CN109276523A

CN109276523A - A kind of peppermint facial mask liquid and preparation method thereof

Info

Publication number: CN109276523A
Application number: CN201811452593.XA
Authority: CN
Inventors: 兰海宁
Original assignee: Individual
Current assignee: Individual
Priority date: 2018-11-30
Filing date: 2018-11-30
Publication date: 2019-01-29

Abstract

The present invention relates to cosmetic technical fields, more particularly to a kind of peppermint facial mask liquid and preparation method thereof, the proportion of its percentage of peppermint facial mask liquid by weight is as follows: propylene glycol 6-10%, hamamelis extract 0.1-1%, aloe barbadensis Miller leaf extract 0.1-1%, purslane extract 0.1-1%, golden yellow camomile extract 0.1-1%, peppermint leaf extract 0.1-1%, glycine betaine 0.5-5%, dipotassium glycyrrhizinate 0.1-0.4%, Sodium Hyaluronate 0.05-0.3%, allantoin 0.1-0.5%, carbomer 0.03-0.3%, xanthan gum 0.1-0.2%, hydroxyethyl cellulose 0.1-0.2%, -1 0.00005-0.0005% of oligopeptides, -3 0.00004- of oligopeptides 0.0004%, triethanolamine 0.03-0.3%, menthol 0.01-0.02%, Vitamin C Ethyl Ether 0.5-2%, 1,2- hexylene glycol 0.4-1.0%, parahydroxyacet-ophenone 0.4-0.6%, Cremophor RH40 0.1-0.5%, peppermint leaf oil 0.01-0.05% are gone from water 10-90%；It can quickly replenishing water and preserving moisture, skin whitening, oil-control, anti-acne, bright color, while the susceptibility for the skin that can also effectively releive.

Description

A kind of peppermint facial mask liquid and preparation method thereof

[technical field]

The present invention relates to cosmetic technical fields, and in particular to a kind of peppermint facial mask liquid and preparation method thereof.

[background technique]

As the improvement of people's living standards, requirement of the people for beauty also increasingly improves.Facial mask becomes people's beauty Maintenance is preferred.Facial mask is a classification in skin care item, and its most basic and most important purpose is to make up makeup removing and wash one's face still Right insufficient cleaning cooperates other essential ingredients to realize other maintenance functions, such as replenishing water and preserving moisture, beauty on this basis White, anti-aging, Sage Extract etc..

Instantly facial mask has become the category that beauty market increasingly occupies the initiative position, and facial mask application method is simple, both saves Nursing time, and can easily enjoy the nursing of beauty parlor's formula.The principle of facial mask is that the of short duration time of face is covered on using it, It is temporarily isolating extraneous air and pollution by Face film towel, expands the pore of skin, promotes the secretion and metabolism of sweat gland, The oxygen content of skin is risen, and skin is promoted to exclude the product of the metabolism of epidermal cell and the grease type object of accumulation Matter is rapidly soaked into highly condensed nutritious ingredient in facial mask liquid in the cuticula of skin epidermis, to realize quickly having for skin The effects of effect is nursed, and replenishing water and preserving moisture, whitening and anti-aging, Sage Extract, Eradicates acne are played, thus have by numerous people seeking beauties' Like.

Currently, facial mask in the market is many kinds of, effect is also each different.Purification is played in peppermint addition in facial mask Skin, anti-acne, oil-control, anti-inflammatory and calm effect of releiving, but there are the following problems in actual use:

It is poor for there is assimilation effects after some peppermint facial mask liquid uses in the market, irritation is big, moistening effect is poor etc. Problem.Therefore develop it is a have oil-control, anti-acne, moisturizing, whitening, irritation small, pack preparation safely and effectively very must It wants.

[summary of the invention]

In view of the defects and deficiencies of the prior art, the present invention intends to provide a kind of peppermint facial mask liquid and its preparation sides Method.

A kind of peppermint facial mask liquid of the present invention and preparation method thereof, the percentage of peppermint facial mask liquid by weight is matched Than as follows:

Propylene glycol 6-10%, hamamelis extract 0.1-1%, aloe barbadensis Miller leaf extract 0.1-1%, purslane Extract 0.1-1%, golden yellow camomile extract 0.1-1%, peppermint leaf extract 0.1-1%, glycine betaine 0.5-5%, Radix Glycyrrhizae Sour dipotassium 0.1-0.4%, Sodium Hyaluronate 0.05-0.3%, allantoin 0.1-0.5%, carbomer 0.03-0.3%, xanthan gum 0.1-0.2%, hydroxyethyl cellulose 0.1-0.2%, -1 0.00005-0.0005% of oligopeptides, -3 0.00004- of oligopeptides 0.0004%, triethanolamine 0.03-0.3%, menthol 0.01-0.02%, Vitamin C Ethyl Ether 0.5-2%, 1,2- hexylene glycol 0.4-1.0%, parahydroxyacet-ophenone 0.4-0.6%, Cremophor RH40 0.1-0.5%, peppermint leaf oil 0.01- 0.05%, it goes from water 10-90%.

The preparation method of its peppermint facial mask liquid, using following steps:

Step 1:

(1) menthol, peppermint leaf oil, Cremophor RH40 are stirred in formula composition ratio Hybrid Heating to molten Solution, obtains the first mixture；

(2) by 1,2- hexylene glycol, parahydroxyacet-ophenone, in formula composition ratio Hybrid Heating, stirring obtains the to dissolving Two mixtures；

Step 2: by propylene glycol, glycine betaine, dipotassium glycyrrhizinate, Sodium Hyaluronate, allantoin, carbomer, xanthan gum, hydroxyl Ethyl cellulose is gone from water, and emulsion pot is added in formula composition ratio, is heated with stirring to 80-85 DEG C, homogeneous 3 minutes, is kept the temperature It 20-25 minutes, stirs evenly, cools the temperature to 60 DEG C, the second mixture in step 1 is added, form third mixture；

Step 3: being cooled to 40 degree for the third mixture in step 2, and hamamelis is added in formula composition ratio Extract, aloe barbadensis Miller leaf extract, purslane extract, golden yellow camomile extract, peppermint leaf extract, the first mixing Object, oligopeptides -1, oligopeptides -3, Vitamin C Ethyl Ether, triethanolamine continue stirring 10-15 minutes to get facial mask liquid.

Further, the weight ratio of 1, the 2- hexylene glycol and parahydroxyacet-ophenone in step 1 is 0.5:0.5 or 0.8: 0.4。

The invention has the following beneficial effects: a kind of peppermint facial mask liquid of the present invention and preparation method thereof, it can quick moisturizing Moisturizing, skin whitening, oil-control, anti-acne, bright color, while the susceptibility for the skin that can also effectively releive are particularly suitable for sensitivity The advantages that skin uses.

[specific embodiment]

With specific embodiment, the present invention will be described in detail below, and illustrative examples therein and explanation are only used to explain The present invention, but it is not as a limitation of the invention.

A kind of peppermint facial mask liquid described in present embodiment and preparation method thereof, peppermint facial mask liquid by weight hundred Divide the proportion of ratio as follows:

Propylene glycol 6-10%, hamamelis extract 0.1-1%, aloe barbadensis Miller leaf extract 0.1-1%, purslane Extract 0.1-1%, golden yellow camomile extract 0.1-1%, peppermint leaf extract 0.1-1%, glycine betaine 0.5-5%, Radix Glycyrrhizae Sour dipotassium 0.1-0.4%, Sodium Hyaluronate 0.05-0.3%, allantoin 0.1-0.5%, carbomer 0.03-0.3%, xanthan gum 0.1-0.2%, hydroxyethyl cellulose 0.1-0.2%, -1 0.00005-0.0005% of oligopeptides, -3 0.00004- of oligopeptides 0.0004%, triethanolamine 0.03-0.3%, menthol 0.01-0.02%, Vitamin C Ethyl Ether 0.5-2%, 1,2- hexylene glycol 0.4-1.0%, parahydroxyacet-ophenone 0.4-0.6%, Cremophor RH40 0.1-0.5%, peppermint leaf oil 0.01- 0.05%, it goes from water 10-90%；

Step 1:

" 1,2- hexylene glycol, parahydroxyacet-ophenone " in the present invention is known in the art cosmetic material, this field skill Art personnel, which can understand, determines its composition.When the concentration of 1,2- hexylene glycol is 1.0%, there is certain sterilizing ability；When to hydroxyl When the concentration of acetophenone is 0.5%, there is killing ability to fungi, the two is used in combination, when 1,2- hexylene glycol is to para hydroxybenzene second When ketone dosage is (weight ratio) 0.5:0.5 or 0.8:0.4, it can be tested by the preservation challenge in lotion, cream and gel. Preferably, the weight ratio of 1,2- hexylene glycol and parahydroxyacet-ophenone is 0.5:0.5.

In facial mask liquid of the invention, epithelical cell growth factor (EGF) content is in 500-5000IU/mg, basic fibroblast Porcine HGF (bFGF) content is in 200-2000IU/mg, using the reasonable complementary synergistic component of a variety of proportions, effectively The effect of improving the facial mask liquid of invention performance.The effect of its each composition, is as follows:

Wherein:

(1) menthol: by being extracted in the leaf and stem of peppermint, white crystal is used as excitants in medicine, acts on skin Skin or mucous membrane have refrigerant antipruritic, sterilization and antisepsis.It is purchased from the permanent really natural perfume material oil Co., Ltd in Jiangxi.

(2) oligopeptides -1: being a kind of intracorporal active material of people, by 53 ammonia also referred to as epithelical cell growth factor (EGF) The active peptides of base composition reach repairing hyperplasia skin by the tyrosine phosphorylation of stimulation epidermal growth factor receptor Cells of superficial layer possesses good curative effect to injured, impaired epidermis skin.Its biggest characteristic is that the proliferation point of cell can be promoted Change, to replace aging and dead cell with newborn cell, so that epidermal cell become full, restored young state, play Crease-resistant effect.EGF can also stop blooding, and the effect of have and accelerate skin and mucous membrane wound healing, anti-inflammatory analgesic, prevent ulcer. EGF stability is good, initially mainly uses medical domain, is primarily to facilitate the reparation and regeneration of impaired epidermis, such as treatment burn, Scald etc..The vigor for the epithelical cell growth factor (EGF) that the present embodiment uses is greater than 100,000 IU/mg, is purchased from Hangzhou knob Imperial Biotechnology Co., Ltd.

(3) oligopeptides -3: also referred to as basic fibroblast growth factor (bFGF), strong rush is proliferated in 3T3 cell And Mitosis, it is widely used in cell repair.Mesoderm is acted on, deep layer reparation is mainly played and improves skin quality Function.Also known as corium growth factor, is primarily present in the keratinocyte of epidermal basal, is important rush cell mitogenic Splitting factor and angiogenesis factor have a plurality of types of cells from mesoderm and neuroderm extensive raw Object activity, can promote cell Proliferation, growth, differentiation, promote angiogenesis, improve the microenvironment of cell life, promote impaired Nerve regneration and blood vessel, muscle, skin etc. are repaired, and are neurotrophic and regeneration factor, there is the title of cell activating agent.This The vigor for the epithelical cell growth factor (bFGF) that embodiment uses is greater than 50,000 IU/mg, is purchased from Hangzhou knob dragon biotechnology Co., Ltd.

(4) dipotassium glycyrrhizinate: corticosteroid compound (inhibiting metabolic enzyme) can be activated, enhances corticosteroid compound indirectly Effect, there are the multiple efficacies such as antibacterial, anti-inflammatory, removing toxic substances, antiallergic, deodorization.It is purchased from Gansu Fan Zhi pharmaceutical Co. Ltd.

(5) Sodium Hyaluronate: Sodium Hyaluronate itself is one of composition of human skin, is distribution is most wide in human body one The acid glutinous sugar of kind, is present in the matrix of connective tissue, has good moisture-keeping function.It is purchased from Shandong Fu Ruida medicine collection Co., Ltd of group.

(6) peppermint leaf oil: being the fresh cauline leaf of Lamiaceae plant peppermint or family peppermint through distillable aromatic oil.It is purchased from In the permanent really natural perfume material oil Co., Ltd in Jiangxi.

(7) peppermint leaf extract: main ingredient is Flavonoid substances, have analgesic, antiphlogistic antibacterial, convergence, vasoconstriction, Refrigerant, removing blackhead.It is water-soluble powder shape extract that the present embodiment, which uses, is purchased from the gloomy not natural product in Shaanxi Co., Ltd.

(8) it is a variety of as Ellagitannin and Hamamlitannin can be adjusted hamamelis extract: to include tannin matter Save sebum secretion, Hydrolyzed Protein and Milk Protein.Promote lymph blood circulation, specially overcomes morning eye bladder and black eye.With town Cracking, sunburn, acne are had improvement by effect that is quiet, pacifying.The power of regeneration at skin night can effectively be helped.Remove eye Bag loosens and mitigates and has very excellent effect for the skin of oily skin or allergy.It releives, restrains, antibacterial Effect, because there is the significant curative effect of convergence oil-control, sterilization, the skin more serious for children in adolescence or fuel-displaced situation, is not Two selections.It is Powder Extract that the present embodiment, which uses, is purchased from Shaanxi Sen Fu natural product Co., Ltd.

(9) purslane extract: the flavones and saponin contained, which has, removes free radical and antioxidation, has apparent antipruritic Function.It is water-soluble powder shape extract that the present embodiment, which uses, is purchased from Shaanxi Sen Fu natural product Co., Ltd.

(10) golden yellow camomile extract: be rich in flavones active component, the ingredient have anti-oxidant, antiangiogenic, Anti-inflammatory and antiviral effect.It is water-soluble powder shape extract that the present embodiment, which uses, is purchased from the gloomy not natural system in Shaanxi Product Co., Ltd.

(11) aloe barbadensis Miller leaf extract: being rich in a variety of amino acid and vitamin, can supplement the nutrients for skin, therein Mucus substance can prevent skin aging, make skin high resilience.With good lubrication and moisture-keeping function, Anhydroalkannin and rush are gone back Into the effect of damaging skin healing.It is water-soluble powder shape extract that the present embodiment, which uses, is purchased from gloomy not natural in Shaanxi Products Co., Ltd.

(12) glycine betaine: also known as amino acid humectant, the entitled trimethylglycine of chemistry, is a kind of amphoteric ion type moisturizing Ingredient can improve rapidly the moisture holding capacity of skin and hair, activated cell vigor has in personal care product uses Keep skin effect that is moist, smooth, preventing drying and obfuscation.It is purchased from Dezhou Onlystar Biotechnology Co., Ltd..

(13) allantoin: alias Allantoin, Allantoin, Allantion, Allantoin are one Kind hydantoin derivatives.It is a kind of amphoteric compound, double salt can be formed in conjunction with many kinds of substance, there is sterilization and anticorrosion, analgesic, resist Oxidation can make skin keep moisture content, moisten and soft, can promote tissue growth, cell metabolism, cutin-softening layer egg It is white.It is purchased from Clariant Chemical Group.

(14) parahydroxyacet-ophenone also known as 4-hydroxyacetophenone, 4- acetyl phenol, to acetyl phenol, 4- hydroxyphenyl first Base ketone is commonly called as piceol, is white, needle-shaped crystals under room temperature.It is naturally present in stem, the leaf of compositae plant artemisia scoparia, Artemisia capillaris, trailing plants In the roots of plants such as Japonica section plant kerr tylophora root.It is clinically used for treatment hepatitis, has certain curative effect to removing jaundice.It is widely used in curing Medicine, cosmetics, industrial circle are a anti-corrosion promotors, have both anti-oxidant, anti-irritant and other effects, main inside cosmetics It is to be used as no added preservative.It is purchased from one ball Bioisystech Co., Ltd of Guangzhou.

(15) 1,2- hexylene glycol Chinese name 2- methyl -2,4- pentanediol, colourless transparent liquid.There is mild sweet fragrance, it is molten Yu Shui, ethyl alcohol, ether, low-carbon aliphatic hydrocarbon.As solvent, fragrance, medical disinfectant.The hydrophilic radical having captures hydrone hair Moisture-keeping function is waved, while also there is the ability of certain inhibition bacterium and fungi.It is purchased from limited in one ball biotechnology of Guangzhou Company.

(16) Vitamin C Ethyl Ether is a kind of more stable vitamin C derivatives, with hydrophilic and oleophylic property, is held Easily entered skin corium by cuticula, it, which enters after body, is very easy to intracorporal biological enzyme and decomposes to play ascorbic Biological effectiveness.Skin Cell activity is repaired in the synthesis that collagen is directly participated in after into skin corium, increases collagen, To make skin become full high resilience, keep skin moist.It can inhibit tyrosinase activity, inhibit the shape of melanin At reduction melanin is colourless, efficient skin whitening.With anti-inflammatory and antioxidant effect.It is purchased from the gloomy not natural system in Shaanxi Product Co., Ltd.

(17) by the above ingredient as it can be seen that containing in the present invention there are many a variety of potent moisturizings and water lock ingredient, except containing basic Polyol humectant outside, also collocation glycine betaine, Sodium Hyaluronate, a variety of moisturizing ingredients synergistic effect continue moisturizing and moisten Skin is effectively improved dry water deficient skin, has the function that deeply preserving moisture moisturizing.A variety of anti-inflammatory anti-mistakes of addition simultaneously Quick ingredient, such as dipotassium glycyrrhizinate, hamamelis extract, aloe barbadensis Miller leaf extract, purslane extract, golden yellow ocean is sweet Chrysanthemum extract, peppermint leaf extract etc., Multiple components are synergistic, and skin itching, cusalgia and inflammation allergic phenomena is effectively relieved, It is substantially reduced the allergy rate of sensitive skin.In addition, being added to oligopeptides -1, oligopeptides -3 in facial mask liquid of the invention, stimulation epidermis is thin Intracellular growth and reparation；It also added Vitamin C Ethyl Ether, play the effect for keeping fragile muscle and skin white.Test effect shows of the invention Facial mask liquid can replenishing water and preserving moisture, repair skin, bright color, Sage Extract, anti-acne, reduce allergic reaction, make skin Shui Run, bright White, flexible, product safety is effective.

The present invention is for example, the composition that embodiment 1- implements 3 is as follows:

The preparation process of above embodiments 1- embodiment 3 and comparative example is as follows:

Step 1: by menthol, peppermint leaf oil, Cremophor RH40, Hybrid Heating, stirring obtains the to dissolving One mixture, it is spare.By 1,2- hexylene glycol, parahydroxyacet-ophenone Hybrid Heating, stirring obtains the second mixture to dissolving, standby With.

Step 2: by propylene glycol, glycine betaine, dipotassium glycyrrhizinate, Sodium Hyaluronate, allantoin, carbomer, xanthan gum, hydroxyl Ethyl cellulose is gone from water, and emulsion pot is added in formula composition ratio, is heated with stirring to 80-85 DEG C, homogeneous 3 minutes, is kept the temperature It 20-25 minutes, stirs evenly, cools the temperature to 60 DEG C, the second mixture is added.

Step 3: being cooled to 40 degree, hamamelis extract is added in formula composition ratio, Aloe Barbadensis Miller extracts Object, purslane extract, golden yellow camomile extract, peppermint leaf extract, the first mixture, oligopeptides -1, oligopeptides -3, vitamin C ethylether, triethanolamine continue stirring 10-15 minutes to get facial mask liquid.

Embodiment 1- implements 3 experiment effect evaluation:

Below by facial mask liquid of the invention after invisible film towel is filling, efficacy validation is carried out, chooses obscure, oiliness, sensitivity The crowd of three kinds of skin of property, three kinds of skin choose 80 people altogether, are divided into four groups, every group of 20 people,

Wherein: group 1 uses the facial mask of embodiment 1；Group 2 uses the facial mask of embodiment 2；

Group 3 uses the facial mask of embodiment 3；Group 4 uses the facial mask (basic components) of comparative example；

Aforementioned four group uses 2-3 times weekly, is used continuously 1 month, records user's feedback, specific following table:

Illustrate: as can be seen from the above table:

For obscure skin, " being obviously improved ", which refers to skin obviously, becomes white-skinned bright, glossy；Skin obtains " slow Solution " refers to that the obscure degree of skin reduces, and slightly bleaches；" no to improve " shows as obscure skin without significant change.

For oily skin, " being obviously improved " shows as hair pore shrinkage, and skin is fine and smooth, and small pox obviously tails off or disappears substantially It loses；" alleviation " shows as that pore is coarse, and glossy on the face, small pox is reduced；It is coarse that " no improve " shows as pore, glossy on the face, Small pox is obvious.

For sensibility skin, " being obviously improved " shows as red and swollen allergic phenomena and disappears substantially, no longer easily general red or hair Itch；" alleviation " shows as the decline of red and swollen allergic phenomena, slight general red or itch；" no improve " show as red and swollen allergic phenomena without Mitigate, it is easily general red or itch.

From the result on trial of upper table can be seen that facial mask liquid of the invention can effective maintenance skin, improve skin pore The case where coarse and small pox flesh, bright color improves obscure skin, makes skin water profit, brilliant white, flexible；Can also have simultaneously Effect such as alleviates the redness of skin, inflammation, itches at the allergic symptoms, improves sensitive skin.

Various components used in the present invention are the existing material in this field, can by commercial channel buy obtain or It is made by existing method.

The above description is only a preferred embodiment of the present invention, therefore all according to feature described in present patent application range and original Done equivalent change or modification is managed, is included in the scope of the patent application of the present invention.

Claims

1. a kind of peppermint facial mask liquid, it is characterised in that: the proportion of its percentage of peppermint facial mask liquid by weight is as follows:

Propylene glycol 6-10%, hamamelis extract 0.1-1%, aloe barbadensis Miller leaf extract 0.1-1%, purslane extract 0.1-1%, golden yellow camomile extract 0.1-1%, peppermint leaf extract 0.1-1%, glycine betaine 0.5-5%, dipotassium glycyrrhizinate 0.1- 0.4%, Sodium Hyaluronate 0.05-0.3%, allantoin 0.1-0.5%, carbomer 0.03-0.3%, xanthan gum 0.1-0.2%, ethoxy Cellulose 0.1-0.2%, -1 0.00005-0.0005% of oligopeptides, oligopeptides -3 0.00004-0.0004%, triethanolamine 0.03- 0.3%, menthol 0.01-0.02%, Vitamin C Ethyl Ether 0.5-2%, 1,2- hexylene glycol 0.4-1.0%, parahydroxyacet-ophenone 0.4- 0.6%, Cremophor RH40 0.1-0.5%, peppermint leaf oil 0.01-0.05%, go from water 10-90%.

2. a kind of preparation method of peppermint facial mask liquid, it is characterised in that: the preparation method of its peppermint facial mask liquid, using following step It is rapid:

Step 1: (1) by menthol, peppermint leaf oil, Cremophor RH40, in formula composition ratio Hybrid Heating, stirring To dissolution, the first mixture is obtained；

(2) by 1,2- hexylene glycol, parahydroxyacet-ophenone, in formula composition ratio Hybrid Heating, it is mixed to obtain second to dissolving for stirring Close object；

Step 2: by propylene glycol, glycine betaine, dipotassium glycyrrhizinate, Sodium Hyaluronate, allantoin, carbomer, xanthan gum, ethoxy Cellulose is gone from water, and emulsion pot is added in formula composition ratio, is heated with stirring to 80-85 DEG C, homogeneous 3 minutes, is kept the temperature 20-25 Minute, it stirs evenly, cools the temperature to 60 DEG C, the second mixture in step 1 is added, form third mixture；

Step 3: being cooled to 40 degree for the third mixture in step 2, and hamamelis is added in formula composition ratio and extracts Object, aloe barbadensis Miller leaf extract, purslane extract, golden yellow camomile extract, peppermint leaf extract, the first mixture, Oligopeptides -1, oligopeptides -3, Vitamin C Ethyl Ether, triethanolamine continue stirring 10-15 minutes to get facial mask liquid.