremella, green tea extract 1 part, Chinese medicine PUERHUACHA magistery extracting solution 56.2 parts, collagen protein 1 part+pure water 3 parts (being uniformly dissolved in advance).
(3) antiseptic: 0.1 part, the mixture of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol.
(4) essence: rice essence 0.01 part.
The preparation method of Folium camelliae assamicae anti-aging cream of the present invention, comprises the steps:
(1) preparation of oil phase part: by 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, tristerin and PEG-100 stearate, Oleum Camelliae, Jojoba oil, Semen Tritici aestivi germ oil, Oleum Vitis viniferae, V
eoil, white oil, iso-octyl palmitate, Oleum Hippophae, dimethicone, methyl hydroxybenzoate, propylparaben, after ditertbutylparacresol takes in proportion, add in the rustless steel still that band stirs, under the stirring of rotating speed 30 revs/min, heating for dissolving is complete, and constant temperature disinfection 20 minutes is stand-by at 85 DEG C.
(2) preparation of aqueous portion: by the glycerol of formula ratio, propylene glycol, amino acid humectant, the different poly-polysaccharide of Tremella, green tea extract, Chinese medicine PUERHUACHA magistery extracting solution, after taking in proportion, first heating for dissolving in rustless steel still, be extracted into afterwards in (passing through drainage screen) rustless steel homogenizing still, under the stirring of 20 revs/min, continue to be heated to 85 DEG C, and constant temperature disinfection 20 minutes, stand-by.
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 50 revs/min, stir after 3 minutes, start high speed homogenization device, homogenizing 5 minutes under the high speed of 5000 revs/min, wall rotating speed will be scraped afterwards and drop to 30 revs/min, and 50 DEG C are cooled under this rotating speed, add collagen protein solvent in advance, homogenizing 2 minutes, then continue to be cooled to 40 DEG C, add the antiseptic of formula ratio, essence, continue to stir 15 minutes under same rotating speed, get final product discharging.
Embodiment 2
The preparation process of special ratios Chinese medicine Folium camelliae assamicae, scented tea magistery extracting solution is as follows:
(1) dry product Radix Ginseng 13 parts, Ganoderma 10 parts, Radix Et Caulis Acanthopanacis Senticosi 13 parts, Radix Rhodiolae 15 parts, Herb Gynostemmae Pentaphylli 15 parts, Radix Angelicae Sinensis 10 parts, the Radix Astragali 13 parts, Radix Notoginseng 13 parts is taken. foreign glycosides chrysanthemum 4 parts, Myosotis sylvatica 3 parts, Flos Moutan 2 parts, Dianthus carryophyllus 4 parts. add in rustless steel still; Take Folium camelliae assamicae 35 parts for subsequent use.
(2), when first time boils, deionized water 750 parts is taken, ethanol ethanol 5 parts, propylene glycol 5 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.2 hours, namely obtain Chinese medicine Folium camelliae assamicae scented tea magistery extracting solution 1. with 600 order filter-cloth filterings afterwards;
(3) in filtering residue, add the propylene glycol of the deionized water of 550 parts and the ethanol of 3 parts and 2 parts, use little fire after big fire is boiled instead and boil 1.0 hours again, add Folium camelliae assamicae afterwards and soak 0.8 hour, use 600 order filter-cloth filterings afterwards, obtain Chinese medicine Folium camelliae assamicae scented tea magistery extracting solution 2.;
(4) will 1., 2. namely obtain final Chinese medicine Folium camelliae assamicae scented tea magistery extracting solution after filtrate mix homogeneously, its total amount should control about the half of adding total Water.
Substitute the pure water component in Folium camelliae assamicae, scented tea anti-aging cream with obtained Chinese medicine Folium camelliae assamicae, scented tea magistery extracting solution, by following proportioning (mass percent) design Folium camelliae assamicae, scented tea anti-aging cream prescription as follows:
(1) oil phase component: described oil phase component is made up of the component of following mass parts: 16 mixed alcohols 1.2 parts, 16 stearyl alcohol and 16 octadecyl glucosides 2 parts, tristerin and PEG-100 stearate 2 parts, Oleum Camelliae 1.2 parts, Jojoba oil 4 parts, Semen Tritici aestivi germ oil 3 parts, Oleum Vitis viniferae 0.5 part, white oil 3 parts, iso-octyl palmitate 3 parts, Oleum Hippophae 0.7 part, V
eoil 0.4 part, dimethicone 2 parts, methyl hydroxybenzoate 0.2 part, propylparaben 0.1 part, ditertbutylparacresol 0.03 part.
(2) water phase components: glycerol 7 parts, propylene glycol 3 parts, amino acid humectant 3 parts, the different poly-polysaccharide 0.07 part of Tremella, green tea extract 1.2 parts, Chinese medicine PUERHUACHA magistery extracting solution 56.29 parts. collagen protein 1.5 parts+pure water 4.5 parts dissolving.
(3) antiseptic: 0.1 part, the mixture of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol.
(4) essence: rice essence 0.01 part.
The present embodiment the preparation method of Folium camelliae assamicae anti-aging cream, comprise the steps:
(1) preparation of oil phase part: by 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, tristerin and PEG-100 stearate, Oleum Camelliae, Jojoba oil, Semen Tritici aestivi germ oil, Oleum Vitis viniferae, V
eoil, white oil, iso-octyl palmitate, Oleum Hippophae, dimethicone, methyl hydroxybenzoate, propylparaben, after ditertbutylparacresol takes in proportion, add in the rustless steel still that band stirs, under the stirring of rotating speed 25 revs/min, heating for dissolving is complete, and constant temperature disinfection 20 minutes is stand-by at 85 DEG C.
(2) preparation of aqueous portion: by the glycerol of formula ratio, propylene glycol, amino acid humectant, the different poly-polysaccharide of Tremella, green tea extract, Chinese medicine PUERHUACHA magistery extracting solution, after taking in proportion, first heating for dissolving in rustless steel still, be extracted into afterwards in (passing through drainage screen) rustless steel homogenizing still, under the stirring of 25 revs/min, continue to be heated to 85 DEG C, and constant temperature disinfection 20 minutes, stand-by.
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 50 revs/min, stir after 3 minutes, start high speed homogenization device, homogenizing 5 minutes under the high speed of 4800 revs/min, wall rotating speed will be scraped afterwards and drop to 30 revs/min, and 50 DEG C are cooled under this rotating speed, add collagen protein solvent in advance, homogenizing 3 minutes, then continue to be cooled to 40 DEG C, add the antiseptic of formula ratio, essence, continue to stir 15 minutes under same rotating speed, get final product discharging.
Embodiment 3
The preparation process of special ratios Chinese medicine Folium camelliae assamicae, scented tea magistery extracting solution is as follows:
(1) dry product Radix Ginseng 15 parts, Ganoderma 15 parts, Radix Et Caulis Acanthopanacis Senticosi 10 parts, Radix Rhodiolae 13 parts, Herb Gynostemmae Pentaphylli 10 parts, Radix Angelicae Sinensis 13 parts, the Radix Astragali 10 parts, Radix Notoginseng 10 parts is taken. foreign glycosides chrysanthemum 3 parts, Myosotis sylvatica 2 parts, Flos Moutan 4 parts, Dianthus carryophyllus 2 parts. add in rustless steel still; Take Folium camelliae assamicae 40 parts for subsequent use.
(2), when first time boils, deionized water 800 parts is taken, ethanol ethanol 4 parts, propylene glycol 5 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.2 hours, namely obtain Chinese medicine Folium camelliae assamicae scented tea magistery extracting solution 1. with 600 order filter-cloth filterings afterwards.
(3) in filtering residue, add the propylene glycol of the deionized water of 500 parts and the ethanol of 3 parts and 2 parts, use little fire after big fire is boiled instead and boil 1.0 hours again, add Folium camelliae assamicae afterwards and soak 1.0 hours, use 600 order filter-cloth filterings afterwards, obtain Chinese medicine Folium camelliae assamicae scented tea magistery extracting solution 2..
(4) will 1., 2. namely obtain final Chinese medicine Folium camelliae assamicae scented tea magistery extracting solution after filtrate mix homogeneously, its total amount should control about the half of adding total Water.
Substitute the pure water component in Folium camelliae assamicae, scented tea anti-aging cream with obtained Chinese medicine Folium camelliae assamicae, scented tea magistery extracting solution, by following proportioning (mass percent) design Folium camelliae assamicae, scented tea anti-aging cream prescription as follows:
(1) oil phase component: described oil phase component is made up of the component of following mass parts: 16 mixed alcohols 1.5 parts, 16 stearyl alcohol and 16 octadecyl glucosides 2 parts, tristerin and PEG-100 stearate 1 part, Oleum Camelliae 1.5 parts, Jojoba oil 3 parts, Semen Tritici aestivi germ oil 2 parts, Oleum Vitis viniferae 0.6 part, V
eoil 0.5 part, white oil 4 parts, iso-octyl palmitate 3 parts, Oleum Hippophae 1 part, dimethicone 4 parts, methyl hydroxybenzoate 0.2 part, propylparaben 0.1 part, ditertbutylparacresol 0.03 part.
(2) water phase components: glycerol 8 parts, propylene glycol 2 parts, amino acid humectant 3 parts, the different poly-polysaccharide 0.05 part of Tremella, green tea extract 1.4 parts, Chinese medicine PUERHUACHA magistery extracting solution 53.01 parts. collagen protein 2 parts+pure water 6 parts dissolving.
(3) antiseptic: 0.1 part, the mixture of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol.
(4) essence: rice essence 0.01 part.
The preparation method of Folium camelliae assamicae anti-aging cream of the present invention, comprises the steps:
(1) preparation of oil phase part: by 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, tristerin and PEG-100 stearate, Oleum Camelliae, Jojoba oil, Semen Tritici aestivi germ oil, Oleum Vitis viniferae, V
eoil, white oil, iso-octyl palmitate, Oleum Hippophae, dimethicone, methyl hydroxybenzoate, propylparaben, after ditertbutylparacresol takes in proportion, add in the rustless steel still that band stirs, under the stirring of rotating speed 30 revs/min, heating for dissolving is complete, and constant temperature disinfection 20 minutes is stand-by at 85 DEG C.
(2) preparation of aqueous portion: by the glycerol of formula ratio, propylene glycol, amino acid humectant, the different poly-polysaccharide of Tremella, green tea extract, Chinese medicine PUERHUACHA magistery extracting solution, after taking in proportion, first heating for dissolving in rustless steel still, be extracted into afterwards in (passing through drainage screen) rustless steel homogenizing still, under the stirring of 20 revs/min, continue to be heated to 85 DEG C, and constant temperature disinfection 20 minutes, stand-by.
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 50 revs/min, stir after 3 minutes, start high speed homogenization device, homogenizing 5 minutes under the high speed of 5000 revs/min, wall rotating speed will be scraped afterwards and drop to 30 revs/min, and 50 DEG C are cooled under this rotating speed, add collagen protein solvent in advance, homogenizing 4 minutes, then continue to be cooled to 40 DEG C, add the antiseptic of formula ratio, essence, continue to stir 15 minutes under same rotating speed, get final product discharging;
Effect example:
Detection method:
The sample preparation of previous embodiment become concentration to be the concentration of mass volume ratio 1% respectively with dimethyl sulfoxide, carry out following experiment.
The mensuration of free radical scavenging effect
(1) extracting sample solution 2ml and concentration are that diphenyl picryl Ben Jing ﹙ DPPH ﹚ solution (solvent of this solution the is water) 2ml of 100umol/L first adds in same tool plug test tube, shake up, left at room temperature 30 minutes take solvent as blank, working sample absorbance under 517nm wavelength.
Suppression ratio: k%=[1-(Ai-Aj)/AC] × 100%
The absorbance of Ai:2mlDPPH solution+2ml sample solution
The absorbance of Aj:2ml sample solution+2ml solvent (i.e. dimethyl sulfoxide)
The absorbance of AC:2mlDPPH solution+2ml solvent (i.e. dimethyl sulfoxide)
Experimental result
The mensuration of free radical scavenging effect, result is as table
| Suppression ratio (%) | |
| Embodiment 1 | 89．2 |
| Embodiment 2 | 90．7 |
| Embodiment 3 | 90．5 |
Above-described embodiment is the present invention's preferably embodiment; but embodiments of the present invention are not restricted to the described embodiments; the Gai Bian ﹑ Xiu Shi ﹑ Ti Dai ﹑ Zu He ﹑ done under other any does not deviate from spirit of the present invention and principle simplifies; all should be the substitute mode of equivalence, be included within protection scope of the present invention.
Claims (2)
1. a Folium camelliae assamicae anti-aging cream, is characterized in that being prepared from by following component:
(1) oil phase component: described oil phase component is made up of the component of following mass parts: 16 mixed alcohol 1-1.5 parts, 16 stearyl alcohol and 16 octadecyl glucosides 2-4 parts, tristerin and PEG-100 stearate 1-3 parts, Oleum Camelliae 1-1.5 parts, Jojoba oil 2-4 parts, Semen Tritici aestivi germ oil 2-4 parts, Oleum Vitis viniferae 0.1-1.0 parts, V
eoil 0.2-0.5 part, white oil 2-4 parts, iso-octyl palmitate 2-4 parts, Oleum Hippophae 0.5-1.0 parts, dimethicone 2-4 parts, methyl hydroxybenzoate 0.2-0.3 part, propylparaben 0.1-0.15 part, ditertbutylparacresol 0.03-0.05 part;
(2) water phase components: glycerol 6--8 part, propylene glycol 2-3 parts, amino acid humectant 3-4 parts, the different poly-polysaccharide 0.05-0.08 part of Tremella, green tea extract 1-2 parts, collagen protein 1-2 parts, pure water 3-6 parts, Chinese medicine PUERHUACHA constituents extraction liquid 53-57 part; Described Chinese medicine PUERHUACHA constituents extraction liquid is that the raw material of following mass parts is made: Folium camelliae assamicae 20-40 parts, Radix Ginseng, Ganoderma, Radix Et Caulis Acanthopanacis Senticosi, Radix Rhodiolae, Herb Gynostemmae Pentaphylli, Radix Angelicae Sinensis, the Radix Astragali, each 10-15 parts of Radix Notoginseng, Flos Matricariae chamomillae, Myosotis sylvatica, Flos Moutan, each 2-4 parts of Dianthus carryophyllus;
Described Chinese medicine PUERHUACHA constituents extraction liquid prepares by the following method:
A () takes dry product Radix Ginseng, Ganoderma, Radix Et Caulis Acanthopanacis Senticosi, Radix Rhodiolae, Herb Gynostemmae Pentaphylli, Radix Angelicae Sinensis, the Radix Astragali, each 10-15 parts of Radix Notoginseng, Flos Matricariae chamomillae, Myosotis sylvatica, Flos Moutan, each 2-4 parts of Dianthus carryophyllus, add in rustless steel still and boil; Take Folium camelliae assamicae 20-40 parts for subsequent use;
B () first time, when boiling, takes deionized water 700-800 parts, ethanol 4-6 parts, propylene glycol 4-6 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.0-1.2 hours, namely obtain Chinese medicine PUERHUACHA constituents extraction liquid 1. with 600 order filter-cloth filterings afterwards;
C () adds the propylene glycol of the deionized water of 500-600 mass parts and the ethanol of 1-3 mass parts and 1-3 mass parts in filtering residue, use little fire after big fire is boiled instead and boil 0.8-1.0 hours again, add Folium camelliae assamicae afterwards to soak 0.5-1.0 hours, use 600 order filter-cloth filterings afterwards, obtain Chinese medicine PUERHUACHA constituents extraction liquid 2.;
D () will 1., 2. namely obtain final Chinese medicine PUERHUACHA constituents extraction liquid after filtrate mix homogeneously, and its total amount should control in the half of adding total Water;
(3) antiseptic: 0.1-0.15 part, the mixture of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol;
(4) essence: rice essence 0.01-0.02 part.
2. a preparation method for Folium camelliae assamicae anti-aging cream as claimed in claim 1, is characterized in that, comprise the steps:
(1) preparation of phase 1: by 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, tristerin and PEG-100 stearate, Oleum Camelliae, Jojoba oil, Semen Tritici aestivi germ oil, Oleum Vitis viniferae, V
eoil, white oil, iso-octyl palmitate, Oleum Hippophae, dimethicone, methyl hydroxybenzoate, propylparaben, after ditertbutylparacresol takes in proportion, adds in the rustless steel still of band stirring, under the stirring of rotating speed 20-30 revs/min, heating for dissolving is complete, and constant temperature disinfection 20 minutes is stand-by at 80-85 DEG C;
(2) preparation of phase 2: by the glycerol of formula ratio, propylene glycol, amino acid humectant, the different poly-polysaccharide of Tremella, green tea extract, Chinese medicine PUERHUACHA constituents extraction liquid, after taking in proportion, first heating for dissolving in rustless steel still, be extracted in rustless steel homogenizing still afterwards, under the stirring of 20-30 revs/min, continue to be heated to 80--85 DEG C, and constant temperature disinfection 20 minutes, stand-by;
(3) by phase 1 slowly suction phase 2, and scrape wall stirring, rotating speed is increased to 40-50 revs/min, stir after 2-3 minutes, start high speed homogenization device, homogenizing 3-5 minutes under the high speed of 3000-5000 revs/min, wall rotating speed will be scraped afterwards and drop to 30-40 revs/min, and 50 DEG C are cooled under this rotating speed, add with pure water collagen protein solvent in advance, homogenizing 2-4 minutes, then continue to be cooled to 40 DEG C, add the antiseptic of formula ratio, essence, continue to stir 15-20 minutes under same rotating speed, get final product discharging.
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| CN103860453B (en) * | 2014-04-11 | 2016-03-09 | 六安市丹皇生物科技有限责任公司 | A kind of face of living is compacted emollient cream and preparation method thereof |
| CN103919711B (en) * | 2014-04-14 | 2016-06-01 | 郑州市嘉蓓丽生物科技有限公司 | A kind of anti-ageing whitening cream of oolong tea and manufacture method thereof |
| CN104116701A (en) * | 2014-06-26 | 2014-10-29 | 张少维 | Herbal clay facial mask |
| CN104523561A (en) * | 2014-12-30 | 2015-04-22 | 洛阳万山高新技术应用工程有限公司 | Anti-aging skin-tendering cream and preparation method thereof |
| CN104688620B (en) * | 2015-02-11 | 2018-04-06 | 永腾生技有限公司 | A kind of skin care composition, Its Preparation Method And Use |
| CN104887563B (en) * | 2015-05-13 | 2018-06-22 | 郑州市嘉蓓丽生物科技有限公司 | A kind of coreopsis tinctoria flower tea anti-allergy facial mask frost and preparation method thereof |
| CN105168047A (en) * | 2015-09-08 | 2015-12-23 | 苏州市天灵中药饮片有限公司 | Traditional Chinese medicine type anti-aging serum and preparation method thereof |
| CN105194102A (en) * | 2015-10-30 | 2015-12-30 | 中国科学院昆明植物研究所 | Camellia sinensis var.assamica extract, preparation method thereof and application of Camellia sinensis var.assamica extract in cosmetics |
| CN106074295A (en) * | 2016-07-22 | 2016-11-09 | 郑州景鸿畜牧科技有限公司 | The crease-resistant astringent of Folium camelliae assamicae |
| CN106619452A (en) * | 2016-12-16 | 2017-05-10 | 杨箭 | Wine ganoderma pollen anti-aging cream and manufacture method thereof |
| CN107137267A (en) * | 2017-05-07 | 2017-09-08 | 湖北民族学院 | A kind of preparation method of rhodiola root skin conditioner |
| CN107582450A (en) * | 2017-09-15 | 2018-01-16 | 广州赛莱拉干细胞科技股份有限公司 | A kind of anti-apolexis composition and the skin care item containing said composition |
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| CN1981585B (en) * | 2005-12-14 | 2010-09-29 | 李虹枚 | Flowery pu'er tea |
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