CN108624426A - A kind of cold essential oil soap processed of antibacterial moisturizing wormwood congealed fat and its processing technology - Google Patents

A kind of cold essential oil soap processed of antibacterial moisturizing wormwood congealed fat and its processing technology Download PDF

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CN108624426A
CN108624426A CN201810611462.5A CN201810611462A CN108624426A CN 108624426 A CN108624426 A CN 108624426A CN 201810611462 A CN201810611462 A CN 201810611462A CN 108624426 A CN108624426 A CN 108624426A
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parts
essential oil
wormwood
leaf
rubus parvifolius
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杨林
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Shandong Rongji Health Management Ltd By Share Ltd
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Shandong Rongji Health Management Ltd By Share Ltd
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/02Compositions of detergents based essentially on soap on alkali or ammonium soaps
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/11Pteridophyta or Filicophyta (ferns)
    • AHUMAN NECESSITIES
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    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/282Artemisia, e.g. wormwood or sagebrush
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    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/72Rhamnaceae (Buckthorn family), e.g. buckthorn, chewstick or umbrella-tree
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/73Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
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    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/87Vitaceae or Ampelidaceae (Vine or Grape family), e.g. wine grapes, muscadine or peppervine
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/88Liliopsida (monocotyledons)
    • A61K36/89Cyperaceae (Sedge family)
    • A61K36/8905Cyperus (flatsedge)
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Abstract

The invention discloses a kind of cold essential oil soap processed of antibacterial moisturizing wormwood congealed fat and its processing technologys, the essential oil soap of the present invention is prepared by technological processes such as sorting, cleaning, removal of impurities, ultramicro grinding, distillation, supercritical extract, drying, condensations by wormwood, Lonicera standishii, Rubus parvifolius, common four-o'clock seed, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella plant, Portugal leaf, with warming and activating meridian, skin whitening, moisturizing, bactericidal antiphlogistic, the effect of anti-acne moisturizing, antiallergic sense.

Description

A kind of cold essential oil soap processed of antibacterial moisturizing wormwood congealed fat and its processing technology
Technical field
The present invention relates to daily chemical product field, more particularly, to a kind of cold essential oil soap processed of antibacterial moisturizing wormwood congealed fat and its add Work technique.
Background technology
People is because age growth, climate change, sleep insufficiency, over fatigue, unreasonable diet, used using alkaline daily use chemicals The factors such as product be easy to cause dry skin water shortage, and skin lacks moisture and is easy that people is allowed not feel like oneself, such as skin-bound, drying Skin is itched after decortication, bathing.In order to solve the problems, such as to have dry skin in the case of dry skin, especially dry weather to ask Topic, people's method with the most use are physically to smear the cosmetics with moisture-keeping functions.It is most of currently on the market to have The method for the moisturizing that the cosmetics of moisture-keeping functions use is mainly two kinds:One is preventing moisture of skin from evaporating, this cosmetics Containing fat oil, such as saualane, it can form a thin layer to prevent moisture evaporation on the skin;Another is to absorb air In moisture, this cosmetics mostly contain water suction substance, such as glycerine.It is asked although these cosmetics can solve dry skin Topic, but some discomforts also can be usually brought to people, such as prevent the moisture-keeping cosmetics of moisture evaporation from preventing the same of moisture evaporation Shi Rongyi blocks the eubolism of skin pore, barrier skin, is easy that skin is made the ill symptoms such as acne occur;In addition, such Cosmetics mostly use greatly industrial chemicals and are made, and the purity and processing technology etc. of raw material are very big on product quality influence, are also easy out The adverse reactions such as existing skin allergy.Then handmade soap has just come into people’s lives because its ingredient is controllable, safety is no added.
Handmade soap maintenance is talked about, perhaps you begin attempt to already, or just wait for a chance to cause trouble, and grow grass for a long time.Do not know from assorted When, the article that this morning of handmade soap has dropped out maintenance field starts to return the sight of people again.And this time, it It is no longer merely possible to traditional perfumed soap for washing one's hands etc, but one beauty new trend is started with the identity of " skin care products ". Handmade soap is originated from European ancient traditional handicraft, and any chemical composition is added without in manufacturing process, not only will not be as market after use Those upper skin care products containing chemical composition cause a hidden trouble to skin, and to skin and environment equal 100, pollution-free.Handmade soap because The difference of its all kinds of skin makeup functional component added, these handmade soaps are also derived for various skin quality, various skin demands Size type.Nowadays the maintenance field of handmade soap is also not limited solely to face already, or even expand to hair washing, take a shower etc.. Environmentally protective, the attraction that skin makeup is free of a burden publicized by it, many people also start the fan as " handmade soap beauty ".And Since the manufacturing process of handmade soap itself is filled with the color of DIY, Manual perfumed soap both can be used as washing one's face, makeup removing, and can be used as washing one's hair Bath is used.The foam exquisiteness of Manual perfumed soap is abundant, can thoroughly remove the greasy dirt of pore depths.Skin is set to moisten gloss, high resilience. Production method is also classified into two kinds, and hot preparation method and cold preparation method, heat system form typically common essential oil handmade soap;And it is cold with cold preparation method Made of system, referred to as cold congealed fat handmade soap processed;They expect that the production method period is completely different from former material, it may also be said to It is as far apart as heaven and earth.Essential oil soap make it is fast mostly at translucent, and it is colourful as smart as a new pin, it is not gaudy.Handmade soap contains Natural glycerine, moistening effect is free from worldly cares, and very mild to skin, non-stimulated.Foam exquisiteness is abundant, in addition to surprising clear Except clean power, the cuticula of skin will not be at all destroyed, achievees the effect that protect skin, skin care.Traditional handmade soap is big It all uses with olive oil, palm oil, coconut oil etc. the alkalies raw material for mixing sodium hydroxide solution for glyceride stock and is made, Such soap is easy the strong basicity because of sodium hydroxide, and the content of fatty acid in glyceride stock is destroyed in high temperature process, is made Obtain the problem of soap has coarse sense of touch and stimulation skin in actual use.In existing glyceride stock and hydrogen when the soap also having It adds the chemical substances such as different types of essence, foaming agent, active interface agent in sodium hydroxide solution raw material to form, but non-with cold system Method makes to make or be added water, is still because containing skin is stimulated there are many chemical substance, to sensitive in this way Discomfort is caused, in addition, soap lye waste water there are problems that polluting environment.
Plants essential oil is to be carried from plant different tissues such as root, stem, leaf, flower, fruit, seed, limb or secretion for raw material The general name with fragrance and volatility oily liquid substance taken, it has penetrating power is strong, most of safety is without side-effects etc. Advantage.Plants essential oil be for preparing essence and flavoring agent, but recent decades the study found that essential oil and one pack system have it is very strong Inhibition or kill the microorganisms such as bacterium and fungi characteristic.Aggravate increasingly in the disease caused by bacterium, fungal infection now Situation under, plants essential oil as it is a kind of efficiently, the natural plants fungicide of safety, application prospect is very wide.Soap is Using animal or plant grease by the fatty acid salt obtained by saponification or neutralization reaction, it is relative to using oil as the washing of raw material Product have many advantages, such as easily biological-degradable, it is small to skin irritation, almost without toxicity.Using essential oil as function raw material or fragrance It is added in soap base and essential oil soap is made, essential oil and the common advantage of soap can be given full play to.Essential oil soap is a kind of common daily disappears Fei Pin lives as Development of Urbanization more and more people focus in city in recent years, and what is followed closely is exactly air in city The downslide of quality, more exacerbates demand of the people to preserving moisture and protecting skin type essential oil soap, and the essential oil soap proportioning on existing market it is simple, Effect is single, and bactericidal effect can not just be taken into account by focusing on preserving moisture and protecting skin effect, focuses on bactericidal effect and takes into account moistening effect with regard to lunch, because This needs a kind of Hydrolyzed Protein to sterilize the essential oil soap taken into account.
The usage history of compound essential oil is long, it is generally believed that essential oil can bring allomeric function when being used in mixed way It is promoted.Find that in terms for the treatment of bacterium infection, the combination of essential oil is more than 600 kinds, and combines institute's band by current literature search Effect be also classified into collaboration, addition, unrelated and four kinds of situations of antagonism.In order to overcome the shortcomings of the above technology, exploitation one kind is with pure Plants essential oil is to moisten moisturizing ingredient, and to human body without any stimulation, raising antibiotic and sterilizing ability, it is significantly smart to moisten moistening effect Oil soap product is necessary.
CN200710177304.5 discloses one entitled " a kind of soap containing plants essential oil ", it is by fish pelargonium essence Manufactured essential oil soap in soap matrix is added in oil, chamomile essential oil, honeysuckle essential oil, oil of Cymbopogon winterianus and thyme essential oil, should Publication exist certain application limitation with it is insufficient, such as oil of Cymbopogon winterianus essential oil more excitatory, can only low dosage use, And highest usage amount may stimulate skin up to 3% in embodiment.
CN200910169806.2 discloses one entitled " natural cold process soap and low temperature soap preparing process ", it is by lavender Essential oil or Peppermint essential oil, base oil and Chinese medicine are by cold process soap made of low temperature soap preparing process, and the disclosure patent is only in specification Have effects that moisturize the skin with it in description, but specific effect is not illustrated.
Invention content
The purpose of the present invention is to provide a kind of cold essential oil soap processed of antibacterial moisturizing wormwood congealed fat and its processing technology, essences of the invention Oil soap is by wormwood, Lonicera standishii, Rubus parvifolius, common four-o'clock seed, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, dent Amaranth, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella plant, Portugal leaf pass through sorting, cleaning, removal of impurities, ultramicro grinding, distillation, surpass and face The technological processes such as boundary's extraction, dry, condensation are prepared, and there is warming and activating meridian, skin whitening, moisturizing, bactericidal antiphlogistic, anti-acne moisturizing to resist Sensitive effect.
What the object of the invention was achieved through the following technical solutions:
A kind of cold essential oil soap processed of antibacterial moisturizing wormwood congealed fat, is made of the bulk pharmaceutical chemicals of following weight ratio:50-80 parts of wormwood, 40-70 parts of Lonicera standishii, 40-70 parts of Rubus parvifolius, 30-50 parts of common four-o'clock seed, 30-50 parts of Herba Kalimeridis, 25-45 parts of Selaginella compta Hand- Mazz, spider Hatch 25-40 parts, 20-40 parts of japanese bearbind, 20-30 parts of mottle leaf, 15-30 parts of purslane, 10-30 parts of Semen thlaspis, section section rattan 10-30 Part, 10-25 parts of Herba Chrysosplenii delavayi, 10-30 parts of umbrella plant, 10-20 parts of Portugal leaf, 30-50 parts of dietary alkali, without 30-50 parts of bacterium ice cake.
In another preferred embodiment of the present invention, the essential oil soap is made of the raw material of following parts by weight:Chinese mugwort Grass 80 parts, 50 parts of Lonicera standishii, 45 parts of Rubus parvifolius, 30 parts of common four-o'clock seed, 35 parts of Herba Kalimeridis, 25 parts of Selaginella compta Hand- Mazz, 25 parts of aspidistra, 30 parts of japanese bearbind, 20 parts of mottle leaf, 20 parts of purslane, 15 parts of Semen thlaspis, section section 15 parts of rattan, 20 parts of Herba Chrysosplenii delavayi, 10 parts of umbrella plant, 10 parts of Portugal leaf, 40 parts of dietary alkali, without 40 parts of bacterium ice cake.
In another preferred embodiment of the present invention, the essential oil soap is made of the raw material of following parts by weight:Chinese mugwort Grass 70 parts, 70 parts of Lonicera standishii, 60 parts of Rubus parvifolius, 45 parts of common four-o'clock seed, 50 parts of Herba Kalimeridis, 45 parts of Selaginella compta Hand- Mazz, 40 parts of aspidistra, 30 parts of japanese bearbind, 25 parts of mottle leaf, 30 parts of purslane, 20 parts of Semen thlaspis, section section 30 parts of rattan, 25 parts of Herba Chrysosplenii delavayi, 30 parts of umbrella plant, 15 parts of Portugal leaf, 50 parts of dietary alkali, without 40 parts of bacterium ice cake.
In another preferred embodiment of the present invention, the essential oil soap is made of the raw material of following parts by weight:Chinese mugwort Grass 60 parts, 60 parts of Lonicera standishii, 50 parts of Rubus parvifolius, 40 parts of common four-o'clock seed, 40 parts of Herba Kalimeridis, 35 parts of Selaginella compta Hand- Mazz, 30 parts of aspidistra, 30 parts of japanese bearbind, 25 parts of mottle leaf, 20 parts of purslane, 20 parts of Semen thlaspis, section section 20 parts of rattan, 15 parts of Herba Chrysosplenii delavayi, 15 parts of umbrella plant, 10 parts of Portugal leaf, 30 parts of dietary alkali, without 50 parts of bacterium ice cake.
In a preferred embodiment in accordance with this invention, the essential oil soap is fabricated to by the raw material of following parts by weight:Chinese mugwort Grass 50 parts, 50 parts of Lonicera standishii, 40 parts of Rubus parvifolius, 30 parts of common four-o'clock seed, 30 parts of Herba Kalimeridis, 25 parts of Selaginella compta Hand- Mazz, 30 parts of aspidistra, 25 parts of japanese bearbind, 25 parts of mottle leaf, 15 parts of purslane, 20 parts of Semen thlaspis, section section 15 parts of rattan, 15 parts of Herba Chrysosplenii delavayi, 10 parts of umbrella plant, 15 parts of Portugal leaf, 40 parts of dietary alkali, without 50 parts of bacterium ice cake.
The processing technology of the essential oil soap comprising following steps:
Step 1:Sorting, cleaning, removal of impurities weigh good wormwood, Lonicera standishii, Rubus parvifolius, purple by above-mentioned raw materials parts by weight proportioning Jasmine, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella Nutgrass flatsedge, Portugal leaf, dietary alkali, without bacterium ice cake, it is spare;By Lonicera standishii, Rubus parvifolius, common four-o'clock seed, Herba Kalimeridis, Selaginella compta Hand- Mazz, spider Hatch, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella plant, Portugal leaf are cleaned, sort out impurity Postposition enters in sterilization container, spare;
Step 2:Lonicera standishii essential oil, Rubus parvifolius essential oil are prepared, Lonicera standishii, Rubus parvifolius are sliced respectively, slice thickness 1-2cm, later It is freeze-dried, the moisture after drying is 5- 10%;Lonicera standishii, Rubus parvifolius slice are used into ultra micro respectively in subzero Grinding device crushes, and obtains Lonicera standishii Ultramicro-powder, Rubus parvifolius Ultramicro-powder, is surpassed Lonicera standishii Ultramicro-powder, Rubus parvifolius with deionized water Micro mist infiltrates respectively, and infiltrating time is 30-60 minutes, and Lonicera standishii Ultramicro-powder, the Rubus parvifolius Ultramicro-powder after infiltration are respectively implanted steaming It evaporating in device, the oil water mixture distilled out is collected in water flowing steam distillation, and the oil water mixture distilled out is detached, and retains oil reservoir, Oil reservoir is dried using anhydrous sodium sulfate, is obtained after filtering in Lonicera standishii essential oil, Rubus parvifolius essential oil merging sterilization container, it is standby With;
Step 3:The Chinese medicine material common four-o'clock seed, Semen thlaspis that step 1 obtains is placed in desiccation in dryer, in after drying Medicine raw material is crushed in Study on Supermicro-pulverization of Traditional Chinese Drugs machine, and Chinese herbal ultra-fine powder is put into supercritical CO by the Chinese herbal ultra-fine powder after being crushed In the extraction kettle of 2 abstraction instruments, in pressure 25MPa, temperature 50 C under conditions of 2 flows of CO are 0.6m 3/h, extracts 3-5h, extraction Volatile oil one is obtained to be placed in sterilization container, it is spare;
Step 4:By wormwood, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, section section rattan, kidney calyx gold Waist, umbrella plant, Portugal leaf are freeze-dried, and the moisture after drying is 5- 10%, and crushing sieves with 100 mesh sieve, and adds water logging Then bubble carries out steam distillation, collect distillate, and ether is added and extracts, and the volume ratio of distillate and ether is 2:1, it takes Layer oil reservoir, then plus anhydrous sodium sulfate drying is placed in get volatile oil two in sterilization container, spare;
Step 5:Essential oil of traditional Chinese medicine will be obtained Step 3: four made volatile oil one and volatile oil two are uniformly mixed, then while stirring plus Enter Lonicera standishii essential oil, Rubus parvifolius essential oil, be uniformly mixed, stir 20 minutes, stand 30 minutes, filtering, ultrasonic oscillation 5-10 seconds obtains Composite essential oil is placed in sterilization container, spare;
Step 6:Composite essential oil that step 5 obtains is mixed with dietary alkali and without bacterium ice cake, and is stirred evenly, system is then placed in In soap dye tool, 20 DEG C or less gnotobasis natural coolings are placed into, after its solidification, demoulding packaging, you can obtain a kind of antibacterial The cold essential oil soap processed of moisturizing wormwood congealed fat.
The effect of the effect of each raw material is as follows:
Wormwood, warm-natured, bitter, have Wen Jing, dry, cold dispelling, hemostasis, anti-inflammatory, relieving asthma, cough-relieving, tocolysis, antiallergy the effects that.
Lonicera standishii, fruit mineral essence content is high, and calcium, iron, phosphorus, amino acid content are above other fruits, compares apple Be higher by 24 times, the content of iron is higher by 5 times than peach, the content of phosphorus be all fruits reported most, it is delicious tasty and refreshing, have non- Often good health and beauty effect, and there is antitumaous effect, Lonicera standishii is known as new type of health fruit, pollution-free, mineral nutrition Height is the best foods of health care, beauty, and common wooden fork rake juice is embrocated at face and wrinkle, and skin of face can be made ruddy tender white, go to wrinkle Ecchymose removing.
Rubus parvifolius, bitter, cool in nature, Return liver, stomach, lung, bladder warp, can dissipate the stasis of blood, relieve pain, removing toxic substances, desinsection, for spitting blood, bruise Knife wound, postpartum stasis of blood, dysentery, hemorrhoid, scabies, cold, fever, abscess of throat are spat blood, and are spitted blood, dysentery, enteritis, hepatitis, Eczema is controlled in hepatosplenomegaly, nephritic dropsy, urinary infection, calculus, irregular menstruation, leukorrhea, treating rheumatic ostealgia, treating swelling and pain by traumatic injury, external application, Dermatitis.
Common four-o'clock seed, sweet in flavor, cold nature, can heat-clearing plaque-eliminating, eliminating damp, detoxifying, cure mainly raw macle;Impetigo.
Herba Kalimeridis, cool in nature, acrid-sweet flavor, Return liver, stomach, lung channel can clearing heat and detoxicating, blood-stanching and blood-cooling, promoting urination and removing dampness, anti-inflammation and sterilizations And other effects, to diarrhea due to damp-heat, abscess of throat, carbuncle swells sore, hematemesis hematochezia, jaundice with damp-heat pathogen, difficult urination, parotitis, mastitis It is rich in calcium, phosphorus, iron, carrotene, potassium, vitamin B, vitamin C, niacin, albumen etc. having certain dietary function, Herba Kalimeridis The nutrients such as matter, fat, organic acid, wherein potassium content are 20 times of common vegetable, and often feeding can reduce sodium and assemble in cardiac muscle, It prevents ductus arteriosus wall from thickening, plays a protective role to blood vessel, prevent and reduce the risk of stroke caused by hypertension.
Selaginella compta Hand- Mazz, mildly bitter flavor is cool in nature, there is clearing heat and promoting diuresis, the function of clearing and activating the channels and collaterals, for acute icteric hepatitis, courage Capsulitis, dysentery, enteritis, lung carbuncle, rheumatic arthritis and burn and scald.
Aspidistra, warm-natured, acrid flavour micro-puckery is nontoxic, can be promoting blood circulation and removing obstruction in channels, and expel the heat-evil sharp dung, controls traumatic injury, pain in the back, Amenorrhea Abdominal pain is had a headache, toothache, and heat-syndrome cough hinders heat, diarrhea, sand leaching.
Japanese bearbind, it is warm-natured, it is sweet in flavor, QI invigorating is cured mainly, face Shao- black is removed.
Mottle leaf, acrid flavour is warm-natured, can dispelling wind removing toxic substances, scattered stasis detumescence, reunion of bone controls nettle rash, eczema, anaphylaxis skin Inflammation, the injury of tendon and muscle of fracturing, bruises and sprains, rheumatic numbness.
Purslane, it is sour, it is cold in nature, return large intestine channel, Liver Channel, can clearing heat and detoxicating, cooling blood and hemostasis, with controlling enteritis, bacillary dysentery, furunculosis Pyogenic infections, hemorrhoid gall, eczema, erysipelas, snakebite and bugbite, is had blood in stool, hemorrhoid blood, metrostaxis acute dermatitis, subacute skin at snakebite and bugbite Inflammation, herpes zoster, postpartum and function temper official bleeding, appendicitis, hookworm disease;Play the role of shrinking uterus;Influence it is cardiovascular and Respiratory system;It is in biphasic effect to skeletal muscle, so that intestinal contraction tension, amplitude and frequency is increased, but also have been reported that, this product is decocted Agent has inhibiting effect, antibacterial action to have norcholesterol effect, can promote the normal of epithelial cell function in guinea pig in vitro small intestine Change and the healing of ulcer, alcohol extracting thing or water decoction significantly inhibit effect to a variety of shigella dysenteriaes;Also to Escherichia coli, typhoid fever The pathogenic dermatophytes such as bacillus, staphylococcus aureus and Du small gemma tinea bacterium of Ang Shi have inhibiting effect, to shigella dysenteriae energy Generate drug resistance;It can also promote ulcer healing, vasoconstriction, Adjust-blood lipid.
Semen thlaspis, acrid flavour, tepor, materials for improving vision, mesh pain lacrimation, eliminating impediment, tonifying five zang organs, strengthening the essence light control the accumulation of liver man, and eyes is red It is swollen.
Section section rattan, it is mildly bitter flavor, puckery, it is cool in nature, can clearing heat and detoxicating, astringing to arrest bleeding, cure mainly burn and scald, ulcerative carbuncle furuncle, wound and go out Blood, eczema.
Herba Chrysosplenii delavayi, sweet in flavor, cold in nature, Return liver, the spleen channel, can clearing heat and detoxicating, myogenic, it is swollen to cure mainly child convulsion, scald, ulcerative carbuncle Poison.
Umbrella plant, sour, sweet, slight bitter is cool in nature, can the promoting flow of qi and blood circulation, removing toxic substances, cure mainly hemostasis have a pain, snakebite and bugbite.
Portugal leaf, bitter, cold in nature, thoughts of returning home warp, can be clearing heat and detoxicating, cures mainly aphthae, sore, variola.
Beneficial effects of the present invention:The present invention essential oil soap be by wormwood, Lonicera standishii, Rubus parvifolius, common four-o'clock seed, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella plant, Portugal leaf pass through The technological processes such as sorting, cleaning, removal of impurities, ultramicro grinding, distillation, supercritical extract, drying, condensation are prepared, Lonicera standishii quilt It is described as new type of health fruit, it is pollution-free, mineral nutrition is high, it is the best foods of health care, beauty, skin of face can be made ruddy tender In vain, wrinkle ecchymose removing, purslane is gone to cause a disease Escherichia coli, typhoid bacillus, staphylococcus aureus and Du small gemma tinea bacterium of Ang Shi etc. Property dermatophyte has inhibiting effect, can generate drug resistance to shigella dysenteriae, moreover it is possible to promote ulcer healing, with several kinds of Chinese medicinal materials essential oil By scientific compatibility, there is the effect of warming and activating meridian, skin whitening, moisturizing, bactericidal antiphlogistic, anti-acne moisturizing, antiallergic sense, effectively treat eye The diseases such as eyeball swelling and pain, variola, dry skin, complexion be dark yellow, scytitis, four limbs are numb, it is mild to skin, non-stimulated, make for a long time With that can improve skin condition, moisturizing, enhancing elasticity of skin improve cutaneous immunisation power, while can improve the state of mind of user, It inspires enthusiasm, is dynamic, there is incentive action.
Specific implementation mode
Pass through the following implementation technical solution that present invention be described in more detail.It should be pointed out that following explanation Only to claimed technical solution for example, not to any restrictions of these technical solutions.This hair Bright protection domain be subject to the appended claims record content.
Embodiment 1
A kind of cold essential oil soap processed of antibacterial moisturizing wormwood congealed fat, is made of the raw material of following weight ratio:50-80 parts of wormwood, wooden fork 40-70 parts of rake fruit, 40-70 parts of Rubus parvifolius, 30-50 parts of common four-o'clock seed, 30-50 parts of Herba Kalimeridis, 25-45 parts of Selaginella compta Hand- Mazz, spider embrace 25-40 parts of egg, 20-40 parts of japanese bearbind, 20-30 parts of mottle leaf, 15-30 parts of purslane, 10-30 parts of Semen thlaspis, section section rattan 10-30 Part, 10-25 parts of Herba Chrysosplenii delavayi, 10-30 parts of umbrella plant, 10-20 parts of Portugal leaf, 30-50 parts of dietary alkali, without 30-50 parts of bacterium ice cake.
The processing technology of the essential oil soap comprising following steps:
Step 1:Sorting, cleaning, removal of impurities weigh good wormwood, Lonicera standishii, Rubus parvifolius, purple by above-mentioned raw materials parts by weight proportioning Jasmine, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella Nutgrass flatsedge, Portugal leaf, dietary alkali, without bacterium ice cake, it is spare;By Lonicera standishii, Rubus parvifolius, common four-o'clock seed, Herba Kalimeridis, Selaginella compta Hand- Mazz, spider Hatch, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella plant, Portugal leaf are cleaned, sort out impurity Postposition enters in sterilization container, spare;
Step 2:Lonicera standishii essential oil, Rubus parvifolius essential oil are prepared, Lonicera standishii, Rubus parvifolius are sliced respectively, slice thickness 1-2cm, later It is freeze-dried, the moisture after drying is 5- 10%;Lonicera standishii, Rubus parvifolius slice are used into ultra micro respectively in subzero Grinding device crushes, and obtains Lonicera standishii Ultramicro-powder, Rubus parvifolius Ultramicro-powder, is surpassed Lonicera standishii Ultramicro-powder, Rubus parvifolius with deionized water Micro mist infiltrates respectively, and infiltrating time is 30-60 minutes, and Lonicera standishii Ultramicro-powder, the Rubus parvifolius Ultramicro-powder after infiltration are respectively implanted steaming It evaporating in device, the oil water mixture distilled out is collected in water flowing steam distillation, and the oil water mixture distilled out is detached, and retains oil reservoir, Oil reservoir is dried using anhydrous sodium sulfate, is obtained after filtering in Lonicera standishii essential oil, Rubus parvifolius essential oil merging sterilization container, it is standby With;
Step 3:The Chinese medicine material common four-o'clock seed, Semen thlaspis that step 1 obtains is placed in desiccation in dryer, in after drying Medicine raw material is crushed in Study on Supermicro-pulverization of Traditional Chinese Drugs machine, and Chinese herbal ultra-fine powder is put into supercritical CO by the Chinese herbal ultra-fine powder after being crushed In the extraction kettle of 2 abstraction instruments, in pressure 25MPa, temperature 50 C under conditions of 2 flows of CO are 0.6m 3/h, extracts 3-5h, extraction Volatile oil one is obtained to be placed in sterilization container, it is spare;
Step 4:By wormwood, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, section section rattan, kidney calyx gold Waist, umbrella plant, Portugal leaf are freeze-dried, and the moisture after drying is 5- 10%, and crushing sieves with 100 mesh sieve, and adds water logging Then bubble carries out steam distillation, collect distillate, and ether is added and extracts, and the volume ratio of distillate and ether is 2:1, it takes Layer oil reservoir, then plus anhydrous sodium sulfate drying is placed in get volatile oil two in sterilization container, spare;
Step 5:Essential oil of traditional Chinese medicine will be obtained Step 3: four made volatile oil one and volatile oil two are uniformly mixed, then while stirring plus Enter Lonicera standishii essential oil, Rubus parvifolius essential oil, be uniformly mixed, stir 20 minutes, stand 30 minutes, filtering, ultrasonic oscillation 5-10 seconds obtains Composite essential oil is placed in sterilization container, spare;
Step 6:Composite essential oil that step 5 obtains is mixed with dietary alkali and without bacterium ice cake, and is stirred evenly, system is then placed in In soap dye tool, 20 DEG C or less gnotobasis natural coolings are placed into, after its solidification, demoulding packaging, you can obtain a kind of antibacterial The cold essential oil soap processed of moisturizing wormwood congealed fat.
Embodiment 2
In another preferred embodiment of the present invention, the essential oil soap is made of the raw material of following parts by weight:Wormwood 80 Part, 50 parts of Lonicera standishii, 45 parts of Rubus parvifolius, 30 parts of common four-o'clock seed, 35 parts of Herba Kalimeridis, 25 parts of Selaginella compta Hand- Mazz, 25 parts of aspidistra, japanese bearbind 30 parts, 20 parts of mottle leaf, 20 parts of purslane, 15 parts of Semen thlaspis, section section 15 parts of rattan, 20 parts of Herba Chrysosplenii delavayi, 10 parts of umbrella plant, Portugal 10 parts of leaf, 40 parts of dietary alkali, without 40 parts of bacterium ice cake.
The processing technology of the essential oil soap comprising following steps:
Step 1:Sorting, cleaning, removal of impurities weigh good wormwood, Lonicera standishii, Rubus parvifolius, purple by above-mentioned raw materials parts by weight proportioning Jasmine, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella Nutgrass flatsedge, Portugal leaf, dietary alkali, without bacterium ice cake, it is spare;By Lonicera standishii, Rubus parvifolius, common four-o'clock seed, Herba Kalimeridis, Selaginella compta Hand- Mazz, spider Hatch, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella plant, Portugal leaf are cleaned, sort out impurity Postposition enters in sterilization container, spare;
Step 2:Lonicera standishii essential oil, Rubus parvifolius essential oil are prepared, Lonicera standishii, Rubus parvifolius are sliced respectively, slice thickness 1-2cm, later It is freeze-dried, the moisture after drying is 5%;Lonicera standishii, Rubus parvifolius slice are used into ultramicro grinding respectively in subzero Device crushes, and obtains Lonicera standishii Ultramicro-powder, Rubus parvifolius Ultramicro-powder, with deionized water by Lonicera standishii Ultramicro-powder, Rubus parvifolius Ultramicro-powder It infiltrating respectively, infiltrating time is 30 minutes, and Lonicera standishii Ultramicro-powder, the Rubus parvifolius Ultramicro-powder after infiltration are respectively implanted in distiller, The oil water mixture distilled out is collected in water flowing steam distillation, and the oil water mixture distilled out is detached, and is retained oil reservoir, is used nothing Oil reservoir is dried in aqueous sodium persulfate, is obtained after filtering in Lonicera standishii essential oil, Rubus parvifolius essential oil merging sterilization container, spare;
Step 3:The Chinese medicine material common four-o'clock seed, Semen thlaspis that step 1 obtains is placed in desiccation in dryer, in after drying Medicine raw material is crushed in Study on Supermicro-pulverization of Traditional Chinese Drugs machine, and Chinese herbal ultra-fine powder is put into supercritical CO by the Chinese herbal ultra-fine powder after being crushed In the extraction kettle of 2 abstraction instruments, in pressure 25MPa, temperature 50 C under conditions of 2 flows of CO are 0.6m 3/h, extracts 3h, extraction Volatile oil one is obtained to be placed in sterilization container, it is spare;
Step 4:By wormwood, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, section section rattan, kidney calyx gold Waist, umbrella plant, Portugal leaf are freeze-dried, and the moisture after drying is 5%, and crushing sieves with 100 mesh sieve, and soaks, so After carry out steam distillation, collect distillate, be added ether extraction, the volume ratio of distillate and ether is 2:1, take upper layer oily Layer, then plus anhydrous sodium sulfate drying is placed in get volatile oil two in sterilization container, spare;
Step 5:Essential oil of traditional Chinese medicine will be obtained Step 3: four made volatile oil one and volatile oil two are uniformly mixed, then while stirring plus Enter Lonicera standishii essential oil, Rubus parvifolius essential oil, be uniformly mixed, stir 20 minutes, stand 30 minutes, filtering, ultrasonic oscillation 5 seconds must answer It closes in essential oil merging sterilization container, it is spare;
Step 6:Composite essential oil that step 5 obtains is mixed with dietary alkali and without bacterium ice cake, and is stirred evenly, system is then placed in In soap dye tool, 20 DEG C or less gnotobasis natural coolings are placed into, after its solidification, demoulding packaging, you can obtain a kind of antibacterial The cold essential oil soap processed of moisturizing wormwood congealed fat.
Embodiment 3
In another preferred embodiment of the present invention, the essential oil soap is made of the raw material of following parts by weight:Wormwood 70 Part, 70 parts of Lonicera standishii, 60 parts of Rubus parvifolius, 45 parts of common four-o'clock seed, 50 parts of Herba Kalimeridis, 45 parts of Selaginella compta Hand- Mazz, 40 parts of aspidistra, japanese bearbind 30 parts, 25 parts of mottle leaf, 30 parts of purslane, 20 parts of Semen thlaspis, section section 30 parts of rattan, 25 parts of Herba Chrysosplenii delavayi, 30 parts of umbrella plant, Portugal 15 parts of leaf, 50 parts of dietary alkali, without 40 parts of bacterium ice cake.
The processing technology of the essential oil soap comprising following steps:
Step 1:Sorting, cleaning, removal of impurities weigh good wormwood, Lonicera standishii, Rubus parvifolius, purple by above-mentioned raw materials parts by weight proportioning Jasmine, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella Nutgrass flatsedge, Portugal leaf, dietary alkali, without bacterium ice cake, it is spare;By Lonicera standishii, Rubus parvifolius, common four-o'clock seed, Herba Kalimeridis, Selaginella compta Hand- Mazz, spider Hatch, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella plant, Portugal leaf are cleaned, sort out impurity Postposition enters in sterilization container, spare;
Step 2:Lonicera standishii essential oil, Rubus parvifolius essential oil are prepared, Lonicera standishii, Rubus parvifolius are sliced respectively, slice thickness 1-2cm, later It is freeze-dried, the moisture after drying is 10%;Lonicera standishii, Rubus parvifolius slice are used into ultramicro grinding respectively in subzero Device crushes, and obtains Lonicera standishii Ultramicro-powder, Rubus parvifolius Ultramicro-powder, with deionized water by Lonicera standishii Ultramicro-powder, Rubus parvifolius Ultramicro-powder It infiltrating respectively, infiltrating time is 60 minutes, and Lonicera standishii Ultramicro-powder, the Rubus parvifolius Ultramicro-powder after infiltration are respectively implanted in distiller, The oil water mixture distilled out is collected in water flowing steam distillation, and the oil water mixture distilled out is detached, and is retained oil reservoir, is used nothing Oil reservoir is dried in aqueous sodium persulfate, is obtained after filtering in Lonicera standishii essential oil, Rubus parvifolius essential oil merging sterilization container, spare;
Step 3:The Chinese medicine material common four-o'clock seed, Semen thlaspis that step 1 obtains is placed in desiccation in dryer, in after drying Medicine raw material is crushed in Study on Supermicro-pulverization of Traditional Chinese Drugs machine, and Chinese herbal ultra-fine powder is put into supercritical CO by the Chinese herbal ultra-fine powder after being crushed In the extraction kettle of 2 abstraction instruments, in pressure 25MPa, temperature 50 C under conditions of 2 flows of CO are 0.6m 3/h, extracts 5h, extraction Volatile oil one is obtained to be placed in sterilization container, it is spare;
Step 4:By wormwood, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, section section rattan, kidney calyx gold Waist, umbrella plant, Portugal leaf are freeze-dried, and the moisture after drying is 10%, and crushing sieves with 100 mesh sieve, and soaks, so After carry out steam distillation, collect distillate, be added ether extraction, the volume ratio of distillate and ether is 2:1, take upper layer oily Layer, then plus anhydrous sodium sulfate drying is placed in get volatile oil two in sterilization container, spare;
Step 5:Essential oil of traditional Chinese medicine will be obtained Step 3: four made volatile oil one and volatile oil two are uniformly mixed, then while stirring plus Enter Lonicera standishii essential oil, Rubus parvifolius essential oil, be uniformly mixed, stir 20 minutes, stand 30 minutes, filtering, ultrasonic oscillation 10 seconds must answer It closes in essential oil merging sterilization container, it is spare;
Step 6:Composite essential oil that step 5 obtains is mixed with dietary alkali and without bacterium ice cake, and is stirred evenly, system is then placed in In soap dye tool, 20 DEG C or less gnotobasis natural coolings are placed into, after its solidification, demoulding packaging, you can obtain a kind of antibacterial The cold essential oil soap processed of moisturizing wormwood congealed fat.
Embodiment 4
In another preferred embodiment of the present invention, the essential oil soap is made of the raw material of following parts by weight:Wormwood 60 Part, 60 parts of Lonicera standishii, 50 parts of Rubus parvifolius, 40 parts of common four-o'clock seed, 40 parts of Herba Kalimeridis, 35 parts of Selaginella compta Hand- Mazz, 30 parts of aspidistra, japanese bearbind 30 parts, 25 parts of mottle leaf, 20 parts of purslane, 20 parts of Semen thlaspis, section section 20 parts of rattan, 15 parts of Herba Chrysosplenii delavayi, 15 parts of umbrella plant, Portugal 10 parts of leaf, 30 parts of dietary alkali, without 50 parts of bacterium ice cake.
The processing technology of the essential oil soap comprising following steps:
Step 1:Sorting, cleaning, removal of impurities weigh good wormwood, Lonicera standishii, Rubus parvifolius, purple by above-mentioned raw materials parts by weight proportioning Jasmine, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella Nutgrass flatsedge, Portugal leaf, dietary alkali, without bacterium ice cake, it is spare;By Lonicera standishii, Rubus parvifolius, common four-o'clock seed, Herba Kalimeridis, Selaginella compta Hand- Mazz, spider Hatch, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella plant, Portugal leaf are cleaned, sort out impurity Postposition enters in sterilization container, spare;
Step 2:Lonicera standishii essential oil, Rubus parvifolius essential oil are prepared, Lonicera standishii, Rubus parvifolius are sliced respectively, slice thickness 1-2cm, later It is freeze-dried, the moisture after drying is 8%;Lonicera standishii, Rubus parvifolius slice are used into ultramicro grinding respectively in subzero Device crushes, and obtains Lonicera standishii Ultramicro-powder, Rubus parvifolius Ultramicro-powder, with deionized water by Lonicera standishii Ultramicro-powder, Rubus parvifolius Ultramicro-powder It infiltrating respectively, infiltrating time is 50 minutes, and Lonicera standishii Ultramicro-powder, the Rubus parvifolius Ultramicro-powder after infiltration are respectively implanted in distiller, The oil water mixture distilled out is collected in water flowing steam distillation, and the oil water mixture distilled out is detached, and is retained oil reservoir, is used nothing Oil reservoir is dried in aqueous sodium persulfate, is obtained after filtering in Lonicera standishii essential oil, Rubus parvifolius essential oil merging sterilization container, spare;
Step 3:The Chinese medicine material common four-o'clock seed, Semen thlaspis that step 1 obtains is placed in desiccation in dryer, in after drying Medicine raw material is crushed in Study on Supermicro-pulverization of Traditional Chinese Drugs machine, and Chinese herbal ultra-fine powder is put into supercritical CO by the Chinese herbal ultra-fine powder after being crushed In the extraction kettle of 2 abstraction instruments, in pressure 25MPa, temperature 50 C under conditions of 2 flows of CO are 0.6m 3/h, extracts 4h, extraction Volatile oil one is obtained to be placed in sterilization container, it is spare;
Step 4:By wormwood, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, section section rattan, kidney calyx gold Waist, umbrella plant, Portugal leaf are freeze-dried, and the moisture after drying is 8%, and crushing sieves with 100 mesh sieve, and soaks, so After carry out steam distillation, collect distillate, be added ether extraction, the volume ratio of distillate and ether is 2:1, take upper layer oily Layer, then plus anhydrous sodium sulfate drying is placed in get volatile oil two in sterilization container, spare;
Step 5:Essential oil of traditional Chinese medicine will be obtained Step 3: four made volatile oil one and volatile oil two are uniformly mixed, then while stirring plus Enter Lonicera standishii essential oil, Rubus parvifolius essential oil, be uniformly mixed, stir 20 minutes, stand 30 minutes, filtering, ultrasonic oscillation 8 seconds must answer It closes in essential oil merging sterilization container, it is spare;
Step 6:Composite essential oil that step 5 obtains is mixed with dietary alkali and without bacterium ice cake, and is stirred evenly, system is then placed in In soap dye tool, 20 DEG C or less gnotobasis natural coolings are placed into, after its solidification, demoulding packaging, you can obtain a kind of antibacterial The cold essential oil soap processed of moisturizing wormwood congealed fat.
Embodiment 5
In a preferred embodiment in accordance with this invention, the essential oil soap is fabricated to by the raw material of following parts by weight:Wormwood 50 Part, 50 parts of Lonicera standishii, 40 parts of Rubus parvifolius, 30 parts of common four-o'clock seed, 30 parts of Herba Kalimeridis, 25 parts of Selaginella compta Hand- Mazz, 30 parts of aspidistra, japanese bearbind 25 parts, 25 parts of mottle leaf, 15 parts of purslane, 20 parts of Semen thlaspis, section section 15 parts of rattan, 15 parts of Herba Chrysosplenii delavayi, 10 parts of umbrella plant, Portugal 15 parts of leaf, 40 parts of dietary alkali, without 50 parts of bacterium ice cake.
The processing technology of the essential oil soap, includes the following steps:
Step 1:Sorting, cleaning, removal of impurities weigh good wormwood, Lonicera standishii, Rubus parvifolius, purple by above-mentioned raw materials parts by weight proportioning Jasmine, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella Nutgrass flatsedge, Portugal leaf, dietary alkali, without bacterium ice cake, it is spare;By Lonicera standishii, Rubus parvifolius, common four-o'clock seed, Herba Kalimeridis, Selaginella compta Hand- Mazz, spider Hatch, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella plant, Portugal leaf are cleaned, sort out impurity Postposition enters in sterilization container, spare;
Step 2:Lonicera standishii essential oil, Rubus parvifolius essential oil are prepared, Lonicera standishii, Rubus parvifolius are sliced respectively, slice thickness 1-2cm, later It is freeze-dried, the moisture after drying is 5%;Lonicera standishii, Rubus parvifolius slice are used into ultramicro grinding respectively in subzero Device crushes, and obtains Lonicera standishii Ultramicro-powder, Rubus parvifolius Ultramicro-powder, with deionized water by Lonicera standishii Ultramicro-powder, Rubus parvifolius Ultramicro-powder It infiltrating respectively, infiltrating time is 60 minutes, and Lonicera standishii Ultramicro-powder, the Rubus parvifolius Ultramicro-powder after infiltration are respectively implanted in distiller, The oil water mixture distilled out is collected in water flowing steam distillation, and the oil water mixture distilled out is detached, and is retained oil reservoir, is used nothing Oil reservoir is dried in aqueous sodium persulfate, is obtained after filtering in Lonicera standishii essential oil, Rubus parvifolius essential oil merging sterilization container, spare;
Step 3:The Chinese medicine material common four-o'clock seed, Semen thlaspis that step 1 obtains is placed in desiccation in dryer, in after drying Medicine raw material is crushed in Study on Supermicro-pulverization of Traditional Chinese Drugs machine, and Chinese herbal ultra-fine powder is put into supercritical CO by the Chinese herbal ultra-fine powder after being crushed In the extraction kettle of 2 abstraction instruments, in pressure 25MPa, temperature 50 C under conditions of 2 flows of CO are 0.6m 3/h, extracts 5h, extraction Volatile oil one is obtained to be placed in sterilization container, it is spare;
Step 4:By wormwood, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, section section rattan, kidney calyx gold Waist, umbrella plant, Portugal leaf are freeze-dried, and the moisture after drying is 5%, and crushing sieves with 100 mesh sieve, and soaks, so After carry out steam distillation, collect distillate, be added ether extraction, the volume ratio of distillate and ether is 2:1, take upper layer oily Layer, then plus anhydrous sodium sulfate drying is placed in get volatile oil two in sterilization container, spare;
Step 5:Essential oil of traditional Chinese medicine will be obtained Step 3: four made volatile oil one and volatile oil two are uniformly mixed, then while stirring plus Enter Lonicera standishii essential oil, Rubus parvifolius essential oil, be uniformly mixed, stir 20 minutes, stand 30 minutes, filtering, ultrasonic oscillation 10 seconds must answer It closes in essential oil merging sterilization container, it is spare;
Step 6:Composite essential oil that step 5 obtains is mixed with dietary alkali and without bacterium ice cake, and is stirred evenly, system is then placed in In soap dye tool, 20 DEG C or less gnotobasis natural coolings are placed into, after its solidification, demoulding packaging, you can obtain product.
Antibacterial Activity:
One, disk diffusion method
Respectively by bacteria to be tested (Escherichia coli Escherichia coli ATCC 25922, Staphylococcus aureus Staphylococcus aureus subsp.Aureus ATCC25923, Pseudomonas aeruginosa (Pseudomonas aeruginosa) Each bacterium solution is diluted to 1 × 108CFU by ATCC27583 beef extract-peptone fluid nutrient medium cultures using preceding with than turbid instrument mL-1。
The beef extract-peptone agar medium of sterilizing is poured into the culture dish of diameter 9cm, after culture medium solidification, with shifting Liquid rifle is drawn each 100 μ l of bacterium solution and is spread evenly across on tablet, and the diameter 6mm filter papers after then taking hot air sterilization with tweezers are smooth In tablet center.
Respectively by mixed essential oil in Lonicera standishii essential oil, Rubus parvifolius essential oil, essential oil of traditional Chinese medicine, embodiment 2-5, CN200710177304.5 mixed essential oils, CN200910169806.2 mixed essential oils cross 0.45 μm of miillpore filter, and liquid-transfering gun is inhaled 10 μ l are taken to be added dropwise on filter paper, each three repetition of processing.Setting distilled water makees blank control, to positive selected by three kinds of bacteriums Property control (antibiotic) be respectively penicillin, streptomysin and cefotaxime (1mgmL-1).After essential oil is fully absorbed, 37 DEG C It is inverted culture 24 hours, antibacterial circle diameter is measured, takes and measure average value three times.
The bacteriostasis (inhibition zone radius r=mm) of 1 compound essential oil of table
Note:Inhibition zone size unit is mm, accuracy 0.02mm
As can be seen from the above table, essential oil has one when being used alone to Escherichia coli, staphylococcus aureus and Pseudomonas aeruginosa Fixed inhibition, there are significant differences for the inhibition of different essential oils.For Escherichia coli (bacterium A), essential oil of traditional Chinese medicine inhibits Effect is the most notable, and Rubus parvifolius essential oil inhibition is poor;For staphylococcus aureus (bacterium B), the antibacterial effect of Rubus parvifolius essential oil Fruit is preferable, and the inhibition of Lonicera standishii essential oil is poor;The better resistance of Pseudomonas aeruginosa (bacterium C), essential oil of traditional Chinese medicine inhibit to imitate to it Fruit is preferable, and the essential oil of embodiment 2-4 all has Escherichia coli, Staphylococcus aureus and Pseudomonas aeruginosa preferable antibacterial effect Fruit, antibacterial circle diameter are noticeably greater than essential oil exclusive use and antibiotic control group, and synergy is notable, and wherein embodiment 4 is bright Aobvious to be better than other groups, fungistatic effect is best.
Two, human hand is tested
Subject cleans each hand of right-hand man with clear water, the essential oil soap of embodiment 2-4 and certain commercially available brand bacteriostatic soap respectively Refer to, flowing water cleaning after with by autoclave sterilization non-woven fabrics wipe, after drying again respectively with anhydrous woven fabric 1h, 2h, 3h, To the random swabing sampling of the finger of right-hand man in the 4h periods, anhydrous woven fabric is put into containing containing MH broth bouillons later In conical flask number of bacteria is recorded with than turbid instrument in constant incubator after culture 18h.Compare preparation by the concentration of bacterium The fungistatic effect of essential oil soap.
Study subject bacterial concentration (× 108CFUmL-1) changes in table 1-4h
As can be seen from the above table, it is also either commercially available certain brand bacteriostatic soap with the essential oil soap in embodiment 2-4, with the time Extend, the number of bacteria of subject on hand all can showed increased, but its increased degree is different:Stage on-test (1-4 In hour), three subjects, in certain commercially available brand perfumed soap experimental group, illustrate embodiment using the number of bacteria bottom of essential oil soap on hand Bacteriostasis is better than commercial product to essential oil soap in 2-4 in short-term;Illustrate that subject is increased using the number of bacteria of essential oil soap on hand Slowly, illustrate that fungistatic effect is better than certain commercially available brand perfumed soap experimental group at this time.
Three, the clinical observation of drug of the present invention:
(1)Clinical symptoms
Main dark yellow eyes swelling and pain, variola, dry skin, complexion, scytitis, the four limbs of being presented with are numb;
(2)General information
Meet above-mentioned clinical symptoms;Age, men and women was unlimited between 18~75 years old;It is not used and the relevant external application of this disease in 2 weeks Any endo-medicine for treating this disease is not used in drug in 4 weeks;Important organ function of organization is normal, meet this study into It is 480 to select the patient of standard;Informed consent person;
(3)Exclusion criteria:
To drug ingedient allergy sufferers;It is associated with primary diseases and the essences such as serious cardiovascular and cerebrovascular disease, liver kidney and hemopoietic system Refreshing patient;The gestational period or women breast-feeding their children;
(4)Rejecting and abort criterion:
1. not pressing scheme medication, validity and safety judgement person are influenced;
2. voluntarily bolter in research process;
3. data is not complete, validity and safety judgement person are influenced;
4. in therapeutic process, the person that occurs serious adverse reaction;
(5)Therapy
All patients are equally divided into 6 groups by gender, disease condition, every group of patient uses the embodiment of the present invention 2,3,4,5 respectively Essential oil soap and CN200710177304.5 and CN200910169806.2 in essential oil soap carry out face cleaning, have a bath, therapy For:Have a bath daily 1 time, morning and evening face cleaning it is each primary, 10 days as one therapeutic course, continuous treatment 2 months;
(6)Efficacy determination
It is effective:The symptoms such as patient's eye swelling and pain, variola, dry skin, complexion be dark yellow, scytitis, four limbs are numb are relieved;
Effectively:The symptoms such as patient's eye swelling and pain, variola, dry skin, complexion be dark yellow, scytitis, four limbs are numb are alleviated;
In vain:Illness is unchanged;
(7)Treatment results
Each group patient's treatment see the table below 1;
1 (unit of table:People)
As a result:The effective percentage of embodiment 2-4 is significantly greater than the essential oil in CN200710177304.5 and CN200910169806.2 The effective percentage of the effective percentage of soap, wherein embodiment 4 is substantially better than other control groups, after the essential oil soap for using embodiment 43 days, Patient's eye swelling and pain symptom disappears, and has dry skin, complexion is dark yellow, scytitis, the numb situation of four limbs are obtained for and differ in size Improvement, after using 7 days the apparent anti-inflammatory of variola become smaller, after a course for the treatment of situation skin water moisten, have rosy cheeks, scytitis it is bright Aobvious improvement, variola disappear, the numb improvement of four limbs is more apparent, and in above-mentioned therapeutic process, have no adverse reaction appearance, drug safety;
(8)Conclusion:Pass through clinical observation, it was demonstrated that the present invention is to eyes swelling and pain, variola, dry skin, complexion are dark yellow, dermatitis Disease, four limbs are numb good therapeutic effect.
The content of present invention merely illustrates some claimed specific embodiments, one of them or more skill Recorded technical characteristic can be combined with arbitrary one or more technical solutions in art scheme, these are combined and obtain Technical solution also in the application protection domain, technical solution is disclosed in the present invention just as obtained from these are combined It is specifically recorded in content the same.

Claims (6)

1. a kind of cold essential oil soap processed of antibacterial moisturizing wormwood congealed fat, it is characterised in that:The essential oil soap is by following weight ratio Bulk pharmaceutical chemicals are made:50-80 parts of wormwood, 40-70 parts of Lonicera standishii, 40-70 parts of Rubus parvifolius, 30-50 parts of common four-o'clock seed, Herba Kalimeridis 30-50 Part, 25-45 parts of Selaginella compta Hand- Mazz, 25-40 parts of aspidistra, 20-40 parts of japanese bearbind, 20-30 parts of mottle leaf, 15-30 parts of purslane, Xi 10-30 parts of Mi, 10-30 parts of rattan of section section, 10-25 parts of Herba Chrysosplenii delavayi, 10-30 parts of umbrella plant, 10-20 parts of Portugal leaf, dietary alkali 30-50 parts, without 30-50 parts of bacterium ice cake.
2. a kind of antibacterial cold essential oil soap processed of moisturizing wormwood congealed fat according to claim 1, it is characterised in that:The essential oil soap It is made of the raw material of following parts by weight:80 parts of wormwood, 50 parts of Lonicera standishii, 45 parts of Rubus parvifolius, 30 parts of common four-o'clock seed, 35 parts of Herba Kalimeridis, 25 parts of Selaginella compta Hand- Mazz, 25 parts of aspidistra, 30 parts of japanese bearbind, 20 parts of mottle leaf, 20 parts of purslane, 15 parts of Semen thlaspis, section section rattan 15 Part, 20 parts of Herba Chrysosplenii delavayi, 10 parts of umbrella plant, 10 parts of Portugal leaf, 40 parts of dietary alkali, without 40 parts of bacterium ice cake.
3. a kind of antibacterial cold essential oil soap processed of moisturizing wormwood congealed fat according to claim 1, it is characterised in that:The essential oil soap It is made of the raw material of following parts by weight:70 parts of wormwood, 70 parts of Lonicera standishii, 60 parts of Rubus parvifolius, 45 parts of common four-o'clock seed, 50 parts of Herba Kalimeridis, 45 parts of Selaginella compta Hand- Mazz, 40 parts of aspidistra, 30 parts of japanese bearbind, 25 parts of mottle leaf, 30 parts of purslane, 20 parts of Semen thlaspis, section section rattan 30 Part, 25 parts of Herba Chrysosplenii delavayi, 30 parts of umbrella plant, 15 parts of Portugal leaf, 50 parts of dietary alkali, without 40 parts of bacterium ice cake.
4. a kind of antibacterial cold essential oil soap processed of moisturizing wormwood congealed fat according to claim 1, it is characterised in that:The essential oil soap It is made of the raw material of following parts by weight:60 parts of wormwood, 60 parts of Lonicera standishii, 50 parts of Rubus parvifolius, 40 parts of common four-o'clock seed, 40 parts of Herba Kalimeridis, 35 parts of Selaginella compta Hand- Mazz, 30 parts of aspidistra, 30 parts of japanese bearbind, 25 parts of mottle leaf, 20 parts of purslane, 20 parts of Semen thlaspis, section section rattan 20 Part, 15 parts of Herba Chrysosplenii delavayi, 15 parts of umbrella plant, 10 parts of Portugal leaf, 30 parts of dietary alkali, without 50 parts of bacterium ice cake.
5. a kind of antibacterial cold essential oil soap processed of moisturizing wormwood congealed fat according to claim 1, it is characterised in that:The essential oil soap It is fabricated to by the raw material of following parts by weight:50 parts of wormwood, 50 parts of Lonicera standishii, 40 parts of Rubus parvifolius, 30 parts of common four-o'clock seed, Herba Kalimeridis 30 Part, 25 parts of Selaginella compta Hand- Mazz, 30 parts of aspidistra, 25 parts of japanese bearbind, 25 parts of mottle leaf, 15 parts of purslane, 20 parts of Semen thlaspis, section section rattan 15 parts, 15 parts of Herba Chrysosplenii delavayi, 10 parts of umbrella plant, 15 parts of Portugal leaf, 40 parts of dietary alkali, without 50 parts of bacterium ice cake.
6. according to a kind of processing technology of the antibacterial cold essential oil soap processed of moisturizing wormwood congealed fat of claim 1-5 any one of them, It is characterized in that:It includes the following steps:
Step 1:Sorting, cleaning, removal of impurities weigh good wormwood, Lonicera standishii, Rubus parvifolius, purple by above-mentioned raw materials parts by weight proportioning Jasmine, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella Nutgrass flatsedge, Portugal leaf, dietary alkali, without bacterium ice cake, it is spare;By Lonicera standishii, Rubus parvifolius, common four-o'clock seed, Herba Kalimeridis, Selaginella compta Hand- Mazz, spider Hatch, japanese bearbind, mottle leaf, purslane, Semen thlaspis, section section rattan, Herba Chrysosplenii delavayi, umbrella plant, Portugal leaf are cleaned, sort out impurity Postposition enters in sterilization container, spare;
Step 2:Lonicera standishii essential oil, Rubus parvifolius essential oil are prepared, Lonicera standishii, Rubus parvifolius are sliced respectively, slice thickness 1-2cm, later It is freeze-dried, the moisture after drying is 5- 10%;Lonicera standishii, Rubus parvifolius slice are used into ultra micro respectively in subzero Grinding device crushes, and obtains Lonicera standishii Ultramicro-powder, Rubus parvifolius Ultramicro-powder, is surpassed Lonicera standishii Ultramicro-powder, Rubus parvifolius with deionized water Micro mist infiltrates respectively, and infiltrating time is 30-60 minutes, and Lonicera standishii Ultramicro-powder, the Rubus parvifolius Ultramicro-powder after infiltration are respectively implanted steaming It evaporating in device, the oil water mixture distilled out is collected in water flowing steam distillation, and the oil water mixture distilled out is detached, and retains oil reservoir, Oil reservoir is dried using anhydrous sodium sulfate, is obtained after filtering in Lonicera standishii essential oil, Rubus parvifolius essential oil merging sterilization container, it is standby With;
Step 3:The Chinese medicine material common four-o'clock seed, Semen thlaspis that step 1 obtains is placed in desiccation in dryer, in after drying Medicine raw material is crushed in Study on Supermicro-pulverization of Traditional Chinese Drugs machine, and Chinese herbal ultra-fine powder is put into supercritical CO by the Chinese herbal ultra-fine powder after being crushed In the extraction kettle of 2 abstraction instruments, in pressure 25MPa, temperature 50 C under conditions of 2 flows of CO are 0.6m 3/h, extracts 3-5h, extraction Volatile oil one is obtained to be placed in sterilization container, it is spare;
Step 4:By wormwood, Herba Kalimeridis, Selaginella compta Hand- Mazz, aspidistra, japanese bearbind, mottle leaf, purslane, section section rattan, kidney calyx gold Waist, umbrella plant, Portugal leaf are freeze-dried, and the moisture after drying is 5- 10%, and crushing sieves with 100 mesh sieve, and adds water logging Then bubble carries out steam distillation, collect distillate, and ether is added and extracts, and the volume ratio of distillate and ether is 2:1, it takes Layer oil reservoir, then plus anhydrous sodium sulfate drying is placed in get volatile oil two in sterilization container, spare;
Step 5:Essential oil of traditional Chinese medicine will be obtained Step 3: four made volatile oil one and volatile oil two are uniformly mixed, then while stirring plus Enter Lonicera standishii essential oil, Rubus parvifolius essential oil, be uniformly mixed, stir 20 minutes, stand 30 minutes, filtering, ultrasonic oscillation 5-10 seconds obtains Composite essential oil is placed in sterilization container, spare;
Step 6:Composite essential oil that step 5 obtains is mixed with dietary alkali and without bacterium ice cake, and is stirred evenly, system is then placed in In soap dye tool, 20 DEG C or less gnotobasis natural coolings are placed into, after its solidification, demoulding packaging, you can obtain a kind of antibacterial The cold essential oil soap processed of moisturizing wormwood congealed fat.
CN201810611462.5A 2018-06-14 2018-06-14 A kind of cold essential oil soap processed of antibacterial moisturizing wormwood congealed fat and its processing technology Pending CN108624426A (en)

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