CN109350591A - A kind of U.S. face dried noodle film and preparation method thereof - Google Patents
A kind of U.S. face dried noodle film and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
- A61K8/355—Quinones
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/63—Steroids; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/68—Sphingolipids, e.g. ceramides, cerebrosides, gangliosides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/925—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of animal origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/005—Preparations for sensitive skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/007—Preparations for dry skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
- A61K2800/31—Anhydrous
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/52—Stabilizers
- A61K2800/524—Preservatives
Abstract
The invention discloses a kind of U.S. face dried noodle films and preparation method thereof, and the facial mask includes the ingredient of following parts by weight: 0.2~5 part of ascorbic acid glucoside, 0.2~5 part of honey, 0.2~5 part of Cer NS, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/0.2~5 part of ubiquinone/vitamin E, 0.2~5 part of palmityl tripeptides -5,0.1~2 part of disodium ethylene diamine tetraacetate, 2~15 parts of olive oil and 1~10 part of tocopherol acetate.The dried noodle film of one kind provided by the invention; it can effectively prevent skin moisture loss; the skin moment is enabled to moisten full; and have the characteristics that be easy by percutaneous absorption, texture is soft and smooth, dry skin of releiving; strengthen the defence capability of skin; environmental stimuli and pollution are fought, the skin of people is effectively protected, is more suitable dry skin and sensitive skin.
Description
Technical field
The present invention relates to cosmetic technical field, it is specifically related to a kind of U.S. face dried noodle film and preparation method thereof.
Background technique
Facial mask is a kind of carrier of face beautifying health keeping product, powder reconciliation at present, kaolin, non-woven fabrics, silk mask, tencel face
Film, Biofibre facial mask, nonwoven fabric facial mask material facial mask using very extensive.Its most basic and most important purpose is to more
Makeup removing and the still insufficient cleaning that washes one's face are mended, other essential ingredients is cooperated to realize other maintenance functions on this basis,
Such as replenishing water and preserving moisture, whitening and anti-aging, Sage Extract etc..It is all liquid facial mask, liquid facial mask one that traditional facial mask is most of
Aspect needs to add preservative prevention product and goes bad, inconvenient to carry on the other hand when travelling is outgoing, and it is super to have luggage
The problems such as heavy, and liquid facial mask is typically all disposable.
Summary of the invention
It is an object of the invention to overcome the above problem and provide a kind of U.S. face dried noodle film and preparation method thereof, the facial mask
For anhydrous facial mask, skin surface is directly acted on by being added to active principle, skin is made to obtain deeper and direct reparation
With nutrition.
To achieve the above object, the technical solution adopted by the present invention is that a kind of dried noodle film, the facial mask include following weight
The ingredient of part: 0.2~5 part of ascorbic acid glucoside, 0.2~5 part of honey, 0.2~5 part of Cer NS, safflower seed oil/gold knob
Detain flower/leaf/stem extraction/Astragalus membranacus root extract/0.2~5 part of ubiquinone/vitamin E.
Ascorbic acid glucoside in the present invention is also known as AA2G, is that a kind of form of Vitamin C can after skin absorbs
It is converted to Victoria C, by the way that DOPA quinone is reduced to DOPA, blocks the oxidative chain of melanin production, thus inhibit the formation of melanin,
With whitening effect.Also it is adjustable collagen synthesis.It can be stabilized under the conditions of wide in range pH, be in the present invention whitening
Nti-freckle, moisturizer.
Honey: honey is emollients, moisturizer, wetting agent, thickener.The nutritional ingredient of honey is natural nutrition object
Matter, the bioactive substances such as monosaccharide, vitamin, enzyme are conducive to that skin table can be effectively improved by the absorption of Skin Cell
The nutritional status in face keeps skin fine and smooth, keeps nature ruddy, also help the aging of delaying skin cell, delay to play
Or the effects of mitigating wrinkle.
Cer NS: making the effect of skin conditioning agent, antioxidant and moisturizer in cosmetics, it can improve skin
Inhibit active smegma while adipose membrane, make skin water and oil balance, enhances the self-protection function of skin with neural acyl
Amine 1 is relatively suitble to skin greasing and has the young skin of demand.The ingredient has good action to skin moisturizing maintenance, is cuticula
In important skin-active ingredient, skin barrier, reconstituted cell can be enhanced.The especially needed more ceramides of stimulated skin,
Some researches show that wiping the product containing ceramide ingredient can be reduced red and swollen and percutaneous water loss, play enhancing skin barrier
Effect.
Safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/ubiquinone/vitamin E: oil-soluble is planted
Object active matter imitates anti crease and anti senile old aufhellung wrinkle depth, remodeling epidermal shape, smooth compact skin entirely, repairs generated wrinkle
Line and the generation for preventing new wrinkle.This ingredient is provided by Guangzhou Sheng Kaisi Chemical Industry Science Co., Ltd.
The present invention with ascorbic acid glucoside, honey, Cer NS, safflower seed oil/gold bachelor's button/leaf/stem extraction/
Astragalus membranacus root extract/ubiquinone/vitamin E is moisturizing active constituent, and these types of ingredient is carried out compounding by discovery to be had well
Moistening effect.
Preferably, the dried noodle film further includes the ingredient of following parts by weight: 0.2~5 part of palmityl tripeptides -5, ethylenediamine
0.1~2 part of tetraacethyl disodium, 2~15 parts of olive oil and 1~10 part of tocopherol acetate.
Palmityl tripeptides -5: for skin conditioning agent.Promote skin cell growth, inhibit oxygen radical and hydroxyl radical free radical,
Promote the synthesis of stromatin (matrix protein) especially collagen, while being also possible to increase elastin laminin, transparent
The generation of matter acid, glycosaminoglycan and fibronectin.Such victory peptide promotes collagen by increasing stroma cell activity
Synthesis, so that skin seems more aobvious elasticity and youth.Mode of action retinoids, but do not have Tretinoin side effect, increase collagen egg
The hyaluronic acid (HA) of bletilla cytoplasm synthesizes, and loses microgroove, skin is solid.
Disodium ethylene diamine tetraacetate: mainly making chelating agent use, plays stabilization in cosmetics, mineral sequestration agent,
Antisepsis can be cooperateed with.And there is certain synergistic function to protective system and antioxidant system.
Olive oil: it rich in the squalene and essential fatty acid splendid with skin affinity, absorbs rapidly, effectively
It keeps skin elasticity and moistens；Contained monounsaturated fatty acids abundant and vitamin E, A, D etc. and phenols antioxygen in olive oil
Compound matter can eliminate facial wrinkles, prevent skin aging, have skin or hair care and prevention and treatment rhagadia manus et pedis and other effects, be that " can eat "
Cosmetics and skincare product, ultraviolet light can be resisted and prevent cutaneum carcinoma by addition smearing skin with olive oil.
Tocopherol acetate: belonging to the derivative of vitamin E, and antioxidant use is often done in cosmetics, has well
Antioxidant effect, it is a kind of oil-soluble natural materials, is good nutrition moisturizing agent to skin, makes an addition in skin care products,
It can be avoided the rancid oxidation of grease, stabilize grease.In moisturizing and connective tissue is maintained, and skin is protected not hurt by ultraviolet light
Evil has fine performance, which can make skin soft-touch and keep skin moisture, and wound healing, prevention inflammation is promoted to prevent
The coarse chap of skin improves blackspot, and security risk index is not high therefore uses extensive.Antioxidant, skin are served as in the present invention
Conditioner and moisturizer.
The present invention is extracted with honey, Cer NS, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root
Object/ubiquinone/vitamin E, palmityl tripeptides -5, disodium ethylene diamine tetraacetate, olive oil and tocopherol acetate is antioxygen
Change active constituent, these types of ingredient is carried out compounding by discovery has good antioxidant effect.
Preferably, the dried noodle film further includes emulsifier, thickener, skin conditioning agent, the emulsifier include below at
Point: octadecanoic acid and polyethylene glycol (400) stearate, the thickener include carbopol and 1,3-PD, described
Skin conditioning agent includes Butyrospermum parkii fruit rouge, cetanol ricinoleate, water/propylene glycol/phytosterol.
Octadecanoic acid: being naturally present in various plant and animal derivatives, belongs to a kind of common higher fatty acids,
It is the indispensable raw material of general dairy products, in cream and lotion.Generation " soap base " is reacted with alkali.
A kind of polyethylene glycol (400) stearate: raw material based on plant.Increase in cosmetics, pharmaceutical purpose emulsifier, soap base
Thick dose, softening agent and surfactant etc., have good effect, can improve the quality of product.
Cetanol ricinoleate: unique natural emollient ester can be used as softening agent in cosmetics, emulsifier makes
With, and will not blocked pore.Skin silk cunning, the feeling of non-greasy are assigned, particularly suitable for skin care product and in body temperature
Lower thawing carrys out preferable gloss to skin tape.
Carbopol: carbomer belongs to high molecular polymer, thickener, gelling agent, emulsion stabilizer.With good
Lightness, card wave have good compatibility for pH, and no matter acid neutral or alkalinity can use.For electrolyte,
Also it only says in hydrogel, not electrolyte-resistant.In table living body system and electrolyte has good concertedness.
Water/propylene glycol/phytosterol: the phytosterols content purified using biotechnology, from one kind
Special tropical pteridophyte, can strengthen DEJ, and fine and close dermal extracellular matrix, increases epidermal thickness again, rebuild epidermis,
Skin is set to become more plentiful smooth.This ingredient is provided by hundred Hao Bo Co., Ltd of Guangzhou.
Preferably, each ingredient described in the dried noodle film is based on following parts by weight: 10~20 parts of octadecanoic acid, poly- second two
0.1~2 part of alcohol (400) stearate, 0.1~5 part of carbopol, 2~30 parts of 1,3- propylene glycol, Butyrospermum parkii fruit rouge 20~40
Part, 1~20 part of cetanol ricinoleate and water/0.5~5 part of propylene glycol/phytosterol.
Preferably, the dried noodle film further includes the ingredient of following parts by weight: 5~20 parts of glycerine, smokes clothing at 2~10 parts of water
0.1~1 part of careless essential oil, 5~20 parts of animal saualane, 0.2~10 part of egg oil, 2~30 parts of 1,3- propylene glycol.
Lavender: being refined by lavender, can be clearing heat and detoxicating, cleaning skin, control oil, freckle removing and whitening,
The tender skin of anti-wrinkle, eye haustra -dsipelling black eye may additionally facilitate the skin-protecting functions such as regeneration of damaged tissue recovery.Lavender is also to heart
There is sedation effect, hypertension can be reduced, pacify palpitaition, it is helpful for having a sleepless night.
Egg oil: have the function of heat-clearing moisturizing, anti-inflammatory analgetic, convergence myogenic and protection sore face, as emollients, conditioning
Agent etc. is applied to personal-care supplies field.With good skin care effect, have preferably to removal infant eczema etc.
Effect.
Preferably, the dried noodle film includes the ingredient of following parts by weight: 1.8~2.2 parts of the ascorbic acid glucoside, mind
It is mentioned through 2 1.6~2.5 parts of amide, 1.5~2.8 parts of honey, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root
Take object/1.4~2.8 parts of ubiquinone/vitamin E.In moisturizing active constituent of the present invention, the proportion of component will affect effect, research hair
Existing, within the scope of the preferred parts by weight, moistening effect of the present invention is more preferably.
Preferably, the dried noodle film is based on following parts by weight: 3.5~4.2 parts of tocopherol acetate, Cer NS 1.2
~2.4 parts, 0.5~1.2 part of palmityl tripeptides -5,3.5~5.2 parts of olive oil, disodium ethylene diamine tetraacetate 0.12~
0.23 part, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/ubiquinone/vitamin e1 .2~2.3 part
When.
In oxidation-resistant active ingredient of the present invention, the proportion of component will affect effect, the study found that in the preferred weight
In part range, antioxidant effect of the present invention is more preferably.
Preferably, the dried noodle film includes the ingredient of following parts by weight: 2 parts of ascorbic acid glucoside, 2 parts of honey, nerve
22 parts of amide, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/2 parts of ubiquinone/vitamin E, palm fibre
- 51 parts of palmitic acid acyl tripeptides, 0.2 part of disodium ethylene diamine tetraacetate, 5 parts of olive oil and 4 parts of tocopherol acetate.The application hair
Bright people has been surprisingly found that in many experiments, and under the specific weight proportion, moisturizing antioxidant effect of the invention reaches simultaneously
Most preferably.
Preferably, the dried noodle film further includes the ingredient of following parts by weight: 14 parts of octadecanoic acid, polyethylene glycol (400)
1 part of stearate, 0.4 part of carbopol, 2~30 parts of 1,3- propylene glycol, 24 parts of Butyrospermum parkii fruit rouge, cetanol ricinoleate
4 parts, water/2 parts of propylene glycol/phytosterol, 10 parts of glycerine, 6 parts of water, 0.4 part of Lavender, 8 parts of animal saualane, egg
2 parts and 10 parts of 1,3- propylene glycol of butter.
The present invention also provides a kind of preparation methods of dried noodle film, comprising the following steps: 1) by octadecanoic acid, butter fruit
Tree fruit rouge, tocopherol acetate, cetanol ricinoleate, tocopherol, olive oil, safflower seed oil/gold bachelor's button/leaf/
Stem extraction/Astragalus membranacus root extract/ubiquinone/vitamin E, polyethylene glycol (400) stearate and egg oil is according to weight
Than being added in heating stirring bucket, 200 revs/min of stirring is opened, 70-85 DEG C is warming up to and is stirred uniformly；
2) carbopol, water, disodium ethylene diamine tetraacetate and 1,3- propylene glycol are added to heating stirring according to weight ratio
In bucket, 150 revs/min of stirring is opened, 80-95 DEG C is warming up to and is stirred；
3) mixture obtained in step 2 is added in the mixture of step 1), carries out emulsifying, completes until emulsifying,
Stirring is cooled to 45 DEG C；
4) by ascorbic acid glucoside, Cer NS, palmityl tripeptides -5, water/propylene glycol/phytosterol, honey and
Lavender is added above-mentioned in step 3) mixture according to weight ratio, is stirred；
5) Material in step 4) is taken out, it is filling carries out facial mask.
Beneficial effects of the present invention: the dried noodle film of one kind provided by the invention can effectively prevent skin moisture loss, enable flesh
The skin moment moisten it is full, and have the characteristics that be easy by percutaneous absorption, texture is soft and smooth, dry skin of releiving, strengthen skin
Defence capability fights environmental stimuli and pollution, the skin of people is effectively protected, and is more suitable dry skin and sensitive
Skin.
Specific embodiment
To better illustrate the object, technical solutions and advantages of the present invention, below in conjunction with specific embodiment to the present invention
It is described further.
It is involved in the present invention to water/propylene glycol/phytosterol indicate to be made of water, propylene glycol and phytosterol
Compound, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/ubiquinone/vitamin E is by safflower
The compound that seed oil, golden button floral leaf/stem extraction, Astragalus membranacus root extract, ubiquinone and vitamin E form.
Each raw material manufacturer involved by following embodiment is as shown in table 1:
Table 1
Examples 1 to 6
The component and parts by weight content of the U.S. face dried noodle film of Examples 1 to 6 are as shown in table 2.
The U.S. face dried noodle membrane component and parts by weight content of 2 Examples 1 to 6 of table
The preparation method of U.S. face dried noodle film of the invention the following steps are included: 1) by octadecanoic acid, Butyrospermum parkii fruit rouge,
Tocopherol acetate, cetanol ricinoleate, tocopherol, olive oil, safflower seed oil/gold bachelor's button/leaf/stem extract
Object/Astragalus membranacus root extract/ubiquinone/vitamin E, polyethylene glycol (400) stearate and egg oil is added according to weight ratio
In heating stirring bucket, 200 revs/min of stirring is opened, 70-85 DEG C is warming up to and is stirred uniformly；2) by carbopol, water, second
Edetate disodium and 1,3-PD are added in heating stirring bucket according to weight ratio, open 150 revs/min of stirring, are risen
Temperature is stirred to 80-95 DEG C；3) mixture obtained in step 2 is added in the mixture of step 1), carries out emulsifying, directly
It is completed to emulsification, stirring is cooled to 45 DEG C；4) by ascorbic acid glucoside, Cer NS, palmityl tripeptides -5, water/the third two
Alcohol/phytosterol, honey and Lavender are added above-mentioned in step 3) mixture according to weight ratio, are stirred.5)
Material in step 4) is taken out, it is filling to carry out facial mask.
Embodiment 7~16
The component and parts by weight content of the U.S. face dried noodle film of embodiment 7~16 are as shown in table 3.
The U.S. face dried noodle membrane component and parts by weight content of 3 embodiment 7~16 of table
The component and parts by weight content of the U.S. face dried noodle film of comparative example 1~7 are as shown in table 4.The facial mask of comparative example 1~7
Preparation method it is same as Example 1.
The component and parts by weight content of the U.S. face dried noodle film of 4 comparative example 1~7 of table
7 stability test of embodiment
Facial mask prepared by embodiment 1 to 6 places condition of different temperatures next month, observes its steadiness.As a result
It is as shown in table 5:
5 Examples 1 to 6 stability test of table
| -18℃ | 5℃ | 25℃ | 48℃ | |
| Embodiment 1 | Normally | Normally | Normally | Normally |
| Embodiment 2 | Normally | Normally | Normally | Normally |
| Embodiment 3 | Normally | Normally | Normally | Slight lamination |
| Embodiment 4 | Normally | Normally | Normally | Normally |
| Embodiment 5 | Slight lamination | Normally | Normally | Slight lamination |
| Embodiment 6 | Normally | Normally | Normally | Slight lamination |
As can be known from Table 3, under the conditions of 5 DEG C~25 DEG C, it is in stable state, at -18 DEG C and 48 DEG C, is implemented
Example 2, embodiment 3, embodiment 5~6 will appear slight lamination.
Embodiment 17
Moistening effect test is carried out to Examples 1 to 6 and anti-oxidant test, test method are as follows:
1. moistening effect is tested
Test sample: embodiment sample
Subject: 60 20-24 years old age women
Test equipment: moisture of skin analyzer Corneometer CM 825 is for detecting keratoderma moisture content
Test zone: left hand inner forearm and right hand inner forearm
Test method: test sample carries out single application by the amount of (2.0 ± 0.1) mg/cm2, will be tried using latex finger cot
Sample is coated in the test zone of 3cm × 3cm.
Test period: 0h, 2h, 4h, 6h
Conceptual design: 0h: 2~3 days before recipient site do not use any product, and 1h~3h cannot contact water.System before tested
One cleaning inner forearm and wiped clean.Subject is in 21 ± 1 DEG C of temperature, the laboratory of relative humidity 50 ± 10% before testing
Sit quietly 20min, cannot drink water and beverage, forearm expose.Test carries out keratoderma moisture to sample application area after starting
The parametric measurement of content.
2h: the parametric measurement of keratoderma moisture content is carried out to sample application area.
4h: the parametric measurement of keratoderma moisture content is carried out to sample application area.
6h: the parametric measurement of keratoderma moisture content is carried out to sample application area.
Every group of embodiment randomly selects 10 subjects and tests, and tests left and right inner forearm cuticula moisture content,
Moisture content average value and right arm inside moisture content average value and its increase on the inside of 10 subject's left arms are obtained by data
Value, the results are shown in Table 4.
11, inoxidizability is tested
Experimental method: the measurement of superoxide anion ability is removed
The test method is carried out according to the method that following document provides: Fan Xiao, Yan little Jun, room state are bright etc..High molecular weight is brown
Algae polyphenol antioxidant properties study [J] aquatile journal, 1999,23 (5): 494-499.
Taking 0.05mol/L pH is 8.2 Tris-HCl buffer 4.5ml, is placed in 25 DEG C of water-baths and preheats 20min, respectively
The pyrogallol solution of 1ml sample and 0.4ml, 25mmol/L is added, reacts 5min in 25 DEG C of water-baths after mixing, is added
8mol/L HCl 1.0ml terminates reaction, makees reference with Tris-HCl buffer, and absorbance is measured at 299nm, calculates and removes
Rate.
The calculation formula of clearance rate: ultra-oxygen anion free radical clearance rate (%)=100 (A1-A2)/A1, wherein A1 is sky
White mean light absorbency, A2 are the mean light absorbency of sample.It is as shown in table 6 to ultra-oxygen anion free radical clearance rate.
6 or so inner forearm cuticula moisture content average value of table and value added (Examples 1 to 6)
| The tested time/h | 0 | 2 | 4 | 6 |
| 1 average value of embodiment/MMV | 32.89 | 53.48 | 54.67 | 54.42 |
| 2 average values of embodiment/MMV | 33.57 | 49.47 | 50.27 | 50.08 |
| 3 average values of embodiment/MMV | 34.23 | 52.24 | 52.87 | 52.58 |
| 4 average values of embodiment/MMV | 34.12 | 50.37 | 50.71 | 50.4 |
| 5 average values of embodiment/MMV | 34.86 | 49.55 | 50.05 | 49.84 |
| 6 average values of embodiment/MMV | 33.35 | 48.3 | 48.81 | 48.55 |
| 1 moisture content value added of embodiment/MMV | 0 | 20.59 | 21.78 | 21.53 |
| 2 moisture content value added of embodiment/MMV | 0 | 15.90 | 16.7 | 16.51 |
| 3 moisture content value added of embodiment/MMV | 0 | 18.01 | 18.64 | 18.35 |
| 4 moisture content value added of embodiment/MMV | 0 | 16.25 | 16.59 | 16.28 |
| 5 moisture content value added of embodiment/MMV | 0 | 14.69 | 15.19 | 14.98 |
| 6 moisture content value added of embodiment/MMV | 0 | 14.95 | 15.46 | 15.20 |
As can be seen from Table 6, facial mask described in Examples 1 to 6 all has preferable moistening effect, wherein the guarantor of embodiment 1
Wet effect is best.
7 Examples 1 to 6 of table is to ultra-oxygen anion free radical clearance rate
| Experimental group | Ultra-oxygen anion free radical clearance rate (%) |
| Embodiment 1 | 91.65% |
| Embodiment 2 | 85.23% |
| Embodiment 3 | 88.09% |
| Embodiment 4 | 86.85% |
| Embodiment 5 | 83.94% |
| Embodiment 6 | 83.01% |
As can be seen from Table 7, facial mask described in Examples 1 to 6 all has preferable antioxidant effect, wherein embodiment 1
Antioxidant effect is best.
Embodiment 18
Performance of keeping humidity test is carried out to the facial mask of the preparation of embodiment 7~11, test method such as embodiment 17 is identical, test
The results are shown in Table 8:
8 or so inner forearm cuticula moisture content average value of table and value added (embodiment 7~11)
As seen from the above table, the facial mask of the embodiment of the present invention 7~11 has significant moistening effect, the face of embodiment 7~11
Film the difference from embodiment 1 is that, ascorbic acid glucoside, Cer NS, honey, safflower seed oil/gold bachelor's button/leaf/stem mention
Object/Astragalus membranacus root extract/ubiquinone/vitamin E content difference is taken, and its moistening effect is also different, experimental result hair
It is existing, when based on following parts by weight: 1.8~2.2 parts of ascorbic acid glucoside, 1.6~2.5 parts of Cer NS, honey 1.5~
2.8 parts, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/ubiquinone/vitamin e1 .4~2.8 part
When, moistening effect is preferable, it is found that the effect of embodiment 1 is best.
Embodiment 19
Antioxygenic property test is carried out to the facial mask of the preparation of embodiment 12~16, test method such as embodiment 17 is identical,
Test result is as shown in table 9:
Table 9 embodiment, 12~16 pairs of ultra-oxygen anion free radical clearance rates
| Experimental group | Ultra-oxygen anion free radical clearance rate (%) |
| Embodiment 12 | 85.78% |
| Embodiment 13 | 88.85% |
| Embodiment 14 | 89.05% |
| Embodiment 15 | 87.43% |
| Embodiment 16 | 86.60% |
As seen from the above table, the facial mask of the embodiment of the present invention 12~16 has significant antioxidant effect, embodiment 12~16
Facial mask the difference from embodiment 1 is that, tocopherol acetate, Cer NS, palmityl tripeptides -5, olive oil, second two
Amine tetraacethyl disodium, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/ubiquinone/vitamin E contain
The difference of amount illustrates that its main antioxidant effect is ethylenediamine tetra-acetic acid two as a result, it has been found that its antioxidant effect is also different
Sodium, olive oil, palmityl tripeptides -5, tocopherol acetate, safflower seed oil/gold bachelor's button/leaf/stem extraction/film pod are yellow
Stilbene root extract/ubiquinone/vitamin E, experimental result discovery, when based on following parts by weight: 3.5~4.2 parts of tocopherol acetate,
1.2~2.4 parts of Cer NS, 0.5~1.2 part of palmityl tripeptides -5,3.5~5.2 parts of olive oil, ethylenediamine tetrem
0.12~0.23 part of acid disodium, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/ubiquinone/vitamin
When E1.2~2.3 part, antioxidant effect is preferable, and discovery embodiment does not run affairs moisture retention or its anti-oxidant effect all reaches most
It is good.
Embodiment 20
Performance of keeping humidity test is carried out to the facial mask of the preparation of comparative example 1~7, test method such as embodiment 17 is identical, and with
Embodiment 1 is compared, and test result is as shown in table 10:
The left and right inner forearm cuticula moisture content average value and value added of 10 comparative example 1~7 of table and embodiment 1
| The tested time/h | 0 | 2 | 4 | 6 |
| 1 average value of embodiment/MMV | 32.89 | 53.48 | 54.67 | 54.42 |
| 1 average value of comparative example/MMV | 34.28 | 52.63 | 54.41 | 54.02 |
| 2 average values of comparative example/MMV | 35.16 | 53.42 | 55.19 | 54.81 |
| 3 average values of comparative example/MMV | 35.08 | 53.4 | 55.09 | 54.85 |
| 4 average values of comparative example/MMV | 33.95 | 51.97 | 53.84 | 53.43 |
| 5 average values of comparative example/MMV | 34.58 | 54.53 | 56.09 | 56.01 |
| 6 average values of comparative example/MMV | 34.36 | 52.94 | 55.23 | 55.04 |
| 7 average values of comparative example/MMV | 34.59 | 54.49 | 56.01 | 55.97 |
| 1 moisture content value added of embodiment/MMV | 0 | 20.59 | 21.78 | 21.53 |
| 1 moisture content value added of comparative example/MMV | 0 | 18.35 | 20.13 | 19.74 |
| 2 moisture content value added of comparative example/MMV | 0 | 18.26 | 20.03 | 19.65 |
| 3 moisture content value added of comparative example/MMV | 0 | 18.32 | 20.01 | 19.77 |
| 4 moisture content value added of comparative example/MMV | 0 | 18.02 | 19.89 | 19.48 |
| 5 moisture content value added of comparative example/MMV | 0 | 19.95 | 21.51 | 21.43 |
| 6 moisture content value added of comparative example/MMV | 0 | 18.58 | 20.87 | 20.68 |
| 7 moisture content value added of comparative example/MMV | 0 | 19.90 | 21.42 | 21.38 |
As known from Table 10, by comparing the moistening effect of embodiment 1 and comparative example 1~7, find comparative example 1~7 relative to
For embodiment 1, effect declines, and comparative example 5, the decline of 7 effect of comparative example are unobvious, and comparative example 1~4 and comparative example
Ratio comparative example 5, the comparative example 7 of 6 effects decline are obvious, and comparative example 1~4, comparative example 6 have lacked anti-for comparative example 1
Bad hematic acid glucoside, Cer NS, honey, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/general
Quinone/vitamin E, olive oil tocopherol acetate ingredient, and comparative example 5, comparative example 7 lack for embodiment 1
Palmityl tripeptides -5, olive oil, disodium ethylene diamine tetraacetate ingredient, it is known that, ascorbic acid glucoside, Cer NS,
Honey, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/ubiquinone/vitamin E, olive oil are raw
Phenol acetic acid esters is educated with synergistic function, lacks any of which ingredient, effect can be impacted.
Embodiment 21
Anti-oxidant energy test is carried out to the facial mask of the preparation of comparative example 1~6, test method such as embodiment 17 is identical, and with
Embodiment 1 is compared, and test result is as shown in table 11:
11 comparative example 1~7 of table and embodiment 1 to ultra-oxygen anion free radical clearance rate
| Experimental group | Ultra-oxygen anion free radical clearance rate (%) |
| Embodiment 1 | 91.65% |
| Comparative example 1 | 90.68% |
| Comparative example 2 | 87.89% |
| Comparative example 3 | 90.56% |
| Comparative example 4 | 87.95% |
| Comparative example 5 | 88.05% |
| Comparative example 6 | 88.64% |
| Comparative example 7 | 88.69% |
As can be seen from Table 11, the facial mask of comparative example 1~7 all has preferable antioxidant effect, but relative to comparison
For example 1, less effective, and the antioxidant effect of comparative example 1, comparative example 3 is good relative to other comparative examples, comparative example 1 is
Lacking ascorbic acid glucoside ingredient, comparative example 3 has lacked honey component, show that the two influences less antioxidant effect,
And comparative example 2 has lacked Cer NS ingredient, comparative example 4 has lacked safflower seed oil/gold bachelor's button/leaf/stem extraction/film pod
Radix Astragali root extract/ubiquinone/vitamin E component, comparative example 5 have lacked disodium ethylene diamine tetraacetate ingredient, and comparative example 6 lacks
Olive oil tocopherol acetate ingredient, comparative example 7 have lacked palmityl tripeptides -5, the face that corresponding comparative example is prepared
The antioxygenic property of film also reduces, and shows only when Cer NS, safflower seed oil/gold bachelor's button/leaf/stem extraction/film pod
Radix Astragali root extract/ubiquinone/vitamin E component, disodium ethylene diamine tetraacetate ingredient, olive oil, tocopherol acetate at
Point and palmityl tripeptides -5 can just play optimal antioxidant effect when being used in conjunction with, and from table 10, table 11 it is found that neural acyl
Amine 2, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/ubiquinone/vitamin E component, olea europaea fruit
Oil, tocopherol acetate these ingredients not only have synergistic function with moisturizing ingredient, and play synergy with antioxidant content
Effect.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Within mind and principle, any modification, equivalent substitution, improvement and etc. done be should be included within the scope of the present invention.
Claims (10)
1. a kind of dried noodle film, which is characterized in that the facial mask includes the ingredient of following parts by weight: ascorbic acid glucoside 0.2~5
Part, 0.2~5 part of honey, 0.2~5 part of Cer NS, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root mention
Take object/0.2~5 part of ubiquinone/vitamin E.
2. dried noodle film according to claim 1, which is characterized in that further include the ingredient of following parts by weight: palmityl tripeptides-
5 0.2~5 parts, 0.1~2 part of disodium ethylene diamine tetraacetate, 2~15 parts of olive oil and 1~10 part of tocopherol acetate.
3. dried noodle film according to claim 2, which is characterized in that further include emulsifier, thickener, skin conditioning agent, institute
Stating emulsifier includes following component: octadecanoic acid and polyethylene glycol (400) stearate, the thickener includes carbopol
And 1,3-PD, the skin conditioning agent include Butyrospermum parkii fruit rouge, cetanol ricinoleate, water/propylene glycol/plant steroid
Alcohols.
4. dried noodle film according to claim 3, which is characterized in that each ingredient is based on following parts by weight: 18 carbon
10~20 parts of alkanoic acid, 0.1~2 part of polyethylene glycol (400) stearate, 0.1~5 part of carbopol, 1,3-PD 2~30
Part, 20~40 parts of Butyrospermum parkii fruit rouge, 1~20 part of cetanol ricinoleate and water/propylene glycol/phytosterol 0.5~5
Part.
5. dried noodle film according to claim 4, which is characterized in that further include the ingredient of following parts by weight: glycerine 5~20
Part, 2~10 parts of water, 0.1~1 part of Lavender, 5~20 parts of animal saualane, 0.2~10 part of egg oil, 1,3-PD 2
~30 parts.
6. dried noodle film according to claim 1, which is characterized in that the ingredient including following parts by weight: the ascorbic acid
1.8~2.2 parts of glucoside, 1.6~2.5 parts of Cer NS, 1.5~2.8 parts of honey, safflower seed oil/gold bachelor's button/leaf/stem
Extract/Astragalus membranacus root extract/1.4~2.8 parts of ubiquinone/vitamin E.
7. dried noodle film according to claim 2, which is characterized in that based on following parts by weight: tocopherol acetate 3.5~
4.2 parts, 1.2~2.4 parts of Cer NS, 0.5~1.2 part of palmityl tripeptides -5,3.5~5.2 parts of olive oil, second two
0.12~0.23 part of amine tetraacethyl disodium, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/ubiquinone/
When vitamin e1 .2~2.3 part.
8. dried noodle film according to claim 1, which is characterized in that the ingredient including following parts by weight: ascorbic acid glucose
2 parts of glycosides, 2 parts of honey, 2 parts of Cer NS, safflower seed oil/gold bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/general
2 parts of quinone/vitamin E, 1 part of palmityl tripeptides -5,0.2 part of disodium ethylene diamine tetraacetate, 5 parts of olive oil and tocopherol second
4 parts of acid esters.
9. dried noodle film according to claim 8, which is characterized in that further include the ingredient of following parts by weight: octadecanoic acid
14 parts, 1 part of polyethylene glycol (400) stearate, 0.4 part of carbopol, 2~30 parts of 1,3- propylene glycol, Butyrospermum parkii fruit rouge 24
Part, 4 parts of cetanol ricinoleate, water/2 parts of propylene glycol/phytosterol, 10 parts of glycerine, 6 parts of water, Lavender 0.4
Part, 8 parts of animal saualane, 2 parts of egg oil and 10 parts of 1,3- propylene glycol.
10. a kind of preparation method of the dried noodle film as described in claim 4 or 9, which comprises the following steps: 1) will
Octadecanoic acid, Butyrospermum parkii fruit rouge, tocopherol acetate, cetanol ricinoleate, tocopherol, olive oil, safflower
Seed oil/golden bachelor's button/leaf/stem extraction/Astragalus membranacus root extract/ubiquinone/vitamin E, polyethylene glycol (400) stearate
It is added in heating stirring bucket with egg oil according to weight ratio, opens 200 revs/min of stirring, be warming up to 70-85 DEG C and be stirred
It is even；
2) carbopol, water, disodium ethylene diamine tetraacetate and 1,3-PD are added in heating stirring bucket according to weight ratio,
150 revs/min of stirring is opened, 80-95 DEG C is warming up to and is stirred；
3) mixture obtained in step 2 is added in the mixture of step 1), carries out emulsifying, until emulsification completion, stirring
It is cooled to 45 DEG C；
4) by ascorbic acid glucoside, Cer NS, palmityl tripeptides -5, water/propylene glycol/phytosterol, honey and clothing is smoked
Careless essential oil is added above-mentioned in step 3) mixture according to weight ratio, is stirred；
5) Material in step 4) is taken out, it is filling carries out facial mask.
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| CN110339142A (en) * | 2019-08-07 | 2019-10-18 | 广州雷诺生物科技有限公司 | A kind of fullerene moisturizing maintenance dried noodle film and preparation method thereof |
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| CN112618419A (en) * | 2021-01-12 | 2021-04-09 | 合肥香觉健康咨询有限公司 | Aromatic essential oil face cream |
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