CN112402308A - Multi-effect relieving moisturizing lotion and preparation method thereof - Google Patents
Multi-effect relieving moisturizing lotion and preparation method thereof Download PDFInfo
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- CN112402308A CN112402308A CN202011192885.1A CN202011192885A CN112402308A CN 112402308 A CN112402308 A CN 112402308A CN 202011192885 A CN202011192885 A CN 202011192885A CN 112402308 A CN112402308 A CN 112402308A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/35—Ketones, e.g. benzophenone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
Abstract
The invention discloses multi-effect relieving moisturizing water and a preparation method thereof, wherein the moisturizing water comprises the following components in percentage by weight: skin conditioner: 0.1-1% of centella extract, 0.1-1% of polygonum cuspidatum root extract, 0.1-1% of scutellaria baicalensis root extract, 0.1-1% of tea extract, 0.1-1% of glycyrrhiza glabra root extract and 0.1-1% of mother chrysanthemum extract; 0.1-1% of antioxidant, 1-6.5% of humectant, 0.1-1% of thickening agent, 0.01-0.1% of solubilizer and the balance of water. Has the effects of whitening, resisting oxidation, relieving, tranquilizing and whitening, and is not sticky and sensitive, and suitable for long-term use by consumers.
Description
Technical Field
The invention relates to the technical field of cosmetics, and in particular relates to multi-effect soothing moisturizing lotion and a preparation method thereof.
Background
The toner, also called firming lotion, toning lotion and the like, has the functions of re-cleaning to restore the pH value of the surface of the skin and conditioning the stratum corneum so that the skin can better absorb the toner and is prepared for using the maintenance product in the subsequent steps. The toner also has the following functions: astringing, namely timely shrinking the opened pores after cleaning; the skin care product can be used for deeply cleaning, and dirt in pores can be further removed by toner. The water is supplemented, and the toner can supplement the water loss component and prevent desquamation. It has effects of relieving, reducing irritation of sebaceous gland, and preventing vicious circulatory secretion of oil. Soften cutin, promote metabolism of old and waste cutin, make pore unobstructed, and facilitate absorption of nutrition.
A large amount of denatured alcohol is often added into the skin toner on the market, so that the skin toner has great irritation to the skin and even causes the phenomena of dry skin, peeling, pruritus, allergy and the like. In addition, the toner in the prior art is easy to evaporate after being used, has limited moisturizing effect, and cannot simultaneously give consideration to whitening and moisturizing effects. When the moisture in the toner is rapidly lost in a large amount, the skin is easy to feel tight. Moreover, the skin toner is added with a preservative in general, and can cause great stimulation to the skin, particularly to sensitive muscles.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention aims to provide the multi-effect moisturizing and soothing water and the preparation method thereof, which are free of irritant components such as preservatives and the like, are rich in various plant extracts and have whitening, moisturizing and soothing effects.
The purpose of the invention is realized by adopting the following technical scheme:
the multi-effect relieving moisturizing lotion comprises the following components in percentage by weight:
skin conditioner: 0.1-1% of centella extract, 0.1-1% of polygonum cuspidatum root extract, 0.1-1% of scutellaria baicalensis root extract, 0.1-1% of tea extract, 0.1-1% of glycyrrhiza glabra root extract and 0.1-1% of mother chrysanthemum extract;
0.1-1% of antioxidant, 1-6.5% of humectant, 0.1-1% of thickening agent, 0.01-0.1% of solubilizer and the balance of water.
The main effective components of the multi-effect soothing moisturizing lotion provided by the invention are centella extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, tea extract, glycyrrhiza glabra extract and chamomile flower extract. The main effects of the components are as follows:
centella asiatica extract: the centella asiatica can tighten the connecting part of the epidermis and the dermis, can soften the skin, helps to promote the formation of collagen in the dermis, and has the effect of making the skin tight. Is helpful for solving the problem of skin relaxation and making skin smooth and elastic. Can also help the injured tissue to heal and compact the skin. Can promote the close connection between the epidermis and the dermis, inhibit the increase of fat cells, and prevent skin edema and obesity. Dicotyledon Umbelliferae, has repercussive, toxic materials clearing away, and pus removing effects. The centella asiatica can tighten the connecting part of the epidermis and the dermis, and can soften the skin.
Giant knotweed rhizome root extract: the whitening cream has good inhibition effect on the activity of B-16 melanocytes, has promotion effect on the activity of macrophages, reduces the content of melanin through the two aspects, and has whitening effect; has effects of inhibiting elastase, resisting wrinkle, and activating skin. Meanwhile, the multifunctional soothing moisturizing lotion can also be used as an antibacterial agent, so that no preservative is required to be added.
Radix scutellariae extract: can inhibit elastase, eliminate free radicals, thereby increasing skin metabolism, improving skin elasticity and wrinkle resistance, and resisting aging; promoting cerebral amide, improving sebum and softening skin; has effects in inhibiting dermatitis, enhancing skin resistance, and resisting inflammation; can neutralize released histamine, and has effect in preventing allergy.
Tea extract: the tea extract contains high concentration superoxide dismutase (SOD), and can inhibit melanin deposition process to achieve whitening effect. The tea extracts contain tea polyphenol which can react with protein, so that the facial skin of a human body can be astringed after the tea extracts are used. The tea polyphenol has moisturizing effect, can prevent excessive dissipation of skin moisture, and has the effects of moisturizing.
Glycyrrhiza glabra root extract: the glycyrrhiza glabra extract can penetrate into the skin and keep high activity, effectively inhibit the activity of various enzymes (such as tyrosinase) in the melanin generation process, and inhibit the activity of dopachrome interconversion and DHICA oxidase, and is a quick, efficient, safe and green cosmetic additive for preventing sun, whitening and removing freckles. It also has oxygen free radical scavenging ability similar to superoxide dismutase (SOD), and oxygen free radical resisting ability similar to vitamin E. Meanwhile, the glycyrrhiza glabra extract also has the effects of preventing rough skin, resisting inflammation and resisting bacteria.
Mother chrysanthemum extract: also known as chamomile extract. Flos Matricariae Chamomillae mainly contains parthenium ketone, stachydrine, volatile oil, vitamin b1, flavonoids, amino acids and various active ingredients, 27 kinds of triterpenes compounds with antiinflammatory effect can be separated, and can be used for treating dermatitis and inhibiting induced allergy of skin; can enhance capillary resistance, inhibit capillary permeability, and has antiinflammatory effect; simultaneously, the composition can eliminate free radicals, has oxidation resistance and has the effect of delaying aging; has certain inhibiting effect on melanocyte, and has certain whitening and speckle removing effects. The chamomile extract has a calming effect on the skin, can regulate oil secretion, balance metabolism, prevent melanin precipitation and acne and resist whelk. Also has antibacterial and anti-inflammatory effects.
Further, the multi-effect relaxing and moisturizing water also comprises an aromatic, wherein the aromatic accounts for 0.01-0.1% of the multi-effect relaxing and moisturizing water in percentage by weight.
Still further, the humectant is one or more of butanediol, sodium hyaluronate and 1, 2-hexanediol.
Specifically, the moisturizing agent comprises the following components in percentage by weight: 1-5% of butanediol, 0.01-0.1% of sodium hyaluronate and 0.1-1% of 1, 2-hexanediol.
Further, the antioxidant is p-hydroxyacetophenone. The p-hydroxyacetophenone is a natural plant extract, and is naturally present in stems and leaves of Artemisia scoparia of Compositae, and roots of Artemisia capillaris, Asclepiadaceae, and Heteropappus japonicus. Has antioxidant and soothing effects. Meanwhile, the preservative can also be used as a substitute of the traditional preservative, and has the functions of corrosion prevention and synergism.
Still further, the thickener is xanthan gum.
Further, the solubilizer is PEG-40 hydrogenated castor oil.
The preparation method of the multi-effect relieving moisturizing lotion comprises the following steps:
1) adding water, humectant, thickener and antioxidant into an emulsifying pot, stirring and heating to 90 deg.C, maintaining the temperature for 30min, and dissolving the contents completely to obtain a mixture;
2) and after the temperature of the mixture is reduced to 35 ℃, adding the skin conditioner and the solubilizer, and stirring until the mixture is completely and uniformly dissolved to obtain the multi-effect soothing moisturizing lotion.
Compared with the prior art, the invention has the beneficial effects that:
(1) the multi-effect soothing moisturizing lotion is free of components with irritation such as denatured ethanol, mineral oil petrolatum and preservatives, and has the main effective components of centella extract, polygonum cuspidatum root extract, scutellaria baicalensis root extract, tea extract, glycyrrhiza glabra extract and chamomile extract.
(2) The multi-effect soothing moisturizing lotion adopts a preservative-free system, and the sterilization and inflammation diminishing effects of the multi-effect soothing moisturizing lotion are mainly realized by compounding plant extracts such as p-hydroxyacetophenone, polygonum cuspidatum root extract, scutellaria baicalensis root extract, tea extract, glycyrrhiza glabra extract and chamomile flower extract, so that the irritation is greatly reduced, and the lotion is milder in use.
Detailed Description
The present invention is further described below with reference to specific embodiments, and it should be noted that, without conflict, any combination between the embodiments or technical features described below may form a new embodiment.
The formulas (in weight percentage) of the multi-effect soothing moisturizing lotion of the embodiments 1-3 and the toner of the comparative examples 1-3 are as follows:
the preparation method of the multi-effect soothing moisturizing lotion disclosed in the embodiments 1 to 3 comprises the following steps:
the preparation method of the multi-effect relieving moisturizing lotion comprises the following steps:
1) adding water, humectant, thickener and antioxidant into an emulsifying pot, stirring and heating to 90 deg.C, maintaining the temperature for 30min, and dissolving the contents completely to obtain a mixture;
2) and after the temperature of the mixture is reduced to 35 ℃, adding the skin conditioner and the solubilizer, and stirring until the mixture is completely and uniformly dissolved to obtain the multi-effect soothing moisturizing lotion.
Toner of comparative examples 1 to 6 reference the preparation methods of examples 1 to 3.
Test of moisturizing Effect
Skin stratum corneum moisture test
The experimental basis is as follows: QB/T4256 plus 2011 guide for evaluating moisture retention efficacy of cosmetics
The test method comprises the following steps: selecting 72 women aged 20-40 years old, averagely dividing into 9 groups, and respectively using corresponding toner for 8 women in each group;
the tested part: marking two symmetrical tested parts at the inner sides of the two forearms randomly;
the dosage of the product is as follows: completely wetting the 5cm × 6cm cotton pad without dripping liquid;
the testing steps are as follows: after the testee sits still for 10min, the moisture content of the skin stratum corneum of the tested part is tested before wiping (T0), the moisture content of the skin stratum corneum is tested after wiping the sample (T1), the moisture content of the skin stratum corneum is continuously tested after waiting for 30min (T2) and 1h (T3), and the moisture retention rate is calculated, wherein the results are shown in table 1:
TABLE 1 Water content data of stratum corneum of examples 1-3 and comparative examples 1-6
Hyaluronidase in vitro inhibition assay
First, experiment principle
Hyaluronidase is a participant in type I allergic reactions, hyaluronidase has strong correlation with inflammation and allergy, studies report that various drugs that release histamine from mast cells can regulate the activity of hyaluronidase, and some anti-allergy drugs can strongly inhibit the activity of hyaluronidase because inhibition of hyaluronidase activity is an index for studying anti-allergic effects.
II, reagent
1. Buffer: solution A (0.2mol/L acetic acid, 11.55ml glacial acetic acid in 1L distilled water) 4.8ml
45.2ml of solution B (0.2mol/L sodium acetate, 116.4g anhydrous sodium acetate or 27.2h sodium acetate trihydrate dissolved in 1L distilled water) is mixed and diluted to 100ml to prepare an acetic acid buffer solution with the pH value of 5.6;
2. hyaluronidase (I): the concentration is 500U/ml, and acetic acid buffer solution is used as a solvent;
3. sodium hyaluronate: 0.5mg/ml, using acetic acid buffer solution as solvent;
4. acetylacetone solution: 50ml of 1.0mol/L sodium carbonate solution and 3.5ml of acetylacetone solution are mixed evenly and prepared on site;
5. P-DAB color developing agent: 0.8g of p-dimethylamine benzaldehyde is dissolved in 15ml of concentrated hydrochloric acid and 15ml of absolute ethyl alcohol and is uniformly mixed;
6. calcium chloride solution CaCl 2: 2.5 mol/L;
7. sodium hydroxide solution NaOH: 5 mol/L;
8. sample preparation: the multi-effect soothing moisturizing lotion of examples 1-3 and the toner of comparative examples 1-6 have a sample reference concentration of 1.2 mg/ml.
Third, the experimental procedure
Fourthly, calculating
Hyaluronidase inhibition (%) - (C-D) - (A-B) ]/(C-D) × 100%
In the formula: a is the OD value of the (hyaluronidase + sample + sodium hyaluronate) sample solution; b is the OD value of the blank of the (acetic acid buffer solution + sample + acetic acid buffer solution) sample; c is the OD value of the control solution (hyaluronidase + deionized water + sodium hyaluronate); d is the OD value of the control blank (acetate buffer + deionized water + acetate buffer), and the results are shown in table 2:
TABLE 2 data of experiment for hyaluronidase inhibition in vitro of examples 1 to 3 and comparative examples 1 to 6
| Sample (I) | Inhibition ratio of enzyme activity% |
| Example 1 | 77.32 |
| Example 2 | 75.64 |
| Example 3 | 76.31 |
| Comparative example 1 | 71.02 |
| Comparative example 2 | 74.55 |
| Comparative example 3 | 70.86 |
| Comparative example 4 | 73.56 |
| Comparative example 5 | 69.58 |
| Comparative example 6 | 72.33 |
As can be seen from Table 1, after the skin fresheners of examples 1-3 and comparative examples 1-6 are wiped, the skin moisture content of the subjects is improved to different degrees, wherein the instant moisturizing effect of the multi-effect soothing moisturizing lotion of example 1 is the best. After wiping for 30min and 1h, the moisturizing rates of the examples 1-3 are higher than those of the comparative examples 1-6, which shows that the multi-effect soothing moisturizing lotion has the effects of long-acting moisturizing and water locking.
The enzyme activity inhibition rates of the examples 1 to 3 are higher than those of the comparative examples 1 to 6, which shows that the combination of the centella asiatica extract, the polygonum cuspidatum root extract, the scutellaria baicalensis root extract, the tea leaf extract, the glycyrrhiza glabra extract and the chamomile flower extract can effectively inhibit the activity of hyaluronidase and reduce the decomposition of hyaluronic acid, thereby reducing the release amount of histamine and inflammatory factors and playing the anti-allergic and anti-irritation role. Wherein, the enzyme activity inhibition rates of the comparative examples 1, 3 and 5 are lower, which shows that the centella asiatica extract, the radix scutellariae extract and the glycyrrhiza glabra extract in the six extracts have stronger anti-inflammatory repair capability.
The above embodiments are only preferred embodiments of the present invention, and the protection scope of the present invention is not limited thereby, and any insubstantial changes and substitutions made by those skilled in the art based on the present invention are within the protection scope of the present invention.
Claims (10)
1. The multi-effect relieving moisturizing lotion is characterized by comprising the following components in percentage by weight:
skin conditioner: 0.1-1% of centella extract, 0.1-1% of polygonum cuspidatum root extract, 0.1-1% of scutellaria baicalensis root extract, 0.1-1% of tea extract, 0.1-1% of glycyrrhiza glabra root extract and 0.1-1% of mother chrysanthemum extract;
0.1-1% of antioxidant, 1-6.5% of humectant, 0.1-1% of thickening agent, 0.01-0.1% of solubilizer and the balance of water.
2. The multi-effect soothing moisturizing water of claim 1, further comprising an aromatic agent, wherein the aromatic agent accounts for 0.01-0.1% by weight of the multi-effect soothing moisturizing water.
3. The multi-effect soothing moisturizer of claim 1, wherein the moisturizer is one or more of butylene glycol, sodium hyaluronate and 1, 2-hexanediol.
4. The multi-effect soothing moisturizing lotion of claim 1 or 3, comprising the following components in weight percent: 1-5% of butanediol, 0.01-0.1% of sodium hyaluronate and 0.1-1% of 1, 2-hexanediol.
5. The multipurpose soothing moisturizer of claim 1, wherein the antioxidant is p-hydroxyacetophenone.
6. The multi-effect soothing moisturizing water of claim 1, wherein said thickening agent is xanthan gum.
7. The multi-effect soothing moisturizing lotion of claim 1, wherein said solubilizing agent is PEG-40 hydrogenated castor oil.
8. The method for preparing multi-effect soothing moisturizing water as claimed in any one of claims 1 to 7, comprising the steps of:
1) adding water, humectant, thickener and antioxidant into an emulsifying pot, stirring and heating until the components are completely dissolved to obtain a mixture;
2) and after the mixture is cooled to room temperature, adding the skin conditioner and the solubilizer, and stirring until the skin conditioner and the solubilizer are completely and uniformly dissolved to obtain the multi-effect soothing moisturizing lotion.
9. The method for preparing the multi-effect soothing moisturizing lotion as claimed in claim 8, wherein in the step 1), the solution is stirred and heated to 90 ℃ and the temperature is kept for 30 min.
10. The method of claim 8, wherein in step 2), the skin conditioning agent and the solubilizing agent are added after the mixture is cooled to 35 ℃.
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| CN115463065A (en) * | 2022-10-20 | 2022-12-13 | 广东丸物科技有限公司 | Plant composition with anti-allergy and relieving effects and preparation method and application thereof |
| CN116172929A (en) * | 2023-03-23 | 2023-05-30 | 植物医生(广东)生物科技有限公司 | Whitening composition and preparation method and application thereof |
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| CN115463065A (en) * | 2022-10-20 | 2022-12-13 | 广东丸物科技有限公司 | Plant composition with anti-allergy and relieving effects and preparation method and application thereof |
| CN116172929A (en) * | 2023-03-23 | 2023-05-30 | 植物医生(广东)生物科技有限公司 | Whitening composition and preparation method and application thereof |
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