CN106137875B - A kind of composition and facial mask - Google Patents

A kind of composition and facial mask Download PDF

Info

Publication number
CN106137875B
CN106137875B CN201610718982.7A CN201610718982A CN106137875B CN 106137875 B CN106137875 B CN 106137875B CN 201610718982 A CN201610718982 A CN 201610718982A CN 106137875 B CN106137875 B CN 106137875B
Authority
CN
China
Prior art keywords
extract
facial mask
composition
skin
parts
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201610718982.7A
Other languages
Chinese (zh)
Other versions
CN106137875A (en
Inventor
魏坤
王晓慧
秦烨芝
胡露
谢水林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
GUANGZHOU RUI SEN BIOTECHNOLOGY Co Ltd
Original Assignee
GUANGZHOU RUI SEN BIOTECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by GUANGZHOU RUI SEN BIOTECHNOLOGY Co Ltd filed Critical GUANGZHOU RUI SEN BIOTECHNOLOGY Co Ltd
Priority to CN201610718982.7A priority Critical patent/CN106137875B/en
Publication of CN106137875A publication Critical patent/CN106137875A/en
Application granted granted Critical
Publication of CN106137875B publication Critical patent/CN106137875B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4973—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom
    • A61K8/498—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with oxygen as the only hetero atom having 6-membered rings or their condensed derivatives, e.g. coumarin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/08—Anti-ageing preparations

Abstract

The invention belongs to daily chemical products fields, and in particular to a kind of composition and the facial mask containing the composition.Composition of the present invention includes flue berry extract, Radix seu Caulis Parabarii extract and hesperetin, has the effect of collaboration, makes the composition while having effects that whitening and anti-aging, antiplaque.Facial mask of the present invention contains various plants extract, meets natural skin care theory, provides nutrition needed for skin；Wheat-germ oil and rose can play the role of sterilization.Rose also has the effects that keep the skin wet, moisturizing, quick anti-inflammatory, antiallergy, it is antipruritic, slow down aging, and the fragrance of product pleasure can be assigned.The facial mask of the present invention not only remains the natural red of dragon fruit, assign product good and natural appearance, most of effect of common facial mask is also gathered, such as skin whitening, moisturizing, the anti crease and anti senile, skin that compacts lighten the stain and antiallergic is anti-inflammatory and other effects, it is suitble to various skin, it is safe and non-toxic non-stimulated, meet most of consumer demand.

Description

A kind of composition and facial mask
Technical field
The invention belongs to daily chemical products fields, and in particular to a kind of composition and the facial mask containing the composition, especially With skin whitening, moisturizing, the anti crease and anti senile, skin that compacts, the composition lightened the stain and other effects and containing the facial mask of the composition.
Background technology
Facial mask is a kind of cosmetics for face's nursing, primarily serves cleaning and the quickly effect of conveying nutrition.With The raising of living standards of the people, people are to the pursuit of facial mask not just merely because brand effect, the work being more concerned in facial mask Property ingredient, it is desirable that green natural.Many facial masks currently on the market contain the hazardous compounds such as lead, mercury, though U.S. can be rapidly achieved White effect, but prodigious injury can be caused to human body.Furthermore modern life rhythm is getting faster, and it is desirable to be used only A kind of product can reach multi-effect, without using multiple product.Common facial mask effect is single, therefore, with plant extracts For functional component and the facial mask with multiple efficacies can be favored surely by consumer.
Invention content
In view of the deficiencies in the prior art, the present invention provides a kind of composition including a variety of natural plant extracts and contain There is a facial mask of the composition, the composition has skin whitening, moisturizing, the anti crease and anti senile, skin that compacts, lightens the stain and other effects.
In order to achieve the above-mentioned object of the invention, the present invention provides following technical scheme：
A kind of composition, including flue berry extract, Radix seu Caulis Parabarii extract and hesperetin.
Preferably, in parts by weight, the composition include 3-10 parts of flue berry extract, 2-6 parts of Radix seu Caulis Parabarii extract, 1-4 parts of hesperetin.
Preferably, the composition further includes Radix et Caulis Opuntiae Dillenii extract.
Preferably, the Radix et Caulis Opuntiae Dillenii extract is Mibangta cactus extract.
Preferably, in parts by weight, the composition contains 1.6-5 parts of the meter Ta Bang Radix et Caulis Opuntiae Dillenii extracts.
The present invention also provides a kind of facial mask, including flue berry extract, Radix seu Caulis Parabarii extract, hesperetin, meter Bang Ta are celestial People slaps extract, base peptide 3000, rose, wheat-germ oil, cyclomethicone, cetostearyl alcohol, coco group Portugal Glucosides, propylene glycol, Sodium Hyaluronate, hydroxy-ethyl acrylate, film forming agent, pH adjusting agent and water.
Preferably, the facial mask, it is by percentage to the quality, composed of the following components：Flue berry extract 3-10%, red Du Secondary extract 2-6%, hesperetin 1-4%, Mibangta cactus extract 1.6-5%, 3000 0.5-1.8% of base peptide, rose are pure Reveal 0.2-1%, wheat-germ oil 2-5%, cyclomethicone 1-3%, cetostearyl alcohol 0.3-2.4%, coco group Portugal Glucosides 0.3-3%, propylene glycol 3.6-10%, Sodium Hyaluronate 1-5%, hydroxy-ethyl acrylate 0.5-1%, film forming agent 4-10%, PH adjusting agent 0.04-1.5%, water are supplied.
Preferably, the film forming agent is at least one of polyethylene glycol, algin, xanthan gum, chitosan.
Preferably, the pH adjusting agent is at least one of citric acid, triethanolamine.
The preparation method of facial mask of the present invention, includes the following steps：
A, press Material Percentage, by film forming agent, hydroxy-ethyl acrylate, Sodium Hyaluronate, water, propylene glycol be heated to 70 DEG C- 85 DEG C of dissolvings are complete, stir evenly；
B, wheat-germ oil, cyclomethicone, cetostearyl alcohol, coco group glucoside are heated to 70 DEG C -85 DEG C, it stirs to being completely dissolved, cools down after emulsifying homogeneous；
C, it waits for that temperature is down to 45 DEG C -50 DEG C, flue berry extract, Radix seu Caulis Parabarii extract, hesperetin, meter Bang Ta celestial beings is added Extract, base peptide 3000, rose are slapped, is stirred evenly, adjusting pH to 5.5-6.8 with pH adjusting agent is made facial mask.
As shown from the above technical solution, the present invention provides a kind of composition and contain the facial mask of the composition.The present invention The composition includes flue berry extract, Radix seu Caulis Parabarii extract and hesperetin.Flue berry extract is rich in anthocyanidin, has U.S. It is anti-ageing and other effects in vain；Radix seu Caulis Parabarii extract can inhibit the generation of melanin；Hesperetin is plant whitening most effective so far One of ingredient.It is added while flue berry extract, Radix seu Caulis Parabarii extract and hesperetin, has the effect of collaboration, make the combination Object has effects that whitening and anti-aging, antiplaque simultaneously.Facial mask of the present invention contains various plants extract, meets natural shield Skin theory provides nutrition needed for skin, especially flue berry extract and contains more anthocyanidin, and anthocyanidin is pure natural resist Aging nutritional supplement is effective antioxidant, in addition, Radix seu Caulis Parabarii extract has significant inhibit to tyrosinase activity Effect, can significantly reduce the generation of melanin.Wheat-germ oil and rose in facial mask of the present invention, which can play, to kill The effect of bacterium, without additional addition chemical preservative in formula.Rose, which also has, to keep the skin wet, moisturizing, quick anti-inflammatory, resists Allergy, antipruritic, the effects that slowing down aging, and the fragrance of product pleasure can be assigned.The facial mask of the present invention not only remains flue Fruit it is natural red, assign product good and natural appearance, also gathered most of effect of common facial mask, as whitening is protected Wet, the anti crease and anti senile, skin that compacts lightens the stain and antiallergic is anti-inflammatory and other effects, is suitble to various skin, safe and non-toxic non-stimulated, symbol Close most of consumer demand.
Specific implementation mode
Below in conjunction with the embodiment of the present invention, technical scheme in the embodiment of the invention is clearly and completely described, Obviously, described embodiments are only a part of the embodiments of the present invention, instead of all the embodiments.Based in the present invention Embodiment, every other embodiment obtained by those of ordinary skill in the art without making creative efforts, all Belong to the scope of protection of the invention.
In order to achieve the above-mentioned object of the invention, the present invention provides following technical scheme：
A kind of composition, including flue berry extract, Radix seu Caulis Parabarii extract and hesperetin.
Wherein dragon fruit also known as Green Dragon fruit, Hylocereus undatus are Cactaceae triangular prism platymisciums, have red skin and white flesh, red skin red Meat and Calusena lansium series, sweet juice is more, full of nutrition, and function is unique.Dragon fruit has antitumor, antiviral, Constipation, promotes eye Eyeball health care increases bone density, cell membrane is helped to be formed, preventing anaemia and anti-neuritis, angular stomatitis, reduction cholesterol, skin Outside the effect of whitening anti-blackspot, also solves removing heavy metals, removes free radical, anti-old lesion, weight reducing and other effects.In dragon fruit Anthocyanidin content is higher, and anthocyanidin is a kind of antioxidant with obvious effects, has gathered moisturizing, anti-ageing, wrinkle resistant, antiplaque, anti-skin The functions such as cancer, anti-inflammatory, releasing extravasated blood, antiallergic, radioresistance, indirect whitening.Other than containing anthocyanidin, also have in flue berry extract The nutriments such as vegetable albumin, vitamin C, water-soluble fibre, ferro element have good health-care efficacy to human body.
Red bark of eucommia is Apocynaceae Parabarium plant, mainly contains alkaloid, phenols, organic acid, carbohydrate, flavonoids Equal ingredients, it not only has treatment treating rheumatic ostealgia, fracture, a drug effect of traumatic hemorrhage, also antitumor anticancer, anti-oxidant, anti-inflammatory The effects that.Red bark of eucommia is the civil common herbal medicine in South China of China, and national Chinese medicine protection kind " ZHONGHUA DIEDA WAN " etc. One of raw material of Chinese medicine preparation.《National Chinese herbal medicine compilation》Described in the medicine cure mainly arthralgia pain due to rheumatism, lumbar muscle strain, pain in waist and lower extremities, fall Play damage.But there is not yet Radix seu Caulis Parabarii extract is applied in skin-lightening cosmetic.Some researches show that Radix seu Caulis Parabarii extracts to tyrosine The activity of enzyme has significant inhibiting effect, reduces the synthesis of melanin, is applied in cosmetics and can reach whitening antiplaque Effect.
Hesperetin is a kind of flavone compound, is mostly present in rutaceae with glycoside forms, orange peel, the dried immature fruit of citron orange, Content is quite high in the medicinal materials such as green peel and one of its main drug activity ingredient, and hesperetin has that anti-oxidant, antiplatelet is solidifying Poly-, vasodilator, anti-inflammatory prevent osteoporosis, reduce cardiovascular and antitumor etc. the works of melanin pigmentation, reducing blood lipid, protection With being one of plant whitening ingredient most effective so far.
Composition of the present invention includes flue berry extract, Radix seu Caulis Parabarii extract and hesperetin, flue berry extract, red Eucommia ulmoides extracts and hesperetin add simultaneously, have the effect of collaboration, make the composition while having whitening and anti-aging, antiplaque The effect of.
Preferably, in parts by weight, the composition includes 3-10 parts of flue berry extract, Radix seu Caulis Parabarii extract 2-6 Part, 1-4 parts of hesperetin.
In some embodiments, the composition further includes Radix et Caulis Opuntiae Dillenii extract.Cactus is one kind of Opuntia Plant.Alias celestial being palm, kwan-yin palm, overlord, fire palm etc., are Cactaeous plants.Cactus can clearing heat and detoxicating, scattered stagnation resolvation Swollen, stomach invigorating cough-relieving.It is interior with controlling taste-blindness rate, acute dysentery, cough；Mumps, mastitis, carbuncle are controlled in external application Furuncle poison, snake sting.In addition cactus also has the function of that significant antiallergic is anti-inflammatory, enhances skin barrier.
Preferably, Radix et Caulis Opuntiae Dillenii extract described in the composition is Mibangta cactus extract.
Further, preferably, in parts by weight, the composition contains the Mibangta cactus extract 1.6-5 Part.
Flue berry extract, Radix seu Caulis Parabarii extract and Radix et Caulis Opuntiae Dillenii extract in heretofore described composition are this fields Well known to technical staff, it can be commercially available by commercial sources or be prepared by method disclosed in the prior art, Specification meets country or professional standard.Wherein, the Radix et Caulis Opuntiae Dillenii extract is preferably Mibangta cactus extract.
The present invention also provides a kind of facial mask, including flue berry extract, Radix seu Caulis Parabarii extract, hesperetin, meter Bang Ta are celestial People slaps extract, base peptide 3000, rose, wheat-germ oil, cyclomethicone, cetostearyl alcohol, coco group Portugal Glucosides, propylene glycol, Sodium Hyaluronate, hydroxy-ethyl acrylate, film forming agent, pH adjusting agent and water.
Facial mask of the present invention is carried in addition to containing flue berry extract, Radix seu Caulis Parabarii extract, hesperetin, Mibangta cactus Beyond the region of objective existence is taken also to contain base peptide 3000, rose, wheat-germ oil, cyclomethicone, cetostearyl alcohol, coco group Portugal Glucosides, propylene glycol, Sodium Hyaluronate, hydroxy-ethyl acrylate, film forming agent, pH adjusting agent and water.Wherein base peptide 3000 have it is anti-ageing, The multi-efficiency of face lift and anti-wrinkle；Rose and wheat-germ oil have the function of antibacterial, and wherein wheat embryo Oil can moisturize the skin, and rose can assign the fragrance of product pleasure；Sodium Hyaluronate, propylene glycol have moisture-keeping efficacy.For a long time Using the facial mask made of the above raw material, melanin deposition can be mitigated, remove free radical, compact skin, keeps skin water profit rich Elasticity.
Preferably, the facial mask, by percentage to the quality, composed of the following components：It is flue berry extract 3-10%, red Eucommia ulmoides extracts 2-6%, hesperetin 1-4%, Mibangta cactus extract 1.6-5%, 3000 0.5-1.8% of base peptide, rose Hydrosol 0.2-1%, wheat-germ oil 2-5%, cyclomethicone 1-3%, cetostearyl alcohol 0.3-2.4%, coco group Glucoside 0.3-3%, propylene glycol 3.6-10%, Sodium Hyaluronate 1-5%, hydroxy-ethyl acrylate 0.5-1%, film forming agent 4- 10%, pH adjusting agent 0.04-1.5%, water are supplied.
Preferably, the film forming agent is at least one of polyethylene glycol, algin, xanthan gum, chitosan.
Preferably, the pH adjusting agent is at least one of citric acid, triethanolamine.
In some embodiments provided by the invention, the facial mask is by percentage to the quality, composed of the following components：Fire Imperial berry extract 3%, Radix seu Caulis Parabarii extract 2.5%, hesperetin 1%, Mibangta cactus extract 1.6%, base peptide 3000 0.58%, rose 0.2%, wheat-germ oil 2%, cyclomethicone 1%, cetostearyl alcohol 0.3%, coco group Glucoside 0.3%, propylene glycol 3.6%, Sodium Hyaluronate 1%, hydroxy-ethyl acrylate 0.5%, polyethylene glycol 2%, algin 2%, citric acid 0.04%, water is supplied.
In some embodiments provided by the invention, the facial mask is by percentage to the quality, composed of the following components：Fire Imperial berry extract 6.5%, Radix seu Caulis Parabarii extract 4%, hesperetin 2.5%, Mibangta cactus extract 3.3%, base peptide 3000 1.2%, rose 0.6%, wheat-germ oil 3.5%, cyclomethicone 2%, cetostearyl alcohol 1.4%, coconut Base glucoside 1.7%, propylene glycol 6.8%, Sodium Hyaluronate 3%, hydroxy-ethyl acrylate 0.8%, algin 3%, xanthans 4%, citric acid 0.02%, triethanolamine 0.06%, water is supplied.
In some embodiments provided by the invention, the facial mask is by percentage to the quality, composed of the following components：Fire Imperial berry extract 8%, Radix seu Caulis Parabarii extract 5%, hesperetin 3%, Mibangta cactus extract 3.3%, base peptide 3000 1.5%, rose 0.8%, wheat-germ oil 4.2%, cyclomethicone 2.5%, cetostearyl alcohol 2%, coconut Base glucoside 2.4%, propylene glycol 8%, Sodium Hyaluronate 4.3%, hydroxy-ethyl acrylate 0.8%, xanthans 8%, triethanolamine 0.08%, water is supplied.
In some embodiments provided by the invention, the facial mask is by percentage to the quality, composed of the following components：Fire Imperial berry extract 10%, Radix seu Caulis Parabarii extract 6%, hesperetin 4%, Mibangta cactus extract 5%, base peptide 3000 1.8%, rose 1%, wheat-germ oil 5%, cyclomethicone 3%, cetostearyl alcohol 2.4%, coco group Portugal Glucosides 3%, propylene glycol 10%, Sodium Hyaluronate 5%, hydroxy-ethyl acrylate 1%, xanthans 5%, chitosan 5%, triethanolamine 1.5%, water is supplied.
The present invention also provides the preparation methods of the facial mask, include the following steps：
A, press Material Percentage, by film forming agent, hydroxy-ethyl acrylate, Sodium Hyaluronate, water, propylene glycol be heated to 70 DEG C- 85 DEG C of dissolvings are complete, stir evenly；
B, wheat-germ oil, cyclomethicone, cetostearyl alcohol, coco group glucoside are heated to 70 DEG C -85 DEG C, it stirs to being completely dissolved, cools down after emulsifying homogeneous；
C, it waits for that temperature is down to 45 DEG C -50 DEG C, flue berry extract, Radix seu Caulis Parabarii extract, hesperetin, meter Bang Ta celestial beings is added Extract, base peptide 3000, rose are slapped, is stirred evenly, adjusting pH to 5.5-6.8 with pH adjusting agent is made facial mask.
As shown from the above technical solution, the present invention provides a kind of composition and contain the facial mask of the composition.The present invention The composition includes flue berry extract, Radix seu Caulis Parabarii extract and hesperetin.Flue berry extract is rich in anthocyanidin, has U.S. It is anti-ageing and other effects in vain；Radix seu Caulis Parabarii extract can inhibit the generation of melanin；Hesperetin is plant whitening most effective so far One of ingredient.It is added while flue berry extract, Radix seu Caulis Parabarii extract and hesperetin, has the effect of collaboration, make the combination Object has effects that whitening and anti-aging, antiplaque simultaneously.Facial mask of the present invention contains various plants extract, meets natural shield Skin theory provides nutrition needed for skin, especially flue berry extract and contains more anthocyanidin, and anthocyanidin is pure natural resist Aging nutritional supplement is effective antioxidant, in addition, Radix seu Caulis Parabarii extract has significant inhibit to tyrosinase activity Effect, can significantly reduce the generation of melanin.Wheat-germ oil and rose in facial mask of the present invention, which can play, to kill The effect of bacterium, without additional addition chemical preservative in formula.Rose, which also has, to keep the skin wet, moisturizing, quick anti-inflammatory, resists Allergy, antipruritic, the effects that slowing down aging, and the fragrance of product pleasure can be assigned.The facial mask of the present invention not only remains flue Fruit it is natural red, assign product good and natural appearance, also gathered most of effect of common facial mask, as whitening is protected Wet, the anti crease and anti senile, skin that compacts lightens the stain and antiallergic is anti-inflammatory and other effects, is suitble to various skin, safe and non-toxic non-stimulated, symbol Close most of consumer demand.
For a further understanding of the present invention, with reference to specific embodiment, the present invention will be described in detail.Such as without special Illustrate, the raw material and experiment reagent of facial mask of the present invention, which are bought by commercial channel, to be obtained.As flue berry extract is purchased from Hundred Hao Bo Co., Ltds of Guangzhou, Radix seu Caulis Parabarii extract are wide purchased from Nanjing purchased from Xi'an Bioisystech Co., Ltd of Tianrui, hesperetin Moisten biological products Co., Ltd, Mibangta cactus extract is purchased purchased from Xi'an pelagic organisms Engineering Co., Ltd, rose From Guangzhou Fang Dao cosmetics Science and Technology Ltd.；The water is preferably deionized water.
Embodiment 1
1, experiment material
Composition 1：1 part of 3 parts of flue berry extract, 2.5 parts of Radix seu Caulis Parabarii extract and hesperetin；
Composition 2：2.5 parts of 6.5 parts of flue berry extract, 4 parts of Radix seu Caulis Parabarii extract and hesperetin；
Composition 3：3 parts of 8 parts of flue berry extract, 5 parts of Radix seu Caulis Parabarii extract and hesperetin.
Composition 4：8 parts of flue berry extract, 5 parts of Radix seu Caulis Parabarii extract and 3 parts of hesperetin, Mibangta cactus extract 3.3 part.
2, experimental method and result carry out the test of pesticide effectiveness, specific experiment side using above-mentioned composition and each taste plant extracts Method is as follows：
Above-mentioned each composition and each plant extracts are dissolved in respectively and are configured in absolute ethyl alcohol by 5% (g/ml, w/v's) Sample solution.(note：The total concentration of composition is 5%, included in ratio between extract concentrations be aforementioned proportion).
1) measurement of scavenging ability of DPPH free radical：
6.8 phosphate buffers of 4mL pH, 5mL 0.4mmol/L DPPH absolute ethyl alcohols are sequentially added into 10mL centrifuge tubes Solution, 0.1mL sample solutions mix well.After 20min, centrifuges (12000rpm, 5min), supernatant is taken to be measured at 571nm Light absorption value.Each sample solution is calculated to the clearance rate of DPPH free radicals, the results are shown in Table 1.Wherein, to the clear of DPPH free radicals Except rate=[1- (A1-A2)/A3], A in formula1To be not added with the light absorption value of DPPH solution after sample；A2(absolute ethyl alcohol is used to be not added with DPPH Instead of), only add the light absorption value of each sample solution；A3To be not added with sample solution, only add DPPH and the light absorption value of aqueous solution.
2) measurement of ability is inhibited tyrosinase activity：
3mL 0.05%L- tyrosine, 6.8 phosphate buffers of 4mL pH, 0.3mL samples are once added into 10mL centrifuge tubes Product solution shakes up and heats 10min in 37 DEG C of water-baths, adds 1mL 500U/mL tyrosinases and continues to heat 5min, centrifugation (12000rpm, 5min) measures light absorption value A under 475nm1, it is instead of the absorbance measured when sample solution with phosphate buffer A2.Sample solution is calculated to the inhibiting rate of tyrosinase, the results are shown in Table 2.Wherein to the inhibiting rate of tyrosinase=(A2- A1)/A2
The measurement result of 1 scavenging ability of DPPH free radical of table
Group The clearance rate (%) of DPPH free radicals
Composition 1 93.5
Composition 2 94.2
Composition 3 95.3
Composition 4 91.6
Flue berry extract 88.5
Radix seu Caulis Parabarii extract 83.9
Hesperetin 80.7
Mibangta cactus extract 73.8
Table 2 inhibits tyrosinase activity the measurement result of ability
Group Tyrosinase inhibition rate (%)
Composition 1 90.3
Composition 2 91.7
Composition 3 92.6
Composition 4 87.5
Flue berry extract 80.2
Radix seu Caulis Parabarii extract 82.4
Hesperetin 86.9
Mibangta cactus extract 71.5
By table 1,2 it is found that composition of the present invention has significant free radical scavenging ability, junket ammonia can be effectively inhibited The activity of sour enzyme, and it is with obvious effects more excellent better than a kind of extract is used alone, have good complementary synergistic Effect.
Embodiment 2
Raw material components and mass percent are：Flue berry extract 3%, Radix seu Caulis Parabarii extract 2.5%, hesperetin 1%, rice Nation tower Radix et Caulis Opuntiae Dillenii extract 1.6%, base peptide 3,000 0.58%, rose 0.2%, wheat-germ oil 2%, ring poly dimethyl Siloxanes 1%, cetostearyl alcohol 0.3%, coco group glucoside 0.3%, propylene glycol 3.6%, Sodium Hyaluronate 1%, acrylic acid Hydroxyl ethyl ester 0.5%, polyethylene glycol 2%, algin 2%, citric acid 0.04%, deionized water is supplied.
Preparation process is as follows：By above-mentioned raw materials percentage, by polyethylene glycol, algin, hydroxy-ethyl acrylate, hyaluronic acid Sodium, water, propylene glycol, which are put into emulsification pot, is heated to 70 DEG C of -85 DEG C of dissolvings completely, stirs evenly；Wheat-germ oil, ring are gathered Dimethyl siloxane, cetostearyl alcohol, coco group glucoside, which are put into oil phase pot, is heated to 70 DEG C -85 DEG C, stirs to complete Dissolving, is then transferred in water phase pot and carries out emulsifying homogeneous, and heat preservation after twenty minutes, starts to cool down；Wait for that temperature is down to 45 DEG C -50 DEG C, sequentially add flue berry extract, Radix seu Caulis Parabarii extract, hesperetin, Mibangta cactus extract, base peptide 3000, rose Hydrosol, and stir evenly；PH is finally adjusted to 5.5 with citric acid, the facial mask is made.
Embodiment 3
Raw material components and mass percent are：Flue berry extract 6.5%, Radix seu Caulis Parabarii extract 4%, hesperetin 2.5%, Mibangta cactus extract 3.3%, base peptide 3,000 1.2%, rose 0.6%, wheat-germ oil 3.5%, the poly- diformazan of ring Radical siloxane 2%, cetostearyl alcohol 1.4%, coco group glucoside 1.7%, propylene glycol 6.8%, Sodium Hyaluronate 3%, propylene Sour hydroxyl ethyl ester 0.8%, algin 3%, xanthans 4%, citric acid 0.02%, triethanolamine 0.06%, deionized water is supplied.
Preparation process is as follows：By above-mentioned raw materials percentage, by xanthans, algin, hydroxy-ethyl acrylate, hyaluronic acid Sodium, water, propylene glycol, which are put into emulsification pot, is heated to 70 DEG C of -85 DEG C of dissolvings completely, stirs evenly；Wheat-germ oil, ring are gathered Dimethyl siloxane, cetostearyl alcohol, coco group glucoside, which are put into oil phase pot, is heated to 70 DEG C -85 DEG C, stirs to complete Dissolving, is then transferred in water phase pot and carries out emulsifying homogeneous, and heat preservation after twenty minutes, starts to cool down；Wait for that temperature is down to 45 DEG C -50 DEG C, sequentially add flue berry extract, Radix seu Caulis Parabarii extract, hesperetin, Mibangta cactus extract, base peptide 3000, rose Hydrosol, and stir evenly；PH is finally adjusted to 6 with citric acid and triethanolamine, the facial mask is made.
Embodiment 4
Raw material components and mass percent are：Flue berry extract 8%, Radix seu Caulis Parabarii extract 5%, hesperetin 3%, rice nation Tower Radix et Caulis Opuntiae Dillenii extract 3.3%, base peptide 3,000 1.5%, rose 0.8%, wheat-germ oil 4.2%, ring poly dimethyl silicon Oxygen alkane 2.5%, cetostearyl alcohol 2%, coco group glucoside 2.4%, propylene glycol 8%, Sodium Hyaluronate 4.3%, acrylic acid hydroxyl Ethyl ester 0.8%, xanthans 8%, triethanolamine 0.08%, deionized water is supplied.
Preparation process is as follows：By above-mentioned raw materials percentage, by xanthans, hydroxy-ethyl acrylate, Sodium Hyaluronate, water, third Glycol, which is put into emulsification pot, is heated to 70 DEG C of -85 DEG C of dissolvings completely, stirs evenly；By wheat-germ oil, ring poly dimethyl silicon Oxygen alkane, cetostearyl alcohol, coco group glucoside, which are put into oil phase pot, is heated to 70 DEG C -85 DEG C, stirs to being completely dissolved, then It is transferred in water phase pot and carries out emulsifying homogeneous, heat preservation after twenty minutes, starts to cool down；It waits for that temperature is down to 45 DEG C -50 DEG C, sequentially adds Flue berry extract, Radix seu Caulis Parabarii extract, hesperetin, Mibangta cactus extract, base peptide 3000, rose, and stir Uniformly；PH is finally adjusted to 6.5 with triethanolamine, the facial mask is made.
Embodiment 5
Raw material components and mass percent are：Flue berry extract 10%, Radix seu Caulis Parabarii extract 6%, hesperetin 4%, rice Nation tower Radix et Caulis Opuntiae Dillenii extract 5%, base peptide 3,000 1.8%, rose 1%, wheat-germ oil 5%, cyclomethicone 3%, cetostearyl alcohol 2.4%, coco group glucoside 3%, propylene glycol 10%, Sodium Hyaluronate 5%, hydroxy-ethyl acrylate 1%, Xanthans 5%, chitosan 5%, triethanolamine 1.5%, deionized water is supplied.
Preparation process is as follows：By above-mentioned raw materials percentage, by xanthans, chitosan, hydroxy-ethyl acrylate, hyaluronic acid Sodium, water, propylene glycol, which are put into emulsification pot, is heated to 70 DEG C of -85 DEG C of dissolvings completely, stirs evenly；Wheat-germ oil, ring are gathered Dimethyl siloxane, cetostearyl alcohol, coco group glucoside, which are put into oil phase pot, is heated to 70 DEG C -85 DEG C, stirs to complete Dissolving, is then transferred in water phase pot and carries out emulsifying homogeneous, and heat preservation after twenty minutes, starts to cool down；Wait for that temperature is down to 45 DEG C -50 DEG C, sequentially add flue berry extract, Radix seu Caulis Parabarii extract, hesperetin, Mibangta cactus extract, base peptide 3000, rose Hydrosol, and stir evenly；PH is finally adjusted to 6.8 with triethanolamine, the facial mask is made.
6 acute dermal toxicity test of embodiment：
Test material：SD rats, half male and half female, totally 5 groups, every group has 6；Facial mask described in test specimen embodiment 5.
Test method：Before experiment, SD rat back backbone diamond wools are cut, cropping area is no less than rat body surface area 10%.The rat of 2 kinds of genders is grouped at random, every group 6, according to dosage difference is divided into 5 groups, respectively 500,1000,1500, 2000、2500mg/kg.The facial mask is equably applied to rat back, oilpaper and 2 layers of gauze covering is used in combination, it is clear with warm water afterwards for 24 hours Removal of residue.Systemic toxicity profiles performance and the death condition for observing rat, include the variation of skin, hair, eyes and mucous membrane, exhale The variation of suction, four limbs activity and behavior etc., is observed 1 week.In smearing mask latter week, the water inlet of each group rat is normal, not Appearance is poisoned and death condition, skin, hair and eyes do not occur exception, is not occurred trembling, is fainted from fear, salivates, is diarrhea, thermophilic Phenomena such as sleeping, going into a coma, upgrowth situation is good, illustrates made facial mask to skin without any harmful effect.In addition, by acute toxicity point Grade standard is it is found that tested material applies skin median lethal dose LD50>=2180mg/kg is practical nontoxic, and in this experiment, maximum dose is most , there is not animal dead in up to 2500mg/kg, thus can determine that the facial mask is actually nontoxic.
According to the method described above, the facial mask made to embodiment 2-4 carries out acute dermal toxicity test, as a result with embodiment 5 Result it is similar.
Embodiment 7 inhibits tyrosinase activity the measurement of ability：
It is each that 3mL 0.05%L- tyrosine, 6.8 phosphate buffers of 4mL pH, 0.3mL are once added into 10mL centrifuge tubes Film sample (phosphate buffer containing facial mask, 0.1g/mL), shakes up and heats 10min in 37 DEG C of water-baths, add 1mL 500U/mL tyrosinases continue to heat 5min, centrifuge (12000rpm, 5min), and light absorption value A is measured under 475nm1, slow with phosphoric acid It is A that fliud flushing, which replaces the absorbance measured when film sample,2.Inhibiting rate of each film sample to tyrosinase is calculated, as a result such as table 3 It is shown.
Wherein to the inhibiting rate of tyrosinase=(A2-A1)/A2
3 film sample of the present invention of table inhibits tyrosinase activity the measurement result of ability
Embodiment film sample Inhibiting rate (%)
2 25.0
3 39.1
4 47.3
5 52.8
Table 3 is the results show that facial mask of the present invention has the ability that inhibits tyrosinase activity, and with facial mask moderate heat The raising of imperial berry extract, Radix seu Caulis Parabarii extract, orange peel cellulose content, effect are more notable.
The measurement of 8 scavenging ability of DPPH free radical of embodiment：
6.8 phosphate buffers of 4mL pH, 5mL 0.4mmol/L DPPH absolute ethyl alcohols are sequentially added into 10mL centrifuge tubes Solution, each film samples of 0.1mL (phosphate buffer containing facial mask, 0.1g/mL) mix well.After 20min, centrifugation (12000rpm, 5min) takes supernatant to measure light absorption value at 571nm.Calculate removing of each film sample to DPPH free radicals Rate, the results are shown in Table 4.
Wherein, to the clearance rate of DPPH free radicals=[1- (A1-A2)/A3],
A in formula1To be not added with the light absorption value of DPPH solution after sample；
A2To be not added with DPPH (being replaced with absolute ethyl alcohol), only add the light absorption value of each film sample solution；
A3To be not added with each film sample, only add DPPH and the light absorption value of aqueous solution.
The measurement result of 4 facial mask scavenging ability of DPPH free radical of the present invention of table
Embodiment film sample Clearance rate (%)
2 30.9
3 43.8
4 54.0
5 60.7
Table 4 is the results show that facial mask of the present invention has the ability for removing DPPH free radicals, and with flue in facial mask The raising of berry extract, Radix seu Caulis Parabarii extract, orange peel cellulose content, effect are more notable.
The beauty functions of 9 made facial mask of embodiment：
Trier is the healthy women voluntarily participated in, is by age divided into 2 groups, and 20-35 Sui is A groups, and 35-55 Sui is B groups, 16 people of each group of people, wherein 8 people are professional person.Every trier uses 5 made facial mask of the embodiment of the present invention one month, every night Once.Occupation mode is：The facial mask is uniformly applied to the face after cleaning, is eluted with water after keeping 20min.
Result on trial：After one month, all triers do not occur allergic reaction, unanimously think that the product safety is stingless Swash, it is with obvious effects, and to the present invention in terms of skin sense, moisture-retaining capacity, whitening capability, skin ability of compacting and moisturizing ability four Facial mask evaluated, the results are shown in Table 5.
The trial effect of 5 all volunteers of table
Project Significant effect (%) Effect is general (%) To no effect (%)
Skin sense 94 6 0
Moisture-retaining capacity 92 8 0
Whitening capability 88 12 0
It compacts skin ability 83 17 0
Moisturizing ability 89 11 0
The results show that there is facial mask of the present invention good skin sense, skin-moisturizing, skin significant effect to be used for a long time, can make Reach shining skin whitening, the skin that compacts good result.
According to the method described above, the facial mask made to embodiment 2-4 carries out Efficacy experiments, as a result with the result phase of embodiment 5 Seemingly.

Claims (6)

1. a kind of composition, in parts by weight, the composition is by 3-8 parts of flue berry extract, Radix seu Caulis Parabarii extract 2.5-5 1-3 parts of part, hesperetin compositions.
2. a kind of composition, in parts by weight, the composition is by 8 parts of flue berry extract, 5 parts of Radix seu Caulis Parabarii extract, orange peel 3.3 parts of 3 parts of element, Mibangta cactus extract compositions.
3. a kind of facial mask, by percentage to the quality, composed of the following components：Flue berry extract 3-10%, Radix seu Caulis Parabarii extract 2.5-6%, hesperetin 1-4%, Mibangta cactus extract 1.6-5%, 3000 0.5-1.8% of base peptide, rose 0.2-1%, Wheat-germ oil 2-5%, cyclomethicone 1-3%, cetostearyl alcohol 0.3-2.4%, coco group glucoside 0.3-3%, third Glycol 3.6-10%, Sodium Hyaluronate 1-5%, hydroxy-ethyl acrylate 0.5-1%, film forming agent 4-10%, pH adjusting agent 0.04-1.5%, Water is supplied.
4. facial mask according to claim 3, which is characterized in that the film forming agent is polyethylene glycol, algin, xanthan gum, shell At least one of glycan.
5. facial mask according to claim 3, which is characterized in that the pH adjusting agent is citric acid, in triethanolamine at least It is a kind of.
6. the preparation method of facial mask described in claim 3, which is characterized in that include the following steps：
A, Material Percentage is pressed, film forming agent, hydroxy-ethyl acrylate, Sodium Hyaluronate, water, propylene glycol are heated to 70 DEG C -85 DEG C Dissolving is complete, stirs evenly；
B, wheat-germ oil, cyclomethicone, cetostearyl alcohol, coco group glucoside are heated to 70 DEG C -85 DEG C, stirred It mixes to being completely dissolved, cools down after emulsifying homogeneous；
C, it waits for that temperature is down to 45 DEG C -50 DEG C, flue berry extract, Radix seu Caulis Parabarii extract, hesperetin, Mibangta cactus is added and carries Object, base peptide 3000, rose are taken, is stirred evenly, adjusting pH to 5.5-6.8 with pH adjusting agent is made facial mask.
CN201610718982.7A 2016-08-24 2016-08-24 A kind of composition and facial mask Active CN106137875B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610718982.7A CN106137875B (en) 2016-08-24 2016-08-24 A kind of composition and facial mask

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610718982.7A CN106137875B (en) 2016-08-24 2016-08-24 A kind of composition and facial mask

Publications (2)

Publication Number Publication Date
CN106137875A CN106137875A (en) 2016-11-23
CN106137875B true CN106137875B (en) 2018-09-28

Family

ID=57342535

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610718982.7A Active CN106137875B (en) 2016-08-24 2016-08-24 A kind of composition and facial mask

Country Status (1)

Country Link
CN (1) CN106137875B (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106727155A (en) * 2017-01-13 2017-05-31 广州美中生物科技有限公司 A kind of facial mask of natural skin care composition and preparation method thereof
CN107970177A (en) * 2018-01-30 2018-05-01 庄陈子 A kind of moisturizing skin-active creams and preparation method thereof
CN109364008A (en) * 2018-12-05 2019-02-22 广州蔻赛生物科技有限公司 A kind of multiple-effect moisturiser and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1691930A (en) * 2001-06-27 2005-11-02 久光制药株式会社 Sheet-type packs
CN104083314A (en) * 2014-07-16 2014-10-08 福州萍晴日用化妆品有限公司 Whitening and moistening facial mask and preparation method thereof
CN105616467A (en) * 2015-12-23 2016-06-01 庄信修 Application of cortex parabarii and cortex parabarii extract both serving as whitening effective ingredients
CN105708782A (en) * 2016-03-21 2016-06-29 赵洪军 Preparation method of anthocyanin cream pack
CN105769746A (en) * 2014-12-25 2016-07-20 刘海燕 Pitaya peel mask

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1691930A (en) * 2001-06-27 2005-11-02 久光制药株式会社 Sheet-type packs
CN104083314A (en) * 2014-07-16 2014-10-08 福州萍晴日用化妆品有限公司 Whitening and moistening facial mask and preparation method thereof
CN105769746A (en) * 2014-12-25 2016-07-20 刘海燕 Pitaya peel mask
CN105616467A (en) * 2015-12-23 2016-06-01 庄信修 Application of cortex parabarii and cortex parabarii extract both serving as whitening effective ingredients
CN105708782A (en) * 2016-03-21 2016-06-29 赵洪军 Preparation method of anthocyanin cream pack

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
红杜仲的美白活性及其途径研究;林锦彬等;《中国生化药物杂志》;20151231;第35卷(第12期);第21-28页 *

Also Published As

Publication number Publication date
CN106137875A (en) 2016-11-23

Similar Documents

Publication Publication Date Title
CN106473987B (en) The anti-ageing composition of whitening and cosmetics
Aburjai et al. Plants used in cosmetics
KR101769416B1 (en) Multifunctional mask composition and preparing method of the same including anti-wrinkles and whitening functions
JPH0717847A (en) Skin external preparation
KR20090055309A (en) A cosmetic composition for skin whitening and treating wrinkles
KR101928386B1 (en) Cream type cosmetic composition having skin tone correcting, UV protecting, anti-wrinkle and whitening effect, and preparing method of the same
CN108653013A (en) A kind of plant moisturizing water profit after-sun frost and preparation method thereof
WO2018121973A1 (en) Composition comprising a plant extract of the specie hedychium coronarium, for use in a method for treatment of the human body by therapy
KR101798026B1 (en) Functional composition having blood circulation and atopy-soothing effect
KR20070002409A (en) Cosmetic composition containing as available ingredient the extracts of Equisetum arvense L.
KR100564108B1 (en) Cosmetic composition comprising plant extract having anti-aging effect
CN106137875B (en) A kind of composition and facial mask
KR101142541B1 (en) Anti-wrinkle cosmetic composition containing oriental herb extract treated by enzyme and its extraction method
KR101417710B1 (en) Hair restorer composition and producing process thereof
CN108653137B (en) Composition and application thereof in preparation of beauty cosmetics
KR102037927B1 (en) Cosmetic composition composed of including extracts of drynaria fortunei and cosmetics using the same
CN109157459A (en) A kind of smoothing toner and preparation method containing Chinese herbal medicine extract
Mamillapalli et al. Formulation, phytochemical, physical, biological evaluation of polyherbal vanishing cream, and facewash
CN105342916A (en) Plant extract product composition, and preparation method and application thereof
CN108703911B (en) Composition with moisturizing and whitening effects and preparation method and application thereof
JP7338842B2 (en) wrinkle-improving composition and wrinkle-improving skin cosmetic
KR100937187B1 (en) Method for the Preparation of Functional Cosmetics from Bokbunja Wine Processing Waste
KR101459742B1 (en) Cosmetic composition for improving acne containing extracts of natural substance
KR101252560B1 (en) Cosmetic composition containing extracts of Impatiens balsamina L. for controlling anti-acne or anti-comedone
KR101456059B1 (en) The cosmetic composition effective in whitening and anti-aging mainly comprised of roasted licorice extract

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant