CN103705421A - Moisturizing and anti-aging milk cream and preparation method thereof - Google Patents
Moisturizing and anti-aging milk cream and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a moisturizing and anti-aging milk cream and a preparation method thereof. The moisturizing anti-aging milk cream comprises two moisturizing anti-aging active ingredients (whey protein powder extracted from milk, and casein polypeptide), and effective constituents extracted from traditional Chinese medicinal materials including ginseng, Ganoderma lucidum, Angelica, Astragalus root, seaweeds, Gynostemma pentaphyllum, Rhodiola rosea and ginkgo leaf as well as moisturizing and anti-aging ingredients extracted from tremella and medical stone flour, and all the effective ingredients, biochemical additive (VE oil), sodium hyaluronate and skin-care basic ingredients such as jojoba oil, wheat germ oil, evening primrose seed oil, an amino acid moisturizing agent, cetostearyl alcohol, an emulsifying agent, an antioxidant and preservatives are cooperated in a balanced manner and scientifically formulated to obtain the safe and effective moisturizing anti-aging milk cream convenient for use.
Description
Technical field
The present invention relates to a kind of moisturizing anti-aging cream and manufacture method thereof that milk extracts composition that contain, belong to cosmetics and skincare product technical field.
Background technology
Along with the development of material progress, people, when material is rich, also more and more note oneself beauty treatment and skin protection, this be also nearly decades cosmetics and skincare product develop reason place rapidly.Milk, as traditional food, is also the non-defective unit of beauty and skin care since ancient times.With milk, wash one's face, making facial film, to apply the record of face etc. a lot, are now with the current mostly, because fresh milk complicated component, though nutritious, but easily corrupt, this has just limited the extensive use in cosmetics and skincare product.Because modern's rhythm of life is fast, like using ready-made cosmetics and skincare product, the general out of patience and time is gone oneself allotment.This just need to extract the active component in milk, and and the balanced collocation of other cosmetics and skincare product raw material, reach both keep milk active component beauty and skin care effect and with the synergistic function of other composition, reach again client's effect easy to use.
The present invention is directed to current milk skin protection cosmetics and be difficult for adding milk complete nutrition ingredients, be difficult for to preserve and be difficult for the defects such as finished product supply market, preferably the milk of state-of-the-art, tool activity extracts composition, and and Chinese herbal medicine extract, the perfect cooperations such as biochemical component.Both reached nutrition equilibrium, moisturizing defying age effect is remarkable, the finished product supply effect that reaching again to make things convenient for customers uses.
Summary of the invention
Although fresh milk is nutritious, complicated component, and some composition may be little to the moisturizing senile-resistant efficacy of skin, is also difficult for preserving.The many scientific research institutions of recent domestic carry out deep separated and purify to the active component in milk, obtained some at the milk that has fine activity aspect the skin moisturizing defying age composition that skims the cream off milk, as lactalbumin powder, and casein polypeptide etc.These milk extracts not only concentration are high, active strong, but also have good stability.With Chinese herbal medicine extracting composition and V such as Radix Ginseng, Ganoderma, Tremella, Sargassum, Folium Ginkgos
eoil, after the balanced collocation of the biochemical components such as hyaluronate sodium, more can play mutual supplement with each other's advantages, the effect of Synergistic, trace element in Chinese herbal medicine and multiple nutritional components also can obtain absorbing fully by this carrier of milk casein polypeptide, thereby reach desirable moisturizing defying age effect.Therefore primary and foremost purpose of the present invention is to provide a kind of by multiple milk skim the cream off milk composition, Chinese herbal medicine extracting composition and biochemical component, through equilibrium, arrange in pairs or groups, the Novel milk moisturizing anti-aging cream product forming after reasonable formula, to meeting the numerous women demand growing to cosmetics and skincare product.Another object of the present invention, is to provide the preparation method of said herbal medicine extract and the preparation method of final milk moisturizing anti-aging cream.
To achieve these goals, the technical solution used in the present invention is as follows:
Final products of the present invention, milk moisturizing anti-aging cream, is prepared from by following component:
(1) oil phase component: described oil phase component is comprised of the component of following mass parts: 16 mixed alcohol 1.5-2.0 parts, 2-4 parts of 16 stearyl alcohol and 16 octadecyl glucosides, 2-3 parts of tristerin and PEG-100 stearates, 2-4 parts of Jojoba oils, 2-4 parts of Semen Tritici aestivi germ oils, V
e0.3-0.6 part of oil, 3-5 parts of white oils, 1-2 parts of isopropyl palmitate 2-3 part, Radix Oenotherae erythrosepalae oil, 2-3 parts of dimethicones, 0.2-0.3 part of methyl hydroxybenzoate, 0.1-0.15 part of propylparaben, 0.03-0.05 part of ditertbutylparacresol.
(2) water component: 8-10 parts of glycerol, 2-3 parts of propylene glycol, 0.1-0.2 part of hyaluronate sodium, 3-4 parts of amino acid humectants, 50.41-55.61 parts of Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution, described Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution are mainly made by the raw material of following mass parts: Radix Ginseng, Ganoderma, Radix Angelicae Sinensis, the Radix Astragali, Sargassum, Herb Gynostemmae Pentaphylli, each 10-15 part of Radix Rhodiolae, 0.1-0.5 part, Tremella, 1-2 parts of Folium Ginkgos, long-lived stone powder (crossing 20 object medical stone powders) 0.1-0.3 part.
(3) after, add component: 1.0-2.0 parts of lactalbumin powders, 0.2-0.3 part of milk casein polypeptide, deionized water 3-6 part.
(4) co-emulsifier: 0.5-0.8 part of ethoxy acrylates/sodium acryloyldimethyl taurate copolymers.
(5) antiseptic: 0.1-0.15 part, the mixture (commercial disignation MIT) of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol.
(6) essence: 0.01-0.02 part, green tea essence.
The preparation method of milk moisturizing anti-aging cream of the present invention, comprises the steps:
(1) preparation of oil phase component: by 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, tristerin and PEG-100 stearate, Jojoba oil, Semen Tritici aestivi germ oil, V
eoil, white oil, isopropyl palmitate, Radix Oenotherae erythrosepalae oil, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol add after taking in proportion in the rustless steel still of band stirring, heating for dissolving under the stirring of 20-30 revs/min of rotating speeds, and under 80-85 ℃ of constant temperatures, sterilize 20 minutes stand-by.
(2) preparation of aqueous portion: after the glycerol of formula ratio, propylene glycol, hyaluronate sodium, amino acid humectant, Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution are taken in proportion, elder generation's heating for dissolving in rustless steel still, be extracted into afterwards in (passing through drainage screen) rustless steel homogenizing still, under the stirring of 20-30 revs/min, continue to be heated to 80--85 ℃, and constant temperature disinfection 20 minutes, stand-by.
(3) by oil phase slowly in suction water, and scrape wall and stir, rotating speed is increased to 40-50 revs/min, stir after 2-3 minute, start high speed homogenization device, under the high speed of 3000-5000 revs/min, homogenizing is 3-5 minutes, will scrape afterwards wall rotating speed and drop to 30-40 revs/min, and be cooled to 60 ℃ under this rotating speed, add lactalbumin powder and casein polypeptide that prior dissolving is good, homogenizing 2-4 minutes, adds co-emulsifier, continues to stir 20-30 minutes, while cooling to 40 ℃, add antiseptic, essence, then stir after 15-20 minutes, get final product discharging.
Described Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution, prepare by the following method:
(1) take dry product Radix Ginseng, Ganoderma, Radix Angelicae Sinensis, the Radix Astragali, Sargassum, Herb Gynostemmae Pentaphylli, each 10-15 part of Radix Rhodiolae, 0.1-0.5 part, Tremella, 1-2 parts of Folium Ginkgos, add in rustless steel still, take 0.1-0.3 part of long-lived stone powder standby.
(2) while boiling for the first time, take 700-800 parts of deionized waters, 4-6 parts of ethanol, 4-6 parts of propylene glycol, boil front first immersion 30 minutes, then big fire is boiled, after use little fire instead and boil 1-1.2 hours, with 600 order filter-cloth filterings, obtain the long-lived stone magistery of Chinese herbal medicine Tremella extracting solution 1. afterwards.
(3) in filtering residue, add the propylene glycol of the deionized water of 600-700 mass parts and the ethanol of 1-3 mass parts and 1-3 quality, after big fire is boiled, use little fire instead and boil again 0.8-1.0 hours, add afterwards long-lived stone powder to soak 0.5-1.0 hours, use afterwards 600 order filter-cloth filterings, obtain Chinese herbal medicine, the long-lived stone magistery of Tremella extracting solution 2..
(4) will 1. 2. after filtrate mix homogeneously, obtain the long-lived stone magistery of final Chinese medicine Tremella extracting solution (its total amount should be controlled at half left and right of adding water inventory).
The present invention is directed to modern's rhythm of life fast, think slow down aging, replenishing water and preserving moisture but the reality of not free and patient self-control milk class skin care item, normal growth metabolic rule according to skin, add the following milk composition that skims the cream off milk, Chinese herbal medicine, Tremella, long-lived stone extract composition and biochemical skin care ingredient, make and have replenishing water and preserving moisture, the milk moisturizing anti-aging cream product of delay skin aging.
Milk casein polypeptide: the micromolecule polypeptide that enzymolysis extract from milk casein, there is good adjusting immunity and resisting fatigue, defying age effect. not only easily absorb, the transport agent that can also serve as various trace elements in Chinese herbal medicine, long-lived stone, promote absorbing of trace element, be a kind of biological activity height again stable milk extract composition, can give full play to many moisturizing senile-resistant efficacies of milk.
Lactalbumin powder: the precious protein of separating from milk, high with its purity, absorbance is high, and aminoacid composition the most rationally waits many advantages to be pushed away as " king of albumen ", has defying age, improves immunity, the effect of health invigorating and removing toxic substances.
Radix Ginseng: < < Sheng Nong's herbal classic > > thinks, Radix Ginseng energy " tonifying five ZANG-organs, pacifies spirit, determines soul, and spasmolytic is throbbed with fear, and except pathogen, the happy Fructus Alpiniae Oxyphyllae of improving eyesight, takes to make light of one's life by commiting suicide for a long time and prolongs life ".Modern study finds, the effects such as it also has antioxidation, defying age, resisting fatigue, protects the liver, regulates cardiovascular function, excited hemopoietic system function.
Ganoderma: < < Sheng Nong's herbal classic > > thinks, Ganoderma energy " tonifying liver gas, peace soul ", " food, makes light of one's life by commiting suicide not old for a long time, and angle prolongs life ".Modern study confirmation, Ganoderma has regulating action to nervous system, respiratory system, systema cariovasculare functional, has immunomodulating, removes the functions such as free radical, balance metabolism, directly affects human senility process.
Radix Angelicae Sinensis: can enrich blood and invigorate blood circulation, menstruction regulating and pain relieving, loosening bowel to relieve constipation, to rheumatic arthralgia, traumatic injury, asthenia cold abdominalgia, blood deficiency and yellow complexion etc. are effective in cure.Modern age the analysis and research of Radix Angelicae Sinensis were shown: it contains V
a﹑ V
b12the plurality of active ingredients such as ﹑ Zong Lv Suan ﹑ You Suan ﹑ Ya You Suan ﹑ Rou Dou Kou Suan – sitosterol, have enhancement blood circulation, promote cell metabolism, suppress pigmentation, the effects such as nourishing the human Body skin.
The Radix Astragali: the traditional Chinese medical science is thought " the spleen being the foundation of acquired constitution ".Think the Radix Astragali " beneficial vigour and mend three warmers ", be " all medicines of QI invigorating ".Modern study finds, the Radix Astragali can not only coronary artery dilator, improves blood supply of cardiac muscle, improves immunologic function, and can delaying cell aging.
Sargassum: contain multiple micro-raw element, inorganic matter, aminoacid and polysaccharide in Sargassum, as Sargassum polysaccharides, rock polysaccharide etc. all has the wet effect of good moisturizing, also there is antiinflammatory, antibacterial action.
Herb Gynostemmae Pentaphylli: Herb Gynostemmae Pentaphylli loses its name in book on Chinese herbal medicine in ancient times.Discovered in recent years, Herb Gynostemmae Pentaphylli has defying age, resisting fatigue, anticancer, endocrine regulation function, can improve human body adaptability to changes and immunity, reduces cholesterol and transaminase, and prophylaxis of tumours suppresses ulcer, keeping tensions down, calm, analgesia.
Radix Rhodiolae: there is no in ancient times the record of Radix Rhodiolae in book on Chinese herbal medicine, is the defying age rising star who just found modern age.It has tonification vigour, heat clearing away, removing toxic substances, hemostasis, the effect of the mind calming and mentality promoting.Radix Rhodiolae has the benefiting action of similar Radix Ginseng, and energy anti-hypoxia, cold resistance, resisting fatigue, radioprotective, antiviral, anticancer growth, increase work efficiency, and delays body aging.
Tremella is a kind of famous and precious tonic, can be used as again the fine raw material of cosmetics and skincare product.Wherein contain protein, fat and several amino acids, mineral and polysaccharose substance.
Folium Ginkgo: wherein contained flavonoid glycoside and flavonol are all the street cleaners of free radical, can protect skin corium cell, improve blood circulation, prevents the oxidized generation wrinkle of cell, also contains the trace element such as manganese, molybdenum, also can remove free radical and check melanin growth.
Long-lived stone powder: i.e. medical stone powder, be rich in the necessary trace element of multiple human body, pure natural, nonhazardous, after protein-based extract in milk effectively coordinates, more can be convenient to absorb, and has given play to the beauty and skin care effect of mutual supplement with each other's advantages.
Hyaluronate sodium: efficient moisture-retention agent, has stronger hygroscopicity and very strong water conservation and lubricity.
The invention has the beneficial effects as follows: will in milk, there is lactalbumin and casein polypeptide and the Chinese medicine Radix Ginseng that moisturizing activity of fighting against senium is very high, Ganoderma, Radix Angelicae Sinensis, the Radix Astragali, Sargassum, Herb Gynostemmae Pentaphylli, Radix Rhodiolae, Folium Ginkgo and Tremella, effective ingredient in long-lived stone powder combines, and with biochemical moisturizing of modern times, antioxidation, anti-corrupt balanced composition collocation, learn from other's strong points to offset one's weaknesses, the milk moisturizing anti-aging cream developing thus, both perfectly kept the beauty and skin care of milk active, given full play to again the synergy of protein and polypeptide composition delivery trace element and multiple nutrients defying age composition in milk. this scientific composition based on pure natural basis can improve the effect of skin-protection product and fool proof. in the market still not by multiple efficacies composition and Chinese medicine in milk, Tremella, the organic cooperations of effective ingredient such as long-lived stone, have complementary advantages, after scientific formula, the both safety developing, efficient milk moisturizing anti-aging product again.The invention of this product, in the time of can reducing people and improve looks with milk, now by the trouble that need now join, can also increase Chinese medicine ingredients, effectively absorbing of long-lived stone composition, this has just reached both easy to use, again moisturizing anti-aging product effect safely and efficiently, and energy life-time service, without any side effects.
The specific embodiment
Embodiment 1
(1), the preparation process of special ratios Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution is as follows:
(1) take 10 parts of dry product Radix Ginsengs, 12 parts of Ganodermas, 15 parts of Radix Angelicae Sinensis, 10 parts of the Radixs Astragali, 12 parts of Sargassums, 15 parts of Herb Gynostemmae Pentaphyllis, 10 parts of Radix Rhodiolaes, 0.2 part, Tremella, 2 parts of Folium Ginkgos, add in rustless steel still, take 0.2 part of long-lived stone powder standby.
(2) while boiling for the first time, take 800 parts of deionized waters, 5 parts of ethanol, 5 parts of propylene glycol, boil front first immersion 30 minutes, then big fire is boiled, after use little fire instead and boil 1.2 hours, with 600 order filter-cloth filterings, obtain the long-lived stone magistery of Chinese herbal medicine Tremella extracting solution 1. afterwards.
(3) in filtering residue, add the propylene glycol of the deionized water of 600 mass parts and the ethanol of 2 mass parts and 2 quality, after big fire is boiled, use little fire instead and boil again 1.0 hours, add afterwards long-lived stone powder to soak 1.0 hours, use afterwards 600 order filter-cloth filterings, obtain Chinese herbal medicine, the long-lived stone magistery of Tremella extracting solution 2..
(4) will 1. 2. after filtrate mix homogeneously, obtain the long-lived stone magistery of final Chinese medicine Tremella extracting solution (its total amount should be controlled at half left and right of adding water inventory).
(2), with the Chinese herbal medicine that makes, Tremella, long-lived stone magistery extracting solution, substitute the pure water component in milk moisturizing anti-aging cream, the prescription that designs milk moisturizing anti-aging cream by following proportioning (mass percent) is as follows:
(1) oil phase component: described oil phase component is comprised of the component of following mass parts: 16 1.5 parts of mixed alcohols, 3 parts of 16 stearyl alcohol and 16 octadecyl glucosides, 2.5 parts of tristerin and PEG-100 stearates, 3 parts of Jojoba oils, 3 parts of Semen Tritici aestivi germ oils, V
e0.5 part of oil, 4 parts of white oils, 2 parts of isopropyl palmitates, 1 part of Radix Oenotherae erythrosepalae oil, 3 parts of dimethicones, 0.2 part of methyl hydroxybenzoate, 0.1 part of propylparaben, 0.03 part of ditertbutylparacresol.
(2) water component: 10 parts of glycerol, 2.5 parts of propylene glycol, 0.15 part of hyaluronate sodium, 3 parts of amino acid humectants, 55.61 parts of Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution.
(3) after, add component: 1.0 parts of lactalbumin powders, 0.3 part of milk casein polypeptide, 3 parts of deionized waters.
(4) co-emulsifier: 0.5 part of ethoxy acrylates/sodium acryloyldimethyl taurate copolymers.
(5) antiseptic: 0.1 part, the mixture of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol.
(6) essence: 0.01 part, green tea essence.
(3), the preparation method of milk moisturizing anti-aging cream of the present invention, comprise the steps:
(1) preparation of oil phase component: by 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, tristerin and PEG-100 stearate, Jojoba oil, Semen Tritici aestivi germ oil, V
eoil, white oil, isopropyl palmitate, Radix Oenotherae erythrosepalae oil, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol add after taking in proportion in the rustless steel still of band stirring, heating for dissolving under the stirring of 30 revs/min of rotating speeds, and under 85 ℃ of constant temperatures, sterilize 20 minutes stand-by.
(2) preparation of aqueous portion: after the glycerol of formula ratio, propylene glycol, hyaluronate sodium, amino acid humectant, Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution are taken in proportion, elder generation's heating for dissolving in rustless steel still, be extracted into afterwards in (passing through drainage screen) rustless steel homogenizing still, under the stirring of 30 revs/min, continue to be heated to 85 ℃, and constant temperature disinfection 20 minutes, stand-by.
(3) by oil phase slowly in suction water, and scrape wall and stir, rotating speed is increased to 50 revs/min, stir after 3 minutes, start high speed homogenization device, under the high speed of 5000 revs/min, homogenizing is 5 minutes, to scrape afterwards wall rotating speed and drop to 40 revs/min, and under this rotating speed, be cooled to 60 ℃, add lactalbumin powder and casein polypeptide that prior dissolving is good, homogenizing 4 minutes, adds co-emulsifier, continues to stir 30 minutes, while cooling to 40 ℃, add antiseptic, essence, then stir after 15 minutes, get final product discharging.
Embodiment 2
(1), the preparation process of special ratios Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution is as follows:
(1) take 12 parts of dry product Radix Ginsengs, 15 parts of Ganodermas, 10 parts of Radix Angelicae Sinensis, 15 parts of the Radixs Astragali, 10 parts of Sargassums, 12 parts of Herb Gynostemmae Pentaphyllis, 12 parts of Radix Rhodiolaes, 0.3 part, Tremella, 1.5 parts of Folium Ginkgos, add in rustless steel still, take 0.1 part of long-lived stone powder standby.
(2) while boiling for the first time, take 900 parts of deionized waters, 6 parts of ethanol, 6 parts of propylene glycol, boil front first immersion 30 minutes, then big fire is boiled, after use little fire instead and boil 1.2 hours, with 600 order filter-cloth filterings, obtain the long-lived stone magistery of Chinese herbal medicine Tremella extracting solution 1. afterwards.
(3) in filtering residue, add the propylene glycol of the deionized water of 600 mass parts and the ethanol of 2 mass parts and 2 quality, after big fire is boiled, use little fire instead and boil again 1.0 hours, add afterwards long-lived stone powder to soak 1.0 hours, use afterwards 600 order filter-cloth filterings, obtain Chinese herbal medicine, the long-lived stone magistery of Tremella extracting solution 2..
(4) will 1. 2. after filtrate mix homogeneously, obtain the long-lived stone magistery of final Chinese medicine Tremella extracting solution (its total amount should be controlled at half left and right of adding water inventory).
(2), with the Chinese herbal medicine that makes, Tremella, long-lived stone magistery extracting solution, substitute the pure water component in milk moisturizing anti-aging cream, the prescription that designs milk moisturizing anti-aging cream by following proportioning (mass percent) is as follows:
(1) oil phase component: described oil phase component is comprised of the component of following mass parts: 16 1.7 parts of mixed alcohols, 2 parts of 16 stearyl alcohol and 16 octadecyl glucosides, 3 parts of tristerin and PEG-100 stearates, 4 parts of Jojoba oils, 3 parts of Semen Tritici aestivi germ oils, V
e0.4 part of oil, 5 parts of white oils, 2 parts of isopropyl palmitates, 2 parts of Radix Oenotherae erythrosepalae oil, 2.5 parts of dimethicones, 0.2 part of methyl hydroxybenzoate, 0.1 part of propylparaben, 0.03 part of ditertbutylparacresol.
(2) water component: 9 parts of glycerol, 3 parts of propylene glycol, 0.2 part of hyaluronate sodium, 4 parts of amino acid humectants, 50.41 parts of Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution.
(3) after, add component: 1.5 parts of lactalbumin powders, 0.25 part of milk casein polypeptide, 5 parts of deionized waters.
(4) co-emulsifier: 0.6 part of ethoxy acrylates/sodium acryloyldimethyl taurate copolymers.
(5) antiseptic: 0.1 part, the mixture of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol.
(6) essence: 0.01 part, green tea essence.
(3), the preparation method of milk moisturizing anti-aging cream of the present invention, comprise the steps:
(1) preparation of oil phase component: by 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, tristerin and PEG-100 stearate, Jojoba oil, Semen Tritici aestivi germ oil, V
eoil, white oil, isopropyl palmitate, Radix Oenotherae erythrosepalae oil, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol add after taking in proportion in the rustless steel still of band stirring, heating for dissolving under the stirring of 30 revs/min of rotating speeds, and under 85 ℃ of constant temperatures, sterilize 20 minutes stand-by.
(2) preparation of aqueous portion: after the glycerol of formula ratio, propylene glycol, hyaluronate sodium, amino acid humectant, Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution are taken in proportion, elder generation's heating for dissolving in rustless steel still, be extracted into afterwards in (passing through drainage screen) rustless steel homogenizing still, under the stirring of 30 revs/min, continue to be heated to 85 ℃, and constant temperature disinfection 20 minutes, stand-by.
(3) by oil phase slowly in suction water, and scrape wall and stir, rotating speed is increased to 50 revs/min, stir after 3 minutes, start high speed homogenization device, under the high speed of 5000 revs/min, homogenizing is 5 minutes, to scrape afterwards wall rotating speed and drop to 40 revs/min, and under this rotating speed, be cooled to 60 ℃, add lactalbumin powder and casein polypeptide that prior dissolving is good, homogenizing 4 minutes, adds co-emulsifier, continues to stir 30 minutes, while cooling to 40 ℃, add antiseptic, essence, then stir after 15 minutes, get final product discharging.
Embodiment 3
(1), the preparation process of special ratios Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution is as follows:
(1) take 15 parts of dry product Radix Ginsengs, 10 parts of Ganodermas, 12 parts of Radix Angelicae Sinensis, 12 parts of the Radixs Astragali, 15 parts of Sargassums, 10 parts of Herb Gynostemmae Pentaphyllis, 15 parts of Radix Rhodiolaes, 0.5 part, Tremella, 1 part of Folium Ginkgo, adds in rustless steel still, takes 0.3 part of long-lived stone powder standby.
(2) while boiling for the first time, take 850 parts of deionized waters, 5 parts of ethanol, 5 parts of propylene glycol, boil front first immersion 30 minutes, then big fire is boiled, after use little fire instead and boil 1.2 hours, with 600 order filter-cloth filterings, obtain the long-lived stone magistery of Chinese herbal medicine Tremella extracting solution 1. afterwards.
(3) in filtering residue, add the propylene glycol of the deionized water of 600 mass parts and the ethanol of 2 mass parts and 2 quality, after big fire is boiled, use little fire instead and boil again 1.0 hours, add afterwards long-lived stone powder to soak 1.0 hours, use afterwards 600 order filter-cloth filterings, obtain Chinese herbal medicine, the long-lived stone magistery of Tremella extracting solution 2..
(4) will 1. 2. after filtrate mix homogeneously, obtain the long-lived stone magistery of final Chinese medicine Tremella extracting solution (its total amount should be controlled at half left and right of adding water inventory).
(2), with the Chinese herbal medicine that makes, Tremella, long-lived stone magistery extracting solution, substitute the pure water component in milk moisturizing anti-aging cream, the prescription that designs milk moisturizing anti-aging cream by following proportioning (mass percent) is as follows:
(1) oil phase component: described oil phase component is comprised of the component of following mass parts: 16 2 parts of mixed alcohols, 3 parts of 16 stearyl alcohol and 16 octadecyl glucosides, 3 parts of tristerin and PEG-100 stearates, 3 parts of Jojoba oils, 4 parts of Semen Tritici aestivi germ oils, V
e0.3 part of oil, 3 parts of white oils, 1 part of isopropyl palmitate, 1 part of Radix Oenotherae erythrosepalae oil, 3 parts of dimethicones,, 0.2 part of methyl hydroxybenzoate, 0.1 part of propylparaben, 0.03 part of ditertbutylparacresol.
(2) water component: 8 parts of glycerol, 3 parts of propylene glycol, 0.2 part of hyaluronate sodium, 4 parts of amino acid humectants, 52.46 parts of Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution.
(3) after, add component: 2.0 parts of lactalbumin powders, 0.1 part of milk casein polypeptide, 6 parts of deionized waters.
(4) co-emulsifier: 0.5 part of ethoxy acrylates/sodium acryloyldimethyl taurate copolymers.
(5) antiseptic: 0.1 part, the mixture of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol.
(6) essence: 0.01 part, green tea essence.
(3), the preparation method of milk moisturizing anti-aging cream of the present invention, comprise the steps:
(1) preparation of oil phase component: by 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, tristerin and PEG-100 stearate, Jojoba oil, Semen Tritici aestivi germ oil, V
eoil, white oil, isopropyl palmitate, Radix Oenotherae erythrosepalae oil, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol add after taking in proportion in the rustless steel still of band stirring, heating for dissolving under the stirring of 30 revs/min of rotating speeds, and under 85 ℃ of constant temperatures, sterilize 20 minutes stand-by.
(2) preparation of aqueous portion: after the glycerol of formula ratio, propylene glycol, hyaluronate sodium, amino acid humectant, Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution are taken in proportion, elder generation's heating for dissolving in rustless steel still, be extracted into afterwards in (passing through drainage screen) rustless steel homogenizing still, under the stirring of 30 revs/min, continue to be heated to 85 ℃, and constant temperature disinfection 20 minutes, stand-by.
(3 by oil phase slowly in suction water, and scrapes wall and stir, and rotating speed is increased to 50 revs/min, stir after 3 minutes, start high speed homogenization device, under the high speed of 5000 revs/min, homogenizing is 5 minutes, to scrape afterwards wall rotating speed and drop to 40 revs/min, and under this rotating speed, be cooled to 60 ℃, add lactalbumin powder and casein polypeptide that prior dissolving is good, homogenizing 4 minutes, adds co-emulsifier, continues to stir 30 minutes, while cooling to 40 ℃, add antiseptic, essence, then stir after 15 minutes, get final product discharging.
Part in above-described embodiment is kilogram.
Effect embodiment
Detection method:
(1) detection of moistening effect:
Keratodermatitis hydration rate test: operation principle is to take capacitor as instrument probe, because water is the material of dielectric constant maximum on skin, when skin moisture content changes, the capacitance of skin also changes, so can be by measuring skin capacitance, analyzing skin surface moisture content.Conventional instrument is Cor neometer CM825.By measurement, use the variation of product front and back keratodermatitis capacitance to weigh the variation of water content of stratum corneum, thereby evaluate the moisture-keeping efficacy of cosmetics, this kind of method carried out quantification to the moisture of keratodermatitis, can react delicately the variation of skin moisture content, and favorable reproducibility is one of conventional method of current moisture-keeping cosmetics effect evaluation.
Experimental technique: bend side at candidate left and right forearm and mark 3 * 3cm
2the square Experimental Area of size, the test zone at left arm as moisturizer, the corresponding symmetrical region of right arm is blank, then with Cor neometer CM825 test, detect the moisture at each test position, repeat respectively 3 times, draw meansigma methods, by formula (1) calculated hydration rate.
Hydration rate=
test value-blank value* 100%
The detection of moistening effect, it is as shown in the table for result:
| ? | Embodiment 1 | Embodiment 2 | Embodiment 3 |
| 1h | 79% | 80% | 78% |
| 2h | 61% | 60% | 62% |
| 4h | 40% | 41% | 40% |
| 6h | 40% | 40% | 40% |
| 8h | 39% | 40% | 39% |
(2) with dimethyl sulfoxide, the sample preparation of previous embodiment being become to concentration is respectively the concentration of mass volume ratio 1%, carries out following experiment.
The mensuration of free radical scavenging effect
(1) extracting sample solution 2ml and concentration are that diphenyl picryl Ben Jing ﹙ DPPH ﹚ solution (solvent of this solution is the to be water) 2ml of 100 u mol/L first adds in same tool plug test tube, shake up, under room temperature standing 30 minutes, take solvent as blank, working sample absorbance under 517nm wavelength.
Suppression ratio: k%=[1-(Ai-Aj)/AC] * 100%
The absorbance of Ai:2ml DPPH solution+2ml sample solution
The absorbance of Aj:2ml sample solution+2ml solvent (being dimethyl sulfoxide)
The absorbance of AC:2ml DPPH solution+2ml solvent (being dimethyl sulfoxide)
The mensuration of free radical scavenging effect, result is as table
| ? | Suppression ratio (%) |
| Embodiment 1 | 90．2 |
| Embodiment 2 | 89．7 |
| Embodiment 3 | 89．5 |
Above-described embodiment is preferably embodiment of the present invention; but embodiments of the present invention are not restricted to the described embodiments; other any Gai Bian ﹑ Xiu Shi ﹑ Ti Dai ﹑ Zu He ﹑ doing under spirit of the present invention and principle that do not deviate from simplifies; all should be equivalent substitute mode, within being included in protection scope of the present invention.
Claims (3)
1. a milk moisturizing anti-aging cream, is characterized in that being prepared from by following component:
(1) oil phase component: described oil phase component is comprised of the component of following mass parts: 16 mixed alcohol 1.5-2.0 parts, 2-4 parts of 16 stearyl alcohol and 16 octadecyl glucosides, 2-3 parts of tristerin and PEG-100 stearates, 2-4 parts of Jojoba oils, 2-4 parts of Semen Tritici aestivi germ oils, V
e0.3-0.6 part of oil, 3-5 parts of white oils, 1-2 parts of isopropyl palmitate 2-3 part, Radix Oenotherae erythrosepalae oil, 2-3 parts of dimethicones, 0.2-0.3 part of methyl hydroxybenzoate, 0.1-0.15 part of propylparaben, 0.03-0.05 part of ditertbutylparacresol;
(2) water component: 8-10 parts of glycerol, 2-3 parts of propylene glycol, 0.1-0.2 part of hyaluronate sodium, 3-4 parts of amino acid humectants, 50.41-55.61 parts of Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution, described Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution are mainly made by the raw material of following mass parts: Radix Ginseng, Ganoderma, Radix Angelicae Sinensis, the Radix Astragali, Sargassum, Herb Gynostemmae Pentaphylli, each 10-15 part of Radix Rhodiolae, 0.1-0.5 part, Tremella, 1-2 parts of Folium Ginkgos, long-lived stone powder 0.1-0.3 part;
(3) after, add component: 1.0-2.0 parts of lactalbumin powders, 0.2-0.3 part of milk casein polypeptide, deionized water 3-6 part;
(4) co-emulsifier: 0.5-0.8 part of ethoxy acrylates/sodium acryloyldimethyl taurate copolymers;
(5) antiseptic: 0.1-0.15 part, the mixture of MIT and butyl carbamic acid-3-iodo-2-propynyl ester and propylene glycol;
(6) essence: 0.01-0.02 part, green tea essence.
2. the preparation method of milk moisturizing anti-aging cream claimed in claim 1, is characterized in that, comprises the steps:
(1) preparation of oil phase component: by 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, tristerin and PEG-100 stearate, Jojoba oil, Semen Tritici aestivi germ oil, V
eoil, white oil, isopropyl palmitate, Radix Oenotherae erythrosepalae oil, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol add after taking in proportion in the rustless steel still of band stirring, heating for dissolving under the stirring of 30 revs/min of rotating speeds, and under 85 ℃ of constant temperatures, sterilize 20 minutes stand-by;
(2) preparation of aqueous portion: after the glycerol of formula ratio, propylene glycol, hyaluronate sodium, amino acid humectant, Chinese herbal medicine, Tremella, long-lived stone magistery extracting solution are taken in proportion, elder generation's heating for dissolving in rustless steel still, be extracted into afterwards in rustless steel homogenizing still, under the stirring of 30 revs/min, continue to be heated to 85 ℃, and constant temperature disinfection 20 minutes, stand-by;
(3) by oil phase slowly in suction water, and scrape wall and stir, rotating speed is increased to 50 revs/min, stir after 3 minutes, start high speed homogenization device, under the high speed of 5000 revs/min, homogenizing is 5 minutes, to scrape afterwards wall rotating speed and drop to 40 revs/min, and under this rotating speed, be cooled to 60 ℃, add lactalbumin powder and casein polypeptide that prior dissolving is good, homogenizing 4 minutes, adds co-emulsifier, continues to stir 30 minutes, while cooling to 40 ℃, add antiseptic, essence, then stir after 15 minutes, get final product discharging.
3. the preparation method of milk moisturizing anti-aging cream according to claim 2, is characterized in that the long-lived stone magistery of described Chinese medicine Tremella extracting solution prepares by the following method:
(1) take dry product Radix Ginseng, Ganoderma, Radix Angelicae Sinensis, the Radix Astragali, Sargassum, Herb Gynostemmae Pentaphylli, each 10-15 part of Radix Rhodiolae, 0.1-0.5 part, Tremella, 1-2 parts of Folium Ginkgos, add in rustless steel still, take 0.1-0.3 part of long-lived stone powder standby;
(2) while boiling for the first time, take 700-800 parts of deionized waters, 4-6 parts of ethanol, 4-6 parts of propylene glycol, boil front first immersion 30 minutes, then big fire is boiled, after use little fire instead and boil 1-1.2 hours, with 600 order filter-cloth filterings, obtain the long-lived stone magistery of Chinese herbal medicine Tremella extracting solution 1. afterwards;
(3) in filtering residue, add the propylene glycol of the deionized water of 600-700 mass parts and the ethanol of 1-3 mass parts and 1-3 quality, after big fire is boiled, use little fire instead and boil again 0.8-1.0 hours, add afterwards long-lived stone powder to soak 0.5-1.0 hours, use afterwards 600 order filter-cloth filterings, obtain Chinese herbal medicine, the long-lived stone magistery of Tremella extracting solution 2.;
(4) will 1. 2. after filtrate mix homogeneously, obtain the long-lived stone magistery of final Chinese medicine Tremella extracting solution.
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