CN105726363A - Plant care composition and preparation method thereof - Google Patents
Plant care composition and preparation method thereof Download PDFInfo
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- CN105726363A CN105726363A CN201610109519.2A CN201610109519A CN105726363A CN 105726363 A CN105726363 A CN 105726363A CN 201610109519 A CN201610109519 A CN 201610109519A CN 105726363 A CN105726363 A CN 105726363A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
Abstract
The invention relates to a plant care composition which is prepared from the following components in parts by weight: 1 part of pelargonium hortorum bailey flower essential oil, 2-40 parts of neroli essential oil, 1-20 parts of rose essential oil, 1-20 parts of chamomile essential oil and 1-20 parts of jasmine oil. The invention also discloses a method for preparing the plant care composition. The plant care composition disclosed by the invention is reasonable in component formula, synergistic, fresh and pleasant in aroma, natural, non-irritant and suitable for different skins and can achieve the effects of inhibiting bacteria, moisturizing, promoting cell regeneration and repairing injured tissues.
Description
Technical field
The present invention relates to daily cosmetics field, be specifically related to a kind of skin care compositions and methods of pure natural and preparation method thereof being raw material with this plant of flower.
Background technology
The skin care item great majority sold in the market are to be made up of synthetics, wherein it is no lack of and human body can be produced dysgenic material containing inorganic heavy metal (such as lead, hydrargyrum, arsenic), hormone, pigment etc., the such skin care item of life-time service, skin irritation is big, easily caused by allergy and pigmentation, thus causing skin lesion.Along with national economy develops rapidly, living standard and the quality of the life of people improve constantly, and the requirement of the cosmetics and skincare product of daily life indispensability is more and more higher, increasingly focus on skin protection concept natural, plant.
The natural aromatic material extracted from the flower of this plant of flower, without preservative and compound essence, it does not have adverse chemical composition, uses safer.The vegetable oil of this plant extract of not suiting can also be mutually combined use, or proportioning adds performance effect in the products such as water, breast, facial cream, color make-up to by a certain percentage according to the actual requirements.
Skin care compositions and methods is as the recipe ingredient of skin-protection product; it is particularly suitable for the nursing of skin moisturizing; not only can in the purpose instantly realizing immediately effectively nourishing skin smeared; protecting film can be formed in skin surface simultaneously; tightly pin the moisture of skin, thus realizing skin to keep the purpose of moist state for a long time.
Therefore, really it is necessary to improve the formula of current skin-protection product, the natural component of this plant extract of not suiting is prepared the skin care compositions and methods with multiple efficacies according to specific proportioning and meets the demand of people.
Summary of the invention
The present invention is directed to the deficiencies in the prior art part, it is provided that a kind of natural different skin quality non-stimulated, applicable, antibacterial moisturizing, promotion cell regeneration, reparation wounded tissue, the pure and fresh pleasant plant-nursing compositions of fragrance.
The preparation method that it is a further object of the present invention to provide described plant-nursing compositions.
For solving above-mentioned technical problem, the present invention adopts the following technical scheme that
A kind of plant-nursing compositions, is made up of the component including following parts by weight:
Preferably, described plant-nursing compositions, it is made up of the component including following parts by weight:
Preferably, described plant-nursing compositions, it is made up of the component including following parts by weight:
In the plant-nursing composite formula of the present invention, the preparation method of Flos Pelargonii flower essential oil, orange blossom quintessence oil, rose ethereal oil, chamomile essential oil and Flos Jasmini Sambac quintessence oil all comprises the steps: respectively
(1) component raw material of fresh harvesting being cleaned, remove impurity, add distilled water by solid-liquid ratio 1:10～1:12, after soaking 1～2h, heating, to producing water vapour, is distilled 2～2.5h, is obtained distillation when 80～85 DEG C；
(2) distillation obtained in step (1) is first condensed, then carry out oil-water separation when 30～40 DEG C, obtain, from distillation, quintessence oil and the hydrosol that first time extracts, collect the quintessence oil of first time extraction, stand-by；
(3) hydrosol obtained in step (2) is adsorbed by adsorbent；
(4) adsorbent being adsorbed with soluble fine obtained in step (3) is placed in supercritical extraction unit, is 5.5 × 10 resolving pressure3～6.5 × 103KPa, extracting pressure is 20 × 103～22 × 103KPa, temperature is 35～45 DEG C, carries CO with the flow of 15～25L/h2When extract 1.5～2h, obtain from hydrosol second time extract quintessence oil；
(5) quintessence oil that first time of obtaining with step (2) of quintessence oil that the second time obtained in step (4) extracts extracts is merged obtain extraction quintessence oil.
In described step (3), hydrosol flows through the adsorption tube of three series connection with the speed of 500～600mL/min, fills adsorbent in described adsorption tube.
Described adsorbent is XAD-2 adsorbent resin.
Preferably, it is possible to five kinds above-mentioned preparation method obtained extract quintessence oil and join in helical-ribbon type cone blender one by one by formula consumption, seal, toward same direction stirring 1～1.5h, mix homogeneously.
Commercial Flos Pelargonii flower essential oil, orange blossom quintessence oil, rose ethereal oil, chamomile essential oil, Flos Jasmini Sambac quintessence oil can be adopted other mixing arrangement mix homogeneously by the plant-nursing compositions of the present invention, other extracting method can also be adopted to extract, but effect is all not as using the plant-nursing compositions that obtains of extracting method of the present invention.
The plant-nursing composite formula of the present invention can add other required active component.
Preferably, described plant-nursing compositions can also be added in the products such as water, breast, facial cream, color make-up according to product demand, is improving the effect simultaneously working as nourishing skin of product efficacy, and addition is 1～10%.
Compared with prior art, there is advantages that the flower adopting this plant of flower makes raw material, preparation process does not use organic reagent, and skin zest is little；And the plant-nursing compositions collection India sunflower obtained, orange blossom, Flos Rosae Rugosae, Flos Matricariae chamomillae, effects of five kinds of flowers of Flos Jasmini Sambac and the fragrance of a flower, formula is reasonable, and Synergistic；It is possible not only to nourish skin, but also skin can be nursed one's health, there is effect of good antibacterial, moisturizing, moisturizing, cell regeneration can be promoted again simultaneously, repair wounded tissue, reach skin care effect.
Specific embodiment
In order to set forth present invention better, illustrate with some preferably specific embodiments below.But these specific embodiments are simply to illustrate that present disclosure, rather than present invention is limited.
Principle explanation
Five kinds of components that the plant-nursing compositions of the present invention uses in formula have following effect:
India sunflower: flower is pink, and abnormal smells from the patient is sweet and charming, rich in organic principle and the lot of trace mineral element such as citronellol, citronellyl formate, pine alkene, gemic acid, terpineol, citral, menthone, has very strong affinity, it is adaptable to various skin quality.Geranium Essential effect in beauty and skin care is notable, can not only balance sebum secretion, improve pore, has deep layer to purify and convergence antibacterial effect, and can promote that Skin Cell is newborn, strengthen cytophylaxis ability, repair cicatrix, desalination speckle, sensitive skin is had and well alleviates analgesic effect.And owing to Flos Pelargonii can stimulate lymphsystem, blood circulation promoting, meridians of invigorating blood circulation during use, make the ruddy gloss of skin have vigor.
Orange blossom: be the white petal of bigarabe plant, belong to Rutaceae, the fragrance of a flower is fresh and sweet grace slightly bitterness, it is mainly composed of geraniol, nerol, indole, terpineol, orange blossom ester, limonene etc..The primary efficacy of orange blossom quintessence oil is in that to adjust skin, and one is because it has the characteristic strengthening cell viability, can promote cell regeneration, repair and desalinate spot, increase elasticity of skin, soft skin；Two is that its penetrating power is very strong, moisturizing can pacify, restrains moisturizing, improve sensitive fragile and dry skin；Three is it rich in the multiple whitening active factor, can UV harms protection, help to decompose melanin, make skin be purified, shine pale brilliance.And health is also had and well loosens sedation effect, alleviate intense strain, pacify soul, relieving insomnia.
Flos Rosae Rugosae: belonging to rosaceous plant, the bright-coloured beauty of flower, fragrant is graceful, containing vegetable protein, Free amino acid, tannin, vitamin etc., is widely used in beauty treatment, perfume, food, medicine etc..Rose ethereal oil, as the king of natural plant essential oils, is easily absorbed by the skin, and has good beauty care effect.Its permeability and amalgamation are splendid, energy active cell regenerated energy, Free radicals restraining activity, reach effect of antioxidation, defying age；Skin natural moisture preserving system capability can be strengthened again simultaneously, improve dry sensitive skin；Can progressively nurse one's health and restrain capillary vessel, antiallergic of releiving, calmness, antiinflammatory is antibacterial etc. effectively；Can promote that melanin decomposes, strengthen elastic fibers and collagen fiber activity, obtain the healthy skin of pale bullet profit.
Flos Matricariae chamomillae: belong to feverfew, center yellow, petal white, be considered god's flower from ancient times, be known as the jinx of sensitive skin, is particularly suitable for dryness and sensitive skin, there is good Shu Min maintenance, reduce thin red blood streak, antiinflammatory, the unequal effect of the adjustment colour of skin.Chamomile essential oil is as one of the gentleest quintessence oil, all-ages, and gentleness keeps the skin wet, and pacifies skin for moisturizing, calmness, and restrains pore, simultaneously also effect such as antibacterial, healing of wound, help skin tissue regeneration.In addition, also have certain soul curative effect, there is splendid soothing effect, it is possible to the anxiety and tense emotion of the people that releives, make people loosen, soul tranquil, insomnia is helpful.
Flos Jasmini Sambac: being the beauty treatment flower that people commonly use since ancient times, fragrance is elegant pleasant, containing multiple nutritional components, such as vitamin, protein, mineral etc..Flos Jasmini Sambac quintessence oil is referred to as " king of quintessence oil ", can nurse one's health dry hydropenia, cross oily and sensitive skin, also be adapted for all types of skin.Therefore, it has deep water supplement, increases skin elasticity, slow down aging, effects such as calmness of releiving, and simultaneously because it has the calm effect of antiinflammatory, at desalination speckle, repairs in laceration etc. that also effect is notable.In use procedure, it can make people be in a cheerful frame of mind, expulsion worry, pacifies nerve, increases self-confidence.
Five kinds of above-mentioned component Synergistics after composite, have significantly antibacterial, moisturizing, promotion cell regeneration, repair effect of wounded tissue, and fragrance is pure and fresh pleasant, natural non-stimulated, are suitable for different skin quality.
Embodiment 1-12 and comparative example 13
The plant-nursing compositions of embodiment 1-12 and comparative example 13 is made up of the component of following five kinds of parts by weight:
In embodiment 1-12, the preparation method of plant-nursing compositions is as follows:
(1) the India sunflower of fresh harvesting, orange blossom, Flos Rosae Rugosae, Flos Matricariae chamomillae, five kinds of raw materials of Flos Jasmini Sambac are cleaned with clear water respectively, remove impurity, join boiler, distilled water is added by solid-liquid ratio 1:12, after soaking 1h, heating, to producing water vapour, is distilled 2h, is obtained five kinds of distillations when 85 DEG C；
(2) the five kinds of distillations obtained in step (1) are first respectively fed in condenser, after to be condensed, then it is respectively fed in the oil water separator that temperature is maintained at 35 DEG C, quintessence oil and five kinds of hydrosols that five kinds of first times extract are respectively obtained from five kinds of distillations, collect the quintessence oil of these five kinds first time extractions respectively, stand-by；
(3) the XAD-2 adsorbent resin that the five kinds of hydrosols obtained in step (2) flow through three series connection with the speed of 600mL/min respectively is adsorbed；
(4) adsorbent resin being adsorbed with soluble fine that will obtain in step (3), is added separately in the extractor of supercritical extraction instrument, is 6.5 × 10 resolving pressure3KPa, extracting pressure is 22 × 103KPa, temperature is 40 DEG C, carries CO with the flow of 20L/h2When extract 2h, from five kinds of hydrosol, respectively obtain the quintessence oils that five kinds of second time extract, tank analytically collected quintessence oils that these five kinds second time extract respectively；
(5) quintessence oils that quintessence oil obtain with step (2) the five kinds first time five kinds obtained in step (4) second time extracted extracts merge respectively and obtain five kinds of extraction quintessence oils, then extract quintessence oil by these five kinds and join in helical-ribbon type cone blender one by one by formula consumption, seal, toward same direction stirring 1h, quintessence oil mix homogeneously is extracted by these five kinds, namely obtaining plant-nursing compositions, subpackage, sealing preserve.
Wherein, described supercritical extraction instrument can be selected: HA121-50-05 type supercritical extraction unit.
Embodiment 14
A kind of preparation method of plant-nursing compositions, including step as follows:
(1) the India sunflower of fresh harvesting, orange blossom, Flos Rosae Rugosae, Flos Matricariae chamomillae, five kinds of raw materials of Flos Jasmini Sambac are cleaned with clear water respectively, remove impurity, join boiler, distilled water is added by solid-liquid ratio 1:10, after soaking 2h, heating, to producing water vapour, is distilled 2.5h, is obtained five kinds of distillations when 80 DEG C；
(2) the five kinds of distillations obtained in step (1) are first respectively fed in condenser, after to be condensed, then it is respectively fed in the oil water separator that temperature is maintained at 30 DEG C, quintessence oil and five kinds of hydrosols that five kinds of first times extract are respectively obtained from five kinds of distillations, collect the quintessence oil of these five kinds first time extractions respectively, stand-by；
(3) the XAD-2 adsorbent resin that the five kinds of hydrosols obtained in step (2) flow through three series connection with the speed of 500mL/min respectively is adsorbed；
(4) adsorbent resin being adsorbed with soluble fine that will obtain in step (3), is added separately in the extractor of supercritical extraction instrument, is 5.5 × 10 resolving pressure3KPa, extracting pressure is 20 × 103KPa, temperature is 35 DEG C, carries CO with the flow of 15L/h2When extract 1.5h, from five kinds of hydrosol, respectively obtain the quintessence oils that five kinds of second time extract, tank analytically collected quintessence oils that these five kinds second time extract respectively；
(5) quintessence oils that quintessence oil obtain with step (2) the five kinds first time five kinds obtained in step (4) second time extracted extracts merge respectively and obtain five kinds of extraction quintessence oils, then extract quintessence oil by these five kinds and join in helical-ribbon type cone blender one by one by formula consumption, seal and close, toward same direction stirring 1.5h, quintessence oil mix homogeneously is extracted by these five kinds, namely obtaining plant-nursing compositions, subpackage, sealing preserve.
Embodiment 15
A kind of preparation method of plant-nursing compositions, including step as follows:
(1) the India sunflower of fresh harvesting, orange blossom, Flos Rosae Rugosae, Flos Matricariae chamomillae, five kinds of raw materials of Flos Jasmini Sambac are cleaned with clear water respectively, remove impurity, join boiler, distilled water is added by solid-liquid ratio 1:11, after soaking 1.5h, heating, to producing water vapour, is distilled 2h, is obtained five kinds of distillations when 83 DEG C；
(2) the five kinds of distillations obtained in step (1) are first respectively fed in condenser, after to be condensed, then it is respectively fed in the oil water separator that temperature is maintained at 40 DEG C, quintessence oil and five kinds of hydrosols that five kinds of first times extract are respectively obtained from five kinds of distillations, collect the quintessence oil of these five kinds first time extractions respectively, stand-by；
(3) the XAD-2 adsorbent resin that the five kinds of hydrosols obtained in step (2) flow through three series connection with the speed of 550mL/min respectively is adsorbed；
(4) adsorbent resin being adsorbed with soluble fine that will obtain in step (3), is added separately in the extractor of supercritical extraction instrument, is 6.0 × 10 resolving pressure3KPa, extracting pressure is 21 × 103KPa, temperature is 45 DEG C, carries CO with the flow of 25L/h2When extract 2h, from five kinds of hydrosol, respectively obtain the quintessence oils that five kinds of second time extract, tank analytically collected quintessence oils that these five kinds second time extract respectively；
(5) quintessence oils that quintessence oil obtain with step (2) the five kinds first time five kinds obtained in step (4) second time extracted extracts merge respectively and obtain five kinds of extraction quintessence oils, then extract quintessence oil by these five kinds and join in helical-ribbon type cone blender one by one by formula consumption, seal and close, toward same direction stirring 1h, quintessence oil mix homogeneously is extracted by these five kinds, namely obtaining plant-nursing compositions, subpackage, sealing preserve.
Embodiment 16
Being used for preparing moisturizing emulsion as formula material using the plant-nursing compositions prepared by embodiment 1-12, this moisturizing emulsion is made up of the weight percent composition in formula as below table:
Preparation method is as follows:
(1) 1,3 butylene glycol and hyaluronate sodium are evenly stirred until transparent in advance, carbomer is made in advance the aqueous dispersions of 1% mass concentration；
(2) mixture that polyglycereol-3 methyl distearate, PEG-100 stearate, glyceryl stearate, cetearyl alcohol, shea butter, caprylic/capric triglyceride, white Limnanthes Alba Seed Oil, Parleam, Cyclomethicone and polydimethylsiloxane form is put into agitated kettle to heat to 80 DEG C, as oil phase；
(3) mixture of deionized water, EDTA-2Na, glycerol and the 1,3 butylene glycol processed through step (1) and hyaluronate sodium composition puts into emulsifying pot and is heated with stirring to 80 DEG C, as aqueous phase；
(4) oil phase is joined in aqueous phase, with the speed homogenizing 3min of 1000r/min, and stir cooling；
(5) when temperature is down to 65 DEG C, in aqueous phase, add the carbomer processed through step (1), stir, homogenizing 2min；
(6) when temperature is down to 45 DEG C, the plant-nursing compositions that glucosan, phenoxyethanol, methyl hydroxybenzoate, propyl hydroxybenzoate, aminomethyl propanol, essence and embodiment 1-12 prepare is added in aqueous phase, stir, evacuation, wait to be cooled to 38 DEG C with bottom discharge.
Embodiment 17
Being used for preparing Aloe glue as formula material using the plant-nursing compositions prepared by embodiment 1-12, this Aloe glue is made up of the weight percent composition in formula as below table:
Preparation method is as follows:
(1) by the methyl hydroxybenzoate in B component and propyl hydroxybenzoate, in 1.3-butanediol, heating for dissolving is to clear in advance, standby；
(2) mixture that component A acrylic acid (ester) class/C10-30 alkylol acrylamide acid esters cross linked polymer, card ripple 941 aqueous solution of 1% mass concentration, EDETATE SODIUM, allantoin, pantothenylol, hyaluronate sodium, glycerol, deionized water form is put into emulsifying pot to heat to 75～85 DEG C, as aqueous phase；
(3) mixture that the butanediol in B component, methyl hydroxybenzoate and propyl hydroxybenzoate form is put into agitated kettle to heat to 80 DEG C, as oil phase；
(4) treating that aqueous phase is cooled to 60 DEG C, slowly add oil phase while stirring in aqueous phase, stirring is to being uniformly dissolved；
(5) when temperature is down to 40 DEG C, the plant-nursing compositions that component C aminomethyl propanol, glycyrrhizic acid dipotassium, Aloe extract, Folium Aloe juice powder, Sargassum extract, menthol, camomile extract and embodiment 1-12 prepare is added in aqueous phase, stir, evacuation, waits to be cooled to 38 DEG C with bottom discharge.
Embodiment 18
Being used for preparing astringent as formula material using the plant-nursing compositions prepared by embodiment 1-12, this astringent is made up of the weight percent composition in formula as below table:
Preparation method is as follows:
(1) by pre-dispersed with glycerol respectively to xanthan gum and hyaluronate sodium；
(2) methyl hydroxybenzoate, propyl hydroxybenzoate and 1,3 butylene glycol are simply mixed post-heating to 55 DEG C of stirring and dissolving, be cooled to 30 DEG C standby；
(3) by EDETATE SODIUM, pantothenylol and deionized water mixing and stirring, it is warming up to 80 DEG C, is subsequently adding the solution of the xanthan gum, hyaluronate sodium and the glycerol that process through step (1), cooling after stirring 20min；
(4) after being cooled to 45 DEG C, add the solution of methyl hydroxybenzoate, propyl hydroxybenzoate and 1,3 butylene glycol processed through step (2), be subsequently adding phenoxyethanol, plant-nursing compositions that embodiment 1-12 prepares, stir, discharging after being cooled to 35 DEG C.
Checking embodiment 1 Microbial Challenge test
Each two parts of the plant-nursing compositions that Example 1-12 and comparative example 13 prepare respectively, every part of 20g, a copy of it adds 0.2mL mixed cell suspension, and another part adds the mould bacteria suspension of 0.2mL, makes the final bacteria containing amount of sample reach antibacterial 3 × 107CFU/g and mycete 1 × 105CFU/g level.After being sufficiently mixed, sample is placed at 28 DEG C and cultivates, 7d, 14d, 21d, 28d sample analysis after inoculation, adopt flat band method to calculate the bacteria containing amount in sample, result of the test is as shown in the table:
Although it is shown that the plant-nursing compositions of embodiment 1-12 does not add preservative, but still there is good fungistatic effect.
Showing by testing, the cosmetics that the plant-nursing compositions that embodiment 14-15 obtains obtains with embodiment 16-18 also have similar effect.
Checking embodiment 2 rabbit erythrocyte hemolytic test
The plant-nursing compositions 500 μ L that Example 1-12 and comparative example 13 prepare respectively, being placed in 2mL centrifuge tube, then be separately added into 2% rabbit erythrocyte suspension 500 μ L, jog mixes, it is placed in 37 DEG C of constant incubators after incubation 3h, then with the centrifugal 3min of the rotating speed of 2000r/min, Aspirate supernatant, with normal saline for negative control, with distilled water for positive control, measuring light absorption value at wavelength 414nm place, calculate haemolysis degree by formula, result of the test is as shown in the table:
Because the lipid of human skin and albumen and erythrocytic cell membrane are much like, so by measuring the plant-nursing compositions deformation extent to erythrocytic cell membrane damage degree and hemoglobin, simulating and evaluate its zest to human body skin.It is shown that the plant-nursing composite formula of embodiment 1-12 is natural, to no skin irritation.
Showing by testing, the cosmetics that the plant-nursing compositions that embodiment 14-15 obtains obtains with embodiment 16-18 also have similar effect.
Checking embodiment 3 proliferation of human dermal fibroblasts active determination test
The plant-nursing compositions that Example 1-6 and comparative example 13 prepare respectively, is first dissolved in dimethyl sulfoxide, with 0.2 μm of aseptic filter filtration sterilization, then is configured to the culture medium containing 10% sample with DMEM culture fluid.Obtaining human skin fibroblast with tissue mass cell culture, add 0.25% trypsin 1mL and digest, after centrifugal, addition DMEM culture fluid is resuspended, and counting and be diluted to cell concentration is 1 × 105/ mL, is inoculated in 96 orifice plates, every hole 100 μ L.Cultivate 48h, after Microscopic observation cell attachment, siphon away the culture medium in hole, being divided into 8 groups (often organizing 12 holes), first 6 groups is embodiment group, adds the 100 μ L culture medium containing 10% embodiment 1-6,7th group is comparative example group, adding the 100 μ L culture medium containing 10% comparative example 13, the 8th group is blank group, adds the DMEM culture medium of 100 μ L.CO in 37 DEG C, 5%2Incubator is often organized after quiescent culture 24h, 48h, 72h and takes 4 holes, after every hole adds 20 μ LMTT solution, in CO2Continuing to hatch 4h in incubator, every hole adds 150 μ L dimethyl sulfoxide, puts on constant-temperature table after low-speed oscillation 10min, and in microplate reader, 490nm place measures the light absorption value in every hole, and result of the test is as shown in the table:
| Test sample | 24h | 48h | 72h |
| Blank | 0.258 | 0.361 | 0.415 |
| Embodiment 1 | 0.462 | 0.633 | 0.786 |
| Embodiment 2 | 0.432 | 0.668 | 0.745 |
| Embodiment 3 | 0.488 | 0.681 | 0.785 |
| Embodiment 4 | 0.456 | 0.653 | 0.766 |
| Embodiment 5 | 0.478 | 0.642 | 0.779 |
| Embodiment 6 | 0.452 | 0.673 | 0.757 |
| Comparative example 13 | 0.303 | 0.489 | 0.532 |
It is shown that the light absorption value of embodiment 1-6 relatively blank group dramatically increases, and higher than comparative example 13, it was shown that the present invention has the more significant effect promoting cell regeneration, helps lend some impetus to wounded tissue reparation.
Showing by testing, the cosmetics that the plant-nursing compositions that embodiment 7-12,14-15 obtain obtains with embodiment 16-18 also have similar effect.
Checking embodiment 3 it is shown that Flos Pelargonii flower essential oil: orange blossom quintessence oil: rose ethereal oil: chamomile essential oil: the plant-nursing compositions that Flos Jasmini Sambac quintessence oil prepares under the proportion relation of 1:2～25:1～18:1～10:1～10 has and more significant promotes cell regeneration and the effect promoting wounded tissue to repair.And embodiment 1 obtain plant-nursing compositions promote cell regeneration and promote wounded tissue reparation in be best results, the proportion relation of its each component is Flos Pelargonii flower essential oil: orange blossom quintessence oil: rose ethereal oil: chamomile essential oil: Flos Jasmini Sambac quintessence oil=1:2:1:1:1.
Checking embodiment 4 performance of keeping humidity testing experiment
Choosing trier 10 people between 18-60 year, before test, at two the 4cm × 5cm test zones of each labelling of hands forearm around, two is interregional every at least 1cm.Trier enters the 20min that sits quietly between constant temperature and humidity, and forearm exposes, and places in test mode, keeps loosening.During test, left and right arm test zone is arranged to randomly sample smear zone and blank district, initial value before using the skin moisture content Corneometer test probe that Courage+Khazaka company of Germany manufactures that sample smear zone and blank region measurement sample are used, each region is surveyed and is taken average 3 times.Wear latex finger cot by sample by (2.0 ± 0.1) mg/cm2Consumption uniform application in sample smear zone, the plant-nursing compositions that wherein embodiment 7-12 is smeared in sample smear zone and comparative example 13 prepares respectively, blank district not spread product.Then sample smear zone and blank district carry out respectively the measurement of skin moisture value at 0.5h and 2h, and result of the test is as shown in the table:
It is shown that the plant-nursing compositions of embodiment 7-12 has good moisture-keeping efficacy.
Showing by testing, the cosmetics that the plant-nursing compositions that embodiment 1-6,14-15 obtain obtains with embodiment 16-18 also have similar effect.
Checking embodiment 4 it is shown that Flos Pelargonii flower essential oil: orange blossom quintessence oil: rose ethereal oil: chamomile essential oil: the vegetable composition that Flos Jasmini Sambac quintessence oil obtains under the proportion relation preparation in 1:10～33:3～5:5～8:5～7 has good moistening effect.And the moistening effect of the plant-nursing compositions that embodiment 9 obtains is best, the proportion relation of its each component is Flos Pelargonii flower essential oil: orange blossom quintessence oil: rose ethereal oil: chamomile essential oil: Flos Jasmini Sambac quintessence oil=1:10:5:5:5.
In sum, the present invention is natural non-stimulated, is suitable for different skin quality, five kinds of component Synergistics after composite in formula, not only notable antibacterial moisturizing, and may additionally facilitate cell regeneration, contributes to repairing wounded tissue.
Above-described embodiment is the present invention preferably embodiment; but embodiments of the present invention are also not restricted to the described embodiments; the change made under other any spirit without departing from the present invention and principle, modification, replacement, combination, simplification; all should be equivalent replacement mode, be included within protection scope of the present invention.
Claims (9)
1. a plant-nursing compositions, it is characterised in that be made up of the component including following parts by weight:
2. a kind of plant-nursing compositions according to claim 1, it is characterised in that be made up of the component including following parts by weight:
3. a kind of plant-nursing compositions according to claim 1, it is characterised in that be made up of the component including following parts by weight:
4. according to the arbitrary described a kind of plant-nursing compositions of claim 1-3, it is characterised in that the preparation method of described Flos Pelargonii flower essential oil, orange blossom quintessence oil, rose ethereal oil, chamomile essential oil and Flos Jasmini Sambac quintessence oil all comprises the steps:
(1) being cleaned by the raw material of fresh harvesting, add distilled water by solid-liquid ratio 1:10～1:12, after soaking 1～2h, heating, to producing water vapour, is distilled 2～2.5h, is obtained distillation when 80～85 DEG C；
(2) distillation obtained in step (1) is first condensed, then carry out oil-water separation when 30～40 DEG C, from distillation, obtain quintessence oil and hydrosol that first time extracts, collect the quintessence oil of first time extraction, stand-by；
(3) hydrosol obtained in step (2) is adsorbed by adsorbent；
(4) adsorbent being adsorbed with soluble fine obtained in step (3) is placed in supercritical extraction unit, is 5.5 × 10 resolving pressure3～6.5 × 103KPa, extracting pressure is 20 × 103～22 × 103KPa, temperature is 35～45 DEG C, carries CO with the flow of 15～25L/h2When extract 1.5～2h, obtain from hydrosol second time extract quintessence oil；
(5) quintessence oil that first time of obtaining with step (2) of quintessence oil that the second time obtained in step (4) extracts extracts is merged obtain extraction quintessence oil.
5. a kind of plant-nursing compositions according to claim 4, it is characterised in that in described step (3), hydrosol flows through the adsorption tube of three series connection with the speed of 500～600mL/min, fills adsorbent in described adsorption tube.
6. a kind of plant-nursing compositions according to claim 5, it is characterised in that described adsorbent is XAD-2 adsorbent resin.
7. a kind of plant-nursing compositions according to claim 6, it is characterised in that described blender is helical-ribbon type cone blender.
8. the preparation method according to the arbitrary described a kind of plant-nursing compositions of claim 1-3, it is characterised in that: one by one each component is joined in blender by formula consumption, stir 1～1.5h, mix homogeneously.
9. according to the arbitrary described a kind of plant-nursing compositions of claim 1-3, it is characterised in that: in cosmetics, its addition is 1～10%.
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