CN104546650A - Skin-tightening mask and production method thereof - Google Patents
Skin-tightening mask and production method thereof Download PDFInfo
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- CN104546650A CN104546650A CN201410837729.4A CN201410837729A CN104546650A CN 104546650 A CN104546650 A CN 104546650A CN 201410837729 A CN201410837729 A CN 201410837729A CN 104546650 A CN104546650 A CN 104546650A
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Abstract
The invention discloses a skin-tightening mask and a production method thereof. The mask is prepared from water used as a solvent, glycerin, butylene, squalane and sodium hyaluronate which are used as moisturizers, polydimethylsiloxane and polysorbate-60 which are used as emulsifiers, tocopherol, D-panthenol and carnosine which are used as emollients, methylparaben and phenoxyethanol which are used as preservatives, an ammonium acryloyldimethyltaurate/VP copolymer and carbomer which are used as thickeners, royal jelly, a bird's nest extract, hydrolysis collagen and Ultra Filling Spheres which are used as skin conditioners, triethanolamine used as a PH regulator, PEG-40 hydrogenated castor oil used as a solubilizer as well as essence. The mask can reduce looseness caused by skin dryness after makeup, tighten facial skin, shrink pores, delay aging, fade dry and thin winkles, supplement the skin with required nutrition and moisture, keep the healthy function of the skin and keep the skin moistened and transparent all day.
Description
Technical field
The present invention relates to a kind of facial film, be specially facial film of a kind of skin that compacts and preparation method thereof.
Background technology
Make up very important to the damage of skin, if maintain improper, easily accelerate skin ageing, easily occur lax, wrinkle.Facial film, as a special toiletries, does not stimulate skin due to easy to use, safe, can frequently use, become in skin care item market the category of status of being more and more active.2001-2009, facial film is the highest one of speedup in each subclass of skin care item, and speedup is up to 31%.Within 2009, the market share is more than 4,500,000,000 yuan, and along with the recovery of economy, the market sale of 2010-2015 facial film shows a rising trend, and market will be more ripe, and the projected market total volume of retail sales will reach 130-300 hundred million.In recent years, there is brand-new bright spot in skin care item market, and it has led the brand-new faddish trend of skin care item, particularly aging-resistant skin care item to have new development speed, and continues to sell well.At present, facial film market only has a small amount of V face film, but the most of non-facial film aiming at the crowd's customization often making up and focus on maintenance of this series products, there is specific aim not strong, the shortcoming that nursing effect is poor.
Summary of the invention
For overcoming the defect of prior art, of the present inventionly be the facial film that a kind of skin that compacts is provided, it can reduce the relaxation that rear xerosis cutis of making up is brought, to compact facial skin, receive fine, soft fur hole, slow down aging, desalinate dry stricture of vagina microgroove, supplement skin desired nutritional and moisture, keep the healthy function of skin, keep skin to be full of profit water all day saturating.
Another object of the present invention is to the manufacture method of the facial film that a kind of skin that compacts is provided.
The technical solution adopted in the present invention is as follows for achieving the above object:
Compact the facial film of skin, and it is characterized in that, it is prepared from by following raw material by mass percentage:
In above-mentioned formula, using water as solvent; Using glycerol, butanediol, squalane, hyaluronate sodium as wetting agent; Using polydimethylsiloxane, polysorbate-60 as emulsifying agent; Using tocopherol, D-panthenol, carnosine as emollient; Using methyl hydroxybenzoate, phenoxyethanol as antiseptic; Using AVC, carbomer as thickening agent; Using Lac regis apis, Nidus collocaliae extract, hydrolytic collagen, UltraFilling Spheres as skin conditioning agent; Using triethanolamine as PH regulator; Using Cremophor RH40 as solubilizing agent.
In the present invention, above-mentioned raw materials all obtains by buying.
Squalane is pinch highly finished product gone out from the liver of the large-scale shark of principal and interest abyssal environment, and the hydrocarbons be made up of six isoprene double bonds, belongs to polyisoprenoid structure.(Squalane: strengthen maintenance epidermis, effectively forms natural protecting film to squalane, helps the balance between skin and sebum.Squalane is a kind of lipid closest to human sebaceous, and affinity is strong, can combine together, form the natural barrier of one deck at skin surface with the sebum film of mankind itself; Squalane can also suppress the peroxidating of skin lipid, effectively can infiltrate through skin, and promotes the propagation of skin base cell, and to delay skin aging, improving and eliminating chloasma all has obvious physiologic effect; Squalane also can make skin pore open, and promotes blood microcirculation, promotes the metabolism of cell, helps to repair damaged cell.
Lac regis apis contains many nutritional labelings and ingredient, can strengthen the vigor of epidermis cell, improves the metabolism of skin, makes drying, crowfoot cracks, lax skin become sliding tender, flexible.Acidic materials wherein have anti-inflammation, regulation of skin physiology and treat dermopathic effect.Lac regis apis not only can improve the antiseptic property of cosmetics, also helps the injured and blackening from ultraviolet stimulates of protection skin.Because the ultraviolet in sunlight can strengthen the activity of tryrosinase in skin, thus accelerate melanic formation, Royal Jelly acid then can the activity of remarkable restraint of tyrosinase, stops melanic formation.Lac regis apis can not only make skin lubrication, exquisiteness, has beauty treatment to protect effect of face, and effectively can prevent and treat some common skin diseases, has certain curative effect to acne, brown patch, seborrheic dermatitis etc.
Carnosine, formal name used at school β-alanyl-L-histidin, by being a kind of dipeptides be made up of Beta-alanine and L-Histidine two seed amino acid.Carnosine has very strong oxidation resistance, useful to human body.Carnosine has been proved to remove and in oxidative stress process, has made the fatty acid over oxidation of cell membrane and the reactive oxygen free radical (ROS) formed and alpha-beta unsaturated aldehyde.
Nidus collocaliae extract has toxin expelling effect, and the long-term edible object that can reach slow down aging, can strengthen immunologic function on the one hand, has antioxidation again on the other hand, pre-anti-aging in have very strong antagonism.Directly can buy from market, or adopt preparation with the following method: 1) Nidus collocaliae freezing and pulverizing sieves, and adds the water of Nidus collocaliae dry weight 20 times amount, ultrasonic water extraction 1 hour under room temperature, filters; 2) add the water of Nidus collocaliae dry weight 30 times amount in filter cake, under mechanical agitation, boil 60 minutes; 3) be cooled to room temperature, Na2CO3 solution adjust pH to 9.8, adds the alkaline protease of Nidus collocaliae dry weight 1.5%, mechanical agitation lower 55 DEG C of water-baths hydrolysis 3h; 4) 85 DEG C of enzyme-deactivating 20min; 5) be cooled to room temperature, rare HCl adjust pH is to neutral; 6) filter, filtrate and supersound extraction liquid merge, and obtain powdery Nidus collocaliae extract after lyophilization.
Hydrolytic collagen: the collagen protein amount in added body, makes skin recover elasticity, reappears and solidly to compact, reduce sagging phenomenon, smooth fine lines and wrinkle.
Ultra Filling Spheres penetrates into based on dehydration and crosslinked spherula the characteristic that the moisture evaporated from skin corium is also pinned on epidermis upper strata.Due to its moisture pick-up properties, spheroid volume increases sharply, and expands, thus tightens up skin, level and smooth wrinkle, gives elasticity of skin, long-acting moistening effect.
Compact the manufacture method of facial film of skin, its concrete steps are as follows:
1) according to formulation ratio solvent and wetting agent added in aqueous phase pot and carry out homogenizing stirring, make wetting agent dispersing and dissolving even, maintain the temperature at more than 80 DEG C;
2) step 1) process after raw material be transferred in emulsifying pot, in emulsifying pot, add thickening agent according to formulation ratio, carry out homogenizing stirring, make emollient dispersing and dissolving even;
3) according to formulation ratio, emulsifying agent is placed in oil phase pot, is warming up to more than 80 DEG C, then by its suction emulsifying pot, carry out homogenizing stirring, mixing time is 25 minutes; Then the temperature in emulsifying pot pot is kept to be in 70-90 DEG C of high temperature, be stirred to after material body fully dissolves and start cooling, when pot kettle temperature to be emulsified is down to below 45 DEG C, skin conditioning agent, emollient, solubilizing agent, PH regulator, antiseptic, essence is added respectively according to formulation ratio, stirring and dissolving is complete, filter, discharging;
4) leave standstill after discharging, subpackage, packaging, to obtain final product.
Preferably, step 1) in, mixing speed is 20r/min.
Preferably, step 1) in more than 80 DEG C, be incubated 3-8 minute at temperature.
Preferably, it is also included in step 3) step that product detected after discharging.
Preferably, step 4) intermediate package time, with facial mask cloth and PE bag heat-sealing fill.
Beneficial effect of the present invention is:
1, in formula of the present invention using water as solvent; Using glycerol, butanediol, squalane, hyaluronate sodium as wetting agent; Using polydimethylsiloxane, polysorbate-60 as emulsifying agent; Using tocopherol, D-panthenol, carnosine as emollient; Using methyl hydroxybenzoate, phenoxyethanol as antiseptic; Using AVC, carbomer as thickening agent; Using Lac regis apis, Nidus collocaliae extract, hydrolytic collagen, Ul traFilling Spheres as skin conditioning agent; Using triethanolamine as PH regulator; Using Cremophor RH40 as solubilizing agent, between each component, there is synergistic function, utilize the tightening effect of hydrolytic collagen, reduce the generation of microgroove, improve the perfect effect of face mask, strengthen skin tightness, add multiple skin nutrition material simultaneously, eliminate facial edema, activate and repair subcutaneous collagen albumen, strong V face effect.
2, preparation method of the present invention can make each component fully merge, thus has given play to best effect, has step simple, easy to operate, the feature that cost is low.
In sum, the present invention is by the compatibility of above-mentioned raw materials and the production technology that the present invention is directed to above-mentioned recipe design, the relaxation that after enabling whole product reduce cosmetic, xerosis cutis is brought, to compact facial skin, receive fine, soft fur hole, slow down aging, desalinate dry stricture of vagina microgroove, supplement skin desired nutritional and moisture, keep the healthy function of skin, keep skin to be full of profit water all day saturating.This product is especially applicable to cosmetic crowd and uses, and provides effect from following three aspects.Removing edema: enhance metabolism, gets rid of edema, helps steatolysis, and has extraordinary anti-oxidation efficacy, the microgroove preventing cell senescence from producing, wrinkle, promotes face contour.Firming and moisturizing: strengthen skin support force, promotes skin degree of compacting, allows skin water moisten penetrating elastic force pure.Slow down aging: slow down aging, effectively reduces the generation of wrinkle, the appearance retained youth.
Detailed description of the invention
Below in conjunction with concrete embodiment, the present invention is described in further detail.
Embodiment 1-5:
Get following raw material by weight percentage respectively:
Glycerol, butanediol, squalane, polydimethylsiloxane, polysorbate-60, Lac regis apis, hyaluronate sodium, D-panthenol, Nidus collocaliae extract, carnosine, hydrolytic collagen, tocopherol, AVC, ULTRA FILLING SPHERES, carbomer, triethanolamine, methyl hydroxybenzoate, phenoxyethanol, Cremophor RH40, essence, water.
Concrete proportioning is in table 1.
The proportioning table of table 1 embodiment 1-5
Compact the manufacture method of facial film of skin, its concrete steps are as follows:
1) solvent and wetting agent to be added in aqueous phase pot according to formulation ratio and carry out homogenizing stirring, make wetting agent dispersing and dissolving even, mixing speed is 20r/min, more than 80 DEG C, be incubated 3-8 minute at temperature;
2) step 1) process after raw material be transferred in emulsifying pot, in emulsifying pot, add thickening agent according to formulation ratio, carry out homogenizing stirring, make emollient dispersing and dissolving even;
3) according to formulation ratio, emulsifying agent is placed in oil phase pot, is warming up to more than 80 DEG C, then by its suction emulsifying pot, carry out homogenizing stirring, mixing time is 25 minutes; Then the temperature in emulsifying pot pot is kept to be in 70-90 DEG C of high temperature, be stirred to after material body fully dissolves and start cooling, when pot kettle temperature to be emulsified is down to below 45 DEG C, skin conditioning agent, emollient, solubilizing agent, PH regulator, antiseptic, essence is added respectively according to formulation ratio, stirring and dissolving is complete, filter, discharging, detects product;
4) leave standstill after discharging, subpackage, during packaging, with facial mask cloth and PE bag heat-sealing fill., to obtain final product.
The using method of the facial film of the described skin that compacts is:
1, tear packaging, take out and launch facial film, about horizontal hangers hole each 3, each 4 of cervical region hangers hole;
2, adjust the horizontal hangers film of buccal position, select the position, hangers hole more sticked in face, carry and be hung on ear; 3, adjust longitudinal hangers film of neck location, select the position, hangers hole more sticking shape of face, carry and be hung on ear;
4, smooth the bubble of facial film, mind at rest, the 360 degree of three-dimensional skin protections of 4D moment, enjoy the shining change of exquisite V face;
5, after 15-20 minute, facial film is taken off;
6, after using, facial remaining elite can be cleaned with clear water, also can massage gently and allow skin naturally absorb.
Testing example 1: to the moistening effect of skin.
Keratodermatitis hydration rate is tested: operation principle take capacitor as instrument probe, because water is the material that on skin, dielectric constant is maximum, when skin moisture content changes, the capacitance of skin also changes, so can by measuring skin pricktest capacitance, analyzing skin surface moisture content.Conventional instrument is Corneometer CM825.By measuring the change using the change of keratodermatitis capacitance before and after product to weigh water content of stratum corneum, thus moisture-keeping efficacy this kind of method evaluating facial film carries out quantification to the moisture of keratodermatitis, the change of skin moisture content can be reacted delicately, and favorable reproducibility, be one of method that current moisture saver mask efficacy assessments is conventional.
Experimental technique: bend side at candidate left and right forearm and mark 3 × 3cm
2the square Experimental Area of size, using left arm as the test zone of moisturizer, the corresponding symmetrical region of right arm is blank, then detects the moisture at each test position with Corneometer CM825 test, repeats 5 times respectively, draw meansigma methods.By formula (1) calculated hydration rate.
Hydration rate=(test value-blank value)/blank value × 100% formula (1)
The detection of moistening effect, result is as shown in table 2:
Table 2
| Time | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| 1h | 75％ | 75％ | 76％ | 75％ | 75％ |
| 2h | 60％ | 61％ | 65％ | 62％ | 60％ |
| 4h | 38％ | 44％ | 49％ | 44％ | 45％ |
| 6h | 37％ | 40％ | 48％ | 40％ | 37％ |
| 8h | 36％ | 35％ | 47％ | 36％ | 35％ |
As can be seen from Table 2, in moisturizing, the effect of the use of the skin adornment facial film that compacts described in embodiment 1-5 is all very excellent, and the result of use of the skin adornment facial film that compacts described in embodiment 3 is best.
Testing example 2: the effect of the skin that compacts.
Evaluating method: the facial film of what Example 1-5 obtained compact skin, whether to some extent then select 500 volunteers, it is one group that every 100 volunteers compile, the facial film of the skin that compacts respectively, the texture consolidation of skin before and after contrast uses.
Compacting effect adopts following three indexs:
A is effective: skin pattern obviously shoals;
B effect is general: skin pattern shoals a little;
C weak effect: skin pattern is unchanged;
Concrete outcome refers to following table 3:
Table 3: the measure of merit tables of data of the skin that compacts of embodiment 1-5 facial film
| Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 | |
| A | 92 | 94 | 99 | 97 | 96 |
| B | 7 | 4 | 1 | 3 | 3 |
| C | 1 | 2 | 0 | 0 | 1 |
Note: the digitized representation in table 2 be number, in form as crossing with A in embodiment 1 100, represent, use in the volunteer of the facial film of embodiment 1, the effective number of test facial film is 92 people.
Data as can be seen from this form, in skin effect of compacting, the effect of the use of the facial film of the skin that compacts described in embodiment 1-5 is all very excellent, and the result of use of the facial film of the skin that compacts described in embodiment 3 is best.
Testing example 3: crease-resistant effect.
Body aging is a complicated process, if improve body self to the Scavenging activity of free radical, just can reach the effect of antioxidation, slow down aging.The present invention adopts DPPH method (Zhao Jun, Zhang Yi, Deng, comparing [J] of the activity of 20 kinds of Chinese herbal medicine alcohol extracts and aqueous extract scavenging free radicals. Tianjin Chinese medicine, 2007,24 (1): 69-70) the clearance rate of DPPH is tested to the facial film of embodiment 1-5, concrete test result refers to following table 4:
The clearance rate tables of data to DPPH of the facial film of table 4: embodiment 1-5
| Group | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Embodiment 5 |
| Clearance rate | 88％ | 92％ | 99％ | 95％ | 93％ |
In order to test the wrinkle resistance of facial film of the present invention more intuitively, inventor finds 500 face volunteers wrinkly, every 100 volunteers are 1 group, use the facial film of embodiment 1-5 respectively, sooner or later respectively apply once, each 30min, continues 2 months, then record the 10th day, the 20th day, the 30th day that starts from face mask film and the 60th day the number that wrinkle attenuates, number tails off, concrete outcome refers to following table 5:
The facial film wrinkle resistance test data table of table 5 embodiment 1-5
| Rating scale | 10 days | 20 days | 30 days | 60 days | Effective percentage |
| Embodiment 1 | 13 | 32 | 78 | 90 | 90％ |
| Embodiment 2 | 14 | 35 | 79 | 94 | 94％ |
| Embodiment 3 | 23 | 53 | 90 | 98 | 98％ |
| Embodiment 4 | 19 | 40 | 82 | 95 | 95％ |
| Embodiment 5 | 19 | 42 | 86 | 94 | 94％ |
As can be seen from data in table 5, in wrinkle resistance, the effect of the use of the facial film of the skin that compacts described in embodiment 1-5 is all very excellent, and the result of use of the facial film of the skin that compacts described in embodiment 3 is best.
Above-mentioned embodiment is only the preferred embodiment of the present invention; can not limit the scope of protection of the invention with this, change and the replacement of any unsubstantiality that those skilled in the art does on basis of the present invention all belong to the present invention's scope required for protection.
Claims (6)
1. compact the facial film of skin, and it is characterized in that, it is prepared from by following raw material by mass percentage:
In above-mentioned formula, using water as solvent; Using glycerol, butanediol, squalane, hyaluronate sodium as wetting agent; Using polydimethylsiloxane, polysorbate-60 as emulsifying agent; Using tocopherol, D-panthenol, carnosine as emollient; Using methyl hydroxybenzoate, phenoxyethanol as antiseptic; Using AVC, carbomer as thickening agent; Using Lac regis apis, Nidus collocaliae extract, hydrolytic collagen, UltraFi l l ing Spheres as skin conditioning agent; Using triethanolamine as PH regulator; Using Cremophor RH40 as solubilizing agent.
2. the manufacture method of the facial film of the skin that compacts according to claim 1, is characterized in that, its concrete steps are as follows:
1) according to formulation ratio solvent and wetting agent added in aqueous phase pot and carry out homogenizing stirring, make wetting agent dispersing and dissolving even, maintain the temperature at more than 80 DEG C;
2) step 1) process after raw material be transferred in emulsifying pot, in emulsifying pot, add thickening agent according to formulation ratio, carry out homogenizing stirring, make emollient dispersing and dissolving even;
3) according to formulation ratio, emulsifying agent is placed in oil phase pot, is warming up to more than 80 DEG C, then by its suction emulsifying pot, carry out homogenizing stirring, mixing time is 25 minutes; Then the temperature in emulsifying pot pot is kept to be in 70-90 DEG C of high temperature, be stirred to after material body fully dissolves and start cooling, when pot kettle temperature to be emulsified is down to below 45 DEG C, skin conditioning agent, emollient, solubilizing agent, PH regulator, antiseptic, essence is added respectively according to formulation ratio, stirring and dissolving is complete, filter, discharging;
4) leave standstill after discharging, subpackage, packaging, to obtain final product.
3. the manufacture method of the facial film of the skin that compacts according to claim 2, is characterized in that: step 1) in, mixing speed is 20r/min.
4. the manufacture method of the facial film of the skin that compacts according to claim 2, is characterized in that: step 1) in more than 80 DEG C, be incubated 3-8 minute at temperature.
5. the manufacture method of the facial film of the skin that compacts according to claim 2, is characterized in that: it is also included in step 3) step that product detected after discharging.
6. the manufacture method of the facial film of the skin that compacts according to claim 2, is characterized in that: step 4) intermediate package time, with facial mask cloth and PE bag heat-sealing fill.
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| CN107320355A (en) * | 2017-07-27 | 2017-11-07 | 广州赛莱拉干细胞科技股份有限公司 | A kind of collagen protein face and preparation method thereof |
| CN107374992A (en) * | 2017-08-07 | 2017-11-24 | 吕玲 | The crease-resistant Face-protecting mask that compacts of lycopene |
| CN108714207A (en) * | 2018-05-31 | 2018-10-30 | 李珍 | Activating qi and collateral cream |
| CN109172506A (en) * | 2018-11-14 | 2019-01-11 | 大连欧麦莎实业有限公司 | It is a kind of containing there are many bird's nest facial masks of Sodium Hyaluronate and preparation method thereof |
| CN109223610A (en) * | 2018-11-09 | 2019-01-18 | 艾因特丽（苏州）生物科技有限公司 | A kind of multifunctional beauty film patch with 4D |
| CN109966234A (en) * | 2019-05-10 | 2019-07-05 | 西安天久肽健康科技有限公司 | A kind of donkey-hide gelatin bird's nest peptide facial mask and preparation method thereof |
| CN110169940A (en) * | 2019-07-01 | 2019-08-27 | 广州市如馨化妆品有限公司 | A kind of Biofibre facial mask Essence having thin face function, preparation method and the facial mask using Essence preparation |
| CN110693744A (en) * | 2019-10-29 | 2020-01-17 | 佛山科学技术学院 | Semi-permeable cubilose cream |
| CN111317684A (en) * | 2018-12-13 | 2020-06-23 | 宋超 | Mask containing cyperus esculentus root oil and preparation method thereof |
| CN111773170A (en) * | 2020-08-03 | 2020-10-16 | 广州虹美生物科技有限公司 | Facial mask patch added with grease and preparation method |
| US20220133622A1 (en) * | 2020-10-30 | 2022-05-05 | Mary Kay Inc. | Instant effect eye cream |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107320355A (en) * | 2017-07-27 | 2017-11-07 | 广州赛莱拉干细胞科技股份有限公司 | A kind of collagen protein face and preparation method thereof |
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| CN109172506A (en) * | 2018-11-14 | 2019-01-11 | 大连欧麦莎实业有限公司 | It is a kind of containing there are many bird's nest facial masks of Sodium Hyaluronate and preparation method thereof |
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| CN109966234A (en) * | 2019-05-10 | 2019-07-05 | 西安天久肽健康科技有限公司 | A kind of donkey-hide gelatin bird's nest peptide facial mask and preparation method thereof |
| CN110169940A (en) * | 2019-07-01 | 2019-08-27 | 广州市如馨化妆品有限公司 | A kind of Biofibre facial mask Essence having thin face function, preparation method and the facial mask using Essence preparation |
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| CN111773170A (en) * | 2020-08-03 | 2020-10-16 | 广州虹美生物科技有限公司 | Facial mask patch added with grease and preparation method |
| US20220133622A1 (en) * | 2020-10-30 | 2022-05-05 | Mary Kay Inc. | Instant effect eye cream |
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Effective date of registration: 20180523 Address after: 510550 Room 201, Hongqi Road, bamboo material industrial zone, Zhong Luo Tan Town, Baiyun District, Guangzhou, Guangdong, China, 72 Patentee after: Guangzhou Jie Xin Cosmetics Co., Ltd. Address before: 528400 2 Zhongshan science and Technology Road 32, torch high tech Industrial Development Zone, Guangdong Patentee before: GUANGDONG JIEXIN BIOTECHNOLOGY CO., LTD. |
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