CN111317684A

CN111317684A - Mask containing cyperus esculentus root oil and preparation method thereof

Info

Publication number: CN111317684A
Application number: CN201811559514.5A
Authority: CN
Inventors: 宋超
Original assignee: Individual
Current assignee: Individual
Priority date: 2018-12-13
Filing date: 2018-12-13
Publication date: 2020-06-23

Abstract

The invention discloses a mask containing cyperus esculentus root oil and a preparation method thereof, wherein cyperus esculentus root oil rich in vitamin E and linoleic acid is compatible with water replenishing, moisturizing, soothing and antioxidant components, and the mask containing cyperus esculentus root oil is prepared by adopting a modern technology.

Description

Mask containing cyperus esculentus root oil and preparation method thereof

Technical Field

The invention relates to the technical field of skin care products, in particular to a mask containing cyperus esculentus root oil and a preparation method thereof.

Background

With the improvement of living standard of people, people pay more and more attention to the pursuit of beauty, so that people pay more and more attention to skin care in daily life, wherein the facial mask is also a choice of many people due to the convenience in use and the instant effect. Daily makeup, long-term use of air conditioners, more and more people facing computer screens, and also people having over-cleansing of facial skin, frequent exfoliation, etc., all of which cause the skin barrier to be damaged, thus causing a series of skin problems such as: after the face is cleaned, the skin is dry and tight, and has scurf, but the skin grease is exuberantly secreted in a short time, so that pores are blocked, and acnes, pimples, mouth closure and the like are caused; the acquired sensitive muscles are formed, so that the skin is easy to generate red and stabbing pain and the like due to external stimulation. These are all due to the impaired skin barrier and the reduced barrier function. However, the traditional mask can only achieve the effects of temporarily supplementing water, controlling oil and the like generally at present, and the problem of skin barrier damage is difficult to be solved fundamentally.

Research shows that the roots of the cyperus rotundus contain rich grease, the cyperus rotundus root oil extracted from the cyperus rotundus roots is rich in vitamin E and linoleic acid, can prevent skin damage, can be used as a skin conditioner to be added into skin care products and cosmetics, can enhance the barrier function of the skin, has the effects of moisturizing, improving the glossiness of the skin and tendering the skin, and enables the skin to be kept in a healthy state. The applicant manages agricultural science and technology companies to plant a large amount of cyperus esculentus, and cyperus esculentus roots can extract cyperus esculentus root oil, so the applicant invents a mask added with cyperus esculentus root oil to solve various skin problems caused by the damage of skin barriers which cannot be fundamentally solved by the existing mask.

Disclosure of Invention

The invention aims to provide a mask containing cyperus esculentus root oil and a preparation method thereof, so as to repair damaged skin barriers and fundamentally solve the problems of skin dryness, oil generation, sensitivity and aging.

In order to achieve the purpose, the invention provides the following scheme:

the invention provides a mask containing cyperus rotundus root oil, which comprises the following components in percentage by weight:

preferably, the extraction method of the cyperus esculentus root oil comprises the following steps: cleaning and airing the cyperus esculentus roots, squeezing, extracting at 25-45 ℃ to obtain oily liquid, and distilling the obtained oily liquid to obtain the pure cyperus esculentus root oil.

The invention provides a preparation method of a mask containing cyperus rotundus root oil, which comprises the following steps:

(1) putting the phase B into a heating container, heating to 75-84 ℃, stirring to uniformly mix the components, homogenizing for 6-10 minutes, cooling to 58-62 ℃, and preserving heat for 30-60 minutes;

(2) adding the phase A into the phase B, stirring to uniformly mix the components in the phase A into the phase B, and homogenizing for 10-15 minutes;

(3) adding the phase C and stirring uniformly;

(4) and cooling to 20-30 ℃, adding the phase D, uniformly stirring, homogenizing for 30-45 minutes, and performing vacuum deaeration to obtain the smearing type mask containing the cyperus oil.

Preferably, the mask containing cyperus esculentus root oil prepared by the method comprises 1.5-3% by mass of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer and 0.2-0.55% by mass of carbomer.

The invention also provides a preparation method of the mask containing the cyperus rotundus root oil, which comprises the following steps:

(3) adding the phase C and stirring uniformly;

(4) and cooling to 20-30 ℃, adding the phase D, uniformly stirring, homogenizing for 30-45 minutes, and soaking the mask base cloth in the mask base cloth after vacuum defoaming to obtain the sheet mask containing the cyperus oil.

Preferably, the mask containing cyperus esculentus root oil prepared by the method is 0.5-2% of hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer by mass and 0.05-0.3% of carbomer by mass.

Preferably, the mask containing the cyperus rotundus oil prepared by the method is a mask base cloth which is a mixture of one or more of silk, non-woven fabrics, cotton fibers, bamboo charcoal fibers, keratin fibers and chitosan fibers.

The main components and the effects of the invention are as follows:

1. cyperus oil: the essential oil extracted from the cyperus esculentus roots is rich in vitamin E and linoleic acid, can prevent skin damage, can be added into skin care products and cosmetics as a skin conditioner, can enhance the barrier function of skin, has the effects of moisturizing, improving the glossiness of the skin and tendering the skin, and keeps the skin in a healthy state.

2. Butanediol: the skin care product is widely used as a small molecular moisture retention component in skin care products, can retain water in the horny layer, has good hygroscopicity, can absorb water which is equivalent to 12.5 percent (relative humidity is 50 percent) and 38.5 percent (relative humidity is 80 percent) of the mass of the skin care product, and also has a certain bacteriostatic action.

3. Propylene glycol: has good viscosity and hygroscopicity, and is non-toxic, and thus is widely used as a moisture absorbent, an anti-freezing agent, a lubricant and a solvent in the food, pharmaceutical and cosmetic industries. Propylene glycol is also used as a solvent, a softener and the like of cosmetics because of better intersolubility with various perfumes.

4. Erythritol: has strong moisture retention and moisture absorption, can be used as a humectant for cosmetics like glycerin, but has no greasy and sticky feeling like glycerin.

5. Saccharide isomerate: is a natural humectant extracted from natural plant saccharide complex, is similar to carbohydrate complex in human body, and has good skin-friendly effect. The keratin of the horny layer is assisted in combining water by combining with free amino acid groups of lysine on the keratin in cells of the horny layer, and the keratin cannot be easily washed off, so that the lasting moisturizing effect is achieved.

6. Carbohydrate hydrolysate: has good moisture absorption, and can be added into cosmetic to achieve effects of absorbing moisture and keeping moisture.

7. The hydrolyzed oat protein can be quickly absorbed by skin, has no greasy feeling, is suitable for being used as a nutritional skin-care raw material of cosmetics, the transforming growth factor β is also called a multifunctional proliferation factor, exists in the dermis layer of the skin, the increase of the transforming growth factor is equal to the proliferation of fibroblasts and the promotion of collagen generation, so the hydrolyzed oat protein can increase the content of collagen in the cortex, maintain the integrity of the skin structure, keep the skin elasticity and have the functions of resisting senility and wrinkles, and the hydrolyzed oat protein has certain surface activity and has the functions of assisting emulsification, foaming and stabilizing foam.

8. Dipotassium glycyrrhizinate: the glycyrrhizin (glycyrrhizic acid) component mainly comprising root and stem parts of Glycyrrhrizae radix is suitable for allergic skin, and has effects of resisting irritation, controlling oil, reducing red swelling, relieving inflammation and healing. Can effectively prevent sensitive inflammation phenomenon when skin is stimulated. Has the effects of diminishing inflammation and tranquilizing caused by sunshine, and is often used in antiallergic and repairing cosmetics.

9. Sodium hyaluronate: the acid mucopolysaccharide belongs to a skin conditioner, is naturally present in corneal epithelium, and can absorb 1000 times of moisture of the corneal epithelium by weight so as to achieve the purposes of keeping skin moisture, preventing the moisture from losing through epidermis, and repairing a barrier when the skin is damaged, so that the skin does not feel dry after being used, and the luster is increased. It can improve skin nutrition metabolism, make skin soft and smooth, remove wrinkle, increase elasticity, prevent aging, and keep moisture while being good skin penetration enhancer. The nutrient can be used together with other nutrient components to achieve the more ideal effect of promoting nutrient absorption.

10. Hydrolyzing sclerotium rolfsii gum: the natural polysaccharide polymer is stable at various pH values under high temperature, is a polysaccharide polymer, has good compatibility with skin, can effectively form a film, and is stable.

11. Hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer: can be used as emulsifier, thickener, and viscosity regulator in cosmetics.

12. Disodium EDTA: mainly used as chelating agent for stabilizing in cosmetics, and mineral chelating agent for synergistic antiseptic effect. And has a certain synergistic effect on an anticorrosion system and an antioxidant system.

13. Carbomer: belongs to high molecular polymer, thickening agent, gel and emulsion stabilizer. Has good transparency, and carbomer has good compatibility with pH, and can be used in neutral acid or alkaline environment. In the case of electrolytes, the hydrogel is not electrolyte-resistant. In the surfactant system, the surfactant has good cooperativity with electrolyte.

14. Triethanolamine: a white loose powder; has characteristic slight odor and hygroscopicity, and can be used for regulating pH of cosmetic. Triethanolamine is the most common neutralizer of acidic polymer gel containing carbomer and the like, and forms a stable polymer structure through neutralization with carboxyl of carbomer, so that the application effects of thickening and moisturizing are achieved.

15. P-hydroxyacetophenone: is a natural plant extract, and is naturally present in stems and leaves of Artemisia scoparia of Compositae, and roots of Artemisia capillaris Thunb, Asclepiadaceae plant, and radix Ginseng Tylophorae Yunnanensis. A multifunctional cosmetic ingredient having antioxidant and soothing effects; the preservative can be used as a substitute of the traditional preservative in cosmetics, has the functions of antisepsis and synergism, can promote the efficacy of various preservatives, and has excellent stability in high and low pH and temperature ranges. Can be used in various formulas, and has good compatibility with various cosmetic components and packaging materials.

16. Caprylyl hydroximic acid: is an ideal bacteriostatic organic acid. Has high-efficiency and selective chelating capacity for ferrous ions and ferric ions, and has limited growth of mould in an environment with limited ferric ions. And has the optimal carbon chain length capable of promoting the degradation of the cell membrane structure. Therefore, the antibacterial agent has stronger antibacterial capability and is a novel substitute substance for the preservative.

17. Glyceryl caprylate: the cosmetic can be used as skin softening agent and emulsifier.

Compared with the prior art, the invention has the following beneficial technical effects:

1. according to the mask containing the cyperus esculentus root oil, the cyperus esculentus root oil rich in vitamin E and linoleic acid is compatible with water replenishing, moisturizing, soothing and antioxidant ingredients, and the mask containing the cyperus esculentus root oil is prepared by adopting a modern technology.

2. The mask containing the cyperus esculentus root oil does not contain essence and traditional preservatives, is high in safety and does not irritate the skin.

3. The mask containing the cyperus esculentus root oil provided by the invention is simple in material components, reasonable in formula, low in cost and easy to popularize.

4. The mask containing the cyperus esculentus root oil widens the new application field of cyperus esculentus and brings great economic and social benefits.

5. The preparation method of the mask containing the cyperus esculentus root oil, provided by the invention, is simple in process, easy to operate and easy to realize large-scale production.

Detailed Description

The technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.

The invention aims to provide a mask containing cyperus rotundus root oil and a preparation method thereof, aiming at solving various skin problems caused by the fact that the existing mask cannot fundamentally solve skin barriers, cyperus rotundus root oil is compatible with water replenishing, moisturizing, soothing and antioxidant components, and the mask containing cyperus rotundus root oil is prepared by adopting a modern technology.

The present invention will be described in further detail with reference to specific embodiments in order to make the above objects, features and advantages more apparent and understandable.

Examples 1-5 components and mass percentages of components in the mask containing cyperus rotundus oil are shown in table 1:

TABLE 1

The preparation of example 1 is as follows:

(1) putting the phase B into a heating container, heating to 80 ℃, stirring to uniformly mix the components, homogenizing for 8 minutes, cooling to 60 ℃, and preserving heat for 45 minutes;

(2) adding the phase A into the phase B, stirring to uniformly mix the components in the phase A into the phase B, and homogenizing for 12 minutes;

(3) adding the phase C and stirring uniformly;

(4) and cooling to 25 ℃, adding the phase D, uniformly stirring, homogenizing for 38 minutes, and performing vacuum defoaming to obtain the smearing type facial mask containing the cyperus oil.

The preparation of example 2 is as follows:

(1) putting the phase B into a heating container, heating to 75 ℃, stirring to uniformly mix the components, homogenizing for 10 minutes, cooling to 58 ℃, and preserving heat for 60 minutes;

(2) adding the phase A into the phase B, stirring to uniformly mix the components in the phase A into the phase B, and homogenizing for 15 minutes;

(3) adding the phase C and stirring uniformly;

(4) cooling to 20 ℃, adding the phase D, stirring uniformly, homogenizing for 45 minutes, and performing vacuum deaeration to obtain the smearing type facial mask containing the cyperus oil.

The preparation of example 3 is as follows:

(1) putting the phase B into a heating container, heating to 84 ℃, stirring to uniformly mix the components, homogenizing for 9 minutes, cooling to 62 ℃, and preserving heat for 40 minutes;

(2) adding the phase A into the phase B, stirring to uniformly mix the components in the phase A into the phase B, and homogenizing for 10 minutes;

(3) adding the phase C and stirring uniformly;

(4) cooling to 30 ℃, adding the phase D, stirring uniformly, homogenizing for 30 minutes, and performing vacuum deaeration to obtain the smearing type facial mask containing the cyperus oil.

The preparation of example 4 is as follows:

(1) putting the phase B into a heating container, heating to 76 ℃, stirring to uniformly mix the components, homogenizing for 8 minutes, cooling to 59 ℃, and preserving heat for 30 minutes;

(2) adding the phase A into the phase B, stirring to uniformly mix the components in the phase A into the phase B, and homogenizing for 14 minutes;

(3) adding the phase C and stirring uniformly;

(4) and cooling to 21 ℃, adding the phase D, uniformly stirring, homogenizing for 42 minutes, and performing vacuum defoaming to obtain the application type facial mask containing the cyperus oil.

The preparation of example 5 is as follows:

(1) putting the phase B into a heating container, heating to 83 ℃, stirring to uniformly mix the components, homogenizing for 7 minutes, cooling to 61 ℃, and preserving heat for 50 minutes;

(2) adding the phase A into the phase B, stirring to uniformly mix the components in the phase A into the phase B, and homogenizing for 11 minutes;

(3) adding the phase C and stirring uniformly;

(4) and cooling to 29 ℃, adding the phase D, uniformly stirring, homogenizing for 33 minutes, and performing vacuum deaeration to obtain the smearing type facial mask containing the cyperus oil.

Examples 6 to 10 components and mass percentages of the components in the mask containing cyperus rotundus oil are shown in table 2:

TABLE 2

The preparation of example 6 is as follows:

(1) putting the phase B into a heating container, heating to 77 ℃, stirring to uniformly mix the components, homogenizing for 6 minutes, cooling to 60 ℃, and preserving heat for 35 minutes;

(2) adding the phase A into the phase B, stirring to uniformly mix the components in the phase A into the phase B, and homogenizing for 13 minutes;

(3) adding the phase C and stirring uniformly;

(4) cooling to 22 ℃, adding the phase D, uniformly stirring, homogenizing for 40 minutes, and soaking the mask base cloth in the mask base cloth after vacuum defoaming to obtain the sheet mask containing the cyperus oil.

The preparation of example 7 is as follows:

(1) putting the phase B into a heating container, heating to 82 ℃, stirring to uniformly mix the components, homogenizing for 10 minutes, cooling to 58 ℃, and preserving heat for 55 minutes;

(3) adding the phase C and stirring uniformly;

(4) cooling to 28 ℃, adding the phase D, homogenizing for 35 minutes after uniformly stirring, and soaking the mask base cloth in the mask base cloth after vacuum defoaming to obtain the sheet mask containing the cyperus oil.

The preparation of example 8 is as follows:

(1) putting the phase B into a heating container, heating to 78 ℃, stirring to uniformly mix the components, homogenizing for 7 minutes, cooling to 62 ℃, and preserving heat for 45 minutes;

(3) adding the phase C and stirring uniformly;

(4) cooling to 23 ℃, adding the phase D, uniformly stirring, homogenizing for 43 minutes, and soaking the mask base cloth in the mask base cloth after vacuum defoaming to obtain the sheet mask containing the cyperus oil.

The preparation of example 9 is as follows:

(1) putting the phase B into a heating container, heating to 81 ℃, stirring to uniformly mix the components, homogenizing for 9 minutes, cooling to 59 ℃, and keeping the temperature for 38 minutes;

(3) adding the phase C and stirring uniformly;

(4) and cooling to 27 ℃, adding the phase D, uniformly stirring, homogenizing for 32 minutes, and soaking the mask base cloth in the mask base cloth after vacuum defoaming to obtain the sheet mask containing the cyperus oil.

The preparation of example 10 is as follows:

(1) putting the phase B into a heating container, heating to 79 ℃, stirring to uniformly mix the components, homogenizing for 6 minutes, cooling to 61 ℃, and preserving heat for 52 minutes;

(3) adding the phase C and stirring uniformly;

(4) cooling to 24 ℃, adding the phase D, homogenizing for 37 minutes after uniformly stirring, and soaking the mask base cloth in the mask base cloth after vacuum defoaming to obtain the sheet mask containing the cyperus oil.

The extraction method of the cyperus alternifolius root oil in the embodiments 1-10 comprises the following steps: cleaning and airing the cyperus esculentus roots, squeezing, extracting at 25-45 ℃ to obtain oily liquid, and distilling the obtained oily liquid to obtain the pure cyperus esculentus root oil.

And (3) efficacy verification:

400 volunteers are selected and randomly divided into 10 groups, and each group contains 40 persons, and the mask containing cyperus esculentus root oil prepared in the embodiments 1-10 is tried for three times per week and is continuously tried for one month, and the frequency is three times per week. The mask containing cyperus esculentus root oil prepared in examples 1-5 is a coating type mask which can be used as a night sleep mask, and the mask is uniformly coated on the face skin after the face is cleaned and washed off in the morning of the next day. The mask containing the cyperus oil prepared in the examples 6-10 is a sheet-shaped mask, the mask is attached to the face after the face is cleaned, and the mask is removed after 15-20 minutes and is massaged until the skin of the face is fresh and not sticky. The results are summarized in Table 3:

TABLE 3

The masks prepared in examples 1 to 5 were sheet-like masks, and as can be seen from table 3, the effects of the masks obtained in examples 6 to 10 were not much different. Overall, for the embodiments 1-10, the effects of moisturizing, anti-allergy and tendering skin after more than 85% of the volunteers use the facial mask are better, and more than 80% of the volunteers show that the facial skin still keeps moist, tender and elastic after the trial is finished, and the sensitive phenomenon of stabbing pain and redness is obviously relieved, so that the mask containing the cyperus esculentus root oil provided by the invention can effectively and fundamentally solve the skin problem caused by the damaged skin barrier.

The principle and the implementation mode of the invention are explained by applying specific examples, and the description of the above examples is only used for helping understanding the method and the core idea of the invention; meanwhile, for a person skilled in the art, according to the idea of the present invention, the specific embodiments and the application range may be changed. In summary, this summary should not be construed to limit the present invention.

Claims

1. The mask containing cyperus esculentus root oil is characterized by comprising the following components in percentage by weight:

2. the mask containing cyperus esculentus oil according to claim 1, wherein: the extraction method of the cyperus esculentus root oil comprises the following steps: cleaning and airing the cyperus esculentus roots, squeezing, extracting at 25-45 ℃ to obtain oily liquid, and distilling the obtained oily liquid to obtain the pure cyperus esculentus root oil.

3. The method for preparing a mask containing cyperus esculentus root oil according to any one of claims 1 to 2, which comprises the following steps:

(3) adding the phase C and stirring uniformly;

4. A mask containing cyperus esculentus root oil prepared according to the method of claim 3, wherein: the mass percentage of the hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer is 1.5-3%, and the mass percentage of the carbomer is 0.2-0.55%.

5. The method for preparing a mask containing cyperus esculentus root oil according to any one of claims 1 to 2, which comprises the following steps:

(3) adding the phase C and stirring uniformly;

6. A mask containing Cyperus esculentus root oil prepared by the method according to claim 5, wherein: the mass percentage of the hydroxyethyl acrylate/sodium acryloyldimethyl taurate copolymer is 0.5-2%, and the mass percentage of the carbomer is 0.05-0.3%.

7. A mask containing Cyperus esculentus root oil prepared by the method according to claim 5, wherein: the facial mask base cloth is one or a mixture of silk, non-woven fabrics, cotton fibers, bamboo charcoal fibers, keratin fibers and chitosan fibers.