CN109602653B - Composition, cosmetic and essence with whitening effect and preparation method thereof - Google Patents
Composition, cosmetic and essence with whitening effect and preparation method thereof Download PDFInfo
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Abstract
The invention relates to a composition with a whitening effect, a cosmetic, an essence and a preparation method thereof, wherein the composition with the whitening effect comprises the following components in parts by mass: 0.3-5 parts of dendrobium officinale stem extract, 0.1-4 parts of angelica root extract, 0.1-4 parts of pseudo-ginseng root extract and 0.1-4 parts of astragalus membranaceus root extract. The components in the composition with the whitening effect are matched with each other, and the components can fully exert the respective effects and simultaneously have the synergistic effect by controlling the reasonable dosage of the components. The composition with the whitening effect not only has a good whitening effect, but also has the effects of moisturizing, anti-allergy and relieving.
Description
Technical Field
The invention relates to the field of cosmetics, and particularly relates to a composition, a cosmetic, an essence and a preparation method thereof.
Background
With the continuous improvement of living standard of people, the market demand of cosmetics with whitening and skin-care effects is continuously increased. However, most of the conventional whitening cosmetics contain chemically synthesized whitening substances, and have great side effects on human bodies while whitening, while the commercially available whitening cosmetics containing natural extracts have poor whitening effects.
Disclosure of Invention
Accordingly, there is a need to provide a composition, a cosmetic, an essence and a preparation method thereof with good whitening effect, aiming at the problem of poor whitening effect of the traditional whitening cosmetic containing natural extract.
The composition with the whitening effect comprises the following components in parts by mass:
the components in the composition with the whitening effect are matched with each other, and the components can fully exert the respective effects and simultaneously have the synergistic effect by controlling the reasonable dosage of the components. The composition with the whitening effect not only has a good whitening effect, but also has the effects of moisturizing, anti-allergy and relieving.
In one embodiment, the components of the composition with whitening effect further include at least one of a glossy privet fruit extract, a licorice root extract, a daisy flower extract, a rosa centifolia flower extract, and a bisque flower extract.
In one embodiment, the material comprises the following raw material components in parts by mass:
in one embodiment, the material comprises the following raw material components in parts by mass:
the invention also provides a cosmetic.
A cosmetic comprises the composition with whitening effect.
The invention also provides essence.
An essence comprises the composition with the whitening effect, 1.3-15.5 parts of a humectant and 75-80 parts of water.
In one embodiment, the essence further comprises a preservative.
In one embodiment, the humectant is selected from at least one of sodium acetylated hyaluronate, polyglutamic acid, and 1.3-propanediol.
The essence has good whitening effect, and also has effects of keeping moisture, resisting allergy and relieving.
A preparation method of essence comprises the following steps: based on the mass portion of the raw materials,
mixing 1.3-15.5 parts of humectant with 75-80 parts of water to obtain phase A;
adding the composition with the whitening effect into the phase A and uniformly mixing to obtain a phase B;
filtering the phase B, and reserving filtrate to obtain the essence.
The preparation method of the essence is simple, and the prepared essence not only has a good whitening effect, but also has the effects of moisturizing, anti-allergy and relieving.
Detailed Description
The present invention will be described in detail with reference to the following embodiments in order to make the aforementioned objects, features and advantages of the invention more comprehensible. In the following description, numerous specific details are set forth in order to provide a thorough understanding of the present invention. This invention may, however, be embodied in many different forms and should not be construed as limited to the embodiments set forth herein.
Unless defined otherwise, all technical and scientific terms used herein have the same meaning as commonly understood by one of ordinary skill in the art to which this invention belongs. The terminology used in the description of the invention herein is for the purpose of describing particular embodiments only and is not intended to be limiting of the invention. As used herein, the term "and/or" includes any and all combinations of one or more of the associated listed items.
The invention provides a composition with a whitening effect, which is prepared from the following components in parts by mass:
the key substance influencing the white skin is melanin, during the formation of the melanin, tyrosinase plays a key role, and the amount of melanin produced has a direct relationship with tyrosinase. Therefore, the skin whitening mechanism is mainly to block the oxidation pathway of the tyrosine to generate the melanin and reduce the generation of the melanin to achieve the effect of whitening the skin by inhibiting the activity of the tyrosinase.
Wherein, the angelica has the functions of anti-inflammation, scavenging oxygen free radicals, enhancing immunity and the like. Research shows that the angelica root extract can inhibit the activity of tyrosinase, block the oxidation path of the melanin generated by the tyrosine, reduce the generation of the melanin and achieve the effect of whitening the skin. In addition, the radix Angelicae sinensis extract also has effects of enhancing skin epidermis water content and cell SOD activity.
The dendrobium officinale stem extract can promote the expression of AQP3 of cell aquaporins, dredge the whole transmembrane protein channel, and facilitate nutrient substances in the composition to enter the horny layer of the skin without obstacle, and has various pharmacological effects such as enhancing the immunity of the organism, resisting oxidation and aging, reducing blood sugar, supplementing fluid and promoting the production of body fluid, promoting blood circulation and benefiting qi, fundamentally adjusting the functions of a human body, improving the sub-health state of the human body, and fundamentally improving the brightness of the skin. In addition, the dendrobium officinale stem extract is rich in nutrient substances such as polysaccharide, dendrobine, free amino acid, vitamin A, vitamin C, vitamin E and the like, and can be used for supplementing nutrition to the skin, improving the skin elasticity, preserving the moisture and increasing the resistance of the skin to the external adverse environment.
The panax notoginseng root extract can be used as an anti-inflammatory agent besides the whitening effect, and the active ingredient panax notoginseng saponins have strong inhibition effect on certain fungi, have certain inhibition effect on staphylococcus aureus and escherichia coli, and relieve various uncomfortable symptoms of the skin.
Wherein, the astragalus membranaceus root extract is derived from the root of the astragalus membranaceus, and contains important active ingredient astragalus saponin, which can stimulate the proliferation of cortical cells and improve the microenvironment of the skin surface. The extract and the pseudo-ginseng extract are mutually balanced, traditional Chinese medicine harmful components which are easy to cause skin allergy in the dendrobium officinale stem extract and the pseudo-ginseng root extract are inhibited together with the pseudo-ginseng extract, the inhibition effect of the dendrobium officinale stem extract and the pseudo-ginseng root extract on tyrosinase is promoted, and the purpose of mild nourishing is finally achieved.
In one embodiment, the components of the composition with whitening effect further include at least one of a glossy privet fruit extract and a licorice root extract. The glossy privet fruit extract and the licorice root extract are used as auxiliary materials, and the whitening effect of the composition with the whitening effect can be further improved.
In one embodiment, the components of the composition further comprise at least one of a daisy extract, a rosa centifolia extract, and a bisque flower extract. The marguerite extract, the rosa multiflora flower extract and the vegetarian square flower extract are neutral and mild in shape and contain anti-allergy and soothing components, so that on one hand, harmful traditional Chinese medicine components which are easy to cause skin allergy in the dendrobium officinale stem extract and the pseudo-ginseng root extract can be inhibited, on the other hand, the microenvironment of the skin can be regulated, components with whitening effects can enter the interior of the skin more easily, the tyrosinase activity is inhibited, the formation of melanin is avoided, and the purposes of mildness and nourishing are achieved.
In one embodiment, the composition with whitening effect comprises the following components in parts by mass:
in one embodiment, the composition with whitening effect comprises the following components in parts by mass:
in one embodiment, the composition with whitening effect comprises the following components in parts by mass:
wherein, the rosa multiflora flower extract, the vegetarian square flower extract, the daisy flower extract, the dendrobium officinale stem extract, the angelica root extract, the pseudo-ginseng root extract, the astragalus membranaceus root extract, the glossy privet fruit extract and the licorice root extract can be purchased from the market, and each extract can be extracted and prepared by the following method respectively, and each extract of the embodiment of the invention is prepared by the following method, and concretely comprises the following steps:
1) selecting high-quality fresh and high-quality plant raw materials, cleaning with purified water, drying, dehydrating, and pulverizing into raw material powder with particle size less than 800 meshes.
2) Conveying the raw material powder into a supercritical extraction kettle for supercritical CO2Extracting by a method, and introducing CO into a supercritical extraction kettle2Gas, CO2The flow rate of the extraction is 8kg/h, and the extraction is carried out for 8h under the conditions that the extraction pressure is 20MPa-25MPa and the extraction temperature is 35 ℃ to obtain an extract.
3) Adding the extract into purified water according to the feed-liquid ratio of 1:7g/L, heating and distilling for 5h, and condensing and refluxing to obtain the extract.
The components in the composition with the whitening effect are matched with each other, and the components can fully exert the respective effects and simultaneously have the synergistic effect by controlling the reasonable dosage of the components. The composition with the whitening effect not only has a good whitening effect, but also has the effects of moisturizing, anti-allergy and relieving.
The invention also provides a cosmetic.
A cosmetic comprising the composition having whitening efficacy according to any one of the embodiments of the present invention.
It can be understood that the cosmetics of the present invention can be various products such as lotion, essence, skin cream, moisturizing cream, etc., and are not described herein in any greater detail.
The invention also provides essence.
An essence comprises the composition with the whitening effect according to any embodiment of the invention, 1.3-15.5 parts of a humectant and 75-80 parts of water.
It can be understood that the essence of the invention can be uniformly coated on a mask substrate to prepare a mask.
In one embodiment, the essence further comprises a preservative.
The preservative can be a preservative commonly used in the field of cosmetics, preferably at least one of food-grade preservatives potassium sorbate and sodium benzoate is selected, and the food-grade preservative has small side effect on human bodies. Furthermore, a combination of food-grade preservatives potassium sorbate and sodium benzoate is selected, wherein the addition amount of the potassium sorbate is 0.1 to 0.5 part by mass, and the addition amount of the sodium benzoate is 0.05 to 0.4 part by mass.
In one embodiment, the humectant is selected from at least one of sodium acetylated hyaluronate, polyglutamic acid, and 1.3-propanediol.
In one embodiment, the humectant is a combination of acetylated sodium hyaluronate, polyglutamic acid and 1.3-propylene glycol, preferably, the acetylated sodium hyaluronate is 0.01-0.2 parts, the polyglutamic acid is 0.01-0.3 parts and the 1.3-propylene glycol is 1-15 parts by mass.
Carboxyl groups and other polar groups in the molecule of the acetylated sodium hyaluronate can combine with water to form hydrogen bonds, and about 1g of the acetylated sodium hyaluronate can lock 1000g of water. Preferably, the molecular weight of the acetylated sodium hyaluronate is less than 30000Da, namely the molecular weight of the acetylated sodium hyaluronate is ultra-small, and the acetylated sodium hyaluronate has remarkable repairing capability on skin cells damaged by ultraviolet rays besides the effects of strong water locking and moisture retention, and the lower the molecular weight is, the stronger the repairing capability is. Meanwhile, the acetylated sodium hyaluronate molecules also have the effect of preventing sunburn caused by ultraviolet rays.
The polyglutamic acid has excellent moisturizing performance, can enhance the skin elasticity, mildly inhibits the tyrosine kinase activity, has comprehensive and deep certification on the safety and efficacy, is safe in source, is an edible raw material, and greatly improves the skin elasticity after long-term testing.
1.3-propylene glycol A plant moisturizer made by fermenting sugar can improve the moisture content of the skin at the moment of use. By being compounded with other moisturizing agents, the moisturizing agent can continuously keep the moisture content of the corneous layer improved instantly when being used, and can endow the skin with smooth, fine and moist using feeling after being used.
The essence has good whitening effect, and also has effects of keeping moisture, resisting allergy and relieving.
The invention also provides a preparation method of the essence.
A preparation method of essence comprises the following steps:
uniformly mixing 1.3-15.5 parts of humectant with 75-80 parts of water to obtain phase A, adding the composition with the whitening effect into the phase A, uniformly mixing to obtain phase B, filtering the phase B, and retaining filtrate to obtain the essence.
In one embodiment, the preparation method of the essence comprises the following steps: according to the mass parts, 0.05 part of acetylated sodium hyaluronate, 0.05 part of polyglutamic acid, 8 parts of 1.3-propylene glycol and 78.5 parts of deionized water are mixed in a stirring pot and stirred uniformly to obtain phase A, then the composition with the whitening effect is added into the phase A and stirred uniformly, wherein the stirring speed is 40 revolutions per minute, the mixture is stirred for 60 minutes until all components are uniformly dispersed to obtain phase B, 0.2 part of potassium sorbate and 0.2 part of sodium benzoate are added, the stirring is continued for 50 minutes until preservatives are uniformly dispersed in the phase B, the stirring is stopped, the mixture is kept standing for 30 minutes, and the filtrate is reserved after the mixture is filtered by a 500-mesh filter screen to obtain the essence.
The preparation method of the essence is simple, and the prepared essence not only has a good whitening effect, but also has the effects of moisturizing, anti-allergy and relieving.
In order that the objects and advantages of the invention will be more clearly understood, the invention is further described in detail below with reference to examples. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Example 1
A preparation method of essence comprises the following steps:
mixing 0.05 part of acetylated sodium hyaluronate, 8 parts of 1.3-propylene glycol and 78.5 parts of deionized water in a stirring pot, uniformly stirring to obtain a phase A, adding the components of the composition with the whitening effect in the table 1 into the phase A, uniformly stirring, wherein the stirring speed is 40 revolutions per minute, stirring for 60 minutes until the components are uniformly dispersed to obtain a phase B, adding 0.2 part of potassium sorbate and 0.2 part of sodium benzoate, continuously stirring for 50 minutes until the preservative is uniformly dispersed in the phase B, stopping stirring, standing for 30 minutes, filtering by a 500-mesh filter screen, and retaining a filtrate to obtain an essence.
TABLE 1
| Name of raw materials | Content (in) |
| Dendrobium officinale stem extract | 0.4 |
| Angelica root extract | 0.1 |
| Notoginseng radix extract | 0.5 |
| Astragalus membranaceus root extract | 0.2 |
Example 2
A preparation method of essence comprises the following steps:
mixing 0.05 part of acetylated sodium hyaluronate, 8 parts of 1.3-propylene glycol and 78.5 parts of deionized water in a stirring pot, uniformly stirring to obtain a phase A, adding the components of the composition with the whitening effect in the table 2 into the phase A, uniformly stirring, wherein the stirring speed is 40 revolutions per minute, stirring for 60 minutes until the components are uniformly dispersed to obtain a phase B, adding 0.2 part of potassium sorbate and 0.2 part of sodium benzoate, continuously stirring for 50 minutes until the preservative is uniformly dispersed in the phase B, stopping stirring, standing for 30 minutes, filtering by a 500-mesh filter screen, and retaining a filtrate to obtain an essence.
TABLE 2
Example 3
A preparation method of essence comprises the following steps:
mixing 0.05 part of acetylated sodium hyaluronate, 0.2 part of polyglutamic acid, 8 parts of 1.3-propylene glycol and 78.5 parts of deionized water in a stirring pot, uniformly stirring to obtain a phase A, adding the components of the composition with the whitening effect in the table 3 into the phase A, uniformly stirring, wherein the stirring speed is 40 revolutions per minute, stirring for 60 minutes until the components are uniformly dispersed to obtain a phase B, adding 0.2 part of potassium sorbate and 0.2 part of sodium benzoate, continuously stirring for 50 minutes until the preservative is uniformly dispersed in the phase B, stopping stirring, standing for 30 minutes, filtering through a 500-mesh filter screen, and retaining a filtrate to obtain an essence.
TABLE 3
| Name of raw materials | Content (in) |
| Dendrobium officinale stem extract | 4 |
| Angelica root extract | 3 |
| Notoginseng radix extract | 3.5 |
| Astragalus membranaceus root extract | 3.8 |
| Extract of glossy privet fruit | 2.4 |
| Licorice root extract | 3 |
Example 4
A preparation method of essence comprises the following steps:
mixing 0.1 part of acetylated sodium hyaluronate, 0.25 part of polyglutamic acid, 8 parts of 1.3-propylene glycol and 78.5 parts of deionized water in a stirring pot, uniformly stirring to obtain a phase A, adding the components of the composition with the whitening effect in the table 4 into the phase A, uniformly stirring, wherein the stirring speed is 40 revolutions per minute, stirring for 60 minutes until the components are uniformly dispersed to obtain a phase B, adding 0.2 part of potassium sorbate and 0.2 part of sodium benzoate, continuously stirring for 50 minutes until the preservative is uniformly dispersed in the phase B, stopping stirring, standing for 30 minutes, filtering through a 500-mesh filter screen, and retaining a filtrate to obtain an essence.
TABLE 4
| Name of raw materials | Content (in) |
| Dendrobium officinale stem extract | 4 |
| Angelica root extract | 3 |
| Notoginseng radix extract | 3.5 |
| Astragalus membranaceus root extract | 3.8 |
| Extract of glossy privet fruit | 2.4 |
| Licorice root extract | 3 |
| Extract of Daisy | 1.4 |
| Flos Rosae Davuricae extract | 0.5 |
| Extract of vegetarian square flower | 0.6 |
Comparative example 1
A preparation method of essence comprises the following steps:
mixing 0.05 part of acetylated sodium hyaluronate, 8 parts of 1.3-propylene glycol and 78.5 parts of deionized water in a stirring pot, uniformly stirring to obtain a phase A, adding the components of the composition with the whitening effect in the table 5 into the phase A, uniformly stirring, wherein the stirring speed is 40 revolutions per minute, stirring for 60 minutes until the components are uniformly dispersed to obtain a phase B, adding 0.2 part of potassium sorbate and 0.2 part of sodium benzoate, continuously stirring for 50 minutes until the preservative is uniformly dispersed in the phase B, stopping stirring, standing for 30 minutes, filtering by a 500-mesh filter screen, and retaining a filtrate to obtain an essence.
TABLE 5
| Name of raw materials | Content (in) |
| Dendrobium officinale stem extract | 0.4 |
| Angelica root extract | 0.1 |
Comparative example 2
A preparation method of essence comprises the following steps:
mixing 0.05 part of acetylated sodium hyaluronate, 8 parts of 1.3-propylene glycol and 78.5 parts of deionized water in a stirring pot, uniformly stirring to obtain a phase A, adding the components of the composition with the whitening effect in the table 6 into the phase A, uniformly stirring, wherein the stirring speed is 40 revolutions per minute, stirring for 60 minutes until the components are uniformly dispersed to obtain a phase B, adding 0.2 part of potassium sorbate and 0.2 part of sodium benzoate, continuously stirring for 50 minutes until the preservative is uniformly dispersed in the phase B, stopping stirring, standing for 30 minutes, filtering by a 500-mesh filter screen, and retaining a filtrate to obtain an essence.
TABLE 6
| Name of raw materials | Content (in) |
| Dendrobium officinale stem extract | 0.4 |
| Notoginseng radix extract | 0.5 |
| Astragalus membranaceus root extract | 0.2 |
Comparative example 3
A preparation method of essence comprises the following steps:
mixing 0.05 part of acetylated sodium hyaluronate, 8 parts of 1.3-propylene glycol and 78.5 parts of deionized water in a stirring pot, uniformly stirring to obtain a phase A, adding the components of the composition with the whitening effect in the table 7 into the phase A, uniformly stirring, wherein the stirring speed is 40 revolutions per minute, stirring for 60 minutes until the components are uniformly dispersed to obtain a phase B, adding 0.2 part of potassium sorbate and 0.2 part of sodium benzoate, continuously stirring for 50 minutes until the preservative is uniformly dispersed in the phase B, stopping stirring, standing for 30 minutes, filtering by a 500-mesh filter screen, and retaining a filtrate to obtain an essence.
TABLE 7
| Name of raw materials | Content (in) |
| Angelica root extract | 0.1 |
| Notoginseng radix extract | 0.5 |
| Astragalus membranaceus root extract | 0.2 |
Comparative example 4
A preparation method of essence comprises the following steps:
mixing 0.05 part of acetylated sodium hyaluronate, 8 parts of 1.3-propylene glycol and 78.5 parts of deionized water in a stirring pot, uniformly stirring to obtain a phase A, adding the components of the composition with the whitening effect in the table 8 into the phase A, uniformly stirring, wherein the stirring speed is 40 revolutions per minute, stirring for 60 minutes until the components are uniformly dispersed to obtain a phase B, adding 0.2 part of potassium sorbate and 0.2 part of sodium benzoate, continuously stirring for 50 minutes until the preservative is uniformly dispersed in the phase B, stopping stirring, standing for 30 minutes, filtering by a 500-mesh filter screen, and retaining a filtrate to obtain an essence.
TABLE 8
| Name of raw materials | Content (in) |
| Angelica root extract | 7 |
| Notoginseng radixRoot extract | 0.01 |
| Dendrobium officinale stem extract | 0.05 |
| Astragalus membranaceus root extract | 0.6 |
Performance testing
Test of whitening effectiveness
The inhibition of tyrosinase activity by the essences prepared in examples 1 to 4 and comparative examples 1 to 4 was examined in this test.
1. Test method
Referring to section 2.3 of whitening effectiveness test method of in vitro experimental study on skin aging resistance and whitening efficacy of angelica sinensis extract in the 21 st volume of 2010, 4 th of the journal Shizhen national medicine.
1. Evaluation of Effect
The tyrosinase inhibition results are shown in table 9.
TABLE 9
| Group of | Tyrosinase inhibition (%) |
| Example 1 | 21.1 |
| Example 2 | 21.4 |
| Example 3 | 23.6 |
| Example 4 | 25.3 |
| Comparative example 1 | 9.3 |
| Comparative example 2 | 11.9 |
| Comparative example 3 | 11.3 |
| Comparative example 4 | 8,5 |
As can be seen from table 9, in the tyrosinase inhibition rate test, the inhibition degree of the example group on tyrosinase is significantly better than that of the comparative example group, and the tyrosinase inhibition rate in the example 4 group is the highest, mainly because the example 4 group also contains a soothing component, which adjusts the skin microenvironment, facilitates the components with the whitening effect to enter the inside of the skin, and inhibits the tyrosinase activity, thereby avoiding the formation of melanin and achieving the mild whitening effect. In comparative example 1, the pseudo-ginseng root extract and the astragalus membranaceus root extract are absent, the tyrosinase inhibition rate is the lowest, and although the dendrobium officinale stem extract and the angelica root extract are contained, substances capable of regulating the microenvironment on the surface of the skin are required to open the skin channel, so that the main substances can exert the effects. In the absence of the angelica root extract in comparative example 2 and the dendrobium officinale stem extract in comparative example 3, the sum of the tyrosinase inhibition rates in both groups was not as high as that in the case of the tyrosinase inhibition rate in example 4. Although the group of comparative example 4 includes the four effective ingredients of the composition having whitening efficacy of the present invention, the ratio of the four ingredients is not listed in the formulation of the composition having whitening efficacy of the present invention. The above results indicate that the composition with whitening effect of the present invention has no essential ingredients, and at the same time, the composition needs to be mixed with each other in a reasonable ratio to obtain the maximum synergistic effect, so as to obtain the optimal whitening effect.
Test of practical effect
1. Grouping experiments:
the subjects selected from 20-30 years old people with facial skin allergy (face with acne, pimple, red blood streak, patient) were randomly divided into 8 groups of 10 per group according to examples 1-4 and comparative examples 1-4.
2. The using method comprises the following steps:
after cleaning the face, applying the facial mask containing the essence of the invention on the face of a subject, and gently patting and firmly adhering the face. Taking off the facial mask after 30min, washing with clear water, and continuously using for 45 days by the subject once a day.
3. And (3) testing results:
and carrying out comprehensive scoring by adopting a civil survey scoring method. The trial scoring sheet was filled out immediately after 45 days. The using effect of each item in the scoring table is divided into 5 points, and 5 points are the highest points, which shows that the effect is very satisfactory; 4, the score is better and relatively satisfactory; 3 is acceptable; the following score of 3 is an unacceptable range, and the average score of each use effect is shown in table 5:
watch 10
| Effects of use | Relieving and non-irritating | Moisture retention | Acne removing device | Removing red blood streak |
| Example 1 | 4.2 | 4.3 | 3.9 | 3.8 |
| Example 2 | 4.1 | 4.0 | 4.0 | 4.1 |
| Example 3 | 4.7 | 4.7 | 4.6 | 4.7 |
| Example 4 | 4.9 | 4.7 | 5.0 | 4.8 |
| Comparative example 1 | 2.3 | 3.2 | 2.6 | 2.1 |
| Comparative example 2 | 3.2 | 3.0 | 3.1 | 3.4 |
| Comparative example 3 | 3.6 | 3.2 | 3.3 | 3.4 |
| Comparative example 4 | 3.0 | 3.2 | 3.7 | 3.7 |
The test results are shown in table 10, and the overall effect of the example group is significantly better than that of the control group. The comparative example 1 does not contain the notoginseng root extract and the astragalus membranaceus root extract, has the worst performance in index evaluation of relieving, nonirritating, acne removing and red blood streak removing which can reflect the anti-allergy relieving effect, and also proves that the notoginseng root extract and the astragalus membranaceus root extract can play the anti-allergy relieving effect. Comparative examples 2 to 3 lack an important ingredient of the composition having whitening efficacy of the present invention and each index is low, and in comparative example 4, although the composition having whitening efficacy of the present invention contains four effective ingredients, the ratio of the four ingredients is not in the list of the ratio of the composition having whitening efficacy of the present invention, and each index is also low. Examples 3 and 4 show the best performance in the evaluation of anti-allergy soothing effect because they further contain anti-allergy soothing components such as rosa multiflora extract. The above results indicate that the composition with whitening effect of the present invention has no essential ingredients, and at the same time, the composition needs to be mixed with each other in a reasonable ratio to obtain the maximum synergistic effect, so as to obtain the optimal whitening effect.
The technical features of the embodiments described above may be arbitrarily combined, and for the sake of brevity, all possible combinations of the technical features in the embodiments described above are not described, but should be considered as being within the scope of the present specification as long as there is no contradiction between the combinations of the technical features.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.
Claims (9)
1. The composition with the whitening effect is characterized by comprising the following raw material components in parts by mass:
0.3-5 parts of dendrobium officinale stem extract,
0.1-4 parts of angelica root extract,
0.1-4 parts of pseudo-ginseng root extract,
0.1-5 parts of astragalus membranaceus root extract,
0.1-4 parts of glossy privet fruit extract,
0.1-6 parts of licorice root extract,
0.3-5 parts of daisy extract,
0.3-5 parts of rosa centifolia flower extract, and
0.3-5 parts of a vegetarian square flower extract;
the raw materials are extracted by the following method, and the method comprises the following steps:
1) selecting high-quality fresh and high-quality plant raw materials, cleaning the plant raw materials with purified water, drying and dehydrating the plant raw materials, and putting the plant raw materials into a crusher to be crushed into raw material powder with the particle size of less than 800 meshes;
2) conveying the raw material powder to a supercritical extraction kettle for supercritical CO2Extracting by a method, and introducing CO into a supercritical extraction kettle2Gas, CO2The flow rate of the extraction is 8kg/h, and the extraction is carried out for 8h under the conditions that the extraction pressure is 20MPa-25MPa and the extraction temperature is 35 ℃ to obtain an extract;
3) adding the extract into purified water according to the feed-liquid ratio of 1:7g/L, heating and distilling for 5h, and condensing and refluxing to obtain the extract.
2. The composition with whitening effect according to claim 1, characterized by comprising the following raw material components in parts by mass:
0.5-4 parts of dendrobium officinale stem extract,
0.2-3 parts of angelica root extract,
0.3-4 parts of pseudo-ginseng root extract,
0.2-4 parts of astragalus membranaceus root extract,
0.5 to 3.5 portions of glossy privet fruit extract,
0.8-3 parts of licorice root extract,
0.3-2 parts of daisy extract,
0.4-3 parts of rosa centifolia flower extract, and
0.3-4 parts of extract of the vegetarian square flower.
3. The composition with whitening effect according to claim 1, characterized by comprising the following raw material components in parts by mass:
4 parts of dendrobium officinale stem extract,
3 parts of angelica root extract,
3.5 parts of pseudo-ginseng root extract,
3.8 parts of astragalus membranaceus root extract,
2.4 parts of glossy privet fruit extract,
3 parts of licorice root extract,
1.4 parts of daisy extract,
0.5 part of rosa centifolia flower extract and
0.6 part of extract of the vegetarian square flowers.
4. A cosmetic comprising the composition having whitening efficacy according to any one of claims 1 to 3.
5. An essence comprising the composition having whitening effects according to any one of claims 1 to 3, 1.3 to 15.5 parts of a moisturizer, and 75 to 80 parts of water.
6. The essence of claim 5, further comprising a preservative.
7. The essence of claim 5 or 6, wherein the humectant is selected from at least one of sodium hyaluronate, polyglutamic acid and 1, 3-propanediol.
8. The essence of claim 7, wherein the moisturizer consists of 0.01 to 0.2 parts by mass of acetylated sodium hyaluronate, 0.01 to 0.3 parts by mass of polyglutamic acid and 1 to 15 parts by mass of 1.3-propanediol.
9. The preparation method of the essence is characterized by comprising the following steps: based on the mass portion of the raw materials,
mixing 1.3-15.5 parts of humectant with 75-80 parts of water to obtain phase A;
adding the composition with whitening effect according to any one of claims 1 to 3 into the phase A, and uniformly mixing to obtain a phase B;
filtering the phase B, and reserving filtrate to obtain the essence.
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