Women's privates conditioning liquid and preparation method thereof
Technical field
The invention belongs to health care and Medicines and Health Product field, be specifically related to a kind of women's privates conditioning liquid andIts preparation method.
Background technology
At present, the washing lotion that on market, a variety of women's privates are used, they adopt organic matter or Chinese medicine to join mostlyFang Zuowei sterilization bacteriostat, generally all has clean women's privates, dispels privates peculiar smell, prevents and treats bacterium infectionEtc. effect.
Some women because the factors such as sexual intercourse, childbirth or endocrinopathy easily cause women's privates skin blackout,The bad phenomenon such as privates skin senescence and elasticity deficiency. These situations are not only bad for healthy, but alsoLikely cause life quality to decline, even affect family harmony.
Summary of the invention
The problems referred to above that exist in order to solve prior art, the invention provides a kind of merit with common washing lotionCan, simultaneously can also whitening privates skin, delay privates skin senescence, increase women's private of privates skin elasticityPlace's conditioning liquid and preparation method thereof.
The technical solution adopted in the present invention is:
A kind of women's privates conditioning liquid, comprises the raw material of following weight portion proportioning:
Lavender 1-4 part; Rosa Damascana 1-4 part; Fir essential oil 1-3 part; Basal liquid 89-97 part.
Further: a kind of women's privates conditioning liquid, comprises the raw material of following weight portion proportioning:
2 parts of Lavenders; 2 parts of Rosa Damascanas; 2 parts of fir essential oils; 94 parts of basal liquids.
Preferably: described basal liquid is food stage olive oil.
Preferably: the preparation method of above-mentioned Lavender, comprises the following steps:
(1) by fresh lavender inflorescence, join in sodium chloride solution and soak 2-3h, obtain pretreated feedstock;
(2) described pretreated feedstock is placed in to distilling apparatus and at 100-105 DEG C, carries out air-distillation, normalPress the rear condensation of distillation, obtain condensate liquid;
(3) described condensate liquid is carried out to extracted many times by being equipped with in the adsorption column of ethanolic solution and active carbon,Obtain leaching liquor;
(4) described leaching liquor is carried out to decompression distillation, obtain Lavender.
The preparation method of fir essential oil, comprises the following steps:
(I), by fresh fir leaf, is added to the water and soaks 2-3h, obtains pretreated feedstock;
(II) is placed in distilling apparatus by described pretreated feedstock and at 100-105 DEG C, carries out air-distillation, normalCondensation after distillation, obtains condensate liquid;
(III) carries out extracted many times by described condensate liquid by being equipped with in the adsorption column of ethanolic solution and active carbon,Obtain leaching liquor;
Described leaching liquor is carried out decompression distillation by (IV), obtains fir essential oil.
Further: described in step (1), the concentration of sodium chloride solution is 20%-25%.
Further: described in step (4) and step (IV), the pressure of decompression distillation is 0.1-1.0kPa.
Preferably: the preparation method of above-mentioned Rosa Damascana, comprises the following steps:
(1) after the fresh roseleaf of 400-600 weight portion is pulverized, add 2000-3000 weight portionDistilled water, adds the acidic cellulase of 0.4-0.6 weight portion to carry out enzymolysis for the first time, for the first time enzymolysis afterwardsAfter completing, then add the pectase of 1-3 weight portion and the compound protease of 0.5-2 weight portion composition to carry out secondInferior hydrolysis, obtains enzymolysis head product;
(2) enzymolysis head product is placed in fermentation tank and carries out fermentation reaction, obtain after completion of the reaction tunning,Described tunning is heated to 80 DEG C, stand-by;
(3) by heating after tunning in sheet frame, carry out constant flow filtering, after filtration at 0.1Mpa pressureIn lower 25L Rotary Evaporators, concentrate, add 0.22-0.32 weight portion alcohol and get final product after concentrated 1000 timesRosa Damascana.
Further: the enzymolysis for the first time described in step (1) and for the second time enzymolysis time are 1h, itsIn before enzymolysis for the first time, adopt citric acid to regulate its pH value for 3.8-4.5.
Further: the time of fermentation reaction described in step (2) is 24h, adopt citric acid to regulate fermentationTime pH value be 6.0, fermentation temperature is 26-30 DEG C.
A method of preparing above-mentioned women's privates conditioning liquid, comprises the following steps:
(1) will after the Lavender of above-mentioned weight portion, Rosa Damascana and fir essential oil mixing, stir,Obtain blend of essential oils;
(2) pour the blend of essential oils of gained in step (1) into contain above-mentioned weight portion basal liquid containerMiddle stirring, fully dilution is merged, and obtains women's privates conditioning liquid.
Lavender is to be refined and formed by lavender, can be clearing heat and detoxicating, and cleaning skin, controls oil content,Freckle removing and whitening, the tender skin of anti-wrinkle, eye haustra-dsipelling livid ring around eye, also can promote damaged tissues regeneration recovery to wait skin care meritEnergy. It can purify, pacify soul, alleviate indignation and used-up sensation, makes the people can be even-tempered and good-humouredIn the face of life.
Rosa Damascana can stimulate and landman's immunity and nervous system, contributes to improve incretory simultaneouslySecretion, removes organ sclerosis, and repair cell, can adjust female incretion, nourishes uterus, relieving dysmenorrhea,Improve frigidity and climacteric discomfort. Especially there is good beautifying skin-protection function, can be with desalination outside interior supportingSpot, promote melanin decompose, improve dry skin, recover skin elasticity, allow women have pale, fillFull flexible healthy skin is the volatile oil of suitable female health.
Fir, formal name used at school (Abiesfabri (Mast.) Craib), fir essential oil extracts from fir leaf, hasMoisturizing, moisturizing, anti-inflammation, pore refining, toxin-expelling and face nourishing, smoothing wrinkle dispel line, loosen active, improve loseSleep, promote metabolism, anti crease and anti senile prepared old effect.
Olive oil is to be formed by the fresh direct cold press of olive fruit, without heating and chemical treatment, protectsStay natural nutrient component. High-grade olive oil that can be edible is to pass through with first ripe or ripe olive fresh fruitThe natural fruit oil juice that physical cold squeezing process extracts, olive oil is rich in abundant monounsaturated fatty acids-oleic acid,Also have vitamin A, Cobastab, vitamin D, vitamin E, vitamin K and polyphenoils etc. WomanFemale is edible olive oil often, can strengthen skin elasticity, receives the effect of moistening skin beautifying.
Beneficial effect of the present invention is: the present invention utilizes various plants essential oil to carry out scientific matching, collaborative performanceEffect of plants essential oil, the concrete mechanism of action is as follows: 1, the Lavender multiple pure plants essential oil of can arranging in pairs or groups is livedSex factor complements each other, and rapid osmotic hair follicle disinfecting, antimicrobial promotes cytothesis, recovers skin connective tissue,Balance skin top layer fat secretion, the responsive skin of releiving simultaneously, recovers skin oneself maintenance function, strengthening fleshSkin resistance to external world; 2, pure Lavender, as Joker oil, can carry out with one or more essential oilsAllotment, after allotment, the growth that its effect can be at double, but the ratio that essential oil is allocated is mutually extremely important,Require much skill parameter inside, in the present invention by Lavender and Rosa Damascana and fir essential oil withThe perfect golden ratio allotment of science forms compound essential oil, abandons the drawback of folk prescription essential oil, and multi-efficiency is mutualCooperate, greatly promoted the effect of deep layer maintenance; 3, the present invention is by adding after three kinds of essential oil scientific allocationsIn olive oil base oil clean, that moisturizing effect is splendid, can infiltrate rapidly skin is absorbed, moisten cleanWomen's privates, improves women's privates color and luster, has the effect of clean and whitening, uses for a long time, can delay privatesSkin senescence also increases the elasticity of privates skin, safe and non-stimulating, without allergic reaction, has no side effect, canUse with the women who is applicable to various age brackets, recover women's youth, promote love life.
Detailed description of the invention
Provide 3 specific embodiments below, explanation that the present invention will be further explained, it is to be noted:The present invention is not limited to following preferred forms, any those skilled in the art under enlightenment of the present invention allCan draw other various forms of products, no matter but in its shape or structure, do any variation, every haveIdentical with the application or akin technical scheme, within all dropping on protection scope of the present invention.
In the following embodiments, 1 weight portion acute pyogenic infection of finger tip 1g.
Embodiment 1
A kind of women's privates conditioning liquid, comprises the raw material of following weight portion:
1 part of Lavender; 1 part of Rosa Damascana; 1 part of fir essential oil; 89 parts, food stage olive oil.
The wherein preparation method of Lavender, comprises the following steps:
(1), by fresh lavender inflorescence, joining concentration is to soak 2h in 20% sodium chloride solution,Pretreated feedstock;
(2) described pretreated feedstock is placed in to distilling apparatus and at 100 DEG C, carries out air-distillation, normal pressure steamsHeat up in a steamer rear condensation, obtain condensate liquid;
(3) described condensate liquid is carried out to extracted many times by being equipped with in the adsorption column of ethanolic solution and active carbon,Obtain leaching liquor;
(4) be under 0.1kPa, to carry out decompression distillation by described leaching liquor at pressure, obtain Lavender.
The preparation method of Rosa Damascana, comprises the following steps:
(1) the fresh roseleaf of 400 weight portions is pulverized, added the distilled water of 2000 weight portions, useAfter citric acid is adjusted to 3.8 by the pH of distilled water, the acidic cellulase that adds 0.5 weight portion carries out for the first timeEnzymolysis, enzymolysis time is 1h for the first time, then uses the pectase of 1 weight portion and the compound protein of 0.5 weight portionEnzyme carries out enzymolysis for the second time, and enzymolysis time is 1h for the second time, obtains enzymolysis head product;
(2) enzymolysis head product is placed in to the 24h that ferments in fermentation tank, obtains tunning, before fermentation, use lemonIt is 6.0 that acid regulates the pH value of fermentation, and fermentation temperature is 26 DEG C, after fermentation, tunning is heated to80 DEG C, stand-by;
(3) tunning carries out constant flow filtering in sheet frame, 25L rotation under 0.1Mpa pressure after filtrationIn evaporimeter, concentrate, add 0.22 weight portion alcohol to obtain Rosa Damascana after concentrated 1000 times.
The preparation method of fir essential oil, comprises the following steps:
(1) by fresh fir leaf, be added to the water and soak 2h, obtain pretreated feedstock;
(2) described pretreated feedstock is placed in to distilling apparatus and at 100 DEG C, carries out air-distillation, normal pressure steamsHeat up in a steamer rear condensation, obtain condensate liquid;
(3) described condensate liquid is carried out to extracted many times by being equipped with in the adsorption column of ethanolic solution and active carbon,Obtain leaching liquor;
(4) be under 0.1kPa, to carry out decompression distillation by described leaching liquor at pressure, obtain fir essential oil.
The method of preparing above-mentioned women's privates conditioning liquid, comprises and is prepared as follows step:
(1) after the Lavender of gained, Rosa Damascana and fir essential oil being mixed by above-mentioned weight portion proportioningStir, obtain blend of essential oils;
(2) blend of essential oils of gained in step (1) is poured into and contained above-mentioned weight portion food stage olive oilContainer in, stir, fully dilution is merged, women's privates conditioning liquid.
Embodiment 2
A kind of women's privates conditioning liquid, comprises the raw material of following weight portion:
2 parts of Lavenders; 2 parts of Rosa Damascanas; 2 parts of fir essential oils; 93 parts, food stage olive oil.
The wherein preparation method of Lavender, comprises the following steps:
(1), by fresh lavender inflorescence, joining concentration is to soak 2.5h in 23% sodium chloride solution,Pretreated feedstock;
(2) described pretreated feedstock is placed in to distilling apparatus and at 103 DEG C, carries out air-distillation, normal pressure steamsHeat up in a steamer rear condensation, obtain condensate liquid;
(3) described condensate liquid is carried out to extracted many times by being equipped with in the adsorption column of ethanolic solution and active carbon,Obtain leaching liquor;
(4) be under 0.5kPa, to carry out decompression distillation by described leaching liquor at pressure, obtain Lavender.
The preparation method of Rosa Damascana, comprises the following steps:
(1) the fresh roseleaf of 500 weight portions is pulverized, added the distilled water of 2500 weight portions, useAfter citric acid is adjusted to 4.1 by the pH of distilled water, the acidic cellulase that adds 0.5 weight portion carries out for the first timeEnzymolysis, enzymolysis time is 1h for the first time, then uses the pectase of 2 weight portions and the compound protein of 1.2 weight portionsEnzyme carries out enzymolysis for the second time, and enzymolysis time is 1h for the second time, obtains enzymolysis head product;
(2) enzymolysis head product is placed in to the 24h that ferments in fermentation tank, obtains tunning, before fermentation, use lemonIt is 6.0 that acid regulates the pH value of fermentation, and fermentation temperature is 28 DEG C, after fermentation, tunning is heated to80 DEG C, stand-by;
(3) tunning utilizes ceramic membrane filter, after filtration under 0.1Mpa pressure 25L Rotary EvaporatorsIn concentrate, add 0.27 weight portion alcohol to obtain Rosa Damascana after concentrated 1000 times.
The preparation method of fir essential oil, comprises the following steps:
(1) by fresh fir leaf, be added to the water and soak 2.5h, obtain pretreated feedstock;
(2) described pretreated feedstock is placed in to distilling apparatus and at 103 DEG C, carries out air-distillation, normal pressure steamsHeat up in a steamer rear condensation, obtain condensate liquid;
(3) described condensate liquid is carried out to extracted many times by being equipped with in the adsorption column of ethanolic solution and active carbon,Obtain leaching liquor;
(4) be under 0.5kPa, to carry out decompression distillation by described leaching liquor at pressure, obtain fir essential oil.
The method of preparing above-mentioned women's privates conditioning liquid, comprises and is prepared as follows step:
(1) after the Lavender of gained, Rosa Damascana and fir essential oil being mixed by above-mentioned weight portion proportioningStir, obtain blend of essential oils;
(2) blend of essential oils of gained in step (1) is poured into and contained above-mentioned weight portion food stage olive oilContainer in, stir, fully dilution is merged, women's privates conditioning liquid.
Embodiment 3
A kind of women's privates conditioning liquid, comprises the raw material of following weight portion:
4 parts of Lavenders; 4 parts of Rosa Damascanas; 3 parts of fir essential oils; 97 parts, food stage olive oil.
The wherein preparation method of Lavender, comprises the following steps:
(1), by fresh lavender inflorescence, joining concentration is to soak 3h in 25% sodium chloride solution,Pretreated feedstock;
(2) described pretreated feedstock is placed in to distilling apparatus and at 105 DEG C, carries out air-distillation, normal pressure steamsHeat up in a steamer rear condensation, obtain condensate liquid;
(3) described condensate liquid is carried out to extracted many times by being equipped with in the adsorption column of ethanolic solution and active carbon,Obtain leaching liquor;
(4) be under 1.0kPa, to carry out decompression distillation by described leaching liquor at pressure, obtain Lavender.
The preparation method of Rosa Damascana, comprises the following steps:
(1) the fresh roseleaf of 600 weight portions is pulverized, added the distilled water of 3000 weight portions, useAfter citric acid is adjusted to 4.5 by the pH of distilled water, the acidic cellulase that adds 0.5 weight portion carries out for the first timeEnzymolysis, enzymolysis time is 1h for the first time, then uses the pectase of 3 weight portions and the compound protease of 2 weight portionsCarry out enzymolysis for the second time, enzymolysis time is 1h for the second time, obtains enzymolysis head product;
(2) enzymolysis head product is placed in to the 24h that ferments in fermentation tank, obtains tunning, before fermentation, use lemonIt is 6.0 that acid regulates the pH value of fermentation, and fermentation temperature is 30 DEG C, after fermentation, tunning is heated to80 DEG C, stand-by;
(3) tunning carries out constant flow filtering in sheet frame, 25L rotation under 0.1Mpa pressure after filtrationIn evaporimeter, concentrate, add 0.32 weight portion alcohol to obtain Rosa Damascana after concentrated 1000 times.
The preparation method of fir essential oil, comprises the following steps:
(1) by fresh fir leaf, be added to the water and soak 3h, obtain pretreated feedstock;
(2) described pretreated feedstock is placed in to distilling apparatus and at 105 DEG C, carries out air-distillation, normal pressure steamsHeat up in a steamer rear condensation, obtain condensate liquid;
(3) described condensate liquid is carried out to extracted many times by being equipped with in the adsorption column of ethanolic solution and active carbon,Obtain leaching liquor;
(4) be under 1.0kPa, to carry out decompression distillation by described leaching liquor at pressure, obtain fir essential oil.
The method of preparing above-mentioned women's privates conditioning liquid, comprises and is prepared as follows step:
(1) after the Lavender of gained, Rosa Damascana and fir essential oil being mixed by above-mentioned weight portion proportioningStir, obtain blend of essential oils;
(2) blend of essential oils of gained in step (1) is poured into and contained above-mentioned weight portion food stage olive oilContainer in, stir, fully dilution is merged, women's privates conditioning liquid.
Anti-inflammatory, bactericidal effect:
According to standard GB/T, 15797-2002 operates:
In the women's privates conditioning liquid making in embodiment 1, add Staphylococcus aureus bacteriostasis rate after 2minReach 65%; Antibacterial after 2min to adding white to read bacterial strain in the feminine care liquid making in embodiment 1Rate reaches 70%;
In the women's privates conditioning liquid making in embodiment 2, add Staphylococcus aureus bacteriostasis rate after 2minReach 67%; Antibacterial after 2min to adding white to read bacterial strain in the feminine care liquid making in embodiment 2Rate reaches 78%.
In the women's privates conditioning liquid making in embodiment 3, add Staphylococcus aureus bacteriostasis rate after 2minReach 68%; Antibacterial after 2min to adding white to read bacterial strain in the feminine care liquid making in embodiment 3Rate reaches 80%.
Using method: after it being diluted with warm water in the time using this women's privates conditioning liquid, clean, eachTake 10-15ml, before general sleep every night, use it to nurse.