CN110384644A - Compact sleep mask of a kind of skin whitening, moisturizing rich in natural product extraction ingredient and preparation method thereof - Google Patents
Compact sleep mask of a kind of skin whitening, moisturizing rich in natural product extraction ingredient and preparation method thereof Download PDFInfo
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- CN110384644A CN110384644A CN201910814176.3A CN201910814176A CN110384644A CN 110384644 A CN110384644 A CN 110384644A CN 201910814176 A CN201910814176 A CN 201910814176A CN 110384644 A CN110384644 A CN 110384644A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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Abstract
The present invention relates to cosmetic fields, specifically disclose a kind of compact sleep mask of the skin whitening, moisturizing rich in natural product extraction ingredient；The compact water surface facial mask of the skin whitening, moisturizing is made of the raw material of following weight percent: bigarabe flower extract 0.5%~2%, tea extract 5%~10%, sponge gourd seed extract 0.5%~3%, garden burnet root extracting solution 5%~10%, Semen Litchi extract 0.2%~1%, Herba Swertiae Mileensis extract 0.2%~1%, mango leaf extract 0.5%~3%, star-spangled banner conopsea extraction 0.5%~3%, Radix Notoginseng root extract 0.1%~2%, lipid 5%~10%, emulsifier 2%~8%, moisturizer 5%~30%, preservative 0.5%~2%, thickener 1%~3%, deionized water are mended to 100%.The facial mask can desalinate epidermal pigment, inhibit melanin to be formed, have effects that whitening, nti-freckle, moisturizing, moisturizing.
Description
Technical field
The present invention relates to cosmetic technical fields, and in particular to a kind of skin whitening, moisturizing rich in natural product extraction ingredient is tight
Cause sleep mask and preparation method thereof.
Background technique
Nowadays problem of environmental pollution is serious, and the operating pressure of people is big, lives irregular, leads to more and more application on human skin
There is the problems such as dry, coarse, intensely dark, melanin deposition, color spot, cutis laxa, microgroove, therefore, more and more people
Need the skin care item of skin whitening, moisturizing effect to protect and improve oneself skin.
The content of melanin is the important factor in order of the skin color depth, and the content of melanin is more, the colour of skin of skin
It is more black.Melanin is by tyrosine under the catalysis of tyrosinase, through generating a series of metabolic response shapes such as DOPA, DOPA quinone
At, therefore, inhibiting tyrosinase activity is the key that in place of reducing melanin production.In addition, leading to the most common of aging
Endogenous Some Circulating Factors are free radicals, so particularly important for anti-aging, removing free radical.It finds and stablizes, effectively and to people
Native tyrosine enzyme inhibitor, the powerful antioxidant that body has no adverse reaction have become the trend of cosmetic industry research, with natural
Plant extracts is the Pure natural cosmetic of functional component because of traction with higher and environmental friendliness, therefore is become
The trend of cosmetic product exploitation.But skin care item market, whitening and skin-protecting product common problem are that effect is single at present,
The resultant effect of skin whitening, moisturizing anti-wrinkle is bad, and contains irritant chemical component mostly, larger to skin irritation.
Summary of the invention
In view of the problems of the existing technology and it is insufficient, the object of the present invention is to provide one kind rich in natural product extraction at
The compact sleep mask of skin whitening, moisturizing and preparation method thereof divided.
To realize goal of the invention, The technical solution adopted by the invention is as follows:
The compact sleep mask of a kind of skin whitening, moisturizing rich in natural product extraction ingredient, by the raw material of following weight percent
It is made: bigarabe flower extract 0.5%~2%, tea extract 5%~10%, sponge gourd seed extract 0.5%~3%, garden burnet
Root extracting solution 5%~10%, Semen Litchi extract 0.2%~1%, Herba Swertiae Mileensis extract 0.2%~1%, mango leaf extract
Object 0.5%~3%, star-spangled banner conopsea extraction 0.5%~3%, Radix Notoginseng root extract 0.1%~2%, lipid 5%~10%, cream
Agent 2%~8%, moisturizer 5%~30%, preservative 0.5%~2%, thickener 1%~3%, deionized water mend to
100%.
According to the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient, it is preferable that the bigarabe
Flower extract is cleaned, drying, is crushed the preparation method comprises the following steps: bigarabe is spent, and addition Extraction solvent is uniformly mixed, and ultrasonic extraction mentions
It takes liquid to be filtered, recycle Extraction solvent processing to get bigarabe flower extract, wherein the Extraction solvent is ethyl acetate and second
The alcohol mixture that 1:1 is mixed to get by volume.
According to the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient, it is preferable that the tealeaves
Extracting solution the preparation method comprises the following steps: by tealeaves cleaning, drying, crush, add water refluxing extraction, extracting solution is mentioned through filtering to get tealeaves
Take object；The garden burnet root extracting solution the preparation method comprises the following steps: by garden burnet root cleaning, drying, crush, add water refluxing extraction, extracting solution
It is filtered to get garden burnet root extract.
According to the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient, it is preferable that the sponge gourd
Seed extract the preparation method comprises the following steps: by Seeds of Luffa cylindrica cleaning, drying, crush, be added ethyl alcohol be uniformly mixed, ultrasonic extraction, extracting solution
It filtered, recycle alcohol treatment to get sponge gourd seed extract；The Semen Litchi extract the preparation method comprises the following steps: semen litchi is clear
It washes, dry, crush, ethyl alcohol is added and is uniformly mixed, ultrasonic extraction, extracting solution filtered, recycles alcohol treatment mentions to get semen litchi
Take object；The Herba Swertiae Mileensis extract the preparation method comprises the following steps: by swertia mileensis cleaning, drying, crush, be added ethyl alcohol be uniformly mixed, surpass
Sound extracts, and extracting solution is filtered, recycles alcohol treatment to get Herba Swertiae Mileensis extract；The preparation side of the mango leaf extract
Method are as follows: by the cleaning of mango leaf, drying, crush, ethyl alcohol is added and is uniformly mixed, ultrasonic extraction, extracting solution is filtered, recycles ethyl alcohol
Processing is to get mango leaf extract；The preparation method of the star-spangled banner conopsea extraction is equal are as follows: by American ginseng cleaning, drying, powder
It is broken, ethyl alcohol is added and is uniformly mixed, ultrasonic extraction, extracting solution is filtered, recycles alcohol treatment to get star-spangled banner conopsea extraction.
According to the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient, it is preferable that the Radix Notoginseng
Root extract the preparation method comprises the following steps: by Roots of Panax Notoginseng cleaning, drying, crush, be added methanol be uniformly mixed, ultrasonic extraction, extracting solution
It filtered, recycle methyl alcohol process to get Radix Notoginseng root extract.
According to the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient, it is preferable that the rouge
Matter is propyloxy phenyl base dimethyl silicone polymer, in ring five dimethyl silicone polymer, cyclohexasiloxane, dimethyl silicone polymer
It is one or more.
According to the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient, it is preferable that the moisturizing
Agent is butanediol, glycerol, propylene glycol, Sodium Hyaluronate, 1,2- hexylene glycol, panthenol, xylitol, soluble collagen, hydrolytic collagen
At least one of.
According to the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient, it is preferable that the anti-corrosion
Agent is one or both of P-hydroxybenzoic acid, methyl p-hydroxybenzoate；The emulsifier is MONTANOV 68
(production of Seppic company, main chemical compositions C16-C18Alkylol and C16-C18Alkyl heteroside)；The thickener is
Simulgel 600 (production of Seppic company).
The preparation method of the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient, including following step
It is rapid:
(1) lipid, emulsifier, moisturizer and deionized water are mixed, stirring is warming up to 80~90 DEG C, keeps the temperature 5~20min
It is uniform to each stock dispersion, obtain mixture；
(2) mixture made from step (1) is cooled to 45~55 DEG C, then successively into mixture be added thickener,
Preservative, bigarabe flower extract, tea extract, sponge gourd seed extract, garden burnet root extracting solution, Semen Litchi extract, swertia mileensis
Extract, mango leaf extract, star-spangled banner conopsea extraction, Radix Notoginseng root extract keep the temperature 5~10min of homogeneous, then stirring cooling
The compact sleep mask of skin whitening, moisturizing of natural product extraction ingredient is rich in room temperature.
The main active of skin whitening, moisturizing compact sleep mask of the present invention rich in natural product extraction ingredient are as follows: bigarabe
Flower extract, tea extract, sponge gourd seed extract, garden burnet root extracting solution, Semen Litchi extract, Herba Swertiae Mileensis extract, mango
Leaf extract, star-spangled banner conopsea extraction, Radix Notoginseng root extract.The primary efficacy of each active constituent is as follows:
Bigarabe flower: bigarabe flower has the characteristic of enhancing cellular activity power, can help cytothesis, increases skin elasticity, resists
Aging, antibacterial, soft skin, calm, whitening, moisturizing, light spot, to eliminate the colour of skin uneven and obscure and other effects.The production of its extract
Skin care item be suitable for stemness, sensibility and adult form skin, it is also helpful for other skin problems.
Tealeaves: tea polyphenols rich in tealeaves, tea polyphenols are not only good oil antioxidant, also have anti-
Bacterium, skin-active, moisturizing, anti-inflammatory, healing of wound, enhancement capillary toughness and other effects, while still preferable ultraviolet filter,
The formation that dermal melanin can be reduced, can remove removing freckle and senile plaque, reach skin care purpose.
Seeds of Luffa cylindrica: fatty acid abundant (palmitinic acid, stearic acid, oleic acid, linoleic acid etc.), carbohydrate, ammonia are rich in Seeds of Luffa cylindrica
Base acid, triterpene substance and saualane, wherein saualane is a kind of important cosmetic material.It is used to manufacture skin care item tool
There have to be good to skin compatibility, may additionally facilitate the metabolism of skin, keeps skin gloss flexible.
Garden burnet root: being rich in triterpene saponin componds garden burnet glycosides in garden burnet root, garden burnet glycosides can effectively facilitate collagen
It generates, keeps skin elasticity, its extract, which is added in skin care item, can be improved wrinkle resistance.
Semen litchi: semen litchi surface brown to brownish red slightly has gloss, has irregular recessed gap and fine wrinkle, is rich in xanthorrhiza
The elements such as pure and mild palmitinic acid, extract can enhance cell activity, extend cell life, promote the increasing of human fiber sprout cell
It grows, has effects that crease-resistant.
Swertia mileensis: swertia mileensis is a kind of annual herb, therefrom separation and Extraction caryophyllin, China pink can be known as certain surface
Activity has assistance left and right to the stabilization of emulsion, can also promote the generation of collagen, reduce the decomposition of elastin laminin, have
The anti-ageing crease-resistant effect of skin-active also has certain moisture-keeping efficacy.
Mango leaf: the extractable mangiferin out of mango leaf, mangiferin have stronger anti-oxidant vigor and delay to decline
Old effect, also has anti-inflammatory effect, can improve the barrier function of skin, for the anti-ageing crease-resistant of skin, also act as makeup
The whitening agent of product.
American ginseng: rich in personal saponin(e in American ginseng, ginsenoside easily penetrates skin surface and is dermal absorption, can expand
Peripheral vessel promotes the proliferation of fiber-like cell, makes skin tissue regeneration, can stimulate the conjunction of elastin laminin peptone in skin corium
At；It can also be in inoxidizability by the activity of the oxidoreducing enzyme in human activin, prevent the aging of skin.
Roots of Panax Notoginseng: rich in monosaccharide and the polysaccharide such as rhamnose, xylose, 16 kinds of amino acid, Quercetin and saponin(e etc. in Roots of Panax Notoginseng
Substance, Stratum Corneum cell Proliferation have facilitation, can also increase humidity of skin, have excellent skin-active, crease-resistant and moisturizing function
Effect.
Compared with prior art, the positive beneficial effect that the present invention obtains are as follows:
(1) the compact sleep mask of skin whitening, moisturizing disclosed by the invention using natural products bigarabe flower, tealeaves, Seeds of Luffa cylindrica,
Elm root, semen litchi, swertia mileensis, mango leaf, American ginseng, Roots of Panax Notoginseng extract (liquid) be effective component, it is natural, safety is stingless
Swash, mutually act synergistically between each component, by promoting the proliferation of human fiber sprout cell, promotes the generation of collagen, reduce
The decomposition of elastin laminin can effectively promote the compact effect of sleep mask；By accelerating the metabolism of keratoderma, help thin
Born of the same parents' regeneration, promotes skin metabolism, inhibits tyrosinase activity, and effectively melanin is inhibited to be formed, and nutritional ingredient is promoted to go deep into
Inside skin, it can achieve the purpose that whitening effect replenishing water and preserving moisture.Therefore, the compact sleep mask of skin whitening, moisturizing of the invention passes through
By each herb extract reasonable compatibility, synergistic effect is played between each ingredient, achieves significant whitening, nti-freckle, moisturizing, compact
Cooperative synergism effect, be a to have effects that excellent whitening, moisturizing, moisturizing, compact sleep mask.
(2) the compact sleep mask of skin whitening, moisturizing of the invention is free of irritation chemical component, stingless to human skin safety
Swash, is easily absorbed by the skin.
(3) the compact sleep mask preparation method of skin whitening, moisturizing of the present invention is simple, is convenient for industrialized production, easy to spread to answer
With.
Specific embodiment
Below by way of specific embodiment, invention is further described in detail, but does not limit the scope of the invention.
Embodiment 1:
The compact sleep mask of a kind of skin whitening, moisturizing rich in natural product extraction ingredient, by the raw material of following weight percent
It is made: bigarabe flower extract 1.5%, tea extract 8%, sponge gourd seed extract 2.0%, garden burnet root extracting solution 8%, semen litchi
Extract 0.8%, Herba Swertiae Mileensis extract 0.7%, mango leaf extract 2.0%, star-spangled banner conopsea extraction 2.0%, Roots of Panax Notoginseng mentions
Take object 1.5%, lipid 8%, emulsifier 5%, moisturizer 20%, preservative 1.2%, thickener 2%, deionized water mend to
100%.Wherein, the lipid is propyloxy phenyl base dimethyl silicone polymer；The moisturizer is glycerol；The emulsifier is
MONTANOV 68；The thickener is Simulgel 600；The preservative is P-hydroxybenzoic acid.
The preparation method of the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient the following steps are included:
(1) lipid, emulsifier, moisturizer and deionized water are mixed, stirring is warming up to 85 DEG C, heat preservation 10min to each original
Material is uniformly dispersed, and obtains mixture；
(2) mixture made from step (1) is cooled to 50 DEG C, thickener, anti-corrosion is then successively added into mixture
Agent, bigarabe flower extract, tea extract, sponge gourd seed extract, garden burnet root extracting solution, Semen Litchi extract, swertia mileensis extract
Object, mango leaf extract, star-spangled banner conopsea extraction, Radix Notoginseng root extract keep the temperature homogeneous 6min, and then stirring is cooled to room temperature,
Up to the compact sleep mask of skin whitening, moisturizing for being rich in natural product extraction ingredient.
Wherein, extract/extracting solution preparation method is specific as follows:
Bigarabe flower extract is cleaned, drying, is crushed the preparation method comprises the following steps: bigarabe is spent, and addition Extraction solvent is uniformly mixed,
Ultrasonic extraction, extracting solution are filtered, recycle Extraction solvent processing to get bigarabe flower extract, wherein the Extraction solvent is second
Acetoacetic ester and the ethyl alcohol mixture that 1:1 is mixed to get by volume.
Tea extract the preparation method comprises the following steps: by tealeaves cleaning, drying, crush, add water refluxing extraction, extracting solution passes through
Filter is to get tea extract.
Garden burnet root extracting solution the preparation method comprises the following steps: by the cleaning of garden burnet root, drying, crush, add water refluxing extraction, extracting solution warp
Filtering is to get garden burnet root extract.
Sponge gourd seed extract the preparation method comprises the following steps: by Seeds of Luffa cylindrica cleaning, drying, crush, be added ethyl alcohol be uniformly mixed, ultrasound
It extracts, extracting solution is filtered, recycles alcohol treatment to get sponge gourd seed extract.
Semen Litchi extract the preparation method comprises the following steps: by semen litchi cleaning, drying, crush, be added ethyl alcohol be uniformly mixed, ultrasound
It extracts, extracting solution is filtered, recycles alcohol treatment to get Semen Litchi extract.
Herba Swertiae Mileensis extract the preparation method comprises the following steps: by swertia mileensis cleaning, drying, crush, be added ethyl alcohol be uniformly mixed, ultrasound
It extracts, extracting solution is filtered, recycles alcohol treatment to get Herba Swertiae Mileensis extract.
Mango leaf extract the preparation method comprises the following steps: by mango leaf cleaning, drying, crush, be added ethyl alcohol be uniformly mixed,
Ultrasonic extraction, extracting solution are filtered, recycle alcohol treatment to get mango leaf extract.
The preparation method of star-spangled banner conopsea extraction is equal are as follows: by American ginseng cleaning, drying, crushes, ethyl alcohol is added and is uniformly mixed, surpasses
Sound extracts, and extracting solution is filtered, recycles alcohol treatment to get star-spangled banner conopsea extraction.
Radix Notoginseng root extract the preparation method comprises the following steps: by Roots of Panax Notoginseng cleaning, drying, crush, be added methanol be uniformly mixed, ultrasound
It extracts, extracting solution is filtered, recycles methyl alcohol process to get Radix Notoginseng root extract.
Embodiment 2:
The compact sleep mask of a kind of skin whitening, moisturizing rich in natural product extraction ingredient, by the raw material of following weight percent
It is made: bigarabe flower extract 1.2%, tea extract 6%, sponge gourd seed extract 1.5%, garden burnet root extracting solution 5%, semen litchi
Extract 0.5%, Herba Swertiae Mileensis extract 0.4%, mango leaf extract 1%, star-spangled banner conopsea extraction 1.5%, Roots of Panax Notoginseng extract
Object 1%, lipid 9%, emulsifier 7%, moisturizer 15%, preservative 1%, thickener 1.5%, deionized water are mended to 100%.Its
In, the lipid is propyloxy phenyl base dimethyl silicone polymer；The moisturizer is glycerol；The emulsifier is MONTANOV
68；The thickener is Simulgel 600；The preservative is P-hydroxybenzoic acid.
The preparation method of the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient, including following step
It is rapid:
(1) lipid, emulsifier, moisturizer and deionized water are mixed, stirring is warming up to 80 DEG C, heat preservation 20min to each original
Material is uniformly dispersed, and obtains mixture；
(2) mixture made from step (1) is cooled to 45 DEG C, thickener, anti-corrosion is then successively added into mixture
Agent, bigarabe flower extract, tea extract, sponge gourd seed extract, garden burnet root extracting solution, Semen Litchi extract, swertia mileensis extract
Object, mango leaf extract, star-spangled banner conopsea extraction, Radix Notoginseng root extract keep the temperature homogeneous 10min, and then stirring is cooled to room temperature,
Up to the compact sleep mask of skin whitening, moisturizing for being rich in natural product extraction ingredient.
Wherein, extract/extracting solution preparation method is same as Example 1.
Embodiment 3:
The compact sleep mask of a kind of skin whitening, moisturizing rich in natural product extraction ingredient, by the raw material of following weight percent
It is made: bigarabe flower extract 1.0%, tea extract 6%, sponge gourd seed extract 1.0%, garden burnet root extracting solution 6%, semen litchi
Extract 0.3%, Herba Swertiae Mileensis extract 0.8%, mango leaf extract 1.5%, star-spangled banner conopsea extraction 1.0%, Roots of Panax Notoginseng mentions
Take object 0.8%, lipid 8%, emulsifier 6%, moisturizer 10%, preservative 0.5%, thickener 1%, deionized water mend to
100%.Wherein, the lipid is propyloxy phenyl base dimethyl silicone polymer；The moisturizer is glycerol；The emulsifier is
MONTANOV 68；The thickener is Simulgel 600；The preservative is P-hydroxybenzoic acid.
The preparation method of the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient, including following step
It is rapid:
(1) lipid, emulsifier, moisturizer and deionized water are mixed, stirring is warming up to 90 DEG C, heat preservation 5min to each original
Material is uniformly dispersed, and obtains mixture；
(2) mixture made from step (1) is cooled to 55 DEG C, thickener, anti-corrosion is then successively added into mixture
Agent, bigarabe flower extract, tea extract, sponge gourd seed extract, garden burnet root extracting solution, Semen Litchi extract, swertia mileensis extract
Object, mango leaf extract, star-spangled banner conopsea extraction, Radix Notoginseng root extract keep the temperature homogeneous 5min, and then stirring is cooled to room temperature,
Up to the compact sleep mask of skin whitening, moisturizing for being rich in natural product extraction ingredient.
Wherein, extract/extracting solution preparation method is same as Example 1.
Embodiment 4:
The compact sleep mask of a kind of skin whitening, moisturizing rich in natural product extraction ingredient, by the raw material of following weight percent
It is made: bigarabe flower extract 0.5%, tea extract 5%, sponge gourd seed extract 0.5%, garden burnet root extracting solution 5%, semen litchi
Extract 0.2%, Herba Swertiae Mileensis extract 0.2%, mango leaf extract 0.5%, star-spangled banner conopsea extraction 0.5%, Roots of Panax Notoginseng mentions
Take object 0.1%, lipid 5%, emulsifier 2%, moisturizer 5%, preservative 0.5%, thickener 1%, deionized water mend to
100%.Wherein, the lipid is propyloxy phenyl base dimethyl silicone polymer；The moisturizer is glycerol；The emulsifier is
MONTANOV 68；The thickener is Simulgel 600；The preservative is P-hydroxybenzoic acid.
The preparation method and 1 phase of embodiment of the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient
Together.
Embodiment 5:
The compact sleep mask of a kind of skin whitening, moisturizing rich in natural product extraction ingredient, by the raw material of following weight percent
Be made: bigarabe flower extract 2%, tea extract 10%, sponge gourd seed extract 3%, garden burnet root extracting solution 10%, semen litchi mentions
Take object 1%, Herba Swertiae Mileensis extract 1%, mango leaf extract 3%, star-spangled banner conopsea extraction 3%, Radix Notoginseng root extract 2%, rouge
Matter 10%, emulsifier 8%, moisturizer 30%, preservative 2%, thickener 3%, deionized water are mended to 100%.Wherein, described
Lipid is propyloxy phenyl base dimethyl silicone polymer；The moisturizer is glycerol；The emulsifier is MONTANOV 68；It is described
Thickener is Simulgel 600；The preservative is P-hydroxybenzoic acid.
The preparation method and 1 phase of embodiment of the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient
Together.
Embodiment 6:
The compact sleep mask of a kind of skin whitening, moisturizing rich in natural product extraction ingredient, by the raw material of following weight percent
It is made: bigarabe flower extract 1.0%, tea extract 8%, sponge gourd seed extract 2.5%, garden burnet root extracting solution 5%, semen litchi
Extract 0.5%, Herba Swertiae Mileensis extract 0.4%, mango leaf extract 1.5%, star-spangled banner conopsea extraction 1.0%, Roots of Panax Notoginseng mentions
Take object 1.0%, lipid 8%, emulsifier 6%, moisturizer 25%, preservative 1.0%, thickener 2.5%, deionized water mend to
100%.Wherein, the lipid is propyloxy phenyl base dimethyl silicone polymer；The moisturizer is glycerol；The emulsifier is
MONTANOV 68；The thickener is Simulgel 600；The preservative is P-hydroxybenzoic acid.
The preparation method and 1 phase of embodiment of the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient
Together.
Embodiment 7:
The compact sleep mask of a kind of skin whitening, moisturizing rich in natural product extraction ingredient, by the raw material of following weight percent
It is made: bigarabe flower extract 0.8%, tea extract 9%, sponge gourd seed extract 1.0%, garden burnet root extracting solution 6%, semen litchi
Extract 0.8%, Herba Swertiae Mileensis extract 0.5%, mango leaf extract 1.0%, star-spangled banner conopsea extraction 1.5%, Roots of Panax Notoginseng mentions
Take object 0.8%, lipid 5%, emulsifier 8%, moisturizer 15%, preservative 1.2%, thickener 1.5%, deionized water mend to
100%.Wherein, the lipid is propyloxy phenyl base dimethyl silicone polymer；The moisturizer is glycerol；The emulsifier is
MONTANOV 68；The thickener is Simulgel 600；The preservative is P-hydroxybenzoic acid.
The preparation method and 1 phase of embodiment of the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient
Together.
Embodiment 8:
The compact sleep mask of a kind of skin whitening, moisturizing rich in natural product extraction ingredient, by the raw material of following weight percent
It is made: bigarabe flower extract 1.5%, tea extract 5%, sponge gourd seed extract 2.0%, garden burnet root extracting solution 5%, semen litchi
Extract 0.2%, Herba Swertiae Mileensis extract 0.4%, mango leaf extract 0.8%, star-spangled banner conopsea extraction 0.8%, Roots of Panax Notoginseng mentions
Take object 1.0%, lipid 6%, emulsifier 6%, moisturizer 15%, preservative 1.0%, thickener 2%, deionized water mend to
100%.Wherein, the lipid is propyloxy phenyl base dimethyl silicone polymer；The moisturizer is glycerol；The emulsifier is
MONTANOV 68；The thickener is Simulgel 600；The preservative is P-hydroxybenzoic acid.
The preparation method and 1 phase of embodiment of the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient
Together.
Embodiment 9:
The compact sleep mask of a kind of skin whitening, moisturizing rich in natural product extraction ingredient, by the raw material of following weight percent
It is made: bigarabe flower extract 0.5%, tea extract 8%, sponge gourd seed extract 0.5%, garden burnet root extracting solution 8%, semen litchi
Extract 1%, Herba Swertiae Mileensis extract 0.8%, mango leaf extract 0.8%, star-spangled banner conopsea extraction 1.5%, Roots of Panax Notoginseng extract
Object 1.5%, lipid 6%, emulsifier 5%, moisturizer 10%, preservative 0.5%, thickener 3%, deionized water are mended to 100%.
Wherein, the lipid is propyloxy phenyl base dimethyl silicone polymer；The moisturizer is glycerol；The emulsifier is MONTANOV
68；The thickener is Simulgel 600；The preservative is P-hydroxybenzoic acid.
The preparation method and 1 phase of embodiment of the above-mentioned compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient
Together.
Embodiment 10:
The content of embodiment 10 is substantially the same manner as Example 1, the difference is that: the lipid is hexamethylene silicon oxygen
Alkane；The moisturizer is Sodium Hyaluronate；The emulsifier is MONTANOV 68；The thickener is Simulgel 600；Institute
Stating preservative is methyl p-hydroxybenzoate.
Embodiment 11:
The content of embodiment 11 is substantially the same manner as Example 1, the difference is that: the lipid is poly dimethyl silicon
Oxygen alkane；The moisturizer is hydrolytic collagen；The emulsifier is MONTANOV 68；The thickener is Simulgel 600；Institute
Stating preservative is the mixture that P-hydroxybenzoic acid and methyl p-hydroxybenzoate are mixed to get with arbitrary proportion.
Embodiment 12:
The content of embodiment 12 is substantially the same manner as Example 1, the difference is that: the lipid is propyloxy phenyl base
The mixture that dimethyl silicone polymer and ring five dimethyl silicone polymer are mixed to get with arbitrary proportion；The moisturizer is sweet
The mixture that oil, Sodium Hyaluronate, panthenol, hydrolytic collagen are mixed to get with arbitrary proportion；The emulsifier is MONTANOV
68；The thickener is Simulgel 600；The preservative is P-hydroxybenzoic acid.
Embodiment 13:
The content of embodiment 13 is substantially the same manner as Example 1, the difference is that: the lipid is propyloxy phenyl base
Dimethyl silicone polymer, cyclohexasiloxane, is mixed in dimethyl silicone polymer ring five dimethyl silicone polymer with arbitrary proportion
The mixture arrived；The moisturizer be butanediol, glycerol, propylene glycol, Sodium Hyaluronate, 1,2- hexylene glycol, panthenol, xylitol with
The mixture that arbitrary proportion is mixed to get；The emulsifier is MONTANOV 68；The thickener is Simulgel 600；Institute
Stating preservative is methyl p-hydroxybenzoate.
The effect of compact sleep mask of skin whitening, moisturizing of the present invention rich in natural product extraction ingredient confirmatory experiment:
The effect of in order to verify skin whitening, moisturizing compact sleep mask of the present invention rich in natural product extraction ingredient, with this hair
For the compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient prepared by bright embodiment 1, carries out following effect and test
Confirmation is tested.Meanwhile in order to be compared with the present invention rich in the compact sleep mask of skin whitening, moisturizing of natural product extraction ingredient, this
Invention is also provided with following comparative experiments, i.e. 1~comparative example of comparative example 9；The formula of sleep mask in 1~comparative example of comparative example 9
It is substantially the same manner as Example 1, the difference is that the extract added in formula/extracting solution ingredient is different, wherein comparative example
Only contain bigarabe flower extract in 1, tea extract only contained in comparative example 2, only contains Seeds of Luffa cylindrica extract in comparative example 3,
Only contain garden burnet root extracting solution in comparative example 4, only contains Semen Litchi extract in comparative example 5, only contain swertia mileensis in comparative example 6
Extract only contains mango leaf extract in comparative example 7, only contains American ginseng extract in comparative example 8, in comparative example 9 only
Contain Angelica roots；In 1~comparative example of comparative example 9 each comparative example sleep mask formula in extract or extracting solution
Dosage be equal to embodiment 1 in the sum of each extract or the dosage of extracting solution.
(1) experiment is inhibited tyrosinase activity:
The color of human skin is related with pigment present in skin and quantity, and wherein melanin is to skin color
Maximum is influenced, tyrosinase is the most key in the forming process of melanin, inhibits tyrosinase activity the work that can play whitening
With.Therefore, in order to verify the whitening of skin whitening, moisturizing compact sleep mask of the present invention rich in natural product extraction ingredient, nti-freckle function
Effect, the sleep mask prepared respectively to embodiment 1,1~comparative example of comparative example 9 carry out inhibiting tyrosinase activity experiment (progress
When inhibiting tyrosinase activity experiment, embodiment 1,1~comparative example of comparative example 9 formula in only add corresponding extract/mention
Liquid and deionized water are taken, does not add lipid, emulsifier, moisturizer, preservative and thickener), study the sleep surface of different formulations
For film to the inhibiting rate of tyrosinase activity, testing the results are shown in Table 2.
Inhibiting tyrosinase activity experiment, specific experimental method is as follows:
1, reagent and instrument:
Tyrosinase powder (enzyme activity 25000U), l-tyrosine, alpha-arbutin, PBS buffer solution (0.1mol/L, pH=
6.8), hydrochloric acid (0.1mol/L), microplate reader.
2, solution is prepared:
The l-tyrosine solution that mass fraction is 0.05% is prepared: 0.05g l-tyrosine is dissolved in 35ml 0.1mol/L
Hydrochloric acid in, add 65ml PBS buffer solution.
Sample liquid is prepared: being accurately weighed sample to be tested, is dissolved with PBS buffer solution, is configured to the sample that concentration is 1.0mg/ml
Product liquid.
Tyrosinase solution is prepared: tyrosinase being dissolved in pure water, it is molten that the tyrosinase that enzyme activity is 100U/ml is made
Liquid.
3, experimental implementation:
By shown in table 1, l-tyrosine, sample liquid, PBS buffer solution are sequentially added to the test tube numbered as A1, A2, B1, B2
Middle mixing；Rack for test tube is ploughed under into water-bath 10-15min in 37 DEG C of thermostat water baths, tyrosinase is sequentially added into A1 and B1 is to see
Crowd shakes up, and stops after reacting 15min；The successively thirty on 96 orifice plates measures it at 475nm with microplate reader and absorbance and counts
Calculate inhibiting rate.Inhibiting rate calculation formula are as follows: inhibiting rate={ [(A1-A2)-(B1-B2)]/(A1-A2) } * 100%；In formula, A1 is
Blank template has the absorbance of enzyme (tyrosinase) system, and A2 is absorbance of the blank template without enzyme (tyrosinase) system；B1
There is the absorbance of enzyme (tyrosinase) system for sample sets, B2 is absorbance of the sample sets without enzyme (tyrosinase) system.Experiment
Middle negative control is replaced with PBS buffer solution, and positive control selects the alpha-arbutin aqueous solution of 1.0mg/ml, every group of parallel determination 6
It is secondary.
The composition of 1 reaction solution of table
2 inhibitory activity against tyrosinase experimental result of table
| Embodiment | Inhibiting rate (%) |
| Embodiment 1 | 76.5 |
| Comparative example 1 | 50.4 |
| Comparative example 2 | 46.4 |
| Comparative example 3 | 37.4 |
| Comparative example 4 | 32.9 |
| Comparative example 5 | 41.5 |
| Comparative example 6 | 45.6 |
| Comparative example 7 | 52.3 |
| Comparative example 8 | 51.7 |
| Comparative example 9 | 48.6 |
| Positive control (alpha-arbutin) | 79.2 |
As shown in Table 2, the sleep that prepared by 1~comparative example of comparative example 9 is lower to the inhibiting rate of tyrosinase activity, highest
No more than 53%；Sleep mask prepared by the embodiment of the present invention 1 to the inhibiting rate (76.5%) of tyrosinase activity much higher than pair
1~comparative example of ratio 9 maintains an equal level with the inhibiting rate of alpha-arbutin substantially, moreover, the present invention is real compared with comparative example 7 (52.3%)
The inhibitory activity against tyrosinase for applying the sleep mask of the preparation of example 1 is about 1.5 times of comparative example 7.Thus illustrate, using single group
The sleep mask that the extract/liquid divided is prepared as effective component, Bu Nengyou poor to the inhibitory effect of tyrosinase activity
Effect inhibits melanin to be formed, and whitening effect is poor；The embodiment of the present invention 1 is made by the way that 9 kinds of active extraction components are carried out compounding
Sleep mask, the sleep mask are suitable with alpha-arbutin to the inhibitory effect of tyrosinase activity, thus also further demonstrate that, this
Invention plays synergistic effect, can effectively inhibit by compounding 9 kinds of active extraction components between each ingredient
The activity of tyrosinase plays the role of inhibiting melanin formation, has excellent whitening, spot-removal function.
(2) DPPH radicals scavenging is tested
In order to verify the anti-oxidation efficacy of skin whitening, moisturizing compact sleep mask of the present invention rich in natural product extraction ingredient,
The sleep mask prepared respectively to embodiment 1,1~comparative example of comparative example 9 carries out DPPH radicals scavenging experiment and (carries out DPPH certainly
Removed by base when testing, embodiment 1,1~comparative example of comparative example 9 formula in only add corresponding extract/extracting solution and go
Ionized water does not add lipid, emulsifier, moisturizer, preservative and thickener), the sleep mask of different formulations is studied to DPPH
The clearance rate of free radical, experiment the results are shown in Table 3.
Specific experimental method is as follows for DPPH radicals scavenging experiment:
1, reagent and instrument: DPPH, dehydrated alcohol, ethyl acetate, microplate reader.
2, solution is prepared:
The preparation of DPPH solution: accurately weighing DPPH 7.88mg, is placed in 100ml volumetric flask, is dissolved to quarter with solvent
Degree is 2 × 10 to get concentration-4(0~4 DEG C) is kept in dark place in the DPPH solution of mo1/L；
The preparation of sample liquid: taking sample to be tested, is configured to the analyte sample fluid that concentration is 0.1mg/ml with solvent.
3, specific experiment operates:
Separately sampled product liquid 5ml and 2 × 10-4Mo1/L DPPH solution 5ml is uniformly mixed, and places 30min in the dark,
Using solvent as blank, its absorbance is measured at 525nm, and following formula calculates its clearance rate: clearance rate (%)=[1- (Ai-
Aj)/Ac] × 100%, in formula, Ac is the absorbance that 5ml solvent adds 5ml DPPH solution, and Ai is that 5ml prepare liquid adds 5mlDPPH
The absorbance of solution；Aj is the absorbance that 5ml prepare liquid adds 5ml solvent.
Solvent is water, dehydrated alcohol, the ethyl acetate mixed solvent that 1:1:1 is mixed to get by volume in this experiment.
3 DPPH radicals scavenging experimental result of table
| Embodiment | Clearance rate (%) |
| Embodiment 1 | 98.5 |
| Comparative example 1 | 40.6 |
| Comparative example 2 | 55.1 |
| Comparative example 3 | 41.7 |
| Comparative example 4 | 45.9 |
| Comparative example 5 | 50.2 |
| Comparative example 6 | 48.7 |
| Comparative example 7 | 63.4 |
| Comparative example 8 | 61.5 |
| Comparative example 9 | 58.4 |
As shown in Table 3, the sleep that prepared by 1~comparative example of comparative example 9 is lower to DPPH free radical scavenging activity, not more than
Cross 64%；The embodiment of the present invention 1 prepare sleep mask to DPPH free radical scavenging activity (98.5%) much higher than comparative example 1~
Comparative example 9, moreover, the DPPH free radical of sleep mask prepared by the embodiment of the present invention 1 is clear compared with comparative example 7 (63.4%)
Except rate is about 1.6 times of comparative example 7.Thus illustrate, the sleep prepared using extract/liquid of one-component as effective component
Facial mask, poor to DPPH radicals scavenging effect, whitening effect is poor；9 kinds of activity by being extracted by the embodiment of the present invention 1
Divide compound and sleep mask is made, synergistic effect is played between each active extraction components, can effectively be removed
DPPH free radical plays the role of reducing melanin production, and then plays white-skinned face function.
(3) normal individual trial is tested:
The effect of in order to further verify skin whitening, moisturizing compact sleep mask of the present invention rich in natural product extraction ingredient,
By taking the compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient prepared by embodiment 1 as an example, it is real to carry out white-skinned face function
It tests and is tested with moisture-keeping efficacy.
1, white-skinned face function is tested:
(1) experimental subjects:
Choose 60 subjects and carry out skin tests, subject enrollment standard are as follows: women, the age between 18-50 years old,
There are different degrees of obscure and color spot, no serious systemic disease, no immune deficiency or autoimmune disease, no work on the face
Dynamic property anaphylactia person, i.e., toward no skin disease allergies, whole body does not use hormone medicine and immunosupress in nearly January
Agent, does not participate in other clinical tests, and cannot be used during testing other white-skinned face function products (cosmetics, topical drug or
Health care product for oral administration).
(2) test method:
After subject cleans facial skin every night, appropriate whitening of the present invention rich in natural product extraction ingredient is taken to protect
Wet compact sleep mask, is uniformly applied to face skin, and gently massage is until fully absorb, daily using primary, continuous use 6
Zhou Hou observes the variation of the pale degree of subject's facial skin, determines that whitening of the present invention rich in natural product extraction ingredient is protected
The whitening effect of wet compact sleep mask at least checks weekly once whether there is or not whole body and locally bad anti-with understanding during test
It answers.
Whitening effect criterion are as follows:
Effective: color spot area recession > 60%, color is obviously thin out；Effective: color spot area recession > 30%, color become
It is light；Invalid: color spot area recession < 30%, color change is unobvious.
(3) experimental result:
During test, 60 subjects do not occur phenomena of cutaneous irritation, moreover, this hair is used continuously in 60 subjects
For the compact sleep mask of the bright skin whitening, moisturizing rich in natural product extraction ingredient after 6 weeks, effective number is 45 people, and efficiently individual quantity is
56 people, invalid number are 4 people, therefore, the compact sleep mask of skin whitening, moisturizing of natural product extraction ingredient are rich in using the present invention
Obvious effective rate is 75.0%, and effective percentage is 93.3%, inefficiency 6.7%.Thus illustrate, the present invention is used for a long time rich in natural
The compact sleep mask of the skin whitening, moisturizing of product extract component can be inhibited tyrosinase activity effectively, desalinate epidermal pigment, effectively
The formation for inhibiting melanin, has effects that whitening, nti-freckle and skin lightening, moreover, to human skin safety, it is nonirritant.
2, moisture-keeping efficacy is tested
(1) experimental subjects:
It chooses 50 subjects and carries out skin test, subject enrollment standard are as follows: healthy female of the age between 22-45 years old
Property, middle dry skin, facial skin water content no significant difference, no serious systemic disease, no immune deficiency or autoimmunity
Property disease, no active anaphylactia person, i.e., toward no skin disease allergies, in nearly January not whole body use hormone medicine
And immunosuppressor, other clinical tests are not participated in.
(2) test method:
Subject cleans both hands inner forearm with clear water by unified, carries out test in subject's both hands inner forearm after cleaning
Area's label and measurement markers.Subject is sat quietly in constant environment after 30min, skin moisture content tester (Corneometer
CM825 the skin moisture content for) detecting trial zone, obtains the blank value of trial zone skin moisture content；Then equivalent whitening is taken
The compact sleep mask sample of moisturizing is uniformly applied on trial zone skin, is softly massaged into absorption, after measurement is smeared respectively
The skin moisture content of the test section 30min, 1h, 2h, 4h obtains different time after smearing the compact sleep mask of skin whitening, moisturizing and tests
The moisture content of skin test value in area, different periods are tested after then smearing the compact sleep mask of skin whitening, moisturizing according to the following formula
Area's skin moisture content growth rate: as a result skin moisture content growth rate=(test value-blank value)/blank value × 100% is joined
It is shown in Table 4.
4 skin moisture content test result of table
As shown in Table 4, after using the present invention rich in the compact sleep mask of skin whitening, moisturizing of natural product extraction ingredient
30min and the trial zone 1h skin moisture content growth rate no significant difference, 30min and 1h recipient site moisture content of skin after smearing
Growth rate is apparently higher than the skin moisture content growth rate using rear 2h, 4h；Using the present invention rich in natural product extraction at
Recipient site skin moisture content growth rate remains to reach 50.3% after the compact sleep mask 4h of skin whitening, moisturizing divided；Thus it says
It is bright, smear the compact sleep mask of skin whitening, moisturizing prepared by the embodiment of the present invention 1 and keep the ability of skin moisture content strong, have compared with
Strong moisturizing, moisturizing and water lock effect.
The foregoing is merely illustrative of the preferred embodiments of the present invention, but is not limited only to examples detailed above, all in essence of the invention
Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.
Claims (9)
1. a kind of compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient, which is characterized in that by following weight hundred
The raw material of ratio is divided to be made: bigarabe flower extract 0.5%~2%, tea extract 5%~10%, sponge gourd seed extract 0.5%~3%, ground
Elm root extracting solution 5%~10%, Semen Litchi extract 0.2%~1%, Herba Swertiae Mileensis extract 0.2%~1%, mango leaf extract
0.5%~3%, star-spangled banner conopsea extraction 0.5%~3%, Radix Notoginseng root extract 0.1%~2%, lipid 5%~10%, emulsifier 2%~8%,
Moisturizer 5%~30%, preservative 0.5%~2%, thickener 1%~3%, deionized water are mended to 100%.
2. the skin whitening, moisturizing compact sleep mask according to claim 1 rich in natural product extraction ingredient, feature exist
In, the bigarabe flower extract is cleaned, drying, is crushed the preparation method comprises the following steps: bigarabe is spent, and addition Extraction solvent is uniformly mixed,
Ultrasonic extraction, extracting solution are filtered, recycle Extraction solvent processing to get bigarabe flower extract, wherein the Extraction solvent is second
Acetoacetic ester and the ethyl alcohol mixture that 1:1 is mixed to get by volume.
3. the skin whitening, moisturizing compact sleep mask according to claim 2 rich in natural product extraction ingredient, feature exist
In, the tea extract the preparation method comprises the following steps: by tealeaves cleaning, drying, crush, add water refluxing extraction, extracting solution through filtering,
Up to tea extract；The garden burnet root extracting solution the preparation method comprises the following steps: by garden burnet root cleaning, drying, crush, add water reflux mention
It takes, extracting solution is filtered to get garden burnet root extract.
4. the skin whitening, moisturizing compact sleep mask according to claim 3 rich in natural product extraction ingredient, feature exist
In the system of the sponge gourd seed extract, Semen Litchi extract, Herba Swertiae Mileensis extract, mango leaf extract, star-spangled banner conopsea extraction
Preparation Method is equal are as follows: and it by the raw material cleaning of the extract, drying, crushes, ethyl alcohol is added and is uniformly mixed, ultrasonic extraction, extracting solution
It filtered, recycle alcohol treatment to get the extract of corresponding raw material is arrived.
5. the skin whitening, moisturizing compact sleep mask according to claim 3 rich in natural product extraction ingredient, feature exist
In, the Radix Notoginseng root extract the preparation method comprises the following steps: by Roots of Panax Notoginseng cleaning, drying, crush, methanol is added and is uniformly mixed, ultrasound
It extracts, extracting solution is filtered, recycles methyl alcohol process to get Radix Notoginseng root extract.
6. the skin whitening, moisturizing compact sleep mask according to claim 5 rich in natural product extraction ingredient, feature exist
In the lipid is propyloxy phenyl base dimethyl silicone polymer, ring five dimethyl silicone polymer, cyclohexasiloxane, poly- diformazan
One of radical siloxane is a variety of.
7. the skin whitening, moisturizing compact sleep mask according to claim 6 rich in natural product extraction ingredient, feature exist
In the moisturizer is butanediol, glycerol, propylene glycol, Sodium Hyaluronate, 1,2- hexylene glycol, panthenol, xylitol, soluble glue
At least one of former, hydrolytic collagen.
8. the skin whitening, moisturizing compact sleep mask according to claim 7 rich in natural product extraction ingredient, feature exist
In the preservative is one or both of P-hydroxybenzoic acid, methyl p-hydroxybenzoate；The emulsifier is
MONTANOV 68；The thickener is Simulgel 600.
9. a kind of system of any compact sleep mask of skin whitening, moisturizing rich in natural product extraction ingredient of claim 1~8
Preparation Method, which comprises the following steps:
(1) lipid, emulsifier, moisturizer and deionized water are mixed, stirring is warming up to 80~90 DEG C, and 5~20min of heat preservation is to each
Stock dispersion is uniform, obtains mixture；
(2) mixture made from step (1) is cooled to 45~55 DEG C, thickener, anti-corrosion is then successively added into mixture
Agent, bigarabe flower extract, tea extract, sponge gourd seed extract, garden burnet root extracting solution, Semen Litchi extract, swertia mileensis extract
Object, mango leaf extract, star-spangled banner conopsea extraction, Radix Notoginseng root extract keep the temperature 5~10min of homogeneous, and then stirring is cooled to room
Temperature is to get the compact sleep mask of skin whitening, moisturizing for being rich in natural product extraction ingredient.
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| CN106963701A (en) * | 2017-05-24 | 2017-07-21 | 佛山市汇汾化妆品科技有限公司 | A kind of facial masks for whitening faces and removing spots |
| CN109771348A (en) * | 2019-03-15 | 2019-05-21 | 黄河水利职业技术学院 | Skin whitening, moisturizing smoothing wrinkle face cream rich in natural product extraction ingredient and preparation method thereof |
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2019
- 2019-08-30 CN CN201910814176.3A patent/CN110384644A/en active Pending
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|---|---|---|---|---|
| CN106511220A (en) * | 2016-12-30 | 2017-03-22 | 广东国方医药科技有限公司 | Dendrobium officinale moisturizing and repair sleeping mask and preparation method thereof |
| CN106963701A (en) * | 2017-05-24 | 2017-07-21 | 佛山市汇汾化妆品科技有限公司 | A kind of facial masks for whitening faces and removing spots |
| CN109771348A (en) * | 2019-03-15 | 2019-05-21 | 黄河水利职业技术学院 | Skin whitening, moisturizing smoothing wrinkle face cream rich in natural product extraction ingredient and preparation method thereof |
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