CN110856708A

CN110856708A - Facial mask liquid and preparation method thereof

Info

Publication number: CN110856708A
Application number: CN201810976528.0A
Authority: CN
Inventors: 兰海宁
Original assignee: Individual
Current assignee: Individual
Priority date: 2018-08-25
Filing date: 2018-08-25
Publication date: 2020-03-03

Abstract

The invention relates to the technical field of cosmetics, in particular to a mask liquid and a preparation method thereof, wherein the mask liquid comprises the following components in percentage by weight: 0.1-0.5% of allantoin, 0.5-5% of betaine, 0.1-0.2% of carbomer, 2-8% of propylene glycol, 2-8% of butanediol, 0.1-0.2% of triethanolamine, 0.1-0.2% of xanthan gum, 0.1-0.4% of dipotassium glycyrrhizinate, 0.05-0.3% of sodium hyaluronate, 0.01-0.5% of glutathione, 0-0.0005% of oligopeptide-10.00005, 0-0.0004% of oligopeptide-30.00004, 0.4-1.0% of 1, 2-hexanediol, 0.4-0.6% of p-hydroxyacetophenone, 0.1-1% of rhodiola root extract, 0.1-1% of ginseng root extract, 0.1-1% of horse chestnut extract, 0.1-1% of purslane extract, 0.1-1% of golden chamomile extract, 0.1-1% of polygonum cuspidatum root extract, and 10-90% of deionized water; the skin-whitening moisturizing cream contains various active ingredients, can quickly moisturize and moisturize, whiten the skin and brighten the skin color, can effectively relieve the sensitivity of the skin, and is particularly suitable for sensitive skin.

Description

Facial mask liquid and preparation method thereof

[ technical field ] A method for producing a semiconductor device

The invention relates to the technical field of cosmetics, and particularly relates to a mask liquid and a preparation method thereof.

[ background of the invention ]

The facial mask becomes a more and more active class in the beauty market, the use method of the facial mask is simple, the nursing time is saved, and the facial mask can easily enjoy nursing in a beauty parlor. For the fast-paced life mode of modern women, the mask is more acceptable to the women. The principle of the facial mask is that the facial mask is covered on the face for a short time, external air and pollution are temporarily isolated through the facial mask towel, pores of the skin are expanded, secretion and metabolism of sweat glands are promoted, the oxygen content of the skin is increased, the skin is promoted to remove metabolic products of epidermal cells and accumulated grease substances, high-concentration nutrient contents in facial mask liquid quickly permeate into the cutin layer of the skin, and therefore quick and effective nursing of the skin is achieved.

At present, the facial masks in the market are various in types and different in efficacy. With the increasing environmental pollution, the increasing competitive pressure of people, and the use of skin care products of various brands and qualities, the skin of a user is more sensitive. Therefore, users are pursuing more safe and effective masks.

[ summary of the invention ]

The invention aims to provide a mask liquid and a preparation method thereof aiming at the defects and shortcomings of the prior art, the mask liquid contains multiple active ingredients, can quickly replenish water, moisturize, whiten skin and brighten skin color, can effectively relieve the sensitivity of the skin, and is particularly suitable for sensitive skin.

The invention relates to a mask liquid and a preparation method thereof, wherein the mask liquid comprises the following components in percentage by weight:

0.1-0.5% of allantoin, 0.5-5% of betaine, 0.1-0.2% of carbomer, 2-8% of propylene glycol, 2-8% of butanediol, 0.1-0.2% of triethanolamine, 0.1-0.2% of xanthan gum, 0.1-0.4% of dipotassium glycyrrhizinate, 0.05-0.3% of sodium hyaluronate, 0.01-0.5% of glutathione, 0-0.0005% of oligopeptide-10.00005, 0-0.0004% of oligopeptide-30.00004, 0.4-1.0% of 1, 2-hexanediol, 0.4-0.6% of p-hydroxyacetophenone, 0.1-1% of rhodiola root extract, 0.1-1% of ginseng root extract, 0.1-1% of horse chestnut extract, 0.1-1% of purslane extract, 0.1-1% of golden chamomile extract, 0.1-1% of polygonum cuspidatum root extract, and 10-90% of deionized water;

the preparation method of the mask liquid comprises the following steps:

the method comprises the following steps: adding allantoin, betaine, carbomer, propylene glycol, butanediol, xanthan gum, sodium hyaluronate, dipotassium glycyrrhizinate, 1, 2-hexanediol, p-hydroxyacetophenone and deionized water into an emulsifying pot according to the formula proportion, stirring and heating to 80-85 ℃, homogenizing for 3 minutes, and preserving heat for 20-25 minutes to obtain a first mixture;

step two: cooling to 45 deg.C, adding radix Rhodiolae extract, radix Ginseng extract, horse chestnut extract, herba Portulacae extract, flos Chrysanthemi extract, rhizoma Polygoni Cuspidati extract, glutathione, oligopeptide-1 and oligopeptide-3 into the first mixture according to formula proportion, stirring for 2-3 min, and cooling to 40 deg.C;

step three: adding triethanolamine according to the formula composition proportion, and continuously stirring for 10-15 minutes to obtain the facial mask liquid.

Further, the weight ratio of the 1, 2-hexanediol to the p-hydroxyacetophenone in the first step is 0.5:0.5 or 0.8: 0.4.

The invention has the beneficial effects that: the facial mask liquid and the preparation method thereof contain various active ingredients, can quickly replenish water, moisturize, whiten skin and brighten skin color, can effectively relieve the sensitivity of the skin, and is particularly suitable for sensitive skin.

[ detailed description ] embodiments

The present invention will be described in detail with reference to specific examples, wherein the exemplary examples and descriptions are provided only for explaining the present invention and are not intended to limit the present invention.

The mask liquid and the preparation method thereof according to the specific embodiment comprise the following components in percentage by weight:

the preparation method of the mask liquid comprises the following steps:

The "1, 2-hexanediol, p-hydroxyacetophenone" in the present invention is a cosmetic raw material known in the art, and the composition thereof can be clearly determined by those skilled in the art. When the concentration of the 1, 2-hexanediol is 1.0%, certain sterilization capability is achieved; when the concentration of p-hydroxyacetophenone is 0.5%, the composition has the capability of killing fungi, and when the 1, 2-hexanediol and the p-hydroxyacetophenone are added in the amount of 0.5:0.5 or 0.8:0.4 (weight ratio), the composition can pass the preservative challenge test in emulsion, cream and gel. Preferably, the weight ratio of 1, 2-hexanediol to p-hydroxyacetophenone is 0.5: 0.5.

In the mask liquid, the content of Epidermal Growth Factor (EGF) is 500-5000 international units/mg, the content of basic fibroblast growth factor (bFGF) is 200-2000 international units/mg, and various complementary synergistic components with reasonable proportion are used, so that the efficacy performance of the mask liquid is effectively improved. The efficacy of each component is as follows:

wherein:

(1) glutathione: is tripeptide containing gamma-amido bond and sulfhydryl, and consists of glutamic acid, cysteine and glycine. Is present in almost every cell of the body, helps to maintain the normal function of the immune system, and has antioxidant and antidotal effects. Glutathione can inhibit melanin generation, prevent skin aging, reduce pigmentation, improve skin oxidation resistance, and prevent allergy. The product can be added into cosmetics to be suitable for various skins, and especially has good caring effect on sensitive skin. Available from sienzeiron biotechnology limited.

(2) Oligopeptide-1: also called as Epidermal Growth Factor (EGF), is an active substance in human body, and an active polypeptide consisting of 53 amino groups can repair and proliferate epidermal cells by stimulating tyrosine phosphorylation of epidermal growth factor receptors, and has good curative effect on injured and damaged epidermal skin. The method is mainly characterized in that the proliferation and differentiation of cells can be promoted, so that the aged and dead cells are replaced by the new cells, the epidermal cells become full, the youthful state is recovered, and the anti-wrinkle effect is achieved. EGF also stops bleeding, and has effects of accelerating wound healing of skin and mucosa, diminishing inflammation, relieving pain, and preventing ulcer. EGF has good stability, is mainly used in the medical field initially, and is mainly used for promoting the repair and regeneration of damaged epidermis, such as treating burns, scalds and the like. The Epidermal Growth Factor (EGF) used in this example was greater than 10 ten thousand International units/mg, and was obtained from Newcastle disease, Inc., Hangzhou.

(3) Oligopeptide-3: also called basic fibroblast growth factor (bFGF), has strong proliferation and mitosis actions on 3T3 cells, and is widely applied to cell repair. Acts on mesoderm and mainly plays a role in deeply repairing and conditioning skin. Also called as dermal growth factor, is mainly present in keratinocytes of the epidermal substrate, is an important cell-promoting mitogenic factor and angiogenic factor, has wide biological activity on various cells derived from mesoderm and neuroectoderm, can promote cell proliferation, growth and differentiation, promote angiogenesis, improve microenvironment of cell life, promote regeneration of damaged nerves and repair of blood vessels, muscles, skin and the like, is a nerve cell nutrition and regeneration factor, and is called as a cell activating factor. The viability of epidermal growth factor (bFGF) used in this example was greater than 5 ten thousand International units/mg, available from Newcastle disease, Inc., Hangzhou.

(4) Dipotassium glycyrrhizinate: can activate corticosteroid compound (inhibit metabolic enzyme), indirectly enhance corticosteroid compound effect, and has antibacterial, antiinflammatory, toxic substance removing, antiallergic, and deodorant effects. Available from pharmaceutical co ltd, widely planted in gansu.

(5) Sodium hyaluronate: sodium hyaluronate is one of the constituents of human skin, is an acidic viscous sugar which is widely distributed in human body, exists in a matrix of connective tissue, and has good moisturizing effect. Available from Shandong Furuida pharmaceutical group, Inc.

(6) Rhodiola root extract: the main components are salidroside, aglycone tyrosol and Luoshiwei, and the product has effects of enhancing immunity, protecting cardiovascular and cerebrovascular, resisting cancer and resisting depression. The extract used in this example was a powdered extract available from Shaanxi Freund Natural products, Inc.

(7) Ginseng root extract: the main component of total ginsenoside is extracted and refined from root, stem and leaf of Panax ginseng C.A. Meyer of Araliaceae family, and is rich in eighteen kinds of ginsenoside monomer, and has effects of enhancing activity of human surface cell, and inhibiting aging. The extract used in this example was a powdered extract available from Shaanxi Freund Natural products, Inc.

(8) Horse chestnut extract: it is rich in escin, flavonoid and tannin, has strong edema eliminating effect, and has therapeutic effect on varicosis, red swelling and inflammation of skin. The extract used in this example was a powdered extract available from Shaanxi Freund Natural products, Inc.

(9) And (3) purslane extract: the flavone and saponin have free radical scavenging and antioxidant effects, and have obvious antipruritic effect. The extract used in this example was a powdered extract available from Shaanxi Freund Natural products, Inc.

(10) Golden yellow chamomile extract: is rich in flavonoid active components, and has antioxidant, anti-angiogenesis, antiinflammatory and antiviral effects. The extract used in this example was a powdered extract available from Shaanxi Freund Natural products, Inc.

(11) Giant knotweed rhizome root extract: contains resveratrol and emodin, and has effects of resisting oxidation, clearing away heat and toxic materials, and relieving swelling and pain. The extract used in this example was a powdered extract available from Shaanxi Freund Natural products, Inc.

(12) Betaine: also called as amino acid humectant, the chemical name of which is trimethylglycine, is a zwitterionic moisture retention component, can rapidly improve the moisture retention of skin and hair and stimulate cell activity in the application of personal care products, and has the effects of keeping skin moist and smooth and preventing dryness and darkness. Available from onlida biotechnology limited, texas.

(13) Allantoin: the other names of 5-urethyllactam, ureidoacetic lactam, ureidohydantoin and uretidiodione are hydantoin derivatives. Is an amphoteric compound, can combine with multiple substances to form double salt, has antibacterial, antiseptic, analgesic, antioxidant, skin moisture keeping, moistening and softening effects, and can promote tissue growth, cell metabolism and softening cutin. Available from the clarien chemical group.

(14) P-hydroxyacetophenone is also known as 4-hydroxyacetophenone, 4-acetylphenol, p-acetylphenol, 4-hydroxyphenylmethyl ketone, commonly known as abietyl phenol, and is white needle-like crystal at normal temperature. Is naturally present in stems and leaves of Artemisia scoparia of Compositae, and roots of Artemisia capillaris, Heteropappus japonica of Asclepiadaceae, etc. The Chinese medicinal composition is clinically used for treating hepatitis and has certain curative effect on jaundice. The preservative is widely applied to the fields of medicines, cosmetics and industry, is a preservative promoter, has the effects of resisting oxidation, irritation and the like, and is mainly used as a preservative in cosmetics. Available from Guangzhou Biotechnology, Inc.

(15)1, 2-hexanediol, the name 2-methyl-2, 4-pentanediol, a colorless transparent liquid. Has mild sweet flavor, and is soluble in water, ethanol, diethyl ether, and low carbon aliphatic hydrocarbon. Can be used as solvent, perfume, and medical disinfectant. The hydrophilic groups can capture water molecules to play a moisturizing role, and simultaneously have certain capability of inhibiting bacteria and fungi. Available from Guangzhou Biotechnology, Inc.

(16) According to the components, the skin moisturizing cream contains various strong moisturizing and water locking components, contains the basic polyol humectant, is matched with betaine and sodium hyaluronate, and has the synergistic effect of the various moisturizing components, so that the skin is continuously moisturized and moisturized, the dry and water-deficient skin is effectively improved, and the effects of deeply moisturizing and moisturizing the skin are achieved. Meanwhile, a plurality of anti-inflammatory and antiallergic components such as dipotassium glycyrrhizinate, rhodiola root extract, horse chestnut extract, purslane extract, golden chamomile extract, giant knotweed root extract and the like are added, and the components are synergistic, so that the phenomena of skin pruritus, burning pain and allergic inflammation are effectively relieved, and the allergic rate of sensitive skin is obviously reduced. In addition, glutathione is added into the mask liquid, so that free radicals can be eliminated, heavy metals and other exotoxins can be chelated, skin pigmentation can be prevented, new melanin is prevented from being formed, oxidation of the melanin is reduced, and the whitening effect is achieved. Oligopeptide-1 and oligopeptide-3 are also added to stimulate the growth and repair of epidermal cells. The test results show that the facial mask liquid disclosed by the invention can replenish water, moisturize, repair skin, brighten skin color, reduce anaphylactic reaction, enable skin to be moist, bright white and elastic, and is safe and effective.

The compositions of examples 1-3 are as follows:

the preparation process of the above examples 1-3 and comparative examples is as follows:

(1) adding allantoin, betaine, carbomer, propylene glycol, butanediol, xanthan gum, sodium hyaluronate, dipotassium glycyrrhizinate, 1, 2-hexanediol, p-hydroxyacetophenone and deionized water into an emulsifying pot, stirring and heating to 80-85 ℃, homogenizing for 3 minutes, and keeping the temperature for 20-25 minutes to obtain a first mixture.

(2) Cooling to 45 deg.C, adding radix Rhodiolae extract, radix Ginseng extract, horse chestnut extract, herba Portulacae extract, flos Chrysanthemi extract, rhizoma Polygoni Cuspidati extract, glutathione, oligopeptide-1, and oligopeptide-3 into the first mixture, stirring for 2-3 min, cooling to 40 deg.C, adding triethanolamine, and stirring for 10-15 min to obtain facial mask liquid.

Experimental effect evaluation of examples 1 to 3:

after the facial mask liquid is filled in the invisible facial tissue, the efficacy verification is carried out, the crowd with three kinds of skin, namely, dark skin, dry skin, water shortage and sensitivity is selected, 80 people are selected for each kind of skin and divided into four groups, each group comprises 20 people,

wherein: panel 1 used the mask of example 1; panel 2 used the mask of example 2;

panel 3 used the mask of example 3; panel 4 used the mask of the comparative example (base formula);

the four groups, used 2-3 times a week for 1 month continuously, were recorded with user feedback, as specified in the following table:

description of the drawings: as can be seen from the above table:

for dark skin, "significantly improving" means that the skin becomes significantly white and bright, shiny; "relief" of skin condition means a decrease in skin darkness, slightly whitening; "no improvement" is manifested by dark skin with no obvious change.

For dry and water-deficient skin, the skin is obviously improved, which is characterized in that the skin is moist and elastic, does not have the phenomenon of dry desquamation and has no tight feeling; "alleviate" is no dry desquamation but no obvious moist feeling; "no improvement" is manifested by the skin still being dry and tight.

For sensitive skin, the obvious improvement is that the red swelling and allergy phenomena basically disappear, and the skin is not easily reddened or itchy any more; "relief" is manifested by a decrease in redness, swelling, hypersensitivity, slight redness or itching; "no improvement" is manifested by no reduction in redness, swelling, allergy, and tendency to redness or itching.

The trial results in the table show that the mask liquid can effectively repair the skin, improve the dry and water-deficient condition of the skin, brighten the skin color, improve the dark skin and make the skin moist, bright, white and elastic; meanwhile, the skin allergy symptoms such as red swelling, inflammation and itching can be effectively relieved, and sensitive skin can be improved.

The various components used in the present invention are all materials known in the art, and can be obtained commercially or prepared by known methods

The above description is only for the purpose of illustrating the preferred embodiments of the present invention, and all equivalent changes and modifications made based on the features and principles described in the claims of the present invention are included in the scope of the present invention.

Claims

1. A facial mask liquid is characterized in that: the facial mask liquid comprises the following components in percentage by weight:

0.1-0.5% of allantoin, 0.5-5% of betaine, 0.1-0.2% of carbomer, 2-8% of propylene glycol, 2-8% of butanediol, 0.1-0.2% of triethanolamine, 0.1-0.2% of xanthan gum, 0.1-0.4% of dipotassium glycyrrhizinate, 0.05-0.3% of sodium hyaluronate, 0.01-0.5% of glutathione, 0-0.0005% of oligopeptide-10.00005, 0-0.0004% of oligopeptide-30.00004, 0.4-1.0% of 1, 2-hexanediol, 0.4-0.6% of p-hydroxyacetophenone, 0.1-1% of rhodiola root extract, 0.1-1% of ginseng root extract, 0.1-1% of horse chestnut extract, 0.1-1% of purslane extract, 0.1-1% of golden chamomile extract, 0.1-1% of polygonum cuspidatum root extract and 10-90% of deionized water.

2. A preparation method of facial mask liquid is characterized by comprising the following steps: the method comprises the following steps: