CN109771348B - Whitening, moisturizing and wrinkle-removing face cream rich in natural product extract components and preparation method thereof - Google Patents
Whitening, moisturizing and wrinkle-removing face cream rich in natural product extract components and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components, which is prepared from the following raw materials in percentage by weight: 5 to 35 percent of lipid, 2 to 10 percent of emulsifier, 5 to 10 percent of humectant, 0.5 to 2 percent of preservative, 1 to 5 percent of thickener, 0.5 to 2 percent of bitter orange flower extract, 5 to 10 percent of tea extract, 0.2 to 1 percent of pineapple peel extract, 0.2 to 1 percent of ginkgo leaf extract, 0.2 to 1 percent of lychee seed extract, 0.2 to 1 percent of swertia mileensis extract, 5 to 10 percent of seaweed extract, 2 to 5 percent of beet root extract, 0.2 to 1 percent of strawberry extract and deionized water to 100 percent. The face cream has reasonable formula and remarkable effect, and has excellent whitening, moisturizing and wrinkle removing effects.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components and a preparation method thereof.
Background
The skin is a surface tissue covering the whole body, and can protect internal tissues and organs of the human body from being damaged, prevent water loss in the body, prevent harmful substances from invading the human body and the like. Therefore, the skin is an important component of the human body and more directly expresses the signs of human health and aging.
Because of the skin color problem of yellow people, Chinese people generally have the problems of dark skin color, dark yellow skin color, lack of luster, easy allergy, pigmentation and the like. How to whiten the skin is one of the most concerned problems for Chinese consumers.
The wrinkles refer to small fine lines and wrinkles formed by the skin affected by external environment, which form free radicals, the free radicals destroy collagen and active substances in normal cell membrane tissues and oxidize cells. Wrinkles gradually appear. The order of appearance is typically forehead, upper and lower eyelids, outer canthus, anterior auricular region, cheek, neck, chin, perioral.
There are many kinds of moisturizing creams, but many moisturizing creams are available which can whiten skin, lighten spots, remove wrinkles and resist oxidation, and some commercially available whitening products contain lead, mercury and other substances and have toxic and side effects on skin.
Disclosure of Invention
The invention aims to provide a whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components and a preparation method thereof, which can promote the generation of collagen, reduce the decomposition of elastin and effectively improve the anti-aging and wrinkle-removing effects of the facial cream; promoting skin metabolism, inhibiting melanin formation, promoting nutrient components to penetrate into skin, and whitening and moisturizing.
The object of the invention is achieved in the following way:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 5 to 35 percent of lipid, 2 to 10 percent of emulsifier, 5 to 10 percent of humectant, 0.5 to 2 percent of preservative, 1 to 5 percent of thickener, 0.5 to 2 percent of bitter orange flower extract, 5 to 10 percent of tea extract, 0.2 to 1 percent of pineapple peel extract, 0.2 to 1 percent of ginkgo leaf extract, 0.2 to 1 percent of lychee seed extract, 0.2 to 1 percent of swertia mileensis extract, 5 to 10 percent of seaweed extract, 2 to 5 percent of beet root extract, 0.2 to 1 percent of strawberry extract and deionized water to 100 percent.
The lipid is at least two of castor oil, beeswax, lecithin, squalane, isopropyl linoleate, and fatty acid yogurt fat.
The humectant is at least one of glycerol, polyethylene glycol-8 and sodium hyaluronate.
The preservative is one or two of p-hydroxybenzoic acid or methyl p-hydroxybenzoate.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components comprises the following specific steps:
s1: mixing lipid and emulsifier, adding into oil phase pan, heating and stirring to 80-90 deg.C, dissolving completely, and keeping the temperature to obtain phase A;
s2: mixing humectant and deionized water, adding into water phase pot, heating and stirring to 80-90 deg.C, dissolving completely, and keeping the temperature to obtain phase B;
s3: preheating an emulsifying pot to 70-75 ℃, stirring at the speed of 40-60 r/min, pumping in the phase B, pumping in the phase A, stirring for 20-40 min, and keeping the temperature at 80-90 ℃;
s4: adding the thickening agent into an emulsifying pot, homogenizing for 3-5 minutes, keeping the temperature and stirring for 20-40 minutes, keeping the temperature at 80-85 ℃, and stirring at the speed of 20-40 revolutions per minute;
s5: cooling to 40-50 deg.C, sequentially adding bitter orange flower extract, folium Camelliae sinensis extract, pineapple peel extract, folium Ginkgo extract, semen litchi extract, herba Swertiae Mileensis extract, Sargassum extract, radix Betae extract, strawberry extract and antiseptic, stirring at 25-30 r/min under heat preservation for 10-15 min; stirring and cooling to room temperature to obtain the whitening, moisturizing and wrinkle removing cream.
The preparation method of the extract or the extracting solution comprises the following steps:
bitter orange flower extract: cleaning bitter orange flower, drying, pulverizing, sieving, adding mixed solution of ethyl acetate and ethanol at volume ratio of 1:1, stirring, standing, performing ultrasonic extraction, filtering, and recovering solvent to obtain bitter orange flower extract;
tea leaf extract: cleaning tea leaves, drying, crushing, sieving, adding deionized water, mixing, stirring, standing, performing ultrasonic extraction, and filtering to obtain a solution, namely a tea leaf extracting solution;
pineapple peel extract: cleaning pineapple peel, draining, cutting into sections, adding a phosphate buffer solution with the pH value of 7.8, stirring in a stirrer until the mixture is crushed, centrifuging by using a freezing centrifuge, discarding the precipitate to obtain a crude bromelain extract, performing microfiltration to remove impurities, ultrafiltration concentration and separation to obtain a concentrated solution of the pineapple peel extract, performing precipitation by using an ammonium persulfate method, and finally performing vacuum freeze drying to obtain the pineapple peel extract;
ginkgo leaf extract: cleaning folium Ginkgo, oven drying, pulverizing, sieving, adding ethanol, mixing, stirring, standing, performing ultrasonic extraction, filtering, and recovering ethanol to obtain folium Ginkgo extract;
litchi seed extract: cleaning semen litchi, oven drying, pulverizing, sieving, adding ethanol, mixing, stirring, standing, performing ultrasonic extraction, filtering, and recovering ethanol to obtain semen litchi extract;
swertia mileensis extract: cleaning herba Swertiae Mileensis, oven drying, pulverizing, sieving, adding ethanol, mixing, stirring, standing, ultrasonic extracting, filtering, and recovering ethanol to obtain herba Swertiae Mileensis extract;
extracting the seaweed: cleaning seaweed, drying, pulverizing, sieving, adding deionized water, mixing, stirring, standing, ultrasonic extracting, and filtering to obtain seaweed extract;
beet root extract: cleaning, drying, crushing and sieving beet root, adding deionized water for mixing, stirring, standing, performing ultrasonic extraction, and filtering to obtain beet root extract;
strawberry extract: cleaning strawberry, oven drying, pulverizing, sieving, adding deionized water, mixing, stirring, standing, ultrasonic extracting in hot water bath, filtering, and drying to obtain strawberry extract.
The whitening, moisturizing and wrinkle-removing cream containing the natural product extract components comprises the following active components: the traditional Chinese medicine composition comprises bitter orange flower extract, tea extract, pineapple peel extract, ginkgo leaf extract, lychee seed extract, swertia mileensis extract, seaweed extract, beet root extract and strawberry extract.
Bitter orange flower: the neroli has the characteristics of enhancing cell activity, helping cell regeneration, increasing skin elasticity, resisting aging, resisting bacteria, softening skin, calming, whitening, moisturizing, lightening spots, eliminating uneven and dull skin color and the like. The skin care product prepared from the extract is suitable for dry, sensitive and mature skin, and is helpful for other skin problems.
Tea leaf: the tea leaves contain rich tea polyphenol, the tea polyphenol is not only a good grease antioxidant, but also has the effects of resisting bacteria, activating skin, preserving moisture, resisting inflammation, healing wounds, improving capillary toughness and the like, and simultaneously, the tea leaves are also a good ultraviolet filter, can reduce the formation of skin melanin, can remove freckles and senile plaques and achieve the aim of skin care.
Pineapple peel: the pineapple peel is rich in a large amount of bromelain, the bromelain can hydrolyze amide bonds and ester bonds in protein, can act on aged horny layer on human skin, promote the degradation, decomposition and removal of the aged horny layer, promote the skin metabolism, reduce the skin color depth phenomenon caused by sunshine and ensure that the skin is maintained in a good white and tender state.
Ginkgo leaf: the ginkgo leaf is a plant with high medicinal value, contains natural active flavone and ginkgo leaf terpene, and has high whitening, oxidation resistance and antibacterial property. Can be used in skin care products for reducing lipid peroxidation level, reducing freckle, moistening skin, inhibiting melanin growth, and keeping skin luster and elasticity.
Litchi seeds: the semen litchi surface is brown to brownish red, has slight luster, irregular recesses and fine wrinkles, is rich in xanthorrhizol, palmitic acid and other elements, and the extract can enhance cell activity, prolong cell life, promote proliferation of human fibroblasts and has the effect of resisting wrinkles.
And (3) green leaf gall: the herba Swertiae Mileensis is an annual herb, and can be used for separating and extracting caryophyllin, which has certain surface activity, helps to stabilize emulsion, and can promote collagen generation, reduce elastin decomposition, activate skin, resist aging and wrinkle, and keep moisture.
Seaweed: the seaweed is rich in fucose, and the fucose has good promotion effect on activity of human fibroblast, is beneficial to maintenance and generation of elastic fiber, and can be used in anti-wrinkle and antiaging cosmetics.
Beet root: the beet root is red like fire, and is rich in betaine. Betaine has strong moisture retention, is beneficial to maintaining cell polarity and permeability, is an excellent skin humectant, also has certain compatibility, increases the efficacy of other components, and reduces irritation to skin.
Strawberry: the strawberry can be extracted to obtain galactaric acid, which can accelerate skin stratum corneum metabolism and has good moisture keeping effect.
Compared with the prior art, the whitening, moisturizing and wrinkle-removing facial cream disclosed by the invention adopts natural products, namely extracts of bitter orange flowers, tea leaves, pineapple peels, ginkgo leaves, lychee seeds, mile swertia, seaweed, beet roots and strawberries as effective components, is natural, safe and non-irritant, and the components are mutually synergistic, so that the generation of collagen is promoted, the decomposition of elastin is reduced, and the anti-aging and wrinkle-removing effects of the facial cream are effectively improved by promoting the proliferation of human body fibroblasts; the skin whitening and moisturizing cream has the advantages of accelerating the metabolism of the skin cuticle, helping cell regeneration, promoting the skin metabolism, inhibiting the formation of melanin, and promoting the penetration of nutrient components into the skin, thereby achieving the purpose of whitening and moisturizing. The face cream has reasonable formula and remarkable effect, and has excellent whitening, moisturizing and wrinkle removing effects.
Detailed Description
Example 1:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 5% of lipid, 2% of emulsifier, 5% of humectant, 0.5% of preservative, 1% of thickener, 0.5% of bitter orange flower extract, 5% of tea extract, 0.2% of pineapple peel extract, 0.2% of ginkgo leaf extract, 0.2% of lychee seed extract, 0.2% of swertia mileensis extract, 5% of seaweed extract, 2% of beetroot extract, 0.2% of strawberry extract and the balance of deionized water to 100%.
The lipid is oleum ricini and Cera flava, and is mixed at any ratio.
The humectant is glycerol.
The antiseptic is p-hydroxybenzoic acid.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components comprises the following specific steps:
s1: mixing lipid and emulsifier, adding into oil phase pan, heating and stirring to 80 deg.C, dissolving completely, and keeping the temperature to obtain phase A;
s2: mixing the humectant and deionized water, adding into a water phase pot, heating and stirring to 80 deg.C, dissolving completely, and keeping the temperature to obtain phase B;
s3: preheating an emulsifying pot to 70 ℃, stirring at 40 r/min, pumping in the phase B, pumping in the phase A, and stirring for 20 min, wherein the temperature is kept at 80 ℃;
s4: adding the thickening agent into an emulsifying pot, homogenizing for 3 minutes, keeping the temperature and stirring for 20 minutes, keeping the temperature at 80 ℃, and stirring at the speed of 20 revolutions per minute;
s5: cooling to 40 deg.C, sequentially adding bitter orange flower extract, folium Camelliae sinensis extract, pineapple peel extract, folium Ginkgo extract, semen litchi extract, herba Swertiae Mileensis extract, Sargassum extract, radix Betae extract, strawberry extract and antiseptic, stirring for 10 min at the speed of 25 r/min; stirring and cooling to room temperature to obtain the whitening, moisturizing and wrinkle removing cream.
The preparation method of the extract or the extracting solution comprises the following steps:
bitter orange flower extract: cleaning bitter orange flower, drying, pulverizing, sieving, adding mixed solution of ethyl acetate and ethanol at volume ratio of 1:1, stirring, standing, performing ultrasonic extraction, filtering, and recovering solvent to obtain bitter orange flower extract;
tea leaf extract: cleaning tea leaves, drying, crushing, sieving, adding deionized water, mixing, stirring, standing, performing ultrasonic extraction, and filtering to obtain a solution, namely a tea leaf extracting solution;
pineapple peel extract: cleaning pineapple peel, draining, cutting into sections, adding a phosphate buffer solution with the pH value of 7.8, stirring in a stirrer until the mixture is crushed, centrifuging by using a freezing centrifuge, discarding the precipitate to obtain a crude bromelain extract, performing microfiltration to remove impurities, ultrafiltration concentration and separation to obtain a concentrated solution of the pineapple peel extract, performing precipitation by using an ammonium persulfate method, and finally performing vacuum freeze drying to obtain the pineapple peel extract;
ginkgo leaf extract: cleaning folium Ginkgo, oven drying, pulverizing, sieving, adding ethanol, mixing, stirring, standing, performing ultrasonic extraction, filtering, and recovering ethanol to obtain folium Ginkgo extract;
litchi seed extract: cleaning semen litchi, oven drying, pulverizing, sieving, adding ethanol, mixing, stirring, standing, performing ultrasonic extraction, filtering, and recovering ethanol to obtain semen litchi extract;
swertia mileensis extract: cleaning herba Swertiae Mileensis, oven drying, pulverizing, sieving, adding ethanol, mixing, stirring, standing, ultrasonic extracting, filtering, and recovering ethanol to obtain herba Swertiae Mileensis extract;
extracting the seaweed: cleaning seaweed, drying, pulverizing, sieving, adding deionized water, mixing, stirring, standing, ultrasonic extracting, and filtering to obtain seaweed extract;
beet root extract: cleaning, drying, crushing and sieving beet root, adding deionized water for mixing, stirring, standing, performing ultrasonic extraction, and filtering to obtain beet root extract;
strawberry extract: cleaning strawberry, oven drying, pulverizing, sieving, adding deionized water, mixing, stirring, standing, ultrasonic extracting in hot water bath, filtering, and drying to obtain strawberry extract.
Example 2:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 8% of lipid, 2.5% of emulsifier, 5.5% of humectant, 0.6% of preservative, 1.5% of thickener, 0.6% of bitter orange flower extract, 5.5% of tea extract, 0.25% of pineapple peel extract, 0.25% of ginkgo leaf extract, 0.25% of lychee seed extract, 0.25% of swertia mileensis extract, 5.5% of seaweed extract, 2.2% of beet root extract, 0.25% of strawberry extract and the balance of deionized water to 100%.
The lipid is beeswax and lecithin, and is mixed at any ratio.
The humectant is polyethylene glycol-8.
The antiseptic is methyl p-hydroxybenzoate.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components comprises the following specific steps:
s1: mixing lipid and emulsifier, adding into oil phase pan, heating and stirring to 82 deg.C, dissolving completely, and keeping the temperature to obtain phase A;
s2: mixing the humectant and deionized water, adding into a water phase pot, heating and stirring to 82 deg.C, dissolving completely, and keeping the temperature to obtain phase B;
s3: preheating an emulsifying pot to 71 ℃, stirring at the speed of 44 r/min, pumping in the phase B, pumping in the phase A, and stirring for 24 minutes, wherein the temperature is kept at 82 ℃;
s4: adding the thickening agent into an emulsifying pot, homogenizing for 4 minutes, keeping the temperature and stirring for 24 minutes, keeping the temperature at 81 ℃, and stirring at the speed of 24 revolutions per minute;
s5: cooling to 42 deg.C, sequentially adding bitter orange flower extract, folium Camelliae sinensis extract, pineapple peel extract, folium Ginkgo extract, semen litchi extract, herba Swertiae Mileensis extract, Sargassum extract, radix Betae extract, strawberry extract and antiseptic, stirring for 11 min at the speed of 26 r/min; stirring and cooling to room temperature to obtain the whitening, moisturizing and wrinkle removing cream.
The preparation method of the extract or the extract solution is the same as that of example 1.
Example 3:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 10% of lipid, 3% of emulsifier, 6% of humectant, 0.7% of preservative, 2% of thickener, 0.7% of bitter orange flower extract, 6% of tea extract, 0.3% of pineapple peel extract, 0.3% of ginkgo leaf extract, 0.3% of lychee seed extract, 0.3% of swertia mileensis extract, 6% of seaweed extract, 2.5% of beetroot extract, 0.3% of strawberry extract and the balance of deionized water to 100%.
The lipid is lecithin and squalane, and is mixed at any ratio.
The humectant is sodium hyaluronate.
The antiseptic is p-hydroxybenzoic acid and methyl p-hydroxybenzoate, and is mixed at any ratio.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components comprises the following specific steps:
s1: mixing lipid and emulsifier, adding into oil phase pan, heating and stirring to 84 deg.C, dissolving completely, and keeping the temperature to obtain phase A;
s2: mixing the humectant and deionized water, adding into a water phase pot, heating and stirring to 84 deg.C, dissolving completely, and keeping the temperature to obtain phase B;
s3: preheating an emulsifying pot to 72 ℃, stirring at the speed of 48 r/min, pumping in the phase B, pumping in the phase A, and stirring for 28 min, wherein the temperature is kept at 84 ℃;
s4: adding the thickening agent into an emulsifying pot, homogenizing for 5 minutes, keeping the temperature and stirring for 28 minutes, keeping the temperature at 82 ℃, and stirring at 28 revolutions per minute;
s5: cooling to 44 deg.C, sequentially adding bitter orange flower extract, tea leaf extract, pineapple peel extract, folium Ginkgo extract, semen litchi extract, herba Swertiae Mileensis extract, Sargassum extract, radix Betae extract, strawberry extract and antiseptic, stirring for 12 min at the speed of 27 r/min; stirring and cooling to room temperature to obtain the whitening, moisturizing and wrinkle removing cream.
The preparation method of the extract or the extract solution is the same as that of example 1.
Example 4:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 12% of lipid, 3.5% of emulsifier, 6.5% of humectant, 0.8% of preservative, 2.5% of thickener, 0.8% of bitter orange flower extract, 6.5% of tea extract, 0.35% of pineapple peel extract, 0.35% of ginkgo leaf extract, 0.35% of lychee seed extract, 0.35% of swertia mileensis extract, 6.5% of seaweed extract, 2.8% of beet root extract, 0.35% of strawberry extract and the balance of deionized water to 100%.
The lipid is squalane and isopropyl linoleate, and is mixed in any proportion.
The humectant is glycerol and polyethylene glycol-8.
The antiseptic is p-hydroxybenzoic acid.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components comprises the following specific steps:
s1: mixing lipid and emulsifier, adding into oil phase pan, heating and stirring to 86 deg.C, dissolving completely, and keeping the temperature to obtain phase A;
s2: mixing the humectant and deionized water, adding into a water phase pot, heating and stirring to 86 deg.C, dissolving completely, and keeping the temperature to obtain phase B;
s3: preheating an emulsifying pot to 73 ℃, stirring at a speed of 52 r/min, pumping in the phase B, pumping in the phase A, and stirring for 32 min, wherein the temperature is kept at 86 ℃;
s4: adding the thickening agent into an emulsifying pot, homogenizing for 3 minutes, keeping the temperature and stirring for 32 minutes, keeping the temperature at 83 ℃, and stirring at the speed of 32 revolutions per minute;
s5: cooling to 46 deg.C, sequentially adding bitter orange flower extract, folium Camelliae sinensis extract, pineapple peel extract, folium Ginkgo extract, semen litchi extract, herba Swertiae Mileensis extract, Sargassum extract, radix Betae extract, strawberry extract and antiseptic, stirring for 13 min at 28 r/min; stirring and cooling to room temperature to obtain the whitening, moisturizing and wrinkle removing cream.
The preparation method of the extract or the extract solution is the same as that of example 1.
Example 5:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 15% of lipid, 4% of emulsifier, 7% of humectant, 0.9% of preservative, 3% of thickener, 0.9% of bitter orange flower extract, 7% of tea extract, 0.4% of pineapple peel extract, 0.4% of ginkgo leaf extract, 0.4% of lychee seed extract, 0.4% of swertia mileensis extract, 7% of seaweed extract, 3% of beetroot extract, 0.4% of strawberry extract and the balance of deionized water to 100%.
The lipid is isopropyl linoleate and fatty acid yogurt fat, and is mixed at any ratio.
The humectant is polyethylene glycol-8 and sodium hyaluronate which are mixed in any proportion.
The antiseptic is methyl p-hydroxybenzoate.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components comprises the following specific steps:
s1: mixing lipid and emulsifier, adding into oil phase pan, heating and stirring to 88 deg.C, dissolving completely, and keeping the temperature to obtain phase A;
s2: mixing the humectant and deionized water, adding into a water phase pot, heating and stirring to 88 deg.C, dissolving completely, and keeping the temperature to obtain phase B;
s3: preheating an emulsifying pot to 74 ℃, stirring at the speed of 56 revolutions per minute, pumping in the phase B, pumping in the phase A, stirring for 36 minutes, and keeping the temperature at 88 ℃;
s4: adding the thickening agent into an emulsifying pot, homogenizing for 4 minutes, keeping the temperature and stirring for 36 minutes, keeping the temperature at 84 ℃, and stirring at the speed of 36 revolutions per minute;
s5: cooling to 48 ℃, sequentially adding the bitter orange flower extract, the tea extract, the pineapple peel extract, the ginkgo leaf extract, the lychee seed extract, the swertia mileensis extract, the seaweed extract, the beetroot extract, the strawberry extract and the preservative, keeping the temperature and stirring for 14 minutes at the stirring speed of 29 revolutions per minute; stirring and cooling to room temperature to obtain the whitening, moisturizing and wrinkle removing cream.
The preparation method of the extract or the extract solution is the same as that of example 1.
Example 6:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 18% of lipid, 4.5% of emulsifier, 7.5% of humectant, 1.0% of preservative, 3.5% of thickener, 1.0% of bitter orange flower extract, 7.5% of tea extract, 0.45% of pineapple peel extract, 0.45% of ginkgo leaf extract, 0.45% of lychee seed extract, 0.45% of swertia mileensis extract, 7.5% of seaweed extract, 3.2% of beet root extract, 0.5% of strawberry extract and the balance of deionized water to 100%.
The lipid is castor oil, beeswax and lecithin, and is mixed at any ratio.
The humectant is glycerin and sodium hyaluronate which are mixed in any proportion.
The antiseptic is p-hydroxybenzoic acid and methyl p-hydroxybenzoate, and is mixed at any ratio.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components comprises the following specific steps:
s1: mixing lipid and emulsifier, adding into oil phase pan, heating and stirring to 90 deg.C, dissolving completely, and keeping the temperature to obtain phase A;
s2: mixing the humectant and deionized water, adding into a water phase pot, heating and stirring to 90 deg.C, dissolving completely, and keeping the temperature to obtain phase B;
s3: preheating an emulsifying pot to 75 ℃, stirring at the speed of 60 r/min, pumping in the phase B, pumping in the phase A, and stirring for 40 min, wherein the temperature is kept at 90 ℃;
s4: adding the thickening agent into an emulsifying pot, homogenizing for 5 minutes, keeping the temperature and stirring for 40 minutes, keeping the temperature at 85 ℃, and stirring at the speed of 40 revolutions per minute;
s5: cooling to 50 deg.C, sequentially adding bitter orange flower extract, folium Camelliae sinensis extract, pineapple peel extract, folium Ginkgo extract, semen litchi extract, herba Swertiae Mileensis extract, Sargassum extract, radix Betae extract, strawberry extract and antiseptic, stirring for 15 min at the speed of 30 r/min; stirring and cooling to room temperature to obtain the whitening, moisturizing and wrinkle removing cream.
The preparation method of the extract or the extract solution is the same as that of example 1.
Example 7:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 20% of lipid, 5% of emulsifier, 8% of humectant, 1.1% of preservative, 4% of thickener, 1.1% of bitter orange flower extract, 8% of tea extract, 0.5% of pineapple peel extract, 0.5% of ginkgo leaf extract, 0.5% of lychee seed extract, 0.5% of swertia mileensis extract, 8% of seaweed extract, 3.5% of beetroot extract, 0.5% of strawberry extract and the balance of deionized water to 100%.
The lipid is castor oil, beeswax, lecithin and squalane, and is mixed at any ratio.
The humectant is glycerol, polyethylene glycol-8 and sodium hyaluronate which are mixed in any proportion.
The antiseptic is p-hydroxybenzoic acid.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components is the same as that of example 1.
Example 8:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 22% of lipid, 5.5% of emulsifier, 8.5% of humectant, 1.2% of preservative, 4.5% of thickener, 1.2% of bitter orange flower extract, 8.5% of tea extract, 0.55% of pineapple peel extract, 0.55% of ginkgo leaf extract, 0.55% of lychee seed extract, 0.55% of swertia mileensis extract, 8.5% of seaweed extract, 3.8% of beet root extract, 0.55% of strawberry extract and deionized water to make up 100%.
The lipid is beeswax, lecithin, squalane, isopropyl linoleate and fatty acid sour cream, and is mixed in any proportion.
The humectant is glycerol.
The antiseptic is p-hydroxybenzoic acid.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components is the same as that of example 1.
Example 9:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 25% of lipid, 6% of emulsifier, 9% of humectant, 1.3% of preservative, 5% of thickener, 1.4% of bitter orange flower extract, 9% of tea extract, 0.6% of pineapple peel extract, 0.6% of ginkgo leaf extract, 0.6% of lychee seed extract, 0.6% of swertia mileensis extract, 9% of seaweed extract, 4% of beetroot extract, 0.6% of strawberry extract and the balance of deionized water to 100%.
The lipid is castor oil, beeswax, lecithin, squalane, isopropyl linoleate and fatty acid yoghurt, and is mixed in any proportion.
The humectant is glycerol, polyethylene glycol-8 and sodium hyaluronate which are mixed in any proportion.
The antiseptic is p-hydroxybenzoic acid and methyl p-hydroxybenzoate, and is mixed at any ratio.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components is the same as that of example 1.
Example 10:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 28% of lipid, 7% of emulsifier, 9.5% of humectant, 1.4% of preservative, 1.8% of thickener, 1.5% of bitter orange flower extract, 9.5% of tea extract, 0.7% of pineapple peel extract, 0.7% of ginkgo leaf extract, 0.7% of lychee seed extract, 0.7% of swertia mileensis extract, 9.5% of seaweed extract, 4.2% of beet root extract, 0.7% of strawberry extract and the balance of deionized water to 100%.
The lipid is beeswax and lecithin, and is mixed at any ratio.
The humectant is polyethylene glycol-8.
The antiseptic is p-hydroxybenzoic acid.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components is the same as that of example 1.
Example 11:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 30% of lipid, 8% of emulsifier, 10% of humectant, 1.6% of preservative, 2.8% of thickener, 1.6% of bitter orange flower extract, 10% of tea extract, 0.8% of pineapple peel extract, 0.8% of ginkgo leaf extract, 0.8% of lychee seed extract, 0.8% of swertia mileensis extract, 10% of seaweed extract, 4.5% of beet root extract, 0.8% of strawberry extract and the balance of deionized water to 100%.
The lipid is squalane, isopropyl linoleate and fatty acid yoghurt, and is mixed in any proportion.
The humectant is sodium hyaluronate.
The antiseptic is p-hydroxybenzoic acid.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components is the same as that of example 1.
Example 12:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 32% of lipid, 9% of emulsifier, 5.8% of humectant, 1.8% of preservative, 3.8% of thickener, 1.8% of bitter orange flower extract, 5.8% of tea extract, 0.9% of pineapple peel extract, 0.9% of ginkgo leaf extract, 0.9% of lychee seed extract, 0.9% of swertia mileensis extract, 5.8% of seaweed extract, 4.8% of beet root extract, 0.9% of strawberry extract and the balance of deionized water to 100%.
The lipid is isopropyl linoleate and fatty acid yogurt fat, and is mixed at any ratio.
The humectant is sodium hyaluronate.
The antiseptic is methyl p-hydroxybenzoate.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components is the same as that of example 1.
Example 13:
the whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is prepared from the following raw materials in percentage by weight: 35% of lipid, 10% of emulsifier, 6.8% of humectant, 2% of preservative, 4.8% of thickener, 2.0% of bitter orange flower extract, 6.8% of tea extract, 1% of pineapple peel extract, 1% of ginkgo leaf extract, 1% of lychee seed extract, 1% of swertia mileensis extract, 6.8% of seaweed extract, 5% of beetroot extract, 1% of strawberry extract and the balance of deionized water to 100%.
The lipid is lecithin and squalane, and is mixed at any ratio.
The humectant is glycerol.
The antiseptic is methyl p-hydroxybenzoate.
The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components is the same as that of example 1.
Test example 1
The whitening, moisturizing and wrinkle-removing cream prepared according to the above example 5 was prepared by omitting only the extract of neroli, only the extract of tea leaves, only the extract of pineapple peel, only the extract of ginkgo leaves, only the extract of lychee seeds, only the extract of swertia mileensis, only the extract of seaweed, only the extract of beetroot and only the extract of strawberry, respectively, and evaluated as a comparison of test examples 1 to 9 with example 5, example 7, example 9 and example 11, respectively.
Skin tests were performed on 20 female subjects in each of the 13 groups, with subjects having healthy skin and no history of skin allergy. The face of a subject is cleaned, a proper amount of cream is applied to the palm of the hand, the cream is uniformly smeared on the facial skin, the skin is gently massaged until the cream is completely absorbed, the cream is used once every morning and evening and is continuously used for one month, the change of the fair degree of the facial skin of the subject is observed, the skin is checked at least once every week to know whether systemic and local adverse reactions exist, and the result is detailed in table 1.
Evaluation criteria:
□: the effect was considered to be good in 18 out of 20.
O: the effect was considered good in 15-17 out of 20.
And (delta): 10-14 out of 20 considered good results.
Gamma rays: less than 10 out of 20 persons were considered to be effective.
According to the results of table 1, the creams provided in examples 7, 9 and 11 have very good whitening effects on facial skin of women, so that the formulations of the components except for the cream adjuvant according to the present invention have relatively good skin whitening effects, and according to the effect analysis of table 1, the formulations of test examples 1-9 cannot achieve very good whitening effects due to the absence of one of the natural product extracts of the present invention. Especially, the whitening effect is poor when the neroli extract or the pineapple peel extract is absent, because the neroli extract has the characteristic of enhancing cell activity, can help cell regeneration, increase skin elasticity, resist aging, resist bacteria, soften skin, calm, whiten, moisturize, lighten spots, eliminate uneven and dull skin color and the like; the pineapple peel extract is rich in a large amount of bromelain, so that the pineapple peel extract can promote skin metabolism, reduce the phenomenon of deep skin color caused by sunshine and ensure that the skin is maintained in a good white and tender state.
Test example 2
The whitening, moisturizing and wrinkle-removing cream prepared according to the above example 5 was prepared by omitting only the extract of neroli, only the extract of tea leaves, only the extract of pineapple peel, only the extract of ginkgo leaves, only the extract of lychee seeds, only the extract of swertia mileensis, only the extract of seaweed, only the extract of beetroot and only the extract of strawberry, respectively, and evaluated as a comparison of test examples 1 to 9 with example 5, example 7, example 9 and example 11, respectively.
Skin tests were performed on 20 female subjects in each of the 13 groups, with subjects having healthy skin and no history of skin allergy. The face of a subject is cleaned, a proper amount of face cream is applied to the palm of the hand, the face cream is uniformly smeared on the face skin, the face cream is gently massaged until the face cream is completely absorbed, the face cream is used once every morning and evening, the face cream is used for one month continuously, the change of the moisture retention degree of the face skin of the subject is observed, the face cream is checked at least once every week to know whether systemic and local adverse reactions exist, and the results are detailed in table 2.
Evaluation criteria:
□: the effect was considered to be good in 18 out of 20.
O: the effect was considered good in 15-17 out of 20.
And (delta): 10-14 out of 20 considered good results.
Gamma rays: less than 10 out of 20 persons were considered to be effective.
According to the results shown in table 2, the creams provided in examples 5, 7, 9 and 11 have very good moisturizing effect on the facial skin of women, so the formula of the components except the cream adjuvant has relatively good moisturizing effect; according to the effect analysis of table 2, the formulas of test examples 1-9 could not achieve a good moisturizing effect due to the absence of one of the natural product extracts of the present invention; especially, when the tea extract, the beetroot extract or the strawberry extract is lacked, the moisturizing effect is poor, because the tea extract contains rich tea polyphenol, the effects of resisting bacteria, activating skin, moisturizing, resisting inflammation, healing wounds, improving the toughness of capillary vessels and the like are achieved; the beet root extract is rich in betaine and has strong moisture retention; the strawberry extract is rich in galactaric acid and has good moisturizing effect.
Test example 3
The whitening, moisturizing and wrinkle-removing cream prepared according to the above example 5 was prepared by omitting only the extract of neroli, only the extract of tea leaves, only the extract of pineapple peel, only the extract of ginkgo leaves, only the extract of lychee seeds, only the extract of swertia mileensis, only the extract of seaweed, only the extract of beetroot and only the extract of strawberry, respectively, and evaluated as a comparison of test examples 1 to 9 with example 5, example 7, example 9 and example 11, respectively.
Skin tests were performed on 20 female subjects in each of the 13 groups, with subjects having healthy skin and no history of skin allergy. The face of a subject is cleaned, a proper amount of face cream is applied to the palm of the hand, the face cream is uniformly applied to the face skin, the face skin is gently massaged until the face cream is completely absorbed, the face cream is used once a day in the morning and at night, the wrinkle reduction condition of the face skin of the subject is observed after the face cream is continuously used for one month, the face skin of the subject is inspected at least once a week to know whether systemic adverse reactions and local adverse reactions exist, and the results are detailed in.
Evaluation criteria:
□: more than 18 of 20 people considered significant effects.
O: the effect is considered to be obvious by 15-17 of 20 persons.
And (delta): the significant effect was considered to be apparent in 10-14 out of 20.
Gamma rays: less than 10 out of 20 people are considered to have significant effects.
According to the results shown in table 3, the creams provided in examples 5, 9 and 11 have very good wrinkle removing effect on female facial skin, so that the formula of each component except the cream adjuvant has relatively good wrinkle removing effect in the present invention; according to the effect analysis of table 3, the formulas of test examples 1-9 could not achieve good wrinkle removing effect due to the lack of any one of the natural product extracts of the present invention, especially the poor wrinkle removing effect when the lychee seed extract, the swertia mileensis extract or the seaweed extract is lacked, because the lychee seed extract is rich in xanthorrhizol, palmitic acid and other elements, the extract can enhance cell activity, prolong cell life, promote proliferation of human fibroblasts, and has wrinkle removing effect; the herba Swertiae Mileensis extract contains caryophyllin, and has effects of promoting collagen production, reducing elastin decomposition, activating skin, resisting aging and removing wrinkle; the Sargassum extractive solution is rich in fucose, is beneficial for maintaining and generating elastic fiber, and can be used for resisting wrinkle and resisting aging.
The foregoing is only a preferred embodiment of the present invention, and it should be noted that, for those skilled in the art, various changes and modifications can be made without departing from the overall concept of the present invention, and these should also be considered as the protection scope of the present invention.
Claims (6)
1. The whitening, moisturizing and wrinkle-removing facial cream rich in natural product extract components is characterized in that: the material is prepared from the following raw materials in percentage by weight: 5 to 35 percent of lipid, 2 to 10 percent of emulsifier, 5 to 10 percent of humectant, 0.5 to 2 percent of preservative, 1 to 5 percent of thickener, 0.5 to 2 percent of bitter orange flower extract, 5 to 10 percent of tea extract, 0.2 to 1 percent of pineapple peel extract, 0.2 to 1 percent of ginkgo leaf extract, 0.2 to 1 percent of lychee seed extract, 0.2 to 1 percent of swertia mileensis extract, 5 to 10 percent of seaweed extract, 2 to 5 percent of beet root extract, 0.2 to 1 percent of strawberry extract and deionized water to 100 percent.
2. The whitening, moisturizing and wrinkle-removing cream rich in natural product extract components as claimed in claim 1, characterized in that: the lipid is at least two of castor oil, beeswax, lecithin, squalane, isopropyl linoleate, and fatty acid yogurt fat.
3. The whitening, moisturizing and wrinkle-removing cream rich in natural product extract components as claimed in claim 1, characterized in that: the humectant is at least one of glycerol, polyethylene glycol-8 and sodium hyaluronate.
4. The whitening, moisturizing and wrinkle-removing cream rich in natural product extract components as claimed in claim 1, characterized in that: the preservative is one or two of p-hydroxybenzoic acid or methyl p-hydroxybenzoate.
5. The method for preparing the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components as claimed in claim 1, wherein the method comprises the following steps: the method comprises the following specific steps:
s1: mixing lipid and emulsifier, adding into oil phase pan, heating and stirring to 80-90 deg.C, dissolving completely, and keeping the temperature to obtain phase A;
s2: mixing humectant and deionized water, adding into water phase pot, heating and stirring to 80-90 deg.C, dissolving completely, and keeping the temperature to obtain phase B;
s3: preheating an emulsifying pot to 70-75 ℃, stirring at the speed of 40-60 r/min, pumping in the phase B, pumping in the phase A, stirring for 20-40 min, and keeping the temperature at 80-90 ℃;
s4: adding the thickening agent into an emulsifying pot, homogenizing for 3-5 minutes, keeping the temperature and stirring for 20-40 minutes, keeping the temperature at 80-85 ℃, and stirring at the speed of 20-40 revolutions per minute;
s5: cooling to 40-50 deg.C, sequentially adding bitter orange flower extract, folium Camelliae sinensis extract, pineapple peel extract, folium Ginkgo extract, semen litchi extract, herba Swertiae Mileensis extract, Sargassum extract, radix Betae extract, strawberry extract and antiseptic, stirring at 25-30 r/min under heat preservation for 10-15 min; stirring and cooling to room temperature to obtain the whitening, moisturizing and wrinkle removing cream.
6. The preparation method of the whitening, moisturizing and wrinkle-removing cream rich in natural product extract components as claimed in claim 5, is characterized in that: the preparation method of the extract or the extracting solution comprises the following steps:
bitter orange flower extract: cleaning bitter orange flower, drying, pulverizing, sieving, adding mixed solution of ethyl acetate and ethanol at volume ratio of 1:1, stirring, standing, performing ultrasonic extraction, filtering, and recovering solvent to obtain bitter orange flower extract;
tea leaf extract: cleaning tea leaves, drying, crushing, sieving, adding deionized water, mixing, stirring, standing, performing ultrasonic extraction, and filtering to obtain a solution, namely a tea leaf extracting solution;
pineapple peel extract: cleaning pineapple peel, draining, cutting into sections, adding a phosphate buffer solution with the pH value of 7.8, stirring in a stirrer until the mixture is crushed, centrifuging by using a freezing centrifuge, discarding the precipitate to obtain a crude bromelain extract, performing microfiltration to remove impurities, ultrafiltration concentration and separation to obtain a concentrated solution of the pineapple peel extract, performing precipitation by using an ammonium persulfate method, and finally performing vacuum freeze drying to obtain the pineapple peel extract;
ginkgo leaf extract: cleaning folium Ginkgo, oven drying, pulverizing, sieving, adding ethanol, mixing, stirring, standing, performing ultrasonic extraction, filtering, and recovering ethanol to obtain folium Ginkgo extract;
litchi seed extract: cleaning semen litchi, oven drying, pulverizing, sieving, adding ethanol, mixing, stirring, standing, performing ultrasonic extraction, filtering, and recovering ethanol to obtain semen litchi extract;
swertia mileensis extract: cleaning herba Swertiae Mileensis, oven drying, pulverizing, sieving, adding ethanol, mixing, stirring, standing, ultrasonic extracting, filtering, and recovering ethanol to obtain herba Swertiae Mileensis extract;
extracting the seaweed: cleaning seaweed, drying, pulverizing, sieving, adding deionized water, mixing, stirring, standing, ultrasonic extracting, and filtering to obtain seaweed extract;
beet root extract: cleaning, drying, crushing and sieving beet root, adding deionized water for mixing, stirring, standing, performing ultrasonic extraction, and filtering to obtain beet root extract;
strawberry extract: cleaning strawberry, oven drying, pulverizing, sieving, adding deionized water, mixing, stirring, standing, ultrasonic extracting in hot water bath, filtering, and drying to obtain strawberry extract.
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| CN111329800A (en) * | 2020-02-25 | 2020-06-26 | 广东丸美生物技术股份有限公司 | Citrus aurantium flower extract, preparation method and application thereof, and cosmetic containing same |
| CN111228187A (en) * | 2020-04-07 | 2020-06-05 | 王跃 | Whitening and moisturizing emulsion suitable for oily skin and preparation method thereof |
| CN114042016A (en) * | 2021-11-26 | 2022-02-15 | 上海琴馨文化科技有限公司 | Ginkgo leaf extract face cream with multiple effects and preparation method thereof |
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