CN109646359B

CN109646359B - Rose-agaric mud membrane paste with effects of cleaning, purifying, maintaining beauty and keeping young and preparation method thereof

Info

Publication number: CN109646359B
Application number: CN201910106956.2A
Authority: CN
Inventors: 王斌; 王萍; 王紫文熙; 李尚杰; 李丰源; 陈兴庆蓉
Original assignee: Gansu Jiumei Biotechnology Co ltd
Current assignee: Gansu Jiumei Pharmaceutical Biotechnology Co ltd
Priority date: 2019-02-02
Filing date: 2019-02-02
Publication date: 2021-12-28
Anticipated expiration: 2039-02-02
Also published as: CN109646359A

Abstract

The invention discloses a rose-black fungus mud membrane paste with the effects of cleaning, purifying, maintaining beauty and keeping young and a preparation method thereof, and the rose-black fungus mud membrane paste is composed of the following raw materials in parts by weight: 10-30 parts of rose, 10-30 parts of black fungus, 10-30 parts of fresh lily, 10-20 parts of paper mulberry fruit, 10-20 parts of mountain peach kernel, 5-10 parts of bleaching earth, 1-5 parts of composite polypeptide, 1-3 parts of biological complex enzyme fungicide, 0.5-2 parts of preservative and a proper amount of water. The invention has good synergistic effect, natural active ingredients are rich after biodegradation, and the molecules are small and easy to be absorbed by skin; on the basis of moisturizing, tendering skin, improving susceptible muscle and preventing pigmentation, the effects of cleaning skin, purifying pores, regulating water and oil balance of skin, removing residual powder after makeup and the like are also added. The method of the invention adopts biological enzymolysis and glycolysis to break macromolecular substances into micromolecular components, can improve the bioactivity of the effective components, promote the effective absorption of skin, shorten the external application time and improve the beautifying effect.

Description

Rose-agaric mud membrane paste with effects of cleaning, purifying, maintaining beauty and keeping young and preparation method thereof

Technical Field

The invention belongs to the technical field of beauty cosmetics, and particularly relates to a rose and agaric mud membrane paste with the effects of cleaning, purifying, maintaining beauty and keeping young and a preparation method thereof.

Background

Among the cosmetic methods, the use of a paste for skin care is the earliest one, which dates back to the ancient greek and ancient roman times, where people bathe in a slurry and apply the slurry to their faces, diminish inflammation, sterilize, degrease through the abundant minerals in the slurry, and also serve to care and beautify the skin. These ancient methods have actually influenced modern beauty and have been developed and used to date.

Nowadays, the effect of the simple and unsophisticated mud paste is continued, and a plurality of facial masks prepared into the mud paste are provided. The mud cream-shaped facial mask has the unique advantages of more skin-friendly and veneering, wide coverage, quick absorption of nutrient components, softening of hardened sebum blocking pores, good skin cleaning and purifying effects and the like, so the mud cream-shaped facial mask has an important position in skin care and maintenance and even is applied to dermatology in hospitals and medical beauty clinic.

The commercially available rose mask has various types, including wet cloth, gel and powder, and also has the effect of directly preparing rose powder or rose into paste by adding solvents such as honey, essential oil and egg white. The invention discloses a rose composition, a mask mud and a preparation method thereof, wherein the rose composition is prepared by mixing and stirring rose powder, aloe juice, astragalus extract, commercially available rose essential oil, highland barley powder, pearl powder, purified water and some chemical additives, and the mud cream is not treated by an innovative method.

Disclosure of Invention

The invention aims to solve the technical problems in the prior art and provide the auricularia polytricha mud membrane paste which has the advantages of high safety, obvious effect, good moisturizing effect, no stimulation and allergy, easy cleaning and no skin abrasion and has the effects of cleaning, purifying, maintaining beauty and keeping young.

The invention also aims to provide a preparation method of the rose black fungus mud membrane paste with the effects of cleaning, purifying, maintaining beauty and keeping young.

In order to achieve the purpose, the invention adopts the following technical scheme: the rose black fungus mud membrane paste with the effects of cleaning, purifying, maintaining beauty and keeping young comprises the following raw materials in parts by weight: 10-30 parts of rose, 10-30 parts of black fungus, 10-30 parts of fresh lily, 10-20 parts of paper mulberry fruit, 10-20 parts of mountain peach kernel, 5-10 parts of bleaching earth, 1-5 parts of composite polypeptide, 1-3 parts of biological complex enzyme fungicide, 0.5-2 parts of preservative and a proper amount of water.

Further, the rose black fungus mud membrane paste with the effects of cleaning, purifying, maintaining beauty and keeping young consists of the following raw materials in parts by weight: 20 parts of rose, 20 parts of black fungus, 20 parts of fresh lily, 15 parts of paper mulberry fruit, 15 parts of semen persicae, 8 parts of bleaching earth, 3 parts of composite polypeptide, 2 parts of biological complex enzyme fungicide, 1 part of preservative and a proper amount of water.

Further, the composite polypeptide is 2-3 of collagen polypeptide, soybean peptide, corn polypeptide and glutathione.

Further, the biological complex enzyme microbial inoculum consists of the following components in percentage by weight: 10-25% of starch hydrolase, 10-25% of cellulase, 10-25% of compound pectinase, 10-15% of agaric protease, 3-15% of bifidobacterium, 3-15% of lactic acid bacteria, 3-15% of yeast and 5-15% of wheat starter.

Further, the preservative is dipotassium glycyrrhizinate or sodium benzoate.

Further, the water is rice washing water.

Further, the rose is a bitter rose produced in bitter water in Gansu province.

A preparation method of a rose black fungus mud membrane paste with effects of cleaning, purifying, maintaining beauty and keeping young comprises the following steps:

A. rose, black fungus, fresh lily, paper mulberry fruit, mountain peach kernel, bleaching earth, composite polypeptide, biological composite enzyme fungicide and preservative are respectively weighed according to the proportion;

B. mixing rose, black fungus and paper mulberry, and performing impact, collision, shearing, grinding, dispersion and crushing on the mixed material by using an airflow crusher to obtain 2000-mesh super micro powder I with the particle size of 1500-;

C. impacting, colliding, shearing, grinding, dispersing and crushing the bleaching earth to 2000-mesh super micro powder II with the granularity of 1500-;

D. preparing fresh lily and semen persicae into lily and semen persicae pulp by using a juicer, adding the super micro powder I into the lily and semen persicae pulp, adding rice washing water with the weight 3.5-9.5 times of the super micro powder I, and thoroughly and uniformly stirring to obtain a mixed solution;

E. adjusting the pH value of the mixed solution to 4.0-6.0, placing the mixed solution in a fermentation tank, adding a biological complex enzyme preparation accounting for 10-20% of the total weight of the biological complex enzyme preparation, performing enzymatic glycolysis for 4-8 hours at the temperature of 30-65 ℃, and then heating to boil for 5-25 minutes;

F. when the temperature of the solution in the step E is reduced to 20-30 ℃, adding the super micro powder II and keeping the constant temperature state, and then adding the rest biological complex enzyme microbial inoculum for secondary enzymatic glycolysis for 45-72 hours;

G. inactivating the zymolyte at 80-120 deg.C for 30-100 min, adding the composite polypeptide, stirring, and adding antiseptic when the temperature is reduced to below 50 deg.C to obtain the final product.

Compared with the prior art, the invention has the following beneficial effects:

1. the raw materials of the invention are as follows: the rose contains more than 300 chemical components, is rich in amino acids, proteins, polysaccharides, vitamins, pigments, flavones, fats, volatile oil and other components essential to human bodies, and the water extract of the rose has the strongest oxidation resistance in more than 30 medicinal plants and has the effects of resisting inflammation, relieving pain, resisting bacteria, resisting viruses, resisting fungi, resisting sensitivity and the like. The rose of the invention is the bitter rose which is produced in the Yondden bitter town of Gansu, has unique fragrance, and purplish red color, and has the oil content as high as 0.039 percent. Research shows that 58 kinds of fragrance components are contained in the bitter rose, the main fragrance components comprise citronellol, geraniol, phenethyl alcohol, nerol and esters thereof, and the volatile components have good effects of regulating qi-flowing for relieving pain, promoting blood circulation for removing blood stasis, improving peripheral microcirculation and the like; the petals contain higher polyphenol and flavonoid substances, have obvious antioxidant activity and free radical scavenging capacity, increase the activity of skin cells and assist skin whitening; the polysaccharide has the functions of efficiently resisting aging and improving immunity resistance sensitivity.

Black fungus, as a medicine, is recorded in Shen nong Ben Cao Jing of the Han Dynasty, which means that it can tonify qi, avoid hunger, lighten body and strengthen mind. The Chinese medicine considers that the medicine has moderate nature and sweet taste and enters the stomach and large intestine meridians. Has effects in cooling blood, stopping bleeding, regulating blood, nourishing yin, moistening dryness, and caring skin. Modern medical research finds that black fungus is rich in nutrition, contains a large amount of protein, saccharides, trace elements, a small amount of fat, crude fiber, vitamin B1, vitamin B2, vitamin C, carotene and the like, is a substance basis for beautifying and nourishing the face, and can effectively resist oxidation and aging, nourish and moisten skin, keep the skin smooth and soft, reduce wrinkles and eliminate spots when being externally applied to the skin.

Lily is sweet, cool, clear and moist, enters heart and lung meridians, and is a medicine and food dual-purpose product and also a good beauty and health product. The skin-nourishing cream has both moistening and moistening functions, and has the effects of nourishing yin and moistening the skin so as to remove skin dryness and make the skin tender; clearing away heart-fire, removing heat, tranquilizing mind, replenishing qi and blood, and lubricating and brightening skin; it also has effects in clearing away heat and toxic materials, and removing skin toxin. Modern researches prove that the lily contains rich effective components such as alkaloid, starch, protein, fat, amino acid, sugar, calcium, phosphorus, iron and the like, can effectively improve anemia, avoids the skin problems such as pale skin and lusterless lip color caused by the anemia, has the effect of ruddy skin, can remove harmful substances in the body and delay senility; the lily is also rich in B vitamins, and is beneficial to nourishing skin, reducing wrinkles, eliminating spots and building the skin; in addition, Bulbus Lilii extract also has effects of regulating skin immunity and resisting skin allergy.

Papermulberry fruit is a common traditional Chinese medicine for resisting aging, preserving health and beautifying, and is described in the general examination of drug properties: "tonify skin, help waist and knee, benefit strength, tonify consumptive disease, beautify the color and lighten the body, strengthen the muscles and bones and improve eyesight ·. The herbal Zhenzhen: modern researches show that the papermulberry fruit contains rich amino acids, fatty acids, alkaloids, mineral substances, a plurality of trace elements, vitamin B, grease, polysaccharide and other chemical components, has the effects of obviously resisting oxidation, enhancing immunity, reducing blood fat, resisting tumors, protecting liver function and the like, and the traditional medicine explains the action mechanism of the papermulberry fruit to mainly supplement water for organisms by nourishing yin, so that the skin is moisturized and moist, and the appearance is moisturized and glossy.

Shan Tao ren is bitter and sweet in flavor and neutral in nature. It also has effects in activating blood circulation, dispelling blood stasis, resolving food stagnation, moistening dryness, and relieving swelling, and can be used for treating traumatic injury. The beauty treatment is mainly used for supplementing nutrition, moistening and locking water, promoting blood circulation, improving skin microcirculation, resisting inflammation and allergy and the like; modern researches prove that the fatty oil contained in the semen persicae can soften the horny layer of the skin, moisten dryness, protect the skin, protect the nerve endings and blood vessels of the skin, inhibit bacteria and resist bacteria, eliminate pigmentation and black spots and have remarkable beautifying effect.

Bleaching clay is an off-white or light yellow powder which is refined by a special processing technology by adopting high-quality pure natural non-metallic mineral-attapulgite clay as a main raw material and assisting a scientific formula, has the capacity of adsorbing impurities or colored substances, is also called as activated clay, has stronger stability in application, is very convenient and safe to apply, does not change the original production technology, does not cause pollution to the environment, has wide and natural sources, and is economical and practical. The natural antioxidant, the excellent adsorbability, the purification capacity and other characteristics are mainly utilized in the aspect of beautifying, and the natural antioxidant is effectively combined with other components to achieve a certain adsorption and purification effect on dirt, oil dirt, cosmetic residues and the like in skin pores, so that the balance and the relief of other effective components and the better performance of the beautifying and face nourishing effects are promoted. Modern clinical research proves that bleaching earth contains various trace elements, can adsorb and purify dirt, grease, aged and dead keratinocytes on the surface and in the deep layer of skin and cosmetics remained in pores, has the effects of sterilizing and astringing, and can balance the pH value of the skin; it also has good effects in preventing chloasma, folliculitis, acne, and allergy; it also has certain improving effect on skin with skin pruritus and allergic dermatitis.

The polypeptide is the main component of the skin, is rich in hydrophilic natural moisturizing factors, can strongly lock 30 times of moisture, accounts for more than 75% of the corium layer of the skin, forms a fine elastic net, locks the moisture, supports the skin, enables the skin to be moist, tender, smooth and full of elasticity, and is called as 'soft and golden skin' by experts. With the age, the collagen content of the human body can be gradually lost, so that the elastic net for supporting the skin is broken, the skin tissue is shrunk and collapsed, and the skin is dry, rough, loose, wrinkled, coarse, dull, mottled and other aging problems.

From the modern pharmacological research, the polysaccharide in the rose has strong moisturizing and water locking functions; the black fungus and the lily are rich in polysaccharide, have oxidation resistance and fatigue resistance, can effectively remove harmful substances, and enhance immunity; the papermulberry fruit contains a large amount of nutrient substances, can remove free radicals, enhance immunity, delay skin aging, enhance skin elasticity and has obvious effects of beautifying and resisting aging; the semen persicae is rich in nutrition, and contains polysaccharide, protein, vitamins and trace elements, which are all main components for maintaining beauty and keeping young. The method can make full use of the effective components such as polysaccharide, protein and the like in the rose-agaric mud film paste after enzymatic degradation to form a natural moisture-preserving and water-locking barrier, and can achieve the synergistic interaction and complementary action of the effective components through enzymatic degradation.

In the rose and agaric mud membrane paste, the rose is fragrant and pleasant, the fragrance of the rose is mild in nerves, fragrant in dampness resolving, refreshing skin and regulating qi, and sensitive in repair, and the formula is monarch; the lily and the black fungus have the effects of nourishing yin, moistening dryness, removing skin dryness, tendering skin, clearing heat, removing toxicity, expelling toxin, resisting allergy and purifying skin and are ministerial drugs; the papermulberry fruit and the mountain peach seed are used as adjuvant drugs for tonifying qi, nourishing yin, moistening dryness, promoting blood circulation, removing blood stasis and removing food retention; the bleaching earth is rich in various trace elements, adsorbs and purifies dirt on the surface and deep layer of the skin, has the effects of resisting bacteria, diminishing inflammation, astringing, controlling oil, balancing sebum, simultaneously realizing excipient synergism and improving the beauty treatment effect of the effective components in the rose-agaric mud membrane paste. The medicines are combined to achieve the effects of cleaning and purifying skin, balancing and relieving allergy, maintaining beauty and keeping young. The invention has simple compatibility and good synergistic effect, natural active ingredients after biodegradation are rich, and molecules are small and easy to be absorbed by skin; the formula is natural and safe, has no toxic or side effect, has no stimulation and no sensitization, and is suitable for any skin; on the basis of moisturizing, tendering skin, improving susceptible muscle and preventing pigmentation, the effects of cleaning skin, purifying pores, regulating water and oil balance of skin, removing powder residue after makeup and the like are also added; the rose essence is rich in natural rose fragrance, and no essence is required to be added.

2. The rose and black fungus, the lily, the paper mulberry fruit, the mountain peach kernel and the bleaching earth are compounded and then added with the composite polypeptide and the composite enzyme fungicide, and the rose and black fungus mud membrane cream prepared by the method not only greatly improves the original effects of beautifying, moisturizing and replenishing water, but also has the capabilities of balancing sebum, resisting allergy and relieving, and is added with the remarkable functions of cleaning skin, purifying pores, removing powder residues after makeup and improving skin smoothness. The rose and black fungus mud membrane paste obtained by adopting the biotechnology improves the biological activity of natural plant moisturizing factors such as roses, black fungus and the like, reduces the molecular weight, promotes the absorption of nutrient substances and improves the beautifying effect; on the other hand, the influence of each component on the skin is reduced to the maximum extent, the skin barrier function is maintained, and the skin texture is enhanced.

3. According to the method, by adopting a jet milling technology and aiming at breaking walls, the traditional processing content is enriched, the current situation of traditional Chinese herbal medicine crushing is changed, the natural and specific components of plants are kept, the skin absorbability and the product compatibility are increased, and the super micro powder of the components in the rose-agaric mud membrane paste is finally obtained, so that the materials can be mixed with each other more uniformly, and the stability of the whole product system is ensured; meanwhile, the biological enzymolysis speed and the quality of glycolysis are accelerated, so that the effective components can be fully separated out, and resources are fully utilized.

4. The method adopts biotechnology, carries out biological enzymolysis and glycolysis on the super micro powder of the components in the rose-agaric mud membrane paste, reduces the content of toxic substances in each component through biological enzymolysis and glycolysis, and has prominent substantive characteristics and remarkable progress in the aspects of maintaining the micro-ecological balance of the skin and improving the skin resistance; meanwhile, the macromolecular substances are broken into small molecular components by enzymolysis and glycolysis, so that the rose black fungus mud membrane paste has remarkable progress in improving the bioactivity of the effective components, promoting the effective absorption of skin, shortening the external application time and improving the beauty effect.

5. The rose black fungus mud membrane paste disclosed by the invention does not contain any chemical additive, and animal experiments prove that the rose black fungus mud membrane paste disclosed by the invention is safe and effective, free of irritation, allergy and toxic and side effects, green and safe, and the preparation method is simple and feasible.

Detailed Description

The present invention will be further described with reference to the following specific examples.

Example 1

The rose black fungus mud membrane paste with the effects of cleaning, purifying, maintaining beauty and keeping young comprises the following raw materials in parts by weight: 10g of rose, 30g of black fungus, 10g of fresh lily, 20g of paper mulberry fruit, 10g of mountain peach kernel, 10g of bleaching earth, 0.5g of collagen polypeptide, 0.5g of soybean peptide, 3g of biological complex enzyme microbial inoculum, 0.5g of dipotassium glycyrrhizinate and a proper amount of rice washing water.

Wherein the rose is bitter water rose produced in Gansu bitter water.

The biological complex enzyme microbial inoculum comprises the following components in percentage by weight: 10% of starch hydrolase, 25% of cellulase, 10% of composite pectinase, 15% of agaric protease, 7% of bifidobacterium, 15% of lactic acid bacteria, 3% of saccharomycetes and 15% of wheat starter.

The preparation method of the rose black fungus mud membrane paste with the effects of cleaning, purifying, maintaining beauty and keeping young comprises the following steps:

A. rose, black fungus, fresh lily, paper mulberry fruit, mountain peach kernel, bleaching earth, collagen polypeptide, soybean peptide, biological complex enzyme fungicide and dipotassium glycyrrhizinate are respectively weighed according to the proportion;

D. preparing fresh lily and semen persicae into lily and semen persicae pulp by using a juicer, adding the super micro powder I into the lily and semen persicae pulp, adding rice washing water with the weight 3.5 times of that of the super micro powder I, and thoroughly and uniformly stirring to obtain a mixed solution;

E. adjusting the pH value of the mixed solution to 4.0, placing the mixed solution in a fermentation tank, adding a biological complex enzyme preparation with the total weight of 10% of that of the biological complex enzyme preparation, performing enzymatic glycolysis for 6 hours at the temperature of 45 ℃, and then heating the mixed solution to boil for 5 minutes;

F. when the temperature of the solution in the step E is reduced to 20 ℃, adding the super micro powder II and keeping the constant temperature state, and then adding the rest biological complex enzyme microbial inoculum for secondary enzymatic glycolysis for 72 hours;

G. inactivating the zymolyte at 100 deg.C for 60 min, adding collagen polypeptide and soybean peptide, stirring, and adding dipotassium glycyrrhizinate when the temperature is reduced to below 50 deg.C to obtain the final product.

Example 2

The rose black fungus mud membrane paste with the effects of cleaning, purifying, maintaining beauty and keeping young comprises the following raw materials in parts by weight: 30g of rose, 10g of black fungus, 30g of fresh lily, 10g of paper mulberry fruit, 20g of mountain peach kernel, 5g of bleaching earth, 1.5g of soybean peptide, 1.5g of corn polypeptide, 2g of glutathione, 1g of biological complex enzyme microbial inoculum, 2g of sodium benzoate and a proper amount of rice washing water.

Wherein the rose is bitter water rose produced in Gansu bitter water.

The biological complex enzyme microbial inoculum comprises the following components in percentage by weight: 25% of starch hydrolase, 10% of cellulase, 25% of composite pectinase, 10% of agaric protease, 15% of bifidobacterium, 3% of lactic acid bacteria, 7% of saccharomycetes and 5% of wheat starter.

A. rose, black fungus, fresh lily, paper mulberry fruit, mountain peach kernel, bleaching earth, soybean peptide, corn polypeptide, glutathione, biological complex enzyme fungicide and sodium benzoate are respectively weighed according to the proportion;

D. preparing fresh lily and semen persicae into lily and semen persicae pulp by using a juicer, adding the super micro powder I into the lily and semen persicae pulp, adding rice washing water with the weight 9.5 times of that of the super micro powder I, and thoroughly and uniformly stirring to obtain a mixed solution;

E. adjusting the pH value of the mixed solution to 6.0, placing the mixed solution in a fermentation tank, adding a biological complex enzyme preparation accounting for 20 percent of the total weight of the biological complex enzyme preparation, performing enzymatic glycolysis for 4 hours at the temperature of 65 ℃, and then heating the mixed solution to boil for 15 minutes;

F. when the temperature of the solution in the step E is reduced to 30 ℃, adding the super micro powder II and keeping the constant temperature state, and then adding the rest biological complex enzyme microbial inoculum for secondary enzymatic glycolysis for 45 hours;

G. inactivating the zymolyte at 120 ℃ for 30 minutes, adding soybean peptide, corn polypeptide and glutathione, stirring uniformly, and adding sodium benzoate when the temperature is reduced to below 50 ℃ to obtain the rose-agaric mud membrane paste.

Example 3

The rose black fungus mud membrane paste with the effects of cleaning, purifying, maintaining beauty and keeping young comprises the following raw materials in parts by weight: 20g of rose, 20g of black fungus, 20g of fresh lily, 15g of paper mulberry fruit, 15g of semen pruni armeniacae, 8g of bleaching earth, 1.5g of soybean peptide, 1.5g of corn polypeptide, 2g of biological complex enzyme microbial inoculum, 1g of dipotassium glycyrrhizinate and a proper amount of rice washing water.

Wherein the rose is bitter water rose produced in Gansu bitter water.

The biological complex enzyme microbial inoculum comprises the following components in percentage by weight: 17% of starch hydrolase, 18% of cellulase, 18% of composite pectinase, 12% of agaric protease, 3% of bifidobacterium, 7% of lactic acid bacteria, 15% of saccharomycetes and 10% of wheat starter.

A. rose, black fungus, fresh lily, paper mulberry fruit, mountain peach kernel, bleaching earth, soybean peptide, corn polypeptide, biological complex enzyme fungicide and dipotassium glycyrrhizinate are respectively weighed according to the proportion;

D. preparing fresh lily and semen persicae into lily and semen persicae pulp by using a juicer, adding the super micro powder I into the lily and semen persicae pulp, adding rice washing water with the weight 6 times of that of the super micro powder I, and thoroughly and uniformly stirring to obtain a mixed solution;

E. adjusting the pH value of the mixed solution to 5.0, placing the mixed solution in a fermentation tank, adding a biological complex enzyme preparation accounting for 15 percent of the total weight of the biological complex enzyme preparation, performing enzymatic glycolysis for 8 hours at the temperature of 30 ℃, and then heating the mixed solution to boil for 25 minutes;

F. when the temperature of the solution in the step E is reduced to 25 ℃, adding the super micro powder II and keeping the constant temperature state, and then adding the rest biological complex enzyme microbial inoculum for secondary enzymatic glycolysis for 60 hours;

G. inactivating the zymolyte at 80 deg.C for 100 min, adding soybean peptide and corn polypeptide, stirring, and adding dipotassium glycyrrhizinate when the temperature is reduced to below 50 deg.C to obtain the final product.

Comparative test example:

comparative example 1

Compared with the example 1, the biological complex enzyme microbial inoculum is lacked in the example 1, and other components and contents are the same as those in the example 1. The preparation method comprises weighing flos Rosae Rugosae, Auricularia, fresh Bulbus Lilii, fructus Broussonetiae, semen Persicae, bleaching earth, collagen polypeptide, soybean peptide and dipotassium glycyrrhizinate respectively at a certain proportion; mixing rose, black fungus and paper mulberry, and performing impact, collision, shearing, grinding, dispersion and crushing on the mixed material by using an airflow crusher to obtain 2000-mesh super micro powder I with the particle size of 1500-; impacting, colliding, shearing, grinding, dispersing and crushing the bleaching earth to 2000-mesh super micro powder II with the granularity of 1500-; preparing fresh lily and semen Caryae Cathayensis into lily and semen Persicae pulp by juicing machine, adding superfine powder I and superfine powder II into the lily and semen Persicae pulp, adding rice washing water 3.5 times the weight of the superfine powder I, adding collagen polypeptide, soybean peptide and dipotassium glycyrrhizinate, and stirring.

Comparative example 2

Comparative example 2 compared to example 1, collagen polypeptide and soybean peptide were absent, and other components and contents were the same as those of example 1. The preparation method comprises weighing flos Rosae Rugosae, Auricularia, fresh Bulbus Lilii, fructus Broussonetiae, semen Persicae, bleaching earth, biological complex enzyme microbial inoculum and dipotassium glycyrrhizinate respectively at a certain proportion; mixing rose, black fungus and paper mulberry, and performing impact, collision, shearing, grinding, dispersion and crushing on the mixed material by using an airflow crusher to obtain 2000-mesh super micro powder I with the particle size of 1500-; impacting, colliding, shearing, grinding, dispersing and crushing the bleaching earth to 2000-mesh super micro powder II with the granularity of 1500-; preparing fresh lily and semen persicae into lily and semen persicae pulp by using a juicer, adding the super micro powder I into the lily and semen persicae pulp, adding rice washing water with the weight 3.5 times of that of the super micro powder I, and thoroughly and uniformly stirring to obtain a mixed solution; adjusting the pH value of the mixed solution to 4.0, placing the mixed solution in a fermentation tank, adding a biological complex enzyme preparation with the total weight of 10% of that of the biological complex enzyme preparation, performing enzymatic glycolysis for 6 hours at the temperature of 45 ℃, and then heating the mixed solution to boil for 5 minutes; when the temperature of the solution in the step E is reduced to 20 ℃, adding the super micro powder II and keeping the constant temperature state, and then adding the rest biological complex enzyme microbial inoculum for secondary enzymatic glycolysis for 72 hours; inactivating the zymolysis at 100 deg.C for 60 min, and adding dipotassium glycyrrhizinate when the temperature is reduced to below 50 deg.C.

Comparative example 3

Comparative example 3 compared to example 1, rose and black fungus were absent, and other components and contents were the same as those of example 1. When in preparation, the fresh lily, the paper mulberry fruit, the mountain peach kernel, the bleaching earth, the collagen polypeptide, the soybean peptide, the biological complex enzyme fungicide and the dipotassium glycyrrhizinate are respectively weighed according to the proportion; the paper mulberry fruit is subjected to impact, collision, shearing, grinding, dispersion and crushing to obtain 2000-mesh super micro powder I with the particle size of 1500-; impacting, colliding, shearing, grinding, dispersing and crushing the bleaching earth to 2000-mesh super micro powder II with the granularity of 1500-; preparing fresh lily and semen persicae into lily and semen persicae pulp by using a juicer, adding the super micro powder I into the lily and semen persicae pulp, adding rice washing water with the weight 3.5 times of that of the super micro powder I, and thoroughly and uniformly stirring to obtain a mixed solution; adjusting the pH value of the mixed solution to 4.0, placing the mixed solution in a fermentation tank, adding a biological complex enzyme preparation with the total weight of 10% of that of the biological complex enzyme preparation, performing enzymatic glycolysis for 6 hours at the temperature of 45 ℃, and then heating the mixed solution to boil for 5 minutes; when the temperature of the solution in the step E is reduced to 20 ℃, adding the super micro powder II and keeping the constant temperature state, and then adding the rest biological complex enzyme microbial inoculum for secondary enzymatic glycolysis for 72 hours; inactivating the zymolyte at 100 deg.C for 60 min, adding collagen polypeptide and soybean peptide, stirring, and adding dipotassium glycyrrhizinate when the temperature is reduced to below 50 deg.C to obtain the final product.

Comparative example 4

Compared with the example 1, the comparative example 4 lacks the compound polypeptide and the biological compound enzyme inoculant, and other components and contents are the same as those in the example 1. The preparation method comprises weighing flos Rosae Rugosae, Auricularia, fresh Bulbus Lilii, fructus Broussonetiae, semen Persicae, bleaching earth and dipotassium glycyrrhizinate; mixing rose, black fungus and paper mulberry, and performing impact, collision, shearing, grinding, dispersion and crushing on the mixed material by using an airflow crusher to obtain 2000-mesh super micro powder I with the particle size of 1500-; impacting, colliding, shearing, grinding, dispersing and crushing the bleaching earth to 2000-mesh super micro powder II with the granularity of 1500-; preparing fresh lily and semen Caryae Cathayensis into lily and semen Persicae pulp by using a juicer, adding super micro powder I and super micro powder II into the lily and semen Persicae pulp, adding rice washing water with the weight 3.5 times of that of the super micro powder I, thoroughly and uniformly stirring, and adding dipotassium glycyrrhizinate.

Comparative example 5

The existing beauty treatment mud membrane paste named rose mud paste (Guangzhou Yunyang cosmetics Co., Ltd.) is used, and the main components of the rose mud paste comprise rose pollen, glucose, tartaric acid, citric acid, collagen and the like.

The test method comprises the following steps:

the test population: women and men between 20-50 years of age.

The test method comprises the following steps: using the method of each of the above examples and comparative examples, 2 to 3 times per week for a treatment period of 3 months were tried. During the trial period, no other similar products are used.

And (3) evaluating the curative effect:

and (3) improving the skin smoothness: valid, normal, invalid;

balancing the secretion of skin oil: valid, normal, invalid;

moisture content and moisture retention of skin.

The test result is as follows: skin finish

Tests show that the rose mud mask cream obtained in the examples 1, 2 and 3 has obvious effect on cleaning skin, can effectively improve the skin smoothness, purify skin pores, remove the residual powder after makeup and astringe the skin with fine pores.

And (2) test results: balance skin oil secretion

Experiments show that the rose pellicles obtained in examples 1, 2 and 3 can effectively improve the secretion condition of skin grease, control oil, balance skin, prevent and treat acne or seborrheic dermatitis and the like caused by imbalance of hair follicle flora, and improve skin resistance.

And (3) test results are as follows: skin moisture content and degree of moisturization (skin moisturization)

The evaluation criterion of the moisturizing effect is the water content of epidermal cells. The factors influencing the water content of the skin include physical and chemical factors such as perspiration, skin cleaning, cosmetics and the like. We chose to select three test subjects in each of examples 1, 2 and 3 and comparative examples 1, 2, 3 and 4, and asked to perform no skin care work such as skin cleansing and moisturizing after cleansing the skin in the morning of the day and no perspiration exercise, and then tested their skin moisture content at three times of 10:00, 13:00 and 16:00 of the day, and the average value was counted to analyze the moisture retention of the skin after using one treatment course.

Skin with a percentage of moisture data in the range of 40% -50% was tested as well-nourished skin according to the evaluation criteria for skin moisture content.

Skin moisture content measurement standard

The adopted test instrument is a puzzle SK-IV type high-precision skin humidity test beauty instrument for moisture and oil content. The test results were as follows:

the test shows that: the rose black fungus mud film cream obtained in the examples 1, 2 and 3 can effectively regulate the moisture and oil content ratio of the skin, and can regulate the moisture of the skin. It can be seen that the obvious moisturizing effect is achieved on dry skin after the skin moisturizing cream is used; for oily skin, the oil control and skin humidity regulation effects are realized after the use; for mixed skin, the skin develops towards well-nourished skin after use.

Skin irritation test:

the rose black fungus mud membrane paste provided by the invention is used for testing the skin irritation of rats

The external surface of the skin of the human body of the rose black fungus mud film paste disclosed by the invention is tried and observed to obtain a result

Skin allergy test:

the rose black fungus mud film cream disclosed by the invention scores and evaluates the allergic reaction of rat skin

Flavor test:

please refer to 30 general persons who had no olfactory diseases and were randomly divided into 3 groups, and the flavor of the paste of rosewood ear paste prepared in examples 1, 2 and 3 was evaluated. Wherein, 1 point is no fragrance; 2 is light fragrance; 3 points are medium fragrance; score 4 is a more pronounced fragrance; score 5 is a strong flavor, with an average score. The evaluation results of the rose black fungus mud film paste of each group are as follows:

Claims

1. the rose black fungus mud membrane paste with the effects of cleaning, purifying, maintaining beauty and keeping young is characterized in that: the composition is characterized by comprising the following raw materials in parts by weight: 10-30 parts of rose, 10-30 parts of black fungus, 10-30 parts of fresh lily, 10-20 parts of paper mulberry fruit, 10-20 parts of semen persicae, 5-10 parts of bleaching earth, 1-5 parts of composite polypeptide, 1-3 parts of biological complex enzyme microbial inoculum, 0.5-2 parts of preservative and a proper amount of rice washing water; wherein the composite polypeptide is 2-3 kinds of collagen polypeptide, soybean peptide, corn polypeptide and glutathione; the biological complex enzyme microbial inoculum consists of the following components in percentage by weight: 10-25% of starch hydrolase, 10-25% of cellulase, 10-25% of compound pectinase, 10-15% of agaric protease, 3-15% of bifidobacterium, 3-15% of lactic acid bacteria, 3-15% of yeast and 5-15% of wheat starter;

2. The paste as claimed in claim 1, wherein the paste comprises at least one of the following components: the composition is characterized by comprising the following raw materials in parts by weight: 20 parts of rose, 20 parts of black fungus, 20 parts of fresh lily, 15 parts of paper mulberry fruit, 15 parts of semen persicae, 8 parts of bleaching earth, 3 parts of composite polypeptide, 2 parts of biological complex enzyme fungicide, 1 part of preservative and a proper amount of rice washing water.

3. The paste as claimed in claim 1 or 2, which is characterized by comprising the following components by weight: the antiseptic is dipotassium glycyrrhizinate or sodium benzoate.

4. The paste as claimed in claim 1 or 2, which is characterized by comprising the following components by weight: the rose is bitter rose produced in bitter water in Gansu province.