CN109172422B - Hyaluronic acid mask liquid and preparation method thereof - Google Patents
Hyaluronic acid mask liquid and preparation method thereof Download PDFInfo
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
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- A61Q19/08—Anti-ageing preparations
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A61K2800/52—Stabilizers
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention discloses a hyaluronic acid mask liquid and a preparation method thereof, wherein the hyaluronic acid mask liquid comprises the following components in percentage by weight: 0.05 to 0.2 percent of hydrolyzed sodium hyaluronate, 0.05 to 0.2 percent of betaine, 261.3 to 2.6 percent of glycerol polyether, 0.8 to 1.5 percent of luba gum oil, 2.5 to 4.0 percent of butanediol, 4.0 to 6.0 percent of hydroxyethyl urea, 0.01 to 2.0 percent of thickening agent, 0.1 to 1.0 percent of emollient, 0.1 to 1.0 percent of anti-allergic agent, 0.1 to 1.0 percent of skin conditioner, 0.1 to 5 percent of stabilizer, 1.0 to 5.0 percent of aromatic and the balance of purified water. The mask liquid can effectively solve the problems of poor moisturizing effect, low absorption efficiency and the like of the existing hyaluronic acid mask.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to hyaluronic acid mask liquid and a preparation method thereof.
Background
Hyaluronic acid has a special water retention effect, is the best substance found in nature in the prior art for moisture retention, has super-strong water absorption and water locking capacity, can absorb 1000 times of water of the self volume, and forms an elastic viscous matrix filled in the gaps of tissues. The intradermal HA provides space for collagen and elastin fibers to form a scaffold for the skin, an important extracellular matrix for maintaining skin tissue stability, fusion and elasticity. HA in the human body is distributed mainly in skin tissues and its content is decreasing with age. When the HA content in the skin is lower than a certain level, the water content of the surface layer of the skin gradually decreases, so that the stratum corneum ages, the skin becomes rough, wrinkles appear, elasticity is lost, and aging appears, and the phenomenon generally appears after the age of 25 years. Hyaluronic acid has been widely used in cosmetic formulations as a moisturizing, anti-aging efficacy additive ingredient.
With the improvement of life quality of people and the pursuit of beauty, the types of cosmetics are more and more. At present, hyaluronic acid mask products of hyaluronic acids on the market are full of variety of porcelain, the common hyaluronic acid is hyaluronic acid with high molecular weight, the molecular weight of the hyaluronic acid is hundreds of thousands to millions, and the common hyaluronic acid is only added into the mask, so that the skin cannot be absorbed in a large amount, the problems of poor moisturizing effect, poor moisturizing effect and the like are caused, and the lasting moisturizing effect desired by consumers is difficult to achieve.
Disclosure of Invention
Aiming at the defects in the prior art, the invention provides the hyaluronic acid mask solution and the preparation method thereof, and the hyaluronic acid mask solution can effectively solve the problems of poor moisturizing effect, low absorption efficiency and the like of the existing hyaluronic acid mask.
In order to achieve the purpose, the technical scheme adopted by the invention for solving the technical problems is as follows: the hyaluronic acid facial mask liquid comprises the following components in percentage by weight: 0.05 to 0.2 percent of hydrolyzed sodium hyaluronate, 0.05 to 0.2 percent of betaine, 261.3 to 2.6 percent of glycerol polyether, 0.8 to 1.5 percent of luba gum oil, 2.5 to 4.0 percent of butanediol, 4.0 to 6.0 percent of hydroxyethyl urea, 0.01 to 2.0 percent of thickening agent, 0.1 to 1.0 percent of emollient, 0.1 to 1.0 percent of anti-allergic agent, 0.1 to 1.0 percent of skin conditioner, 0.1 to 5 percent of stabilizer, 1.0 to 5.0 percent of aromatic and the balance of purified water.
Further, the paint comprises the following components in percentage by weight: 0.1% of hydrolyzed sodium hyaluronate, 0.1% of betaine, 262.0% of glycerol polyether, 1.0% of luba gum oil, 3.0% of butanediol, 5.0% of hydroxyethyl urea, 0.2% of thickening agent, 0.5% of emollient, 0.2% of anti-allergy agent, 0.4% of skin conditioner, 2.5% of stabilizer, 3.0% of aromatic and the balance of purified water.
Further, the thickener is at least one of xanthan gum, tara gum or carbomer.
Further, the emollient is PEG/PPG-17/6 copolymer and hydrolyzed jojoba oil at a weight ratio of 1-3: 1-2.
Further, the skin conditioning agent is VB3 and tetrahydro methyl pyrimidine carboxylic acid, and the weight ratio of the VB3 to the tetrahydro methyl pyrimidine carboxylic acid is 1-3: 1-3.
Further, the antiallergic agent is at least two of dipotassium glycyrrhizinate, mantine or matrine.
Further, the stabilizer is pentanediol and menthone, and the weight ratio of the pentanediol to the menthone is 2-4: 4-7.
Further, the aromatic is at least one of rose water, lavender water or orange water.
The preparation method of the hyaluronic acid facial mask liquid comprises the following steps: (1) heating purified water to 60-70 deg.C, sequentially adding thickener, hydrolyzed sodium hyaluronate, betaine, glyceryl polyether-26, Gerber gum oil, butanediol and hydroxyethyl urea, and stirring;
(2) adding the emollient into the product obtained in the step (1), and uniformly stirring;
(3) and (3) sequentially adding a skin conditioner, an anti-allergy agent, a stabilizer and an aromatic into the product obtained in the step (2), uniformly stirring, and sterilizing to obtain the skin care product.
The invention has the beneficial effects that:
1. the luba gum oil is a humectant and has the effects of promoting cell metabolism, adjusting the pH value of skin, regulating oil secretion and shrinking pores, has a unique cage-shaped structure, can firmly lock water, forms a closed oil film protective layer on the surface of the skin and prevents water and other moisture retention components from evaporating and losing; the Gemba gum oil can improve the use feeling of the skin and moisten the skin;
the hydrolyzed sodium hyaluronate can form a water film on the surface of the skin to enable the skin to become smooth and moist, has the functions of removing wrinkles and increasing the elasticity of the skin, has the functions of softening cutin and improving the skin nutrition metabolism, can be used as a transdermal absorption promoter, is added into the facial mask liquid, can promote the cutin softening after being applied for a certain time, promotes the epidermis cell metabolism, promotes the absorption of other nutrient components and moisturizing components, and further has the function of deep moisturizing;
the hydroxyethyl urea is used as a humectant, has high moisturizing effect and smooth touch, can improve the texture of facial mask liquid and the feeling of skin, can permeate into the horny layer of the skin to increase the water content of the skin, has deep moisturizing effect and can increase the hydration of the skin,
in the invention, the luba glue oil and the hydrolyzed sodium hyaluronate have a synergistic effect, and can improve the effects of locking water and moisturizing while forming a layer of water-oil mixed protective film on the surface of skin, so that the skin feels light and thin. The hydroxyethyl urea, the hydrolyzed sodium hyaluronate in the formula and the luba gum oil act together to further improve the hydration of the skin, so that the aims of improving the absorption efficiency of the skin and enhancing the moisturizing effect are fulfilled.
2. Betaine is used as a humectant, has a good moisturizing effect, has a fresh texture, is smooth and elastic to the skin after use, is an ideal sedative, can balance the osmotic pressure of cells, and can play a mild moisturizing role even in a severe external environment; the glyceryl polyether-26 is used as a humectant, has the function of softening cuticle, and after the use, the skin becomes soft and smooth, and the viscosity is low, and the skin sensitivity is good after the use; the facial mask liquid is prepared by adding the betaine, the glyceryl polyether-26 and the butanediol, can assist in hydrolyzing hyaluronic acid, the lugban gum oil and the hydroxyethyl urea to enhance the water replenishing and moisturizing effects, and has the functions of calming the skin and inhibiting bacteria.
3. The jasminolone is a natural plant extract, has multiple effects of oxidation resistance, relieving and the like, also has an antiseptic effect, is combined with the pentanediol and the butanediol according to a certain proportion to form a unique antiseptic system, and can obviously improve the antiseptic effect, so the mask liquid can be stored for a long time even if no preservative is added, and the harm of the preservative to the skin is reduced.
4. The dipotassium glycyrrhizinate is used as a soothing anti-allergy, anti-inflammatory and humectant, has the functions of resisting external stimulation, controlling oil and diminishing inflammation, has good repairing effect on allergic skin, and can be added into the facial mask liquid to be synergistic with butanediol so as to enhance the anti-inflammatory effect of the facial mask liquid.
5. The hydrolyzed sodium hyaluronate, the betaine, the glyceryl polyether-26, the luba gum oil, the butanediol and the hydroxyethyl urea are used as main moisturizing components, different components interact with each other according to a certain weight ratio, so that the moisturizing effect of the facial mask liquid is remarkably improved, and meanwhile, the facial mask liquid has the anti-inflammatory and acne-removing effects by matching with corresponding components such as a stabilizer and a skin conditioner and interacting with the moisturizing components, and can be stored for a long time without adding a preservative.
Detailed Description
Example 1
The hyaluronic acid facial mask liquid comprises the following components in percentage by weight: 0.05% of hydrolyzed sodium hyaluronate, 0.05% of betaine, 261.3% of glycerol polyether, 0.8% of luba gum oil, 2.5% of butanediol, 4.0% of hydroxyethyl urea, 0.01% of thickening agent, 0.1% of emollient, 0.1% of anti-allergy agent, 0.1% of skin conditioner, 0.1% of stabilizer, 1.0% of aromatic and the balance of purified water.
Wherein the thickening agent is xanthan gum;
the emollient is PEG/PPG-17/6 copolymer and hydrolyzed jojoba oil at a weight ratio of 1: 2;
the anti-allergy agent is dipotassium glycyrrhizinate and matrine, and the weight ratio of the dipotassium glycyrrhizinate to the matrine is 3: 2;
the skin conditioner is VB3And tetrahydro-methyl-pyrimidine-carboxylic acid in a weight ratio of 2: 3;
the stabilizer is pentanediol and menthone, and the weight ratio of the pentanediol to the menthone is 3: 7;
the aromatic agent is flos Rosae Multiflorae water.
The preparation method of the hyaluronic acid facial mask liquid comprises the following steps: (1) heating purified water to 60-70 deg.C, sequentially adding thickener, hydrolyzed sodium hyaluronate, betaine, glyceryl polyether-26, Gerber gum oil, butanediol and hydroxyethyl urea, and stirring;
(2) adding the emollient into the product obtained in the step (1), and uniformly stirring;
(3) and (3) sequentially adding a skin conditioner, an anti-allergy agent, a stabilizer and an aromatic into the product obtained in the step (2), uniformly stirring, and sterilizing to obtain the skin care product.
Example 2
The hyaluronic acid facial mask liquid comprises the following components in percentage by weight: 0.2% of hydrolyzed sodium hyaluronate, 0.2% of betaine, 262.6% of glycerol polyether, 1.5% of luba gum oil, 4.0% of butanediol, 6.0% of hydroxyethyl urea, 2.0% of thickening agent, 1.0% of emollient, 1.0% of anti-allergy agent, 1.0% of skin conditioner, 5% of stabilizer, 5.0% of aromatic and the balance of purified water.
Wherein the thickener is Caesalpinia spinosa Gum;
the emollient is PEG/PPG-17/6 copolymer and hydrolyzed jojoba oil at a weight ratio of 2: 1;
the anti-allergy agent is dipotassium glycyrrhizinate and matrine, and the weight ratio of the dipotassium glycyrrhizinate to the matrine is 1: 2;
the skin conditioner is VB3And tetrahydro-methyl-pyrimidine-carboxylic acid in a weight ratio of 3: 2;
the stabilizer is pentanediol and menthone, and the weight ratio of the pentanediol to the menthone is 4: 5;
the aromatic agent is lavender flower water.
The preparation method of the sodium hyaluronate mask solution is the same as that of example 1.
Example 3
The hyaluronic acid facial mask liquid comprises the following components in percentage by weight: 0.1% of hydrolyzed sodium hyaluronate, 0.1% of betaine, 262.0% of glycerol polyether, 1.0% of luba gum oil, 3.0% of butanediol, 5.0% of hydroxyethyl urea, 0.2% of thickening agent, 0.5% of emollient, 0.2% of anti-allergy agent, 0.4% of skin conditioner, 2.5% of stabilizer, 3.0% of aromatic and the balance of purified water.
Wherein the thickener is carbomer;
the emollient is PEG/PPG-17/6 copolymer and hydrolyzed jojoba oil at a weight ratio of 3: 1;
the anti-allergy agent is dipotassium glycyrrhizinate and matrine, and the weight ratio of the dipotassium glycyrrhizinate to the matrine is 1: 1;
the skin conditioner is VB3And tetrahydro-methyl-pyrimidine-carboxylic acid in a weight ratio of 1: 3;
the stabilizer is pentanediol and menthone, and the weight ratio of the pentanediol to the menthone is 3: 4;
the aromatic agent is rose water.
The preparation method of the sodium hyaluronate mask solution is the same as that of example 1.
Example 4
The hyaluronic acid facial mask liquid comprises the following components in percentage by weight: 0.15% of hydrolyzed sodium hyaluronate, 0.08% of betaine, 261.5% of glycerol polyether, 1.2% of luba gum oil, 2.5% of butanediol, 4.3% of hydroxyethyl urea, 0.1% of thickening agent, 0.6% of emollient, 0.5% of anti-allergy agent, 0.6% of skin conditioner, 3% of stabilizer, 2% of aromatic and the balance of purified water.
Wherein the thickener is carbomer;
the emollient is PEG/PPG-17/6 copolymer and hydrolyzed jojoba oil at a weight ratio of 1: 1;
the anti-allergy agent is dipotassium glycyrrhizinate and matrine, and the weight ratio of the dipotassium glycyrrhizinate to the matrine is 3: 1;
the skin conditioner is VB3And tetrahydro-methyl-pyrimidine-carboxylic acid in a weight ratio of 3: 1;
the stabilizer is pentanediol and menthone, and the weight ratio of the pentanediol to the menthone is 2: 6;
the aromatic agent is rose water.
The preparation method of the sodium hyaluronate mask solution is the same as that of example 1.
Comparative example 1
The hyaluronic acid facial mask liquid comprises the following components in percentage by weight: 0.1% of hydrolyzed sodium hyaluronate, 0.1% of betaine, 3.0% of butanediol, 5.0% of hydroxyethyl urea, 0.2% of thickening agent, 0.5% of emollient, 0.2% of anti-allergy agent, 0.4% of skin conditioner, 2.5% of stabilizer, 3.0% of aromatic and the balance of purified water.
Wherein the thickener is carbomer;
the emollient is PEG/PPG-17/6 copolymer and hydrolyzed jojoba oil at a weight ratio of 3: 1;
the anti-allergy agent is dipotassium glycyrrhizinate and matrine, and the weight ratio of the dipotassium glycyrrhizinate to the matrine is 1: 1;
the skin conditioner is VB3And tetrahydro-methyl-pyrimidine-carboxylic acid in a weight ratio of 1: 3;
the stabilizer is pentanediol and menthone, and the weight ratio of the pentanediol to the menthone is 3: 4;
the aromatic agent is rose water.
The preparation method of the sodium hyaluronate mask solution is the same as that of example 1.
Comparative example 2
The hyaluronic acid facial mask liquid comprises the following components in percentage by weight: betaine 0.1%, glyceryl polyether-262.0%, luba gum oil 1.0%, butanediol 3.0%, hydroxyethyl urea 5.0%, thickening agent 0.2%, emollient 0.5%, anti-allergy agent 0.2%, skin conditioner 0.4%, stabilizer 2.5%, fragrance 3.0%, and the balance of purified water.
Wherein the thickener is carbomer;
the emollient is PEG/PPG-17/6 copolymer and hydrolyzed jojoba oil at a weight ratio of 3: 1;
the anti-allergy agent is dipotassium glycyrrhizinate and matrine, and the weight ratio of the dipotassium glycyrrhizinate to the matrine is 1: 1;
the skin conditioner is VB3And tetrahydro-methyl-pyrimidine-carboxylic acid in a weight ratio of 1: 3;
the stabilizer is pentanediol and menthone, and the weight ratio of the pentanediol to the menthone is 3: 4;
the aromatic agent is rose water.
The preparation method of the sodium hyaluronate mask solution is the same as that of example 1.
Comparative example 3
The hyaluronic acid facial mask liquid comprises the following components in percentage by weight: 0.1% of hydrolyzed sodium hyaluronate, 262.0% of glyceryl polyether, 1.0% of luba gum oil, 5.0% of hydroxyethyl urea, 0.2% of thickening agent, 0.5% of emollient, 0.2% of anti-allergy agent, 0.4% of skin conditioner, 2.5% of stabilizer, 3.0% of aromatic and the balance of purified water.
Wherein the thickener is carbomer;
the emollient is PEG/PPG-17/6 copolymer and hydrolyzed jojoba oil at a weight ratio of 3: 1;
the anti-allergy agent is dipotassium glycyrrhizinate and matrine, and the weight ratio of the dipotassium glycyrrhizinate to the matrine is 1: 1;
the skin conditioner is VB3And tetrahydro-methyl-pyrimidine-carboxylic acid in a weight ratio of 1: 3;
the stabilizer is pentanediol and menthone, and the weight ratio of the pentanediol to the menthone is 3: 4;
the aromatic agent is rose water.
The preparation method of the sodium hyaluronate mask solution is the same as that of example 1.
Comparative example 4
The hyaluronic acid facial mask liquid comprises the following components in percentage by weight: 0.1% of hydrolyzed sodium hyaluronate, 0.1% of betaine, 262.0% of glycerol polyether, 1.0% of luba gum oil, 5.0% of hydroxyethyl urea, 0.2% of thickening agent, 0.5% of emollient, 0.2% of anti-allergy agent, 0.4% of skin conditioner, 2.5% of stabilizer, 3.0% of aromatic and the balance of purified water.
Wherein the thickener is carbomer;
the emollient is PEG/PPG-17/6 copolymer and hydrolyzed jojoba oil at a weight ratio of 3: 1;
the anti-allergy agent is dipotassium glycyrrhizinate and matrine, and the weight ratio of the dipotassium glycyrrhizinate to the matrine is 1: 1;
the skin conditioner is VB3And tetrahydro-methyl-pyrimidine-carboxylic acid in a weight ratio of 1: 3;
the stabilizer is menthone;
the aromatic agent is rose water.
The preparation method of the sodium hyaluronate mask solution is the same as that of example 1.
Test examples
1. Stability detection
(1) Sealing the facial mask solutions of examples 1-4 and comparative examples 1-4, placing in an electric-heating constant-temperature incubator at 38-55 ℃ for 30-60 days, observing the condition of the facial mask solution after the temperature is restored to room temperature, and simultaneously detecting the microbial content in the facial mask solution, wherein the specific results are shown in Table 1.
(2) Storing at-4 deg.C and 50 deg.C for 3 times, each time for 24 hr, respectively, storing at-4 deg.C for 24 hr, storing at room temperature for 24 hr, storing in 50 deg.C thermostat for 24 hr, and sequentially circulating for 3 times to observe its stability, with specific results shown in Table 2.
Table 1:
as can be seen from Table 1, the facial mask solutions of examples 1-4 and comparative examples 1-4 have better stability, especially the facial mask solutions of examples 1-4 have the highest stability.
Table 2:
as can be seen from Table 1, the facial mask solutions of examples 1-4 and comparative examples 1-4 have better stability, especially the facial mask solutions of examples 1-4 have the highest stability.
2. Skin feel test
45 rough and lusterless women who are easy to be allergic are randomly searched and divided into 9 groups, 5 persons in each group are respectively allowed to use the moisturizing facial masks of examples 1-4, comparative examples 1-4 and commercially available water-tight codes for 3 times a week, when the moisturizing facial masks are used, the moisturizing facial masks are applied for 15-20 minutes each time, then the redundant facial mask liquid is washed off, and the subsequent skin care steps are normally carried out. After 2 weeks, 4 weeks and 6 weeks of continuous use, the change of the face of each group of experimenters is observed and recorded, and the detailed results are shown in table 3; meanwhile, the skin of each group of experimenters is detected by using a detector, and the specific detection result is shown in table 4.
Table 3:
as can be seen from Table 3, the facial mask solutions of examples 1 to 4 and comparative examples 1 to 4 and the facial mask of the comparative product all have certain water-replenishing and acne-controlling effects on the skin, and the water-replenishing and acne-controlling effects of examples 1 to 4 are more obvious than those of comparative examples 1 to 4 and the comparative product, particularly the water-replenishing and acne-controlling effects of example 3 are most obvious.
Table 4:
as can be seen from Table 4, the average ratio of elasticity improvement and the average ratio of melanin reduction of the facial mask solutions of examples 1 to 4 to the skin were larger than those of comparative examples 1 to 4 and comparative products, and particularly, the average ratio of elasticity improvement and the average ratio of melanin reduction of the skin were the largest in the facial mask solutions of example 3.
Claims (5)
1. The hyaluronic acid facial mask liquid is characterized by comprising the following components in percentage by weight: 0.05-0.2% of hydrolyzed sodium hyaluronate, 0.05-0.2% of betaine, 261.3-2.6% of glycerol polyether, 0.8-1.5% of luba gum oil, 2.5-4.0% of butanediol, and hydroxyethyl urea4.0 to 6.0 percent of water-soluble polymer, 0.01 to 2.0 percent of thickening agent, 0.1 to 1.0 percent of emollient, 0.1 to 1.0 percent of anti-allergy agent, 0.1 to 1.0 percent of skin conditioner, 0.1 to 5 percent of stabilizer, 1.0 to 5.0 percent of aromatic, and the balance of purified water, wherein the skin conditioner is VB3And tetrahydro-methyl-pyrimidine-carboxylic acid in a weight ratio of 1-3: 1-3; the stabilizer is pentanediol and menthone, and the weight ratio of the pentanediol to the menthone is 2-4: 4-7; the emollient is PEG/PPG-17/6 copolymer and hydrolyzed jojoba oil at a weight ratio of 1-3: 1-2; the antiallergic agent is oxitenmin and matrine.
2. The hyaluronic acid mask solution of claim 1, comprising the following components in percentage by weight: 0.1% of hydrolyzed sodium hyaluronate, 0.1% of betaine, 262.0% of glycerol polyether, 1.0% of luba gum oil, 3.0% of butanediol, 5.0% of hydroxyethyl urea, 0.2% of thickening agent, 0.5% of emollient, 0.2% of anti-allergy agent, 0.4% of skin conditioner, 2.5% of stabilizer, 3.0% of aromatic and the balance of purified water.
3. The hyaluronic acid mask solution of claim 1 or 2, wherein the thickener is at least one of xanthan gum, tara gum or carbomer.
4. The hyaluronic acid mask solution of claim 1 or 2, wherein the fragrance is at least one of rose water, lavender water or orange water.
5. The method for preparing a hyaluronic acid mask solution according to claims 1-4, comprising the steps of: (1) heating purified water to 60-70 deg.C, sequentially adding thickener, hydrolyzed sodium hyaluronate, betaine, glyceryl polyether-26, Gerber gum oil, butanediol and hydroxyethyl urea, and stirring;
(2) adding the emollient into the product obtained in the step (1), and uniformly stirring;
(3) and (3) sequentially adding a skin conditioner, an anti-allergy agent, a stabilizer and an aromatic into the product obtained in the step (2), uniformly stirring, and sterilizing to obtain the skin care product.
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| CN110742821A (en) * | 2019-11-22 | 2020-02-04 | 成都珂萝瑞诗化妆品有限公司 | Young rejuvenation and rejuvenation facial mask and preparation method thereof |
| CN110680789A (en) * | 2019-11-22 | 2020-01-14 | 成都珂萝瑞诗化妆品有限公司 | After-sun repair mask and preparation method thereof |
| CN114081850A (en) * | 2021-12-27 | 2022-02-25 | 广州源燊创生物科技有限公司 | Efficient cosmetic humectant |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107184486A (en) * | 2017-07-06 | 2017-09-22 | 曾万祥 | A kind of facial mask liquid and the facial mask containing the facial mask liquid |
| CN107375180A (en) * | 2017-08-11 | 2017-11-24 | 北京斯利安药业有限公司 | A kind of composite skin care product, facial mask and preparation method thereof |
| CN107440932A (en) * | 2017-08-11 | 2017-12-08 | 北京斯利安药业有限公司 | A kind of composite skin care product containing folic acid, facial mask and preparation method thereof |
| CN108042479A (en) * | 2017-12-28 | 2018-05-18 | 广州蜜妆生物科技有限公司 | A kind of probiotics conditioning foster skin facial mask and preparation method thereof |
-
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Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107184486A (en) * | 2017-07-06 | 2017-09-22 | 曾万祥 | A kind of facial mask liquid and the facial mask containing the facial mask liquid |
| CN107375180A (en) * | 2017-08-11 | 2017-11-24 | 北京斯利安药业有限公司 | A kind of composite skin care product, facial mask and preparation method thereof |
| CN107440932A (en) * | 2017-08-11 | 2017-12-08 | 北京斯利安药业有限公司 | A kind of composite skin care product containing folic acid, facial mask and preparation method thereof |
| CN108042479A (en) * | 2017-12-28 | 2018-05-18 | 广州蜜妆生物科技有限公司 | A kind of probiotics conditioning foster skin facial mask and preparation method thereof |
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