CN106580833A - Whitening moisturizing cream - Google Patents
Whitening moisturizing cream Download PDFInfo
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- CN106580833A CN106580833A CN201611240713.0A CN201611240713A CN106580833A CN 106580833 A CN106580833 A CN 106580833A CN 201611240713 A CN201611240713 A CN 201611240713A CN 106580833 A CN106580833 A CN 106580833A
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- extract
- preserving moisture
- whitening skin
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- whitening
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
Abstract
The invention discloses whitening moisturizing cream containing bletilla striata stem extract. The whitening moisturizing cream comprises bletilla striata stem extract, dandelion extract, lily extract, caprylic/capric triglyceride, cyclopentadimethylsiloxane/cyclohexasioxane, polydimethylsiloxane, cetostearyl alcohol, laurocapram, cetostearyl alcohol/cetearyl glucoside, glyceryl stearate/PEG-100 stearate, and polyacrylamide/C13-14 isoparaffin/laureth-7. The components are scientifically combined. Through inhibition of tyrosinase activity and removal of free radicals, SOD activity is improved, water replenishment and locking are realized, skin is nourished and penetration is promoted. The components are complementary with each other so that the cream has good permeability, is easy to absorb and has remarkable effects of whitening and moisturizing skin.
Description
Technical field
The present invention relates to cosmetic field, and in particular to a kind of frost of the whitening skin and preserving moisture containing Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract.
Background technology
The three-dimensional whitening for integrating " water profit, penetrating, pale " has become the gold of current ideal skin specialty whitening
Standard.In recent years people have been no longer satisfied with covering facial defect with foundation cream etc., but more pursue beauty of nature white effect
And focus more on the whitening mode of health.The colour of skin is largely determined by the generation of pigment, divides a word with a hyphen at the end of a line and be distributed, and whitening is dispelled
Speckle research emphasis are concentrated in TYR enzyme.TYR is a kind of common aminoacid of human body, in melanocyte melanocyte is carried, network
Propylhomoserin forms DOPA quinone by DOPA is generated after TYR enzyme catalysis after DOPA dehydrogenation, and is rearranged into 5,6 oxyindoles, Yin
Melanoprotein, i.e. melanin described in us are formed in combination with the structural protein in melanocyte body after diindyl polymerization.It is melanic to contain
Amount determines the color of skin, so, can be during melanin biosynthesis, by suppression TYR enzyme activity or anti-
Each blocking point reaction in chain is answered to carry out or reduce melanic synthesis；Black can be decomposed by redox
Element；Cutin is promoted to peel off, promote melanin to discharge etc..By the mechanism of action, skin-lightening cosmetic be divided into tyrosinase activity inhibitor,
Melanocyte toxic agents, impact melanin metabolism agent, opacifier, reducing agent and Chemical peeling agent.
China's traditional medicine is the traditional Chinese medical science, and in the traditional Chinese medical science a treasure-house is Chinese medicinal plant, contained flavone in Chinese medicinal plant
Class chemical composition is higher, in some special places or some rare Special plants, often containing distinctive active component.
As biochemistry, cytology, Dermatology constantly develop, melanin formation mechanism it is clear and definite, plant with reference to the huge Chinese medicine of China
Thing treasure-house, studies its outer space for being used for skin whitening huge.Moreover, this year often produces safety problem in cosmetic industry,
People are for the favor degree also more and more higher of plant product, healthy to cosmetics, green, the natural demand of consumer, scientific research
Personnel also continue to increase in the input of plant cosmetic field, so, study plant extract and add it in cosmetics,
Make cosmetics that there is notable whitening skin and preserving moisture effect, be a trend of whitening class cosmetics.
The content of the invention
It is an object of the invention to provide a kind of frost of the whitening skin and preserving moisture containing Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract, its good penetrability, whitening guarantor
Wet composition can effectively reach skin deep layer, improve the brightness of skin, make skin water tender glossy.
A kind of frost of the whitening skin and preserving moisture containing Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract that the present invention is provided, the whitening skin and preserving moisture frost contains by Pseudobulbus Bletillae (Rhizoma Bletillae) stem
Extract, Herba Taraxaci extract, the vegetable composition of Bulbus Lilii extract composition, wherein the Pseudobulbus Bletillae (Rhizoma Bletillae) stem in the vegetable composition is carried
It is (3-10) to take thing, Herba Taraxaci extract, the weight part ratio of Bulbus Lilii extract：(2-10)：(2-8).
Described Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract, Herba Taraxaci extract, Bulbus Lilii extract weight portion it is as follows：Pseudobulbus Bletillae (Rhizoma Bletillae) stem is extracted
Thing 0.3-1 parts, Herba Taraxaci extract 0.2-1 parts, Bulbus Lilii extract 0.2-8 parts.
Preferably, the preparation method of the Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract is as follows：
(1) Pseudobulbus Bletillae (Rhizoma Bletillae) stem is taken, clean dry is ground into coarse grain, coarse grain water boiling and extraction 3 times, each 1.5- of decocting time
2h, merges filtrate twice, stands 2-4h, filters, and filtrate is standby；
(2) step (1) gained filtrate reduced in volume is obtained into thick medicinal extract, thick medicinal extract is spray-dried into (inlet temperature 170
DEG C, 60 DEG C of outlet temperature), dried extractum is ground into into the fine powder of 70 mesh sizes, obtain final product the Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract.
Preferably, the preparation method of the Herba Taraxaci extract is as follows：
(1) 1 part of Herba Taraxaci is weighed, by 1:8 solid-liquid ratio, by the Herba Taraxaci 80% ethanol immersion 30-60min is immersed；
(2) mixed liquor of step (1) is placed in into heating and refluxing extraction 2-3h in water-bath, is filtered, collect filtrate, filtering residue uses 8
Again 80% ethanol of amount repeats to extract once, merges filtrate twice；
(3) by the filtrate reduced in volume of step (2) to without alcohol taste, concentrated solution is adsorbed by AB-8 macroporous resin column,
First with distillation water elution, then 60% ethanol elution is used, collect 60% ethanol elution, Herba Taraxaci extraction is obtained after concentrating under reduced pressure
Thing.
Preferably, the preparation method of the Bulbus Lilii extract is as follows：
(1) 1 portion of Bulbus Lilii is weighed, by 1:8 solid-liquid ratio, by the Bulbus Lilii 75% ethanol immersion 30-60min is immersed；
(2) mixed liquor of step (1) is placed in into heating and refluxing extraction 1-3h in water-bath, is filtered, collect filtrate, filtering residue uses 7
Again 80% ethanol of amount repeats to extract once, merges filtrate twice；
(3) by the filtrate reduced in volume of step (2) to without alcohol taste, concentrated solution is adsorbed by AB-8 macroporous resin column,
First with distillation water elution, then 60% ethanol elution is used, collect 60% ethanol elution, Bulbus Lilii extract is obtained after concentrating under reduced pressure.
A kind of whitening skin and preserving moisture frost includes following component：Vegetable composition 0.7-2.8 parts, emollient 3.9-12.5 parts, emulsifying
Agent 2.3-6 parts, preservative 0.45-0.95 parts, thickening agent 0.05-0.2 parts, penetrating agent 0.5-1.6 parts, deionized water 50-80 parts.
Preferably, the emollient is caprylic/capric triglyceride, ring five dimethyl silicone polymer/cyclohexasiloxane, gathers
The mixture of dimethyl siloxane, cetearyl alcohol.
Preferably, the emulsifying agent is that cetearyl alcohol/cetearyl glucoside, glyceryl stearate/PEG-100 are hard
The mixture of fat acid ester, polyacrylamide/C13-14 isoparaffins/laureth -7.
Preferably, the preservative is phenoxyethanol, the mixture of 1,2- hexanediol；The thickening agent is xanthan gum；Institute
Penetrating agent is stated for laurocapram.
A kind of preparation method of whitening skin and preserving moisture frost is：
1) by cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearic acid
Ester, ring five dimethyl silicone polymer/cyclohexasiloxane, polydimethylsiloxane, caprylic/capric triglyceride, laurocapram
Mixing puts into oil phase pot and is heated to 85 degree as A phases, the completely rear heat preservation for standby use of stirring and dissolving；
2) by xanthan gum, deionized water mixing is added in water phase pot as B and is heated to 85 degree, and stirring and dissolving is protected afterwards completely
Temperature is stand-by；
3) emulsifying pot is preheated to into 60-65 degree, 45 revs/min of mixing speed first by B phase suction, then by A phase suction, is stirred
Mix 30 minutes, temperature is maintained at 85 degree；Homogenizing 3 minutes；
4) C is added to into emulsifying pot, homogenizing 4 minutes, insulated and stirred 30 minutes, temperature is maintained at 80-85 degree, mixing speed
35 revs/min；The C phases are polyacrylamide/C13-14 isoparaffins/laureth -7；
5) being cooled to 40 degree adds according to this E phases, insulated and stirred 10 minutes, 35 revs/min of mixing speed to be eventually adding D phases,
Insulation 10-20 minutes；The D phases are phenoxyethanol, 1,2- hexanediol, and the E phases are vegetable composition；
6) stirring is cooled to 40 degree of evacuation dischargings.
Effect or feature of the plant component of the present invention is as follows:
The main chemical compositions of Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract are polysaccharide, bibenzyl and its derivant, such as syringaresinol, β-paddy steroid
Alcohol, gallic acid etc. are more with antioxidation, the generation for suppressing hydroxy radical, slow down aging, prevention of cardiovascular disease and cancer etc.
Plant biological activity.《Compendium of Materia Medica》It is one of famous in ancient whitening prescription " eight white dissipate " to record the Pseudobulbus Bletillae (Rhizoma Bletillae) " shelves are black, go wild dim ".It is modern
Research shows that Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract has good inhibiting effect to tryrosinase.
In Herba Taraxaci extract containing peroxidase, catalase, sterol, flavone, chlorogenic acid etc. it is various effectively into
Point, these materials with very high anti-oxidation activity can be purged rapidly subcutaneous to free radical, effectively blocking free radical pair
The damaging action of skin；Effectively suppress tyrosinase activity, reduce melanic formation, antioxidation is played to skin, it is anti-aging
Effect.
Polysaccharide in Bulbus Lilii has raising SOD vigor, the generation of blocking activity oxygen and free radical；Discharge the work on its hydroxyl
Bold and vigorous hydrogen, captures free radical, so as to block the chain reaction of free radical, reaches antioxidation.Containing various in Bulbus Lilii extract
Aminoacid has strong hydrophilicity power, plays the role of moisture-absorbing moisture-keeping, keeps moisture of skin, is a kind of nature moisturizing factor.Due to skin-friendly
Good, skin can absorb its aminoacid and be translated into Self substances, maintain enough collagen fiber and elastic fiber, lift skin
Skin physiological function, makes skin keep fine and smooth soft and smooth, gloss flexible.Beneficial effects of the present invention：(1) Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract is
Monarch, Herba Taraxaci extract is minister, and Bulbus Lilii extract makes for assistant, by suppressing tyrosinase activity, removing free radical, blocking black
Element is formed, the approach of nutrition skin moistening, and synergism reaches excellent whitening effect；(2) the nonionic emulsifying that the present invention is adopted
Agent, it is gentle non-stimulated；Using emollient easily permeate, easily absorb；The antibacterial sterilizing power of preservative phenoxyethanol is strong, with 1,2- oneself two
Alcohol compound, can not only fortification system efficiency of preservation, moreover it is possible to reduce the zest of system so that the safety of product is higher；(3) originally
The moisturiser of invention, good penetrability, effective ingredient can reach skin deep layer, have nutrition concurrently, moisten and whitening function, make skin white
Fair-skinned, water is tender, smooth.
Description of the drawings
Fig. 1：Vegetable composition to TYR enzyme activity inhibitory action, abscissa be vegetable composition concentration, vertical coordinate
It is the suppression ratio to TYR enzyme activity.
Specific embodiment
Below in conjunction with specific embodiment, the present invention is further elaborated.
The following component title occurred in text is INCI (Internation Nomenclaure Cosmetic
Ingredent, i.e. international cosmetic raw material name) institute to regulation title：It is cetearyl alcohol/cetearyl glucoside, sweet
It is oleostearin acid esters/PEG-100 stearates, ring five dimethyl silicone polymer/cyclohexasiloxane, caprylic/capric triglyceride, poly-
Acrylamide/C13-14 isoparaffins/laureth -7.
The whitening skin and preserving moisture of the present invention of the embodiment of the present invention 1～5 frost formula is shown in Table one
The whitening skin and preserving moisture of embodiment 1～5 frost preparation method be：
1) by cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearic acid
Ester, ring five dimethyl silicone polymer/cyclohexasiloxane, polydimethylsiloxane, caprylic/capric triglyceride, laurocapram
Mixing puts into oil phase pot and is heated to 85 degree as A phases, the completely rear heat preservation for standby use of stirring and dissolving；
2) by xanthan gum, deionized water mixing is added in water phase pot as B and is heated to 85 degree, and stirring and dissolving is protected afterwards completely
Temperature is stand-by；
3) emulsifying pot is preheated to into 60-65 degree, 45 revs/min of mixing speed first by B phase suction, then by A phase suction, is stirred
Mix 30 minutes, temperature is maintained at 85 degree；Homogenizing 3 minutes；
4) C is added to into emulsifying pot, homogenizing 4 minutes, insulated and stirred 30 minutes, temperature is maintained at 80-85 degree, mixing speed
35 revs/min；The C phases are polyacrylamide/C13-14 isoparaffins/laureth -7；
5) being cooled to 40 degree adds according to this E phases, insulated and stirred 10 minutes, 35 revs/min of mixing speed to be eventually adding D phases,
Insulation 10-20 minutes；The D phases are phenoxyethanol, 1,2- hexanediol, and the E phases are vegetable composition；
6) stirring is cooled to 40 degree of evacuation dischargings.
Comparative example 1
It is not add Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 2
It is not add Herba Taraxaci extract with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 3
It is not add Bulbus Lilii extract with the difference of embodiment 1, other preparation conditions and method are same as Example 1.
Comparative example 4
It is 0.2 with the parts by weight that the difference of embodiment 1 is Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract, other preparation conditions and method and enforcement
Example 1 is identical.
Comparative example 5
It is 1.1 parts with the parts by weight that the difference of embodiment 1 is Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract, other preparation conditions and method and reality
Apply example 1 identical.
Vegetable composition of the present invention suppresses TYR enzyme experiment
Method and apparatus
Vegetable composition of the present invention；Ph=6.8 phosphate buffer solutions (PBS solution), sodium hydroxide (Chinese medicines group chemistry examination
Agent company limited)；TYR enzyme, Tyrosinase EC 1.14.18.19 (signa)；L-DOPA(AcrosOrganics)；
AB204-E electronic analytical balances (METTLE TOLEDO)；UV-1600 ultraviolet spectrophotometers (METTLE TOLEDO).
TYR change into it is melanic during, the catalytic action of TYR enzyme occurs mainly in TYR enzyme and is converted into
DOPA and DOPA change into the process of DOPA quinone, and DOPA quinone is a kind of coloring matter, has absorption at 475nm, using light splitting
Photometer measurement content.L-DOPA is substrate, determines the TYR enzyme inhibitory activity of vegetable composition of the present invention.
The testing sample composition of table two
According to vegetable composition extracting solution of the present invention, 0.15% DOPA solution is accurately drawn shown in table two, it is sufficiently mixed
Uniformly, the TYR enzyme solution of 300 μ/mL is added after being incubated 10 minutes in 30 DEG C of water-baths, continues to cultivate ten minutes, existed immediately
475nm determines its light absorption value.
The computing formula of TYR enzyme suppression ratio (I) is as follows：
I=[(A-B)-(C-D)]/[A-B] × 100%
A:Not plus the absorbance A (A) surveyed of the enzyme-added mixed liquor of vegetable composition；
B:Not plus vegetable composition and plus the absorbance A (B) surveyed of enzyme-added mixed liquor；
C：Plus vegetable composition and enzyme-added absorbance A (C) mixed liquor, being surveyed；
D:Plus the absorbance A (D) that the not enzyme-added mixed liquor of vegetable composition is surveyed.
Vegetable composition sample is diluted to into respectively 5%, 10%, 15%, 20% with PBS, 25% detects each concentration suppression
TYR enzyme activity processed.As a result Fig. 1 is seen
As seen from Figure 1 vegetable composition concentration is when 5% to 20%, vegetable composition suppress TYR enzyme activity with
The growth of metering and increase, when suppressing TYR enzyme activity solubility to reach 20%, TYR enzyme suppression ratio can reach 84%.
Performance of keeping humidity is tested
According to cosmetic composition moisture absorption, the gap of moisturizing, different wetting agents are different to the active force of hydrone, absorb moisture
It is different with the ability of moisture is kept.Oil has sealing process to moisture, can prevent scattering and disappearing for moisture.Big right of hygroscopic effect power
Hydrone active force is strong, absorbs and keep the amount of moisture moisture loss also good than larger closure also few.Imitated using adhesive tape
The biomaterials such as horny layer, cortex, are coated with cosmetics on adhesive tape, simulate the applicable cases of actual cosmetics.In constant temperature and humidity
Under the conditions of a period of time after, weigh sample place before and after it is of poor quality, obtain the loss of sample, moisturizing ingredient can be calculated
Moistening effect.
Experiment material
Some pieces of the clean glass plates of 7.5 × 7.5cm, 3M adhesive plasters, 50～500 μ l liquid-transfering guns, analytical balance, potassium acetate
[K2H3O2] saturated solution relative humidity about 60%, a ten thousandth balance.
Experimental technique and testing procedure
(1) 11 pieces of glass plate weight (M for posting 3M adhesive plasters are weighed0), record respectively
(2) 200 μ l sample drops are taken with liquid-transfering gun to be added on the glass plate for posting 3M adhesive plasters, with analytical balance the weight is weighed
M1(being accurate to 0.0001g), sample is uniformly distributed, and glass plate is put into the exsiccator of the constant humidity of requirement, in triplicate.
Remaining 3 pieces of blank glass plates are put into together in the exsiccator of constant humidity.
(3) after 4h, 8h is placed, glass plate is taken out, weighs glass plate weight (M2), test its moisturizing rate and and relative
Humidity ratio, is immediately placed in the exsiccator of constant humidity after weighing.
(4) it is as far as possible uniform when the points for attention of this experiment smear sample, it is impossible to have carry-over on applicator.By sample
Product take out and weigh and be put into, and an exsiccator is controlled within 15min, average one piece of glass plate 1min.Control time be by
External environment its moisture loss is exposed in sample very fast, can have a strong impact on test result.Glass plate is placed on immediately after taking out
On the blank glass plate controlled in advance, also it is upside down in the container of balance during weighing.
(5) moisturizing rate computing formula：
Moisturizing rate=(M2-M0)/(M1-M0) × 100%
In formula：
M0：Hollow plate quality/g
M1：Glass sheet quality/g after sample-adding
M2：Quality/g after some hours is placed in exsiccator
Test its appropriateness relatively for percent 60 when 4h and 8h moisturizing rate.
Experimental result is referring to following table two with the good commercially available whitening skin and preserving moisture facial cream of certain moistening effect as comparative example 6
Comparative example 1～6 is significantly larger than by the moisturizing rate of the visible embodiment 1～5 of table two, it is seen that the present invention has in terms of moisturizing
Significant effect.；The difference of comparative example 1～3 and embodiment respectively do not add Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract, Herba Taraxaci extract, hundred
Extract is closed, visible whitening skin and preserving moisture frost Synergistic in terms of moisturizing of the present invention is contrasted by comparative example 1～3 and embodiment 1.This
Invention has significant effect in terms of moisturizing.
Efficacy validation
Detection results on probation are carried out to product prepared by embodiment 1-5 and comparative example 1-6.Test object：Each experimental group is equal
For 20 women (25-50 year)；Test zone：Face；Use：Twice daily, persistently using 4 weeks；Test event：Whitening is imitated
Really, moistening effect, smooth flexible.
Result on trial see the table below two.
By the visible skin elasticity of embodiment 1～5 of table two, water is tender and wrinkle depth improves obvious number and significantly more than contrasts
Example 1～6, illustrates that whitening skin and preserving moisture facial cream of the present invention has significant whitening effect, moistening effect, smooth flexible；The whitening of comparative example 4
Effect is obviously improved 8 people, and moistening effect is obviously improved 6 people, smooth flexible to be obviously improved 5 people, hence it is evident that less than other embodiment
And comparative example, illustrate vegetable composition principle active component in whitening skin and preserving moisture facial cream of the present invention；Comparative example 1～3 and embodiment 1
Difference does not respectively add Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract, Herba Taraxaci extract, Bulbus Lilii extract, by comparative example 1～3 and embodiment 1 pair
Than visible whitening skin and preserving moisture frost of the present invention in whitening effect, moistening effect, smooth flexible aspect Synergistic.The present invention is in whitening
Effect, moistening effect, smooth flexible there is significant effect.
Above example only illustrates embodiment of the present invention, does not there is any pro forma restriction to the present invention；Appoint
What is engaged in professional and technical personnel, all has the ability to make some changes using the technology contents for disclosing or modifies, and becomes equivalent
The Equivalent embodiments of change, according to the technology of the present invention essence, simply modification, equivalent variations and modification are carried out to the present invention, are belonged to
In the range of technical solution of the present invention.
Claims (10)
1. a kind of whitening skin and preserving moisture is white, it is characterised in that the whitening skin and preserving moisture frost contains by Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract, Herba Taraxaci extraction
The vegetable composition of thing, Bulbus Lilii extract composition, wherein the Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract, Herba Taraxaci in the vegetable composition is extracted
Thing, the weight part ratio of Bulbus Lilii extract are (3-10)：(2-10)：(2-8).
2. whitening skin and preserving moisture according to claim 1 frost, it is characterised in that the Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract, Herba Taraxaci extract,
The weight portion of Bulbus Lilii extract is as follows：
Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract 0.3-1 parts
Herba Taraxaci extract 0.2-1 parts
Bulbus Lilii extract 0.2-0.8 parts.
3. a kind of whitening skin and preserving moisture according to claim 2 is white, it is characterised in that the preparation method of the Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract
It is as follows：
(1) Pseudobulbus Bletillae (Rhizoma Bletillae) stem is taken, clean dry is ground into coarse grain, coarse grain water boiling and extraction 3 times, each 1.5-2h of decocting time is closed
And filtrate twice, 2-4h is stood, to filter, filtrate is standby；
(2) step (1) gained filtrate reduced in volume is obtained into thick medicinal extract, thick medicinal extract is spray-dried (170 DEG C of inlet temperature,
60 DEG C of outlet temperature), dried extractum is ground into into the fine powder of 70 mesh sizes, obtain final product the Pseudobulbus Bletillae (Rhizoma Bletillae) stem extract.
4. a kind of whitening skin and preserving moisture according to claim 2 is white, it is characterised in that the preparation method of the Herba Taraxaci extract
It is as follows：
(1) 1 part of Herba Taraxaci is weighed, by 1:8 solid-liquid ratio, by the Herba Taraxaci 80% ethanol immersion 30-60min is immersed；
(2) mixed liquor of step (1) is placed in into heating and refluxing extraction 2-3h in water-bath, is filtered, collect filtrate, filtering residue is measured with 8 times
80% ethanol repeats to extract once, merges filtrate twice；
(3) by the filtrate reduced in volume of step (2) to without alcohol taste, concentrated solution is adsorbed by AB-8 macroporous resin column, is first used
Distillation water elution, then 60% ethanol elution is used, 60% ethanol elution is collected, Herba Taraxaci extract is obtained after concentrating under reduced pressure.
5. a kind of whitening skin and preserving moisture according to claim 2 is white, it is characterised in that the preparation method of the Bulbus Lilii extract is such as
Under：
(1) 1 portion of Bulbus Lilii is weighed, by 1:8 solid-liquid ratio, by the Bulbus Lilii 75% ethanol immersion 30-60min is immersed；
(2) mixed liquor of step (1) is placed in into heating and refluxing extraction 1-3h in water-bath, is filtered, collect filtrate, filtering residue is measured with 7 times
80% ethanol repeats to extract once, merges filtrate twice；
(3) by the filtrate reduced in volume of step (2) to without alcohol taste, concentrated solution is adsorbed by AB-8 macroporous resin column, is first used
Distillation water elution, then 60% ethanol elution is used, 60% ethanol elution is collected, Bulbus Lilii extract is obtained after concentrating under reduced pressure.
6. a kind of whitening skin and preserving moisture frost according to claim 1, it is characterised in that the whitening skin and preserving moisture frost include it is following into
Point：
Vegetable composition 0.7-2.8 parts
Emollient 3.9-12.5 parts
Emulsifying agent 2.3-6 parts
Preservative 0.45-0.95 parts
Thickening agent 0.05-0.2 parts
Penetrating agent 0.5-1.6 parts
Deionized water 50-80 parts.
7. a kind of whitening skin and preserving moisture according to claim 5 is white, it is characterised in that the emollient is caprylic/capric glycerol
Three esters, ring five dimethyl silicone polymer/cyclohexasiloxane, polydimethylsiloxane, the mixture of cetearyl alcohol.
8. a kind of whitening skin and preserving moisture according to claim 5 is white, it is characterised in that the emulsifying agent is cetearyl alcohol/whale
Wax stearyl glucoside, glyceryl stearate/PEG-100 stearates, polyacrylamide/C13-14 isoparaffins/lauryl alcohol
The mixture of polyethers -7.
9. a kind of whitening skin and preserving moisture frost according to claim 5, it is characterised in that the preservative be phenoxyethanol, 1,2-
The mixture of hexanediol；The thickening agent is xanthan gum；The penetrating agent is laurocapram.
10. a kind of method of the whitening skin and preserving moisture frost prepared described in any one of claim 1-9, it is characterised in that methods described is：
1) by cetearyl alcohol/cetearyl glucoside, cetearyl alcohol, glyceryl stearate/PEG-100 stearates,
Ring five dimethyl silicone polymer/cyclohexasiloxane, polydimethylsiloxane, caprylic/capric triglyceride, laurocapram mixing
Oil phase pot is put into as A phases be heated to 85 degree, the completely rear heat preservation for standby use of stirring and dissolving；
2) by xanthan gum, deionized water mixing is added in water phase pot as B and is heated to 85 degree, and stirring and dissolving completely afterwards treat by insulation
With；
3) emulsifying pot is preheated to into 60-65 degree, 45 revs/min of mixing speed, first by B phase suction, then by A phase suction, stirs 30
Minute, temperature is maintained at 85 degree；Homogenizing 3 minutes；
4) C is added to into emulsifying pot, homogenizing 4 minutes, insulated and stirred 30 minutes, temperature is maintained at 80-85 degree, mixing speed 35
Rev/min；The C phases are polyacrylamide/C13-14 isoparaffins/laureth -7；
5) being cooled to 40 degree adds according to this E phases, insulated and stirred 10 minutes, 35 revs/min of mixing speed to be eventually adding D phases, insulation
10-20 minutes；The D phases are phenoxyethanol, 1,2- hexanediol, and the E phases are vegetable composition；
6) stirring is cooled to 40 degree of evacuation dischargings.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611240713.0A CN106580833A (en) | 2016-12-28 | 2016-12-28 | Whitening moisturizing cream |
Applications Claiming Priority (1)
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| CN201611240713.0A CN106580833A (en) | 2016-12-28 | 2016-12-28 | Whitening moisturizing cream |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107041864A (en) * | 2017-05-04 | 2017-08-15 | 中国林业科学研究院林产化学工业研究所 | A kind of application of dandelion extract in whitening sun protection cosmetics |
| CN108938513A (en) * | 2017-10-25 | 2018-12-07 | 游云利 | A kind of clear skin anti-acne face beautifying cream of quantum and preparation method thereof |
| CN110192999A (en) * | 2019-07-17 | 2019-09-03 | 广州珈纳生物科技有限公司 | A kind of frivolous water profit sun screen and preparation method thereof |
-
2016
- 2016-12-28 CN CN201611240713.0A patent/CN106580833A/en active Pending
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107041864A (en) * | 2017-05-04 | 2017-08-15 | 中国林业科学研究院林产化学工业研究所 | A kind of application of dandelion extract in whitening sun protection cosmetics |
| CN108938513A (en) * | 2017-10-25 | 2018-12-07 | 游云利 | A kind of clear skin anti-acne face beautifying cream of quantum and preparation method thereof |
| CN108938513B (en) * | 2017-10-25 | 2021-08-24 | 游云利 | Skin-cleaning acne-removing beauty cream and preparation method thereof |
| CN110192999A (en) * | 2019-07-17 | 2019-09-03 | 广州珈纳生物科技有限公司 | A kind of frivolous water profit sun screen and preparation method thereof |
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