CN107184486A - A kind of facial mask liquid and the facial mask containing the facial mask liquid - Google Patents

A kind of facial mask liquid and the facial mask containing the facial mask liquid Download PDF

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Publication number
CN107184486A
CN107184486A CN201710547397.XA CN201710547397A CN107184486A CN 107184486 A CN107184486 A CN 107184486A CN 201710547397 A CN201710547397 A CN 201710547397A CN 107184486 A CN107184486 A CN 107184486A
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facial mask
mask liquid
skin
liquid
nmf
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曾万祥
覃敢为
陈海
黄娜
曾嘉
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/02Cosmetics or similar toiletry preparations characterised by special physical form
    • A61K8/0212Face masks
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • A61K8/345Alcohols containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/35Ketones, e.g. benzophenone
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/42Amides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4946Imidazoles or their condensed derivatives, e.g. benzimidazoles
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/60Sugars; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/63Steroids; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/73Polysaccharides
    • A61K8/735Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8141Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • A61K8/8152Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
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    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/88Polyamides
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/52Stabilizers
    • A61K2800/524Preservatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/70Biological properties of the composition as a whole
    • A61K2800/72Hypo-allergenic
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/74Biological properties of particular ingredients
    • A61K2800/75Anti-irritant

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Abstract

The invention discloses a kind of facial mask liquid, the facial mask liquid includes NMF;The NMF includes Sodium Hyaluronate, trehalose, polyglutamic acid sodium, glycine betaine, tremella polysaccharides and glycerine polymethacrylates.The facial mask liquid energy of the present invention is carried out persistently and the moisturizing of deep layer to skin, and mildness is good, and skin sensitivity person is applicable, Nantural non-toxic, and gentle non-stimulated, long-term use will not damage skin, and the improvement to skin is obvious, contributes to skin to recover elasticity and gloss.

Description

A kind of facial mask liquid and the facial mask containing the facial mask liquid
Technical field
The present invention relates to technical field of skin care, and in particular to a kind of non-stimulated deep moisturizing facial mask liquid of antiallergic, use Facial mask of the facial mask liquid and preparation method thereof.
Background technology
Continuous progress and the extreme enrichment of material life with social economy, people are not concerned only with the strong of own bodies Health, the skin nursing of itself also turns into the pith of people's daily life.In particular with the quickening of people's rhythm of life, Modern society environment air pollution increasingly sharpens, and pore is thick, facial oiliness, the colour of skin exception, wrinkle of skin etc. are various Skin problem annoying increasing people.Therefore, people further investigate in medical cosmetology field always, it have developed various each The skin-protection product of sample, facial mask is wherein most popular, skin care takes effect most soon, using one of maximum product of growth rate.
Facial mask is a kind of cosmetics and skincare product applied on the face, and the skin care principle of facial mask is:Using being covered in the of short duration of face Time, facial skin is temporarily isolating to air and the pollution in the external world, while improving skin temperature, stimulates circulation, makes infiltration The nutrient of skin is diffused in iuntercellular, allows skin to draw various nutritional ingredients, reaches inhibiting bacteria and diminishing inflammation, moisturizing whitening, smooth tight And other effects.
However, the facial mask moistening effect of prior art and bad, can only play temporary transient moisture-keeping function to the top layer of skin, And antiallergic effect is poor, allergic phenomena easily occurs.For preservation, existing facial mask generally can all add preservative, due to passing The preservative of system has certain toxicity, so its addition on facial mask can be restricted, causes the antiseptic effect of facial mask It is not good.It is loosely organized and if the preservative addition in facial mask is incorrect, the epidermal cell developmental immaturity of people can be made, with Cause epidermis thinning, defence capability declines, and easily by environmental stimuli, is also easy to produce wrinkle, skin is gradually followed the string.By preservative The Skin Cell of infringement can constantly carry out defect breeding, cause skin only can be worse and worse.Therefore, the preservative addition of skin care item Problem turns into focus of concern.
Such as the Chinese patent of Application No. 201610478435.6, a kind of " moisturizing antiallergy repair surface which disclose Film, contains following components by weight percentage:Macromolecular hyaluronic acid 0.01%~0.1%, middle molecular weight hyaluronic acid 0.01%~0.1%, micromolecule hyaluronic acid 0.01%~0.1%, urea 0.15%~1.5%, ceramide 0.6%~ 5%th, niacinamide 0.6%~5%, dimethyl silicone polymer 1.5%~10%, glycerine 0.3%~0.5%, butanediol 0.3%~ 3%th, boric acid 0.6%~6%, green-tea extract Tea Polyphenols 0.3%~3%, remaining is deionized water." existing patent use The various different hyaluronic acids of molecular weight, urea, dimethyl silicone polymer and glycerine as facial mask moisturizing ingredient, although should Several compositions have certain moisture-keeping function, but can not penetrate into skin inner layer progress deep moisturizing well, can only be to skin Epidermis play moisture-keeping function, and action time is not long, it is impossible to lasting moisturizing.Furthermore, the existing patent is using neural acyl Amine, niacinamide and green-tea extract Tea Polyphenols are as the antiallergic composition of facial mask, and antiallergic effective content is few, antiallergic less effective.And In anti-corrosion, the existing patent is using butanediol and boric acid as the antimicrobial component of facial mask, and butanediol is conventional skin care raw material, Boric acid is pH adjusting agent, and both does not almost work to bacterium and mould, and antiseptic effect is bad.
Therefore, need badly and develop that a kind of antiallergic effect is good, gentle non-stimulated deep moisturizing facial mask.
The content of the invention
It is an object of the invention to solve shortcoming and defect present in above-mentioned prior art, there is provided a kind of antiallergic is non-stimulated Deep moisturizing facial mask liquid, using facial mask of the facial mask liquid and preparation method thereof.
For up to above-mentioned purpose, the technical scheme is that:
A kind of facial mask liquid, the facial mask liquid includes NMF;The NMF includes Sodium Hyaluronate, trehalose, poly- paddy Propylhomoserin sodium, glycine betaine, tremella polysaccharides and glycerine polymethacrylates.
Further, weight/mass percentage composition of each composition in facial mask liquid is Sodium Hyaluronate 0.05% in the NMF ~0.5%, trehalose 0.5%~5%, polyglutamic acid sodium 0.1%~5%, glycine betaine 0.1%~5%, tremella polysaccharides 0.5% ~5%, glycerine polymethacrylates 0.5%~5%.
Further, the NMF also includes butanediol and propane diols, and quality of the butanediol in the facial mask liquid Percentage composition is 1~10%, and weight/mass percentage composition of the propane diols in the facial mask liquid is 1~10%.
Further, the facial mask liquid also contains anti-sensitizer, and the anti-sensitizer includes dipotassium glycyrrhizinate, allantoin, rough gentian Careless extract solution.
Further, weight/mass percentage composition of each composition in facial mask liquid is dipotassium glycyrrhizinate 0.05% in the anti-sensitizer ~0.5%, allantoin 0.1%~1%, felwort extract solution 0.1%~1%.
Further, the facial mask liquid also contains preservative, and the preservative includes decoyl hydroximic acid, para hydroxybenzene second The sad fat of ketone, glycerine, butanediol;Weight/mass percentage composition of the preservative in the facial mask liquid is 0.1%~1.0%.Institute The purchase producer for stating preservative is:B&J Life Technologies, its marque is:HL-01.
Further, the facial mask liquid includes the component of following weight/mass percentage composition:NMF:3.75%~20%, resist Quick dose:0.25%~2.5%, thickener:0.1%~1%, pH adjusting agent:0.05%~0.5%, preservative:0.1%~ 1.0%, surplus is deionized water.
Further, the thickener includes xanthans and carbomer, and matter of the xanthans in the facial mask liquid Measure percentage composition be 0.05%~0.5%, weight/mass percentage composition of the carbomer in the facial mask liquid be 0.05%~ 0.5%;The pH adjusting agent is triethanolamine.
A kind of facial mask, the facial mask contains the facial mask liquid described in the technical program.
A kind of method for preparing facial mask described in the technical program, comprises the following steps:
1. deionized water is added in pot, then carbomer is slowly added under stirring at low speed, it is equal with 50r/min speed Matter stirs 10~15min to being completely dispersed, and then heats to 80~85 DEG C, adds propane diols and xanthans scattered in advance Mixture, dipotassium glycyrrhizinate, allantoin, dispersed with stirring, be incubated 20min;
2. said components are cooled, cools the temperature to 50 DEG C, add scattered butanediol and Sodium Hyaluronate Mixture, trehalose, glycerine polymethacrylates, tremella polysaccharides, felwort extract solution, polyglutamic acid sodium, glycine betaine, stirring It is well mixed;
3. said components are cooled, cools the temperature to 42 DEG C, add deionized water, preservative, dispersed with stirring;
4. formula rate is pressed, triethanolamine is weighed and adds in pot, adjust PH to 6.0~6.5;
5. according to the internal control index of offer, viscosity control 3000~4200, facial mask liquid is obtained;
6. the comprehensive face paper of monolithic is added in the facial mask bag containing above-mentioned facial mask liquid, then taken out and vacuum packet Dress, obtains facial mask.
Compared with prior art, beneficial effects of the present invention are:
Due to molecular weight all very littles of Sodium Hyaluronate, polyglutamic acid sodium and glycine betaine, so skin inner layer can be penetrated into Cell tissue, to skin carry out deep moisturizing.And trehalose, tremella polysaccharides and glycerine polymethacrylates can rest on skin Skin surface, forms one layer of special diaphragm, and external heat can be radiate by the diaphragm, slows down moisture of skin evaporation, Extraneous natural moisture is also can absorb, is that skin supplements enough moisture, the mucus separated out from the diaphragm can moisten top layer Skin Cell.The NMF of this facial mask liquid passes through Sodium Hyaluronate, polyglutamic acid sodium, glycine betaine, trehalose, tremella polysaccharides and sweet The synergy of oily 6 kinds of compositions of polymethacrylates, realizes and carries out deep layer, lasting moisture-keeping function to skin, effect is notable.
Dipotassium glycyrrhizinate has extensive compatibility, can accelerate absorption of the skin to active component, with antioxidation activity, Very strong Green Tea Extract oxidation is shown in chtochrome oxidase system, can substantially suppress institute in internal metabolic processes The free radical of generation, can also in and/or lower cosmetics in noxious material.The antiallergic effect of dipotassium glycyrrhizinate, which is mainly, to be passed through Suppress the release of histamine to prevent rubefaction from itching, especially there is fabulous protective effect to the crowd of anaphylactic shock.
Allantoin has the effect of unique keratin-dissolving and softening keratin, can increase the hydratability of cuticula, delay Solution and treatment xerodermia.Allantoin also has local weak paralysis effect, can alleviate stimulation of the active matter to skin.
The effects such as felwort extract solution has antibacterial, anti-inflammatory, anti-acne, antiallergy, can effectively mitigate the mistake as caused by histamine Quick reaction.It has different degrees of inhibitory action to various pathogens, can be done directly on the root position of acne, whelk, It is rapid to kill Propiobacterium, control the inflammation of skin surface;The elastic collagenous fibres of fracture can also be connected, fundamentally repair because Acne etc. and produce skin histology scar.
The present invention intersects compounding using allantoin, three kinds of natural activity antiallergic raw materials of felwort extract solution and dipotassium glycyrrhizinate Anti-sensitizer is formed, there is local weak paralysis to act on to skin, can effectively alleviate stimulation of the active matter to skin, good antimicrobial effect, Green Tea Extract oxidation is strong, can effectively suppress histamine release, antiallergic is good, can also repairing skin tissue's scar.
The present invention is using decoyl hydroximic acid, parahydroxyacet-ophenone, four kinds of active component compositions of the sad fat of glycerine and butanediol Natural gentle preservative with efficient corrosion resisting function, to replace traditional preservative.The preservative can effectively suppress bacterium With the growth of mould, and effective dose is few, Nantural non-toxic, endless requirement, will not stimulate skin, itself and facial mask liquid it is other The compatibility of composition is good.The preservative of the present invention also has chelating Ca2+、Fe2+And Fe3+Effect, the metal in facial mask can be reduced Ion concentration, can also penetrate into the lipid layer of skin, play a part of deep moisturizing.
The facial mask liquid mildness of the present invention is good, and skin sensitivity person is applicable, Nantural non-toxic, and long-term use will not damage skin Skin, the improvement to skin is obvious, contributes to skin to recover elasticity and gloss.
Embodiment
With reference to specific embodiment, the composition of the present invention is described in more detail.For the technical field of the invention Through the technology contents known and of the invention without direct correlation, unnecessary explanation is omitted, will more clearly to transmit the present invention The core content of realization.But, the record of the scope of the present invention and not according to embodiment and limit, this is technology belonging to the present invention The technical staff in field is self-evident.
《Embodiment 1-5》
Facial mask described by 1-5 of the embodiment of the present invention, it includes facial mask liquid.Wherein, the facial mask liquid of each embodiment include with The composition of lower weight/mass percentage composition, refers to table one.
Table one
The preparation method of above-described embodiment 1-5 facial mask is:
1. all production apparatus are cleaned and disinfected with water, emulsification pot group is carried out at autoclave sterilization Reason;
2. deionized water is added in emulsification pot, carbomer is then slowly added under stirring at low speed, then with 50r/min's Speed homogeneous stirs 10~15min to being completely dispersed, and then heats to 80~85 DEG C, add in advance scattered propane diols with Mixture, dipotassium glycyrrhizinate, the allantoin of xanthans, dispersed with stirring are incubated 20min;
3. said components are cooled, cools the temperature to 50 DEG C, add scattered butanediol and Sodium Hyaluronate Mixture, trehalose, glycerine polymethacrylates, tremella polysaccharides, felwort extract solution, polyglutamic acid sodium, glycine betaine, stirring It is well mixed;
4. said components are cooled, cools the temperature to 42 DEG C, add deionized water, antiseptic substitute, stirring point Dissipate;
5. formula rate is pressed, triethanolamine is weighed and adds in emulsification pot, adjust PH to 6.0~6.5;
6. according to the internal control index of offer, viscosity control 3000~4200, facial mask liquid is obtained;
7. the comprehensive face paper of monolithic is added in the facial mask bag containing above-mentioned facial mask liquid, then taken out and vacuum packet Dress, obtains facial mask.
One, fungistatic effects are tested
Test method:Escherichia coli, staphylococcus aureus are inoculated with cultured solution of broth respectively, in cultivating 24h at 37 DEG C, It is configured to the bacteria suspension of certain mass concentration.Weigh embodiment 1-5 facial mask liquid 1.0mg respectively with aseptic bottle, and be separately added into The bacteria suspension of equivalent, is stirred to be measured repeatedly.It is measured in 4h, 8h, 24h, bacteria technology lecithin-Tween 80 nutrition fine jade Fat, each bacterial strain separately sets one group of control, using ordinary nutrient agar, only adds bacteria suspension, is not added with facial mask liquid;Evaluation criterion:Kill Logarithm value:The logarithm value of bacterial number reduction, referred to as kills logarithm value.It is without fungistatic effect to kill logarithm value < 1;>=1 is to have Obvious fungistatic effect;>=3 be to have stronger fungistatic effect;>=5 be to have strong fungistatic effect.
Result of the test:It is shown in Table two, table three.
Table two is the result to Escherichia coli bacteriostasis.
Table three is the result to staphylococcus aureus bacteriostasis.
Table two
Table three
Conclusion (of pressure testing):Embodiment 2 and embodiment 3 have obvious bacteriostasis, embodiment 1, embodiment 4 and embodiment 5 With stronger bacteriostasis.Prove that the facial mask liquid energy of the present invention effectively suppresses the growth of bacterium and mould, and preservative Effective dose is few.
2nd, Physico-chemical tests
Facial mask liquid to embodiment 1-5 carries out Physico-chemical tests
1. smell
Through human body evaluation, embodiment 1-5 facial mask liquid has no irritating odor, and smell is pure and fresh.
2.pH values are detected
The pH value of each sample is determined with pH meter, after measured, the pH value of embodiment 1-5 facial mask liquid all falls within 6.0~6.5 In the range of.
3. viscosity number is detected
The viscosity number of each sample is determined with viscosimeter, after measured, the viscosity number of embodiment 1-5 facial mask liquid all falls within 800 In the range of~1200.
4. Detection of Stability
With embodiment 1-5 facial mask liquid as sample, the sample of acquirement is packaged in respectively in transparent bottle for cosmetics, It is subsequently placed under quartz lamp illumination and tests, illumination temperature is:- 15 DEG C, 5 DEG C, 25 DEG C and 48 DEG C, the testing time is 3 months, is seen Examine whether each sample the bad phenomenons such as bleed, layering, separation, precipitation, discoloration, peculiar smell, demulsification occurs.Test result shows, The sample for being derived from embodiment 1-5 does not occur above-mentioned bad phenomenon, illustrates that embodiment 1-5 facial mask liquid stability is good.
5. stimulate anaphylaxis to detect
Example 1-5 facial mask fluid samples are appropriate, are applied to volunteer's ear basal part of the ear that 30 age brackets are 18-58 Sui Near, 30min is observed, sees whether it the phenomenons such as redness, dermexanthesis, foaming occurs.Observation indicate that, institute is strong-willed in 30min Hope person does not occur above-mentioned ill symptomses, illustrates embodiment 1-5 facial mask liquid and skin generation stimulation and anaphylaxis will not be asked Topic.
3rd, moistening effect is tested
Facial mask using embodiment 1-5 concurrently sets two control groups as test group.
The facial mask liquid of control group 1 includes the composition of following weight/mass percentage composition:Trehalose 2.5%, tremella polysaccharides 2.5%, It is glycerine polymethacrylates 2.5%, butanediol 5%, propane diols 5%, allantoin 0.5%, felwort extract solution 0.5%, anti- Rotten agent 0.5%, xanthans 0.25%, carbomer 0.25%, triethanolamine 0.25%, surplus is deionized water.
The facial mask liquid of control group 2 includes the composition of following weight/mass percentage composition:Sodium Hyaluronate 0.25%, polyglutamic acid sodium 2.5%th, glycine betaine 2.5%, butanediol 5%, propane diols 5%, allantoin 0.5%, dipotassium glycyrrhizinate 0.25%, preservative 0.5%th, xanthans 0.25%, carbomer 0.25%, triethanolamine 0.25%, surplus is deionized water.
Randomly select 70 volunteers to be tested, 70 volunteers are divided into 7 groups, every group of 10 people.
Test method:First every group of will is tested respectively with Fes Kai Er SK-III type hand-held digital display skin moisture testers The forehead of hope person, left face, the moisture of right face and chin skin, and take arithmetic mean of instantaneous value;Then clean after face, every group of aspiration Person applies the facial mask of embodiment 1-5 and control group 1,2 respectively, and facial mask is removed after 20 minutes, is washed one's face with clear water, dries face, 3 Test the moisture of forehead, left face, right face and the chin skin of every group of volunteer after hour with skin moisture tester again, and Take arithmetic mean of instantaneous value;Test result such as following table:
Test data shows:The present embodiment 1-5 facial mask can significantly improve facial skin moisture, and moisturizing is held Long, wherein, the facial mask moistening effect of embodiment 5 is optimal.
And lack the Sodium Hyaluronate in this facial mask formula of liquid, polyglutamic acid sodium and glycine betaine in the facial mask liquid of control group 1 Three kinds can carry out the composition of deep moisturizing to skin, and its moistening effect is significantly lower than embodiment 1-5.In the facial mask liquid of control group 2 Skin water loss can be slowed down by lacking three kinds of the trehalose in this facial mask formula of liquid, tremella polysaccharides and glycerine polymethacrylates Composition, its moistening effect also be significantly lower than embodiment 1-5.Therefore, the NMF composition in this facial mask formula of liquid has fine Collaboration moisture-keeping function, the water content of skin can be significantly improved.
Finally, it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention rather than the present invention is protected The limitation of scope is protected, although being explained in detail with reference to preferred embodiment to the present invention, one of ordinary skill in the art should Understand, technical scheme can be modified or equivalent substitution, without departing from the essence of technical solution of the present invention And scope.

Claims (10)

1. a kind of facial mask liquid, it is characterised in that the facial mask liquid includes NMF;The NMF includes Sodium Hyaluronate, sea Algae sugar, polyglutamic acid sodium, glycine betaine, tremella polysaccharides and glycerine polymethacrylates.
2. facial mask liquid as claimed in claim 1, it is characterised in that quality hundred of each composition in facial mask liquid in the NMF It is Sodium Hyaluronate 0.05%~0.5%, trehalose 0.5%~5%, polyglutamic acid sodium 0.1%~5%, glycine betaine to divide content 0.1%~5%, tremella polysaccharides 0.5%~5%, glycerine polymethacrylates 0.5%~5%.
3. facial mask liquid as claimed in claim 1, its spy is, the NMF also includes butanediol and propane diols, and fourth two Weight/mass percentage composition of the alcohol in the facial mask liquid is 1~10%, and weight/mass percentage composition of the propane diols in the facial mask liquid is 1 ~10%.
4. facial mask liquid as claimed in claim 1, it is characterised in that the facial mask liquid also contains anti-sensitizer, the anti-sensitizer bag Containing dipotassium glycyrrhizinate, allantoin, felwort extract solution.
5. facial mask liquid as claimed in claim 4, it is characterised in that quality hundred of each composition in facial mask liquid in the anti-sensitizer It is dipotassium glycyrrhizinate 0.05%~0.5%, allantoin 0.1%~1%, felwort extract solution 0.1%~1% to divide content.
6. facial mask liquid as claimed in claim 1, it is characterised in that the facial mask liquid also contains preservative, the preservative bag The sad fat of hydroximic acid containing decoyl, parahydroxyacet-ophenone, glycerine, butanediol;Quality hundred of the preservative in the facial mask liquid It is 0.1%~1.0% to divide content.
7. the facial mask liquid as described in any one of claim 1~6, it is characterised in that the facial mask liquid includes following quality percentage The component of content:NMF:3.75%~20%, anti-sensitizer:0.25%~2.5%, thickener:0.1%~1%, pH is adjusted Agent:0.05%~0.5%, preservative:0.1%~1.0%, surplus is deionized water.
8. facial mask liquid as claimed in claim 7, it is characterised in that the thickener includes xanthans and carbomer, and described Weight/mass percentage composition of the xanthans in the facial mask liquid is 0.05%~0.5%, and the carbomer is in the facial mask liquid Weight/mass percentage composition is 0.05%~0.5%;
The pH adjusting agent is triethanolamine.
9. a kind of facial mask, it is characterised in that the facial mask contains the facial mask liquid as described in any one of claim 1~8.
10. a kind of method for preparing facial mask as claimed in claim 9, it is characterised in that comprise the following steps:
1. deionized water is added in pot, then carbomer is slowly added under stirring at low speed, is stirred with 50r/min speed homogeneous 10~15min is mixed to being completely dispersed, 80~85 DEG C are then heated to, the mixed of scattered propane diols in advance and xanthans is added Compound, dipotassium glycyrrhizinate, allantoin, dispersed with stirring are incubated 20min;
2. said components are cooled, cools the temperature to 50 DEG C, add the mixing of scattered butanediol and Sodium Hyaluronate Thing, trehalose, glycerine polymethacrylates, tremella polysaccharides, felwort extract solution, polyglutamic acid sodium, glycine betaine, stirring mixing Uniformly;
3. said components are cooled, cools the temperature to 42 DEG C, add deionized water, preservative, dispersed with stirring;
4. formula rate is pressed, triethanolamine is weighed and adds in pot, adjust PH to 6.0~6.5;
5. according to the internal control index of offer, viscosity control 3000~4200, facial mask liquid is obtained;
6. the comprehensive face paper of monolithic is added in the facial mask bag containing above-mentioned facial mask liquid, then takes out and be vacuum-packed, obtain To facial mask.
CN201710547397.XA 2017-07-06 2017-07-06 A kind of facial mask liquid and the facial mask containing the facial mask liquid Pending CN107184486A (en)

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Application publication date: 20170922