CN109330917B - Essential oil composition with whitening, anti-aging and moisturizing effects and application thereof - Google Patents
Essential oil composition with whitening, anti-aging and moisturizing effects and application thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
Abstract
The invention discloses an essential oil composition with whitening, anti-aging and moisturizing effects and application thereof, and belongs to the field of cosmetics. The essential oil composition is prepared from the following components in percentage by weight: 0.05-3.0% of rose essential oil; 0.1-3.0% of orange flower essential oil; 0.1-3.0% of osmanthus essential oil; 0.05-3.0% of geranium essential oil; 0.1-5.0% of carrot seed essential oil; the balance of base oil. The essential oil composition 6 disclosed by the invention is subjected to reasonable compounding, has a synergistic effect, is mild and non-irritant, does not contain a preservative and an antioxidant, is green and environment-friendly, has the effects of obviously inhibiting tyrosinase activity, inhibiting melanin generation, removing free radicals and improving skin hydration rate, and also has the effects of resisting ultraviolet rays and promoting skin blood circulation; the cosmetic added with the essential oil composition has the effects of obviously whitening and rejuvenating skin, resisting aging and repairing skin, and moisturizing and repairing skin.
Description
Technical Field
The invention relates to an essential oil composition with whitening, anti-aging and moisturizing effects and application thereof, and belongs to the field of cosmetics.
Background
With the continuous improvement of the living standard and the living quality of people, the requirements of consumers on the beauty and skin care products necessary for daily life are higher and higher, and the influence of the plant skin care concept of returning to nature is emphasized more and more. The essential oil has small molecular weight, is easy to permeate the skin and be absorbed, and the essential oil skin care product is gradually favored by people.
Most essential oil products in the current market have single effect, the using effect is not obvious enough, and if the using effect is obvious, the required using amount is higher, so that stimulation and skin injury are easily caused. Therefore, a group of natural, mild and low-irritation essential oil compositions with various effects of whitening, resisting aging, moisturizing and the like are particularly important.
CN 105030622 a discloses a whitening composition and a preparation method thereof, the whitening composition comprises sweet almond oil, olive fruit oil, rose oil, bitter orange flower oil, geranium oil and the like, can effectively inhibit melanin production, accelerate the decomposition and excretion of melanin, eliminate skin darkness, and achieve the effects of whitening, removing freckles, evening and brightening skin color, but the whitening composition does not have the effects of moisturizing and repairing.
CN 107510621A discloses an anhydrous foaming aerosol for makeup removal, which comprises olive fruit oil, camellia seed oil, argania spinosa seed oil, rose hip oil and the like, has strong makeup removal capability, is moist and not dry after makeup removal, but does not have whitening and anti-aging effects.
CN201310369785.5 discloses an anti-aging essential oil capable of whitening skin, which is prepared from the following raw materials in parts by weight: lemon, lavender, sage, rose, bergamot, cinnamon, frankincense and base oil can effectively whiten skin and delay aging, but do not have moisturizing effect.
Therefore, the essential oil composition which is natural, mild and low in irritation and has the effects of whitening, resisting aging and preserving moisture is provided, and has important significance in the field of cosmetics.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention mainly aims to provide an essential oil composition with whitening, anti-aging and moisturizing effects.
The invention also aims to provide application of the essential oil composition with the whitening, anti-aging and moisturizing effects.
The purpose of the invention is realized by the following technical scheme:
an essential oil composition with whitening, anti-aging and moisturizing effects is prepared from the following components in percentage by weight: 0.05-3.0% of rose essential oil; 0.1-3.0% of orange flower essential oil; 0.1-3.0% of osmanthus essential oil; 0.05-3.0% of geranium essential oil; 0.1-5.0% of carrot seed essential oil; the balance of base oil.
Preferably, the essential oil composition with the whitening, anti-aging and moisturizing effects is prepared from the following components in percentage by weight: 0.1-2.0% of rose essential oil; 0.2-2.0% of orange flower essential oil; 0.2-2.0% of osmanthus essential oil; 0.1-2.0% of geranium essential oil; 0.5-3.0% of carrot seed essential oil; the balance of base oil.
Further preferably, the essential oil composition with the whitening, anti-aging and moisturizing effects is prepared from the following components in percentage by weight: 0.1-2.0% of rose essential oil; 0.2-2.0% of orange flower essential oil; 0.2-0.8% of osmanthus essential oil; 0.8-1.5% of geranium essential oil; 1.0-3.0% of carrot seed essential oil; the balance of base oil.
Preferably, the essential oil composition with the whitening, anti-aging and moisturizing effects is prepared from the following components in percentage by weight: 0.5 percent of rose essential oil; 0.5 percent of orange flower essential oil; 0.8% of osmanthus essential oil; 1.0% of geranium essential oil; 2.0% of carrot seed essential oil; the balance of base oil.
Preferably, the essential oil composition with the whitening, anti-aging and moisturizing effects is prepared from the following components in percentage by weight: 0.1% of rose essential oil; orange flower essential oil 2.0%; 0.2% of osmanthus essential oil; 1.5 percent of geranium essential oil; 1.0% of carrot seed essential oil; the balance of base oil.
Preferably, the essential oil composition with the whitening, anti-aging and moisturizing effects is prepared from the following components in percentage by weight: 0.1% of rose essential oil; 0.2% of orange flower essential oil; 0.2% of osmanthus essential oil; 1.3 percent of geranium essential oil; 3.0% of carrot seed essential oil; the balance of base oil.
Preferably, the essential oil composition with the whitening, anti-aging and moisturizing effects is prepared from the following components in percentage by weight: 2.0% of rose essential oil; 0.2% of orange flower essential oil; 0.4% of osmanthus essential oil; geranium essential oil 0.8%; 1.4% of carrot seed essential oil; the balance of base oil.
The base oil is one or more of grape seed oil, wheat germ oil and olive oil.
The invention further aims to provide application of the essential oil composition with the whitening, anti-aging and moisturizing effects in cosmetics.
The essential oil composition with the whitening, anti-aging and moisturizing effects is applied to the preparation of cosmetics, wherein the essential oil composition with the whitening, anti-aging and moisturizing effects is added into the cosmetics in an amount of 0.1-50% (preferably 5-20%) by mass.
The invention also provides a cosmetic with the whitening, anti-aging and moisturizing effects, which contains the essential oil composition with the whitening, anti-aging and moisturizing effects.
Preferably, the cosmetic contains 0.1-50% (preferably 5-20%) by mass of the essential oil composition with the whitening, anti-aging and moisturizing effects.
The cosmetic is as follows: aqua, emulsion, cream, facial mask, spray, essence, essential oils, and soap.
Specifically, the invention provides a whitening, anti-aging and moisturizing emulsion which comprises the following components in parts by mass:
| composition (I) | Mass fraction/% |
| Glycerol | 5.00 |
| EDTA disodium salt | 0.01 |
| Hyaluronic acid sodium salt | 0.10 |
| Betaine | 0.50 |
| Panthenol | 0.50 |
| Deionized water | Balance of |
| Carbomer 941 | 0.20 |
| Polydimethylsiloxane | 6.00 |
| Cetostearyl alcohol | 2.00 |
| Caprylic/capric triglyceride | 3.00 |
| Shea butter | 1.50 |
| Polysorbate-20 | 2.00 |
| Hydroxy phenyl methyl ester | 0.12 |
| Propyl hydroxybenzoate | 0.02 |
| Butanediol | 7.00 |
| Aminomethyl propanol | 0.10 |
| The essential oil composition of the invention | 20.00 |
Specifically, the invention provides a whitening, anti-aging and moisturizing mask which comprises the following components in parts by mass:
specifically, the invention provides a whitening, anti-aging, moisturizing and skin-care essential oil which comprises the following components in parts by mass:
| component name | Mass fraction/% |
| Squalane | 30 |
| Caprylic/capric triglyceride | 24 |
| Isononyl isononanoate | 20 |
| Jojoba oil | 5 |
| Olive oil | 1 |
| The essential oil composition of the invention | 20 |
The effects of the various essential oils of the invention are as follows:
the rose essential oil has various effects of promoting metabolism, cell regeneration, blood circulation, inhibiting skin melanin, resisting bacteria, whitening skin, resisting aging, and keeping moisture.
The neroli essential oil is rich in various whitening active ingredients, can lead out melanin formed in skin layer by layer under the action of comfortable conduction of aromatic factors, and can be discharged along with metabolism of aged cutin, the melanin is not deposited, the skin is gradually white, and simultaneously turbid substances accumulated in the skin and harmful substances generated by pollution can be discharged.
The sweet osmanthus essential oil can promote blood circulation, improve tissues, keep skin active, has the effects of thinning skin, beautifying, moisturizing and moistening, can accelerate skin blood circulation, and makes skin white, red and transparent.
The geranium essential oil can relieve pain, astringe and resist bacteria, stretch into scars, enhance the cell defense function, deeply clean the skin, balance sebum secretion, promote the regeneration of skin cells, repair scars and striae gravidarum, is particularly suitable for oily skin and pockmarked skin, and has good relieving and eliminating effects on pockmarks and pockmarks.
The carrot seed essential oil can strengthen red blood cells, thereby improving skin color, enabling the skin to be firmer and more elastic, enabling the skin to become young and active, and also can lighten senile plaques and moisturize the skin.
Compared with the prior art, the invention has the following advantages and effects:
(1) the essential oil composition 6 disclosed by the invention is combined reasonably, has a synergistic effect, is mild and non-irritant, and has the effects of obviously inhibiting tyrosinase activity, inhibiting melanin generation, removing free radicals and improving skin hydration rate;
(2) the cosmetic added with the essential oil composition has the effects of obviously whitening and rejuvenating skin, resisting aging and repairing skin, moisturizing and repairing skin;
(3) the essential oil composition also has the effects of resisting ultraviolet rays and promoting skin blood circulation.
(4) The essential oil composition disclosed by the invention is 100% of natural source, does not contain preservatives and antioxidants, and is green and environment-friendly.
Detailed Description
The present invention will be described in further detail with reference to examples, but the embodiments of the present invention are not limited thereto.
The test methods in the following examples, in which specific experimental conditions are not specified, are generally performed according to conventional experimental conditions or according to the experimental conditions recommended by the manufacturer.
Example 1 an essential oil composition (I) having skin whitening, anti-aging, and moisturizing effects
An essential oil composition with whitening, anti-aging and moisturizing effects is characterized by being prepared from the following components in percentage by weight: 0.5 percent of rose essential oil; 0.5 percent of orange flower essential oil; 0.8% of osmanthus essential oil; 1.0% of geranium essential oil; 2.0% of carrot seed essential oil; the balance of grape seed oil.
Example 2 an essential oil composition with skin whitening, anti-aging, and moisturizing effects (II)
An essential oil composition with whitening, anti-aging and moisturizing effects is characterized by being prepared from the following components in percentage by weight: 0.1% of rose essential oil; orange flower essential oil 2.0%; 0.2% of osmanthus essential oil; 1.5 percent of geranium essential oil; 1.0% of carrot seed essential oil; the balance of grape seed oil.
Example 3 an essential oil composition (III) with skin whitening, anti-aging, and moisturizing effects
An essential oil composition with whitening, anti-aging and moisturizing effects is characterized by being prepared from the following components in percentage by weight: 0.1% of rose essential oil; 0.2% of orange flower essential oil; 0.2% of osmanthus essential oil; 1.3 percent of geranium essential oil; 3.0% of carrot seed essential oil; the rest is wheat germ oil.
Example 4 an essential oil composition (IV) with skin whitening, anti-aging, and moisturizing effects
An essential oil composition with whitening, anti-aging and moisturizing effects is characterized by being prepared from the following components in percentage by weight: 2.0% of rose essential oil; 0.2% of orange flower essential oil; 0.4% of osmanthus essential oil; geranium essential oil 0.8%; 1.4% of carrot seed essential oil; the rest is olive oil.
Comparative examples 1-6 compositions of a single essential oil and base oil
The specific combination is shown in table 1.
TABLE 1
| Composition (I) | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | Comparative example 5 | Comparative example 6 |
| Rose essential oil | 4.8％ | 0 | 0 | 0 | 0 | 0 |
| Orange flower essential oil | 0 | 4.8％ | 0 | 0 | 0 | 0 |
| Sweet osmanthus essential oil | 0 | 0 | 4.8％ | 0 | 0 | 0 |
| Geranium essential oil | 0 | 0 | 0 | 4.8％ | 0 | 0 |
| Carrot seed essential oil | 0 | 0 | 0 | 0 | 4.8％ | 0 |
| Grape seed oil | 95.2％ | 95.2％ | 95.2％ | 95.2％ | 95.2％ | 100％ |
Test example 1 whitening anti-aging in vitro evaluation experiment
1. Preparation of the test specimens
The essential oil composition prepared in example 1 and the compositions prepared in comparative examples 1 to 6 were used as samples. 1g of the sample was dissolved in 99g of dimethyl sulfoxide to prepare a sample solution with a mass fraction of 1%, and the following test was performed.
2. Tyrosinase inhibitory activity effect evaluation test
Accurately sucking a sample solution, a Phosphate Buffer Solution (PBS) with the pH value of 6.8 and a dopa solution with the mass fraction of 0.1% according to the table 2, fully mixing, incubating at 30 ℃ for 5min, adding a tyrosinase solution with the activity of 110U/mL, incubating at 30 ℃ for 10min, quickly transferring to a cuvette, and measuring the absorbance at 475 nm.
TABLE 2
The relative inhibition rate (I, inhibition rate for short, the same below) of the sample on tyrosinase was calculated according to the formula (1).
I＝[(A1-A2)-(A3-A4)]×100％÷(A1-A2)(1)
In the formula: a1, A2, A3 and A4 are the absorbances of the solutions of groups 1 to 4, respectively.
3. Test for inhibiting melanin synthesis in melanocytes
B16 melanoma cells (mouse melanoma cells, Shanghai cell bank of Chinese academy of sciences, model TCM2) were cultured at 1X 105one/mL of the cells were seeded in 96-well plates at 90. mu.L/well in CO2After incubation in the incubator for 24 hours, the sample solution was added to each well. A blank control group of medium and cells was set up simultaneously.
After the plates were incubated in an incubator for 72 hours, the supernatant was discarded, washed twice with PBS, and then 0.5mL of trypsinized cells were added to each well for 3min, and 2mL of maintenance solution was added to each well to stop digestion. After mixing, 0.5mL of each concentration was taken out and counted. Centrifuging the rest cell suspension at 2500r/min for 5min, discarding supernatant, adding NaOH solution into the precipitate, heating to dissolve melanin, and measuring absorbance at 490nm under enzyme-linked immunosorbent assay. The melanin synthesis inhibition ratio (I') of the sample was calculated according to the formula (2).
I’＝(1-A5÷P1/A6÷P2)×100％ (2)
In the formula: a5 is the absorbance value of the sample solution hole; p1 is the sample solution well cell density; a6 is control well absorbance value; p2 is control well cell density.
4. Evaluation test of superoxide anion radical scavenging effect
The drug solutions were added as in Table 3. After 2mL of the sample solution was added to 2.25mL of Tris-HCl buffer (pH8.36) and 0.25mL of pyrogallol solution at a concentration of 10mmoL/L, the mixture was subjected to water bath at 25 ℃ and 1 drop of 10mol/L hydrochloric acid was added dropwise at 4min to terminate the reaction. The absorbance values were measured with a UV spectrophotometer at 420 nm. The clearance (D) was calculated according to equation (3).
D＝[1-(A9-A10)÷(A7-A8)]×100％ (3)
In the formula: a7 is O generated by the spontaneous oxidation reaction of pyrogallol in Tris-HCl solution2 -The absorbance value of (a); a8 is the absorbance value of Tris-HCl solution; a9 is a purge O2 -(ii) absorbance value of the reaction; a10 is the absorbance value of the sample solution.
TABLE 3
| Reaction group | Tris-HCl | Pyrogallol | Sample solution | Deionized water |
| F0 | 2.25mL | 0.25mL | 0mL | 2mL |
| F1 | 2.25mL | 0.25mL | 2mL | 0mL |
| F2 | 2.25mL | 0mL | 2mL | 0mL |
5. Results of the experiment
The whitening anti-aging effect evaluation experiment is shown in table 4.
The experimental results in table 4 show that the essential oil composition of the present invention can significantly inhibit tyrosinase activity, inhibit melanin synthesis, and scavenge free radicals, and under the condition of no change of the total dosage, the effect of the essential oil composition of the present invention is significantly improved compared with the effect of a single essential oil and base oil composition and pure base oil, which indicates that the synergistic effect is exerted among different essential oils.
Test example 2 evaluation of moisturizing efficacy
Experimental materials: the products of example 1 and comparative examples 1-6 were diluted to 5 times with olive oil and used as samples to compare the change in moisture content of the skin of the test subjects after the samples were used.
Subject: a total of 30 volunteers, of which women: 15 men and 15 men, the age being 20-40 years old.
The Corneometer CM825 is adopted to measure the change of the moisture content of the stratum corneum by measuring the change of the capacitance of the stratum corneum of the skin before and after the product is used, so that the moisturizing effect of the cosmetics is evaluated.
The experimental method comprises the following steps: the testee should wash the forearm, sit at a set humidity for 30min, and then mark 3 × 3cm on the left and right forearms2The method comprises the steps of taking a left arm as a testing area of a moisturizing product, taking a symmetrical area corresponding to a right arm as a blank control, testing and detecting the moisture content of each experimental part by using a Corneometer CM825, repeating the testing for 5 times respectively to obtain an average value of each testing, recording data, calculating the average hydration rate of 20 volunteers at different time intervals, and calculating the hydration rate by using a formula (1).
The results are shown in Table 5 below.
TABLE 5 average skin hydration Rate for volunteers tested at different time intervals
As can be seen from Table 5, the skin of the sample of example 1 of the present invention still has a high moisture content 8 hours after application, and the average hydration rate still reaches above 40%, which indicates that the essential oil composition with moisturizing and repairing effects prepared by the present invention has a good moisturizing effect. The samples of comparative examples 1 to 6, however, had lower hydration rates per time period than the sample of example 1 of the present invention. Therefore, after the essential oils are scientifically combined, the moisturizing effect is obviously improved under the condition of consistent dosage, and the essential oils have good synergistic effect.
Test example 3 skin irritation test
Experimental materials: the samples of example 1 and comparative examples 1 to 6 were selected, and the change in the moisture content of the skin of the test subjects after the samples were used was compared.
Subject: a total of 30 volunteers, of which women: 15 men and 15 men, the age being 20-40 years old.
The test method comprises the following steps: 0.03mL of the sample was taken by a syringe and placed in a chamber of a spot test tape, and the spot test tape with the sample was immediately stuck to the normal skin of the left forearm from the lower part in the longitudinal direction while gently pressing the chamber one by one to expel air and uniformly distribute the test substance. The test site is marked for easy observation. Every 24 hours, and half an hour after the patch was removed, the examination was performed according to the terms of the CTFA guidelines (1981). The patch test was performed 6 times in total, and on day 6 after completion of the skin application, additional examination was performed to observe delayed reactions. The data is compared using the last examination. The identification was carried out using the following table 6 as a standard:
TABLE 6 skin irritation assay standards
| Grade | Symbol | Identification criteria |
| 0 | - | Negative reaction: has no irritation and erythema |
| 1 | ± | And (3) suspicious reaction: mild erythema |
| 2 | + | Weak positive reaction: erythema |
| 3 | ++ | Strong positive reaction: erythema, papules, blisters |
| 4 | +++ | Extremely strong positive reaction: severe edema and bulla |
And (3) test results: as shown in table 7.
Table 7 skin irritation test results
| Number of times of skin sticking | Example 1 | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | Comparative example 5 | Comparative example 6 |
| 1 | 0 | 1 time +/-) | 1 time +/-) | 1 time +/-) | 0 | 0 | 0 |
| 2 | 0 | 0 | 1 time of | 0 | 0 | 0 | 1 time +/-) |
| 3 | 0 | 1 time +/-) | 0 | 0 | 0 | 0 | 0 |
| 4 | 0 | 0 | 0 | 0 | 1 time +/-) | 0 | 0 |
| 5 | 0 | 0 | 0 | 0 | 0 | 1 time +/-) | 0 |
| 6 | 0 | 0 | 0 | 1 time +/-) | 0 | 1 time +/-) | 0 |
| Total up to | 0 | 2 times +/-) | 1 time plus or minus and 1 time plus | 2 times +/-) | 1 time +/-) | 2 times +/-) | 1 time +/-) |
The results in Table 7 show that the product of example 1 of the invention has better mildness than the products of comparative examples 1-6. Therefore, the essential oil is milder than that used alone under the condition of consistent dosage after being scientifically combined.
Application example 1 whitening, anti-aging and moisturizing emulsion
An emulsion containing the essential oil composition with the effects of whitening, resisting aging and moisturizing has a specific formula shown in table 8:
TABLE 8
The preparation method of the emulsion comprises the following steps:
1. putting the water phase into an emulsifying pot, uniformly stirring, and heating and stirring to 75-85 ℃;
2. putting the oil phase into an oil phase preparation pot, uniformly stirring, and heating and stirring to 75-85 ℃;
3. pumping the materials in the oil phase pot into an emulsifying pot, uniformly stirring, vacuumizing the emulsifying pot, and homogenizing and emulsifying for 10 minutes;
4. preserving the heat for 15 minutes, then cooling to 40 ℃ by cooling water, adding the addition phase, and uniformly stirring;
5. cooling to 35 ℃, and discharging after the inspection is qualified.
Application comparative example 1 ordinary emulsion
Except that the essential oil composition (i) having the whitening, anti-aging and moisturizing effects is not included, the other ingredients and the preparation method are the same as those of application example 1.
Application example 2 whitening, anti-aging and moisturizing mask liquid
The facial mask liquid containing the essential oil composition with the whitening, anti-aging and moisturizing effects has the specific formula shown in table 9:
TABLE 9
The preparation method of the mask liquid comprises the following steps:
1. heating the raw materials of p-hydroxyacetophenone and 1, 2-hexanediol as additive phase in 1, 3-propylene glycol in advance to ensure that the dissolved substances are clear and transparent for later use;
2. putting the water phase raw material into deionized water, heating to 75-85 ℃, and stirring until the water phase raw material is uniformly dissolved;
3. cooling the water phase to 60 ℃, slowly adding the methyl hydroxybenzoate and propyl hydroxybenzoate dissolved in the 1, 3-propylene glycol in advance while stirring, and stirring until the methyl hydroxybenzoate and the propyl hydroxybenzoate are dissolved uniformly;
4. cooling to 40 ℃, adding the essential oil composition (I) described in example 1, and then dropwise adding aminomethyl propanol to adjust the pH to 5-6;
5. stirring uniformly, cooling to 35 ℃, repeatedly measuring pH, and discharging with 300 meshes.
Application example 3 whitening, anti-aging, moisturizing and skin-protecting essential oil
The skin-care essential oil containing the essential oil composition with the effects of whitening, resisting aging and moisturizing comprises the following specific formula shown in table 10:
watch 10
| Component name | Mass fraction (%) |
| Squalane | 30 |
| Caprylic/capric triglyceride | 24 |
| Isononyl isononanoate | 20 |
| Jojoba oil | 5 |
| Olive oil | 1 |
| Essential oil composition (I) described in example 1 | 20 |
The preparation method comprises the following steps: the raw materials of each component are weighed according to the formula proportion in sequence and stirred and mixed evenly at normal temperature.
Effect example 1 evaluation of whitening effect, anti-aging effect and moisturizing effect
1. Test method
The emulsions prepared in application example 1 and application comparative example 1 were subjected to human trial evaluation, respectively. 30 healthy volunteers are selected, wherein the age is 30-45 years, and the healthy volunteers are half of male and female. The emulsion of application example 1 was used on the left side, and the emulsion of application comparative example 1 was used on the right side, once a day, morning, afternoon and evening, for 30 days, and the skin color of the left and right faces was observed after one month of use.
The using effects of the product, such as skin whiteness, glossiness, humidity preservation, temperature, firmness and anti-wrinkle effect, are evaluated in the using process, wherein the highest score is 5, and the lowest score is 1.
2. Test results
Filling out a trial evaluation table according to the sensory evaluation. And collecting a half-face test trial evaluation table, and showing the statistical result in table 11.
TABLE 11 average values of human trial results
| Evaluation results | Application example 1 emulsion | Use of the emulsion of comparative example 1 |
| Whiteness degree | 4.6 | 3.2 |
| Moisture retention | 4.5 | 3.0 |
| Degree of gloss | 4.1 | 3.2 |
| Mildness property | 4.5 | 3.9 |
| Compactness degree | 4.2 | 1.5 |
| Anti-wrinkle effect | 4.3 | 1.9 |
The results of table 11 show that the user considers that the skin whiteness, glossiness, moisture retention, mildness, firmness and anti-wrinkle effects are significantly improved after using the emulsion of application example 1 of the present invention, and the effects are much more significant than those of using the emulsion of application example 1, indicating that the essential oil composition of the present invention has significant whitening, anti-aging and moisturizing effects when applied to cosmetics.
The above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.
Claims (12)
1. An essential oil composition with whitening, anti-aging and moisturizing effects is characterized in that: the composition is prepared from the following components in percentage by weight: 0.05-3.0% of rose essential oil; 0.1-3.0% of orange flower essential oil; 0.1-3.0% of osmanthus essential oil; 0.05-3.0% of geranium essential oil; 0.1-5.0% of carrot seed essential oil; the balance of base oil;
the base oil is one or more of grape seed oil, wheat germ oil and olive oil.
2. The essential oil composition with the effects of whitening, resisting aging and preserving moisture as claimed in claim 1, is characterized in that: the composition is prepared from the following components in percentage by weight: 0.1-2.0% of rose essential oil; 0.2-2.0% of orange flower essential oil; 0.2-2.0% of osmanthus essential oil; 0.1-2.0% of geranium essential oil; 0.5-3.0% of carrot seed essential oil; the balance of base oil.
3. The essential oil composition with the effects of whitening, resisting aging and preserving moisture as claimed in claim 1, is characterized in that: the composition is prepared from the following components in percentage by weight: 0.1-2.0% of rose essential oil; 0.2-2.0% of orange flower essential oil; 0.2-0.8% of osmanthus essential oil; 0.8-1.5% of geranium essential oil; 1.0-3.0% of carrot seed essential oil; the balance of base oil.
4. Use of the essential oil composition with whitening, anti-aging and moisturizing effects as claimed in any one of claims 1 to 3 in preparation of cosmetics.
5. Use according to claim 4, characterized in that:
the addition amount of the essential oil composition with the whitening, anti-aging and moisturizing effects in the cosmetics is 0.1-50% by mass.
6. A cosmetic with whitening, anti-aging and moisturizing effects is characterized in that: the essential oil composition with the whitening, anti-aging and moisturizing effects as claimed in any one of claims 1 to 3.
7. The cosmetic with whitening, anti-aging and moisturizing effects as claimed in claim 6, is characterized in that:
the cosmetic contains 0.1-50% of essential oil composition with whitening, anti-aging and moisturizing effects by mass.
8. The cosmetic with whitening, anti-aging and moisturizing effects as claimed in claim 6 or 7, wherein:
the cosmetic is as follows: emulsions, creams, masks, sprays, essences, essential oils, soaps.
9. The cosmetic with whitening, anti-aging and moisturizing effects as claimed in claim 6 or 7, wherein: the cosmetic is as follows: a water aqua.
10. The cosmetic with whitening, anti-aging and moisturizing effects as claimed in claim 6 or 7, wherein:
the cosmetic with the whitening, anti-aging and moisturizing effects is a whitening, anti-aging and moisturizing emulsion and comprises the following components in parts by mass: 5.00% of glycerin, 0.01% of disodium EDTA, 0.10% of sodium hyaluronate, 0.50% of betaine, 0.50% of panthenol, 0.20% of carbomer 941, 6.00% of polydimethylsiloxane, 2.00% of cetostearyl alcohol, 3.00% of caprylic/capric triglyceride, 1.50% of shea butter, 2.00% of polysorbate-20, 0.12% of methylparaben, 0.02% of propylhydroxybenzoate, 7.00% of butanediol, 0.10% of aminomethyl propanol, 20.00% of an essential oil composition, and the balance of deionized water.
11. The cosmetic with whitening, anti-aging and moisturizing effects as claimed in claim 6 or 7, wherein:
the cosmetic with the whitening, anti-aging and moisturizing effects is a whitening, anti-aging and moisturizing mask and comprises the following components in parts by mass: 5.00% of glycerin, 0.10% of sodium hyaluronate, 0.20% of allantoin, 1.00% of panthenol, 15.00% of carbomer 9411% aqueous solution, 8.00% of 1, 3-propylene glycol, 0.80% of 1, 2-hexanediol, 0.40% of p-hydroxyacetophenone, 0.08% of aminomethyl propanol, 5.00% of an essential oil composition and the balance of deionized water.
12. The cosmetic with whitening, anti-aging and moisturizing effects as claimed in claim 6 or 7, wherein:
the cosmetic with the whitening, anti-aging and moisturizing effects is whitening, anti-aging, moisturizing and skin-care essential oil and comprises the following components in percentage by mass: squalane 30%, caprylic/capric triglyceride 24%, isononyl isononanoate 20%, jojoba oil 5%, olive oil 1%, and essential oil composition 20%.
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| CN110772454B (en) * | 2019-12-13 | 2023-07-21 | 湖北创界生物科技有限公司 | Skin-brightening, moisturizing, soothing and anti-aging compound essential oil, and preparation method and application thereof |
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| US20100233128A1 (en) * | 2009-03-13 | 2010-09-16 | Mci Media Capital Inc. | Natural Skin Products Containing Dairy and Processes |
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